#------------------------------------------------------------------------------
#$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $
#$Revision: 176729 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/43/1514310.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1514310
loop_
_publ_author_name
'Semproni, Scott P.'
'Hojilla Atienza, Crisita Carmen'
'Chirik, Paul J.'
_publ_section_title
;
 Oxidative addition and C--H activation chemistry with a PNP
 pincer-ligated cobalt complex
;
_journal_issue                   5
_journal_name_full               'Chemical Science'
_journal_page_first              1956
_journal_paper_doi               10.1039/c4sc00255e
_journal_volume                  5
_journal_year                    2014
_chemical_formula_sum            'C37 H49 Co N P2'
_chemical_formula_weight         628.64
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                75.4940(10)
_cell_angle_beta                 74.1280(10)
_cell_angle_gamma                64.0320(10)
_cell_formula_units_Z            2
_cell_length_a                   10.4893(2)
_cell_length_b                   11.4272(2)
_cell_length_c                   16.7767(3)
_cell_measurement_reflns_used    9434
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      66.36
_cell_measurement_theta_min      4.77
_cell_volume                     1718.98(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 'ACTA 50'
_diffrn_measured_fraction_theta_max 0.944
_diffrn_measurement_device_type  'Bruker APEX II CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0177
_diffrn_reflns_av_sigmaI/netI    0.0210
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            13542
_diffrn_reflns_theta_full        'ACTA 50'
_diffrn_reflns_theta_max         66.62
_diffrn_reflns_theta_min         4.77
_exptl_absorpt_coefficient_mu    4.967
_exptl_absorpt_correction_T_max  0.7528
_exptl_absorpt_correction_T_min  0.6404
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS v2008/1 (Bruker AXS)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.215
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       diamond
_exptl_crystal_F_000             670
_exptl_crystal_size_max          0.121
_exptl_crystal_size_mid          0.103
_exptl_crystal_size_min          0.051
_refine_diff_density_max         0.320
_refine_diff_density_min         -0.230
_refine_diff_density_rms         0.039
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     380
_refine_ls_number_reflns         5749
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.030
_refine_ls_R_factor_all          0.0288
_refine_ls_R_factor_gt           0.0273
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0391P)²+0.6201P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0696
_refine_ls_wR_factor_ref         0.0706
_reflns_number_gt                5515
_reflns_number_total             5749
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            c4sc00255e2.cif
_cod_data_source_block           sps155
_cod_original_cell_volume        1718.98(5)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               1514310
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.61462(18) 0.45768(16) 0.38141(10) 0.0214(3) Uani 1 1 d .
H1A H 0.5413 0.5137 0.4227 0.026 Uiso 1 1 calc R
H1B H 0.7080 0.4176 0.4006 0.026 Uiso 1 1 calc R
C2 C 0.62848(17) 0.54094(16) 0.29705(10) 0.0220(3) Uani 1 1 d .
C3 C 0.7083(2) 0.61834(18) 0.27578(12) 0.0297(4) Uani 1 1 d .
H3 H 0.7613 0.6172 0.3139 0.036 Uiso 1 1 calc R
C4 C 0.7093(2) 0.69732(19) 0.19795(13) 0.0346(4) Uani 1 1 d .
H4 H 0.7618 0.7520 0.1826 0.042 Uiso 1 1 calc R
C5 C 0.6333(2) 0.69570(18) 0.14306(12) 0.0308(4) Uani 1 1 d .
H5 H 0.6338 0.7485 0.0894 0.037 Uiso 1 1 calc R
C6 C 0.55626(18) 0.61612(16) 0.16714(10) 0.0222(3) Uani 1 1 d .
C7 C 0.47126(18) 0.60677(16) 0.11178(10) 0.0227(3) Uani 1 1 d .
H7A H 0.5345 0.5374 0.0765 0.027 Uiso 1 1 calc R
H7B H 0.4351 0.6915 0.0743 0.027 Uiso 1 1 calc R
C8 C 0.73814(18) 0.18769(16) 0.35561(10) 0.0245(4) Uani 1 1 d .
H8 H 0.7869 0.1698 0.4035 0.029 Uiso 1 1 calc R
C9 C 0.7226(2) 0.06133(16) 0.35376(11) 0.0303(4) Uani 1 1 d .
