Crystallography Open Database

Information card for entry 7216752

Preview

Coordinates	7216752.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H34 N Sb
Calculated formula	C27 H34 N Sb
SMILES	c1(c(cccc1)CN(C)C)[Sb](c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
Title of publication	Palladium(ii) complexes with chiral organoantimony(iii) ligands. Solution behaviour and solid state structures
Authors of publication	Copolovici, Dana; Isaia, Francesco; Breunig, Hans J.; Raţ, Ciprian I.; Silvestru, Cristian
Journal of publication	RSC Advances
Year of publication	2014
Journal volume	4
Journal issue	51
Pages of publication	26569
a	8.8686 ± 0.0006 Å
b	16.5093 ± 0.0012 Å
c	17.0131 ± 0.0012 Å
α	90°
β	97.937 ± 0.001°
γ	90°
Cell volume	2467.1 ± 0.3 Å³
Cell temperature	297 ± 2 K
Ambient diffraction temperature	297 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0528
Residual factor for significantly intense reflections	0.0472
Weighted residual factors for significantly intense reflections	0.1012
Weighted residual factors for all reflections included in the refinement	0.1038
Goodness-of-fit parameter for all reflections included in the refinement	1.174
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180498 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/67.	7216752.cif
118000	2014-06-23	cif/ Adding structures of 7216751, 7216752, 7216753, 7216754 via cif-deposit CGI script.	7216752.cif