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Information card for entry 1552478
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Coordinates | 1552478.cif |
---|---|
Structure factors | 1552478.hkl |
Original IUCr paper | HTML |
Chemical name | Decacarbonyl(μ-ethylidenimino-1κ<i>N</i>:2κ<i>C</i>)-μ-hydrido-<i>triangulo</i>-triosmium(3 <i>Os</i>‒<i>Os</i>) |
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Formula | C12 H5 N O10 Os3 |
Calculated formula | C12 H5 N O10 Os3 |
SMILES | [Os]12([Os]([Os]1(C(=N)C)(C#[O])(C#[O])(C#[O])[H]2)(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | Decacarbonyl(μ-ethylidenimino-1κ<i>N</i>:2κ<i>C</i>)-μ-hydrido-<i>triangulo</i>-triosmium(3<i>Os</i>‒<i>Os</i>) |
Authors of publication | Powell, Cynthia B.; Powell, Gregory L.; Archambeau, Ashley K.; Wilson, Kylie M. |
Journal of publication | IUCrData |
Year of publication | 2019 |
Journal volume | 4 |
Journal issue | 10 |
Pages of publication | x191386 |
a | 9.5647 ± 0.00006 Å |
b | 11.59555 ± 0.00008 Å |
c | 15.6161 ± 0.00011 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1731.95 ± 0.02 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0153 |
Residual factor for significantly intense reflections | 0.0152 |
Weighted residual factors for significantly intense reflections | 0.0368 |
Weighted residual factors for all reflections included in the refinement | 0.0368 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
Revision | Date | Message | Files |
---|---|---|---|
225387 (current) | 2019-11-08 | cif/ Updating files of 1552478 Original log message: Adding full bibliography for 1552478.cif. |
1552478.cif 1552478.hkl |
219513 | 2019-10-25 | cif/ hkl/ Adding structures of 1552478 via cif-deposit CGI script. |
1552478.cif 1552478.hkl |
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Users of the data should acknowledge the original authors of the
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