H9A H 0.6702 0.0767 0.3094 0.045 Uiso 1 1 calc R
H9B H 0.6690 0.0357 0.4080 0.045 Uiso 1 1 calc R
H9C H 0.8186 -0.0092 0.3427 0.045 Uiso 1 1 calc R
C10 C 0.83518(19) 0.22369(18) 0.27578(11) 0.0289(4) Uani 1 1 d .
H10A H 0.9276 0.1481 0.2668 0.043 Uiso 1 1 calc R
H10B H 0.8522 0.2986 0.2817 0.043 Uiso 1 1 calc R
H10C H 0.7878 0.2474 0.2278 0.043 Uiso 1 1 calc R
C11 C 0.47656(18) 0.28552(15) 0.48499(10) 0.0203(3) Uani 1 1 d .
H11 H 0.4111 0.3718 0.5048 0.024 Uiso 1 1 calc R
C12 C 0.3789(2) 0.21507(17) 0.49004(11) 0.0280(4) Uani 1 1 d .
H12A H 0.4378 0.1285 0.4724 0.042 Uiso 1 1 calc R
H12B H 0.3088 0.2676 0.4531 0.042 Uiso 1 1 calc R
H12C H 0.3275 0.2040 0.5479 0.042 Uiso 1 1 calc R
C13 C 0.58211(19) 0.21330(18) 0.54575(10) 0.0281(4) Uani 1 1 d .
H13A H 0.5279 0.2064 0.6032 0.042 Uiso 1 1 calc R
H13B H 0.6412 0.2624 0.5411 0.042 Uiso 1 1 calc R
H13C H 0.6448 0.1249 0.5318 0.042 Uiso 1 1 calc R
C14 C 0.27424(18) 0.50439(16) 0.09945(10) 0.0216(3) Uani 1 1 d .
H14 H 0.3689 0.4420 0.0720 0.026 Uiso 1 1 calc R
C15 C 0.1847(2) 0.42276(18) 0.14135(11) 0.0316(4) Uani 1 1 d .
H15A H 0.0887 0.4797 0.1678 0.047 Uiso 1 1 calc R
H15B H 0.2328 0.3532 0.1840 0.047 Uiso 1 1 calc R
H15C H 0.1750 0.3829 0.0991 0.047 Uiso 1 1 calc R
C16 C 0.2084(2) 0.60863(17) 0.02836(10) 0.0270(4) Uani 1 1 d .
H16A H 0.2057 0.5654 -0.0144 0.041 Uiso 1 1 calc R
H16B H 0.2672 0.6604 0.0032 0.041 Uiso 1 1 calc R
H16C H 0.1100 0.6670 0.0507 0.041 Uiso 1 1 calc R
C17 C 0.17130(18) 0.73246(15) 0.18813(10) 0.0219(3) Uani 1 1 d .
H17 H 0.1526 0.7793 0.1309 0.026 Uiso 1 1 calc R
C18 C 0.2152(2) 0.81536(16) 0.22593(11) 0.0258(4) Uani 1 1 d .
H18A H 0.1333 0.8994 0.2346 0.039 Uiso 1 1 calc R
H18B H 0.2966 0.8319 0.1875 0.039 Uiso 1 1 calc R
H18C H 0.2436 0.7677 0.2798 0.039 Uiso 1 1 calc R
C19 C 0.03160(18) 0.72052(17) 0.23974(11) 0.0280(4) Uani 1 1 d .
H19A H 0.0464 0.6754 0.2965 0.042 Uiso 1 1 calc R
H19B H 0.0044 0.6699 0.2131 0.042 Uiso 1 1 calc R
H19C H -0.0455 0.8086 0.2428 0.042 Uiso 1 1 calc R
C20 C 0.52242(17) 0.30471(15) 0.20666(10) 0.0210(3) Uani 1 1 d .
C21 C 0.57676(18) 0.22257(16) 0.16220(10) 0.0226(3) Uani 1 1 d .
C22 C 0.65008(18) 0.12309(15) 0.10768(10) 0.0221(3) Uani 1 1 d .
C23 C 0.58150(19) 0.10960(16) 0.05212(10) 0.0243(4) Uani 1 1 d .
H23 H 0.4818 0.1625 0.0529 0.029 Uiso 1 1 calc R
C24 C 0.6562(2) 0.02041(16) -0.00431(10) 0.0258(4) Uani 1 1 d .
H24 H 0.6071 0.0150 -0.0423 0.031 Uiso 1 1 calc R
C25 C 0.8008(2) -0.06085(16) -0.00632(10) 0.0261(4) Uani 1 1 d .
