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Information card for entry 4114562
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Coordinates | 4114562.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C60 H94 K2 O16 Si2 |
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Calculated formula | C60 H94 K2 O16 Si2 |
Title of publication | Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion |
Authors of publication | Yuxia Liu; Thomas C. Stringfellow; David Ballweg; Ilia A. Guzei; Robert West |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2002 |
Journal volume | 124 |
Pages of publication | 49 - 57 |
a | 9.499 ± 0.003 Å |
b | 12.856 ± 0.004 Å |
c | 14.846 ± 0.004 Å |
α | 72.274 ± 0.004° |
β | 76.17 ± 0.005° |
γ | 68.932 ± 0.004° |
Cell volume | 1594.3 ± 0.8 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.104 |
Residual factor for significantly intense reflections | 0.0703 |
Weighted residual factors for significantly intense reflections | 0.1722 |
Weighted residual factors for all reflections included in the refinement | 0.1946 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.071 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
178916 (current) | 2016-03-22 | cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/45. |
4114562.cif |
120077 | 2014-07-12 | Adding DOIs to range 4/11 structures. | 4114562.cif |
67892 | 2012-10-08 | cif/ Adding structures of 4114562 via cif-deposit CGI script. |
4114562.cif |
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Users of the data should acknowledge the original authors of the
structural data.