Crystallography Open Database

Information card for entry 4115875

Preview

Coordinates	4115875.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H69 Ag F24 N8 O12 P8 Ru2 S2
Calculated formula	C34 Ag F24 N8 O12 P8 Ru2 S2
Title of publication	Allylic C-H Bond Activation on a Sulfur Center of a Disulfide-Bridged Diruthenium Complex with Concomitant Formation of C-S Bonds
Authors of publication	Md. Munkir Hossain; Yong-Shou Lin; Hiroyasu Sugiyama; Kazuko Matsumoto
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	172 - 173
a	19.43 ± 0.006 Å
b	22.858 ± 0.007 Å
c	16.741 ± 0.004 Å
α	99.99 ± 0.02°
β	93.68 ± 0.02°
γ	104.92 ± 0.02°
Cell volume	7029 ± 4 Å³
Cell temperature	173.2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0821
Weighted residual factors for all reflections included in the refinement	0.104
Goodness-of-fit parameter for all reflections included in the refinement	1.686
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115875.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115875.cif
70427	2012-12-24	cif/ Adding structures of 4115875 via cif-deposit CGI script.	4115875.cif