C26 C 0.8686(2) -0.05115(17) 0.05066(11) 0.0288(4) Uani 1 1 d .
H26 H 0.9671 -0.1075 0.0515 0.035 Uiso 1 1 calc R
C27 C 0.7960(2) 0.03878(17) 0.10626(11) 0.0275(4) Uani 1 1 d .
H27 H 0.8457 0.0436 0.1441 0.033 Uiso 1 1 calc R
C28 C 0.8811(2) -0.15801(19) -0.06764(12) 0.0362(4) Uani 1 1 d .
H28A H 0.9762 -0.1555 -0.0924 0.054 Uiso 1 1 calc R
H28B H 0.8261 -0.1347 -0.1121 0.054 Uiso 1 1 calc R
H28C H 0.8931 -0.2468 -0.0383 0.054 Uiso 1 1 calc R
C29 C 0.28803(17) 0.53267(15) 0.36628(10) 0.0184(3) Uani 1 1 d .
C30 C 0.19941(17) 0.58981(15) 0.42248(10) 0.0191(3) Uani 1 1 d .
C31 C 0.09067(17) 0.66047(15) 0.48670(10) 0.0187(3) Uani 1 1 d .
C32 C 0.03906(17) 0.79732(16) 0.47917(10) 0.0215(3) Uani 1 1 d .
H32 H 0.0753 0.8450 0.4302 0.026 Uiso 1 1 calc R
C33 C -0.06401(18) 0.86483(16) 0.54177(10) 0.0234(4) Uani 1 1 d .
H33 H -0.0969 0.9579 0.5349 0.028 Uiso 1 1 calc R
C34 C -0.12038(18) 0.79902(16) 0.61458(10) 0.0222(3) Uani 1 1 d .
C35 C -0.07102(18) 0.66279(17) 0.62173(10) 0.0239(4) Uani 1 1 d .
H35 H -0.1089 0.6157 0.6703 0.029 Uiso 1 1 calc R
C36 C 0.03196(18) 0.59466(16) 0.55961(10) 0.0219(3) Uani 1 1 d .
H36 H 0.0635 0.5017 0.5664 0.026 Uiso 1 1 calc R
C37 C -0.2328(2) 0.87332(18) 0.68239(11) 0.0304(4) Uani 1 1 d .
H37A H -0.2619 0.9682 0.6634 0.046 Uiso 1 1 calc R
H37B H -0.1923 0.8489 0.7332 0.046 Uiso 1 1 calc R
H37C H -0.3171 0.8511 0.6946 0.046 Uiso 1 1 calc R
N1 N 0.55348(14) 0.54088(12) 0.24330(8) 0.0190(3) Uani 1 1 d .
P1 P 0.56107(4) 0.32653(4) 0.37543(2) 0.01723(10) Uani 1 1 d .
P2 P 0.31761(4) 0.56748(4) 0.17606(2) 0.01694(9) Uani 1 1 d .
Co1 Co 0.42365(3) 0.43417(2) 0.280461(15) 0.01570(8) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C2 C1 P1 110.52(11)
N1 C2 C3 121.16(15)
N1 C2 C1 115.92(14)
C3 C2 C1 122.87(15)
C4 C3 C2 119.01(17)
C5 C4 C3 119.42(17)
C4 C5 C6 119.27(16)
N1 C6 C5 121.31(16)
N1 C6 C7 115.41(14)
C5 C6 C7 123.28(15)
C6 C7 P2 110.19(11)
C9 C8 C10 111.50(14)
C9 C8 P1 112.18(12)
C10 C8 P1 111.45(12)
C13 C11 C12 112.23(14)
C13 C11 P1 114.66(12)
C12 C11 P1 111.70(11)
C15 C14 C16 111.29(15)
C15 C14 P2 112.75(11)
C16 C14 P2 114.83(11)
C19 C17 C18 111.28(14)
C19 C17 P2 110.79(11)
C18 C17 P2 111.83(12)
C21 C20 Co1 176.14(15)
C20 C21 C22 176.98(18)
C23 C22 C27 117.01(15)
C23 C22 C21 121.88(15)
C27 C22 C21 121.06(16)
