Crystallography Open Database

Information card for entry 7005275

Preview

Coordinates	7005275.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H30 B2 F8 Mo2 N8 O2
Calculated formula	C24 H30 B2 F8 Mo2 N8 O2
Title of publication	Substitution chemistry of MM quadruply bonded complexes (M = Mo or W) supported by the anion of 2-hydroxy-6-methylpyridine.
Authors of publication	Brown, Douglas J.; Chisholm, Malcolm H.; Gribble, Christopher W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	18
Pages of publication	1793 - 1801
a	7.2615 ± 0.0001 Å
b	12.0539 ± 0.0002 Å
c	19.1113 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	1672.8 ± 0.04 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	31
Hermann-Mauguin space group symbol	P 21 n m
Hall space group symbol	P -2 2ac
Residual factor for all reflections	0.0324
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0671
Weighted residual factors for all reflections included in the refinement	0.0687
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179756 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/52.	7005275.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005275.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005275.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005275.cif