C24 C23 C22 121.26(16)
C25 C24 C23 121.35(16)
C24 C25 C26 117.75(15)
C24 C25 C28 121.03(16)
C26 C25 C28 121.22(17)
C27 C26 C25 121.43(17)
C26 C27 C22 121.14(16)
C30 C29 Co1 176.52(14)
C29 C30 C31 177.72(17)
C32 C31 C36 117.22(14)
C32 C31 C30 121.42(14)
C36 C31 C30 121.37(14)
C33 C32 C31 121.25(15)
C32 C33 C34 121.37(15)
C35 C34 C33 117.57(15)
C35 C34 C37 121.38(15)
C33 C34 C37 121.04(15)
C36 C35 C34 121.41(15)
C35 C36 C31 121.17(15)
C2 N1 C6 119.82(14)
C2 N1 Co1 120.05(11)
C6 N1 Co1 120.02(11)
C1 P1 C8 101.89(8)
C1 P1 C11 103.13(7)
C8 P1 C11 106.22(7)
C1 P1 Co1 98.77(5)
C8 P1 Co1 123.42(5)
C11 P1 Co1 119.28(5)
C7 P2 C17 102.86(8)
C7 P2 C14 100.96(8)
C17 P2 C14 105.87(7)
C7 P2 Co1 98.25(5)
C17 P2 Co1 122.62(5)
C14 P2 Co1 121.49(5)
C29 Co1 C20 162.04(7)
C29 Co1 N1 97.33(6)
C20 Co1 N1 100.62(6)
C29 Co1 P1 86.06(5)
C20 Co1 P1 95.40(5)
N1 Co1 P1 83.34(4)
C29 Co1 P2 95.75(5)
C20 Co1 P2 86.86(5)
N1 Co1 P2 83.58(4)
P1 Co1 P2 166.920(19)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
C1 C2 1.504(2)
C1 P1 1.8479(16)
C2 N1 1.349(2)
C2 C3 1.392(2)
C3 C4 1.389(3)
C4 C5 1.381(3)
C5 C6 1.388(2)
C6 N1 1.350(2)
C6 C7 1.502(2)
C7 P2 1.8445(17)
C8 C9 1.531(2)
C8 C10 1.531(2)
C8 P1 1.8502(16)
C11 C13 1.530(2)
C11 C12 1.532(2)
C11 P1 1.8507(16)
C14 C15 1.524(2)
C14 C16 1.529(2)
C14 P2 1.8574(16)
C17 C19 1.529(2)
C17 C18 1.534(2)
C17 P2 1.8542(16)
C20 C21 1.188(2)
C20 Co1 1.9155(17)
C21 C22 1.446(2)
C22 C23 1.395(2)
C22 C27 1.404(2)
C23 C24 1.388(2)
C24 C25 1.385(3)
C25 C26 1.388(3)
C25 C28 1.510(2)
C26 C27 1.383(2)
C29 C30 1.215(2)
C29 Co1 1.9112(16)
C30 C31 1.439(2)
C31 C32 1.397(2)
C31 C36 1.405(2)
C32 C33 1.386(2)
C33 C34 1.393(2)
C34 C35 1.393(2)
C34 C37 1.510(2)
C35 C36 1.383(2)
N1 Co1 2.0831(13)
P1 Co1 2.2026(5)
P2 Co1 2.2069(4)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
P1 C1 C2 N1 23.23(17)
P1 C1 C2 C3 -159.40(14)
N1 C2 C3 C4 0.5(3)
C1 C2 C3 C4 -176.77(16)
C2 C3 C4 C5 -1.0(3)
C3 C4 C5 C6 0.6(3)
C4 C5 C6 N1 0.4(3)
C4 C5 C6 C7 -179.53(17)
N1 C6 C7 P2 29.14(18)
C5 C6 C7 P2 -150.94(14)
Co1 C20 C21 C22 -167(2)
C20 C21 C22 C23 -147(3)
C20 C21 C22 C27 30(3)
C27 C22 C23 C24 -2.6(2)
C21 C22 C23 C24 175.05(15)
C22 C23 C24 C25 1.6(3)
C23 C24 C25 C26 0.6(3)
C23 C24 C25 C28 179.74(16)
C24 C25 C26 C27 -1.7(3)
C28 C25 C26 C27 179.20(17)
C25 C26 C27 C22 0.6(3)
C23 C22 C27 C26 1.5(3)
C21 C22 C27 C26 -176.13(16)
Co1 C29 C30 C31 -99(4)
C29 C30 C31 C32 -60(4)
C29 C30 C31 C36 120(4)
C36 C31 C32 C33 1.1(2)
C30 C31 C32 C33 -178.95(15)
C31 C32 C33 C34 -0.1(3)
C32 C33 C34 C35 -1.0(3)
C32 C33 C34 C37 -179.89(16)
C33 C34 C35 C36 1.1(3)
C37 C34 C35 C36 179.98(16)
C34 C35 C36 C31 -0.1(3)
C32 C31 C36 C35 -1.0(2)
C30 C31 C36 C35 179.04(15)
C3 C2 N1 C6 0.6(2)
C1 C2 N1 C6 177.97(14)
C3 C2 N1 Co1 -175.66(13)
C1 C2 N1 Co1 1.76(18)
C5 C6 N1 C2 -1.0(2)
C7 C6 N1 C2 178.94(14)
C5 C6 N1 Co1 175.23(13)
C7 C6 N1 Co1 -4.85(18)
C2 C1 P1 C8 93.23(12)
C2 C1 P1 C11 -156.75(11)
C2 C1 P1 Co1 -33.78(12)
C9 C8 P1 C1 176.18(12)
C10 C8 P1 C1 -57.99(13)
C9 C8 P1 C11 68.54(13)
C10 C8 P1 C11 -165.63(12)
C9 C8 P1 Co1 -74.81(13)
C10 C8 P1 Co1 51.02(14)
C13 C11 P1 C1 -70.69(13)
C12 C11 P1 C1 160.21(12)
C13 C11 P1 C8 36.06(14)
C12 C11 P1 C8 -93.05(13)
C13 C11 P1 Co1 -178.77(10)
C12 C11 P1 Co1 52.12(13)
C6 C7 P2 C17 89.94(12)
C6 C7 P2 C14 -160.80(11)
C6 C7 P2 Co1 -36.35(11)
C19 C17 P2 C7 179.32(12)
C18 C17 P2 C7 -55.90(13)
C19 C17 P2 C14 73.80(13)
C18 C17 P2 C14 -161.42(12)
C19 C17 P2 Co1 -71.97(12)
C18 C17 P2 Co1 52.82(13)
C15 C14 P2 C7 161.11(13)
C16 C14 P2 C7 -70.00(14)
C15 C14 P2 C17 -91.99(13)
C16 C14 P2 C17 36.90(14)
C15 C14 P2 Co1 54.25(14)
C16 C14 P2 Co1 -176.85(10)
C30 C29 Co1 C20 14(2)
C30 C29 Co1 N1 -164(2)
C30 C29 Co1 P1 -81(2)
C30 C29 Co1 P2 112(2)
C21 C20 Co1 C29 15(2)
C21 C20 Co1 N1 -167(2)
C21 C20 Co1 P1 109(2)
C21 C20 Co1 P2 -84(2)
C2 N1 Co1 C29 64.72(12)
C6 N1 Co1 C29 -111.48(12)
C2 N1 Co1 C20 -114.69(12)
C6 N1 Co1 C20 69.11(13)
C2 N1 Co1 P1 -20.42(11)
C6 N1 Co1 P1 163.38(12)
C2 N1 Co1 P2 159.73(11)
C6 N1 Co1 P2 -16.47(11)
C1 P1 Co1 C29 -71.77(7)
C8 P1 Co1 C29 177.65(8)
C11 P1 Co1 C29 38.72(7)
C1 P1 Co1 C20 126.19(7)
C8 P1 Co1 C20 15.61(9)
C11 P1 Co1 C20 -123.32(8)
C1 P1 Co1 N1 26.09(6)
C8 P1 Co1 N1 -84.49(8)
C11 P1 Co1 N1 136.58(7)
C1 P1 Co1 P2 26.74(10)
C8 P1 Co1 P2 -83.84(11)
C11 P1 Co1 P2 137.23(9)
C7 P2 Co1 C29 122.45(7)
C17 P2 Co1 C29 11.36(8)
C14 P2 Co1 C29 -129.25(8)
C7 P2 Co1 C20 -75.37(7)
C17 P2 Co1 C20 173.54(8)
C14 P2 Co1 C20 32.93(8)
C7 P2 Co1 N1 25.69(7)
C17 P2 Co1 N1 -85.40(7)
C14 P2 Co1 N1 133.99(7)
C7 P2 Co1 P1 25.04(10)
C17 P2 Co1 P1 -86.05(10)
C14 P2 Co1 P1 133.34(9)
