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#$Date: 2025-08-18 17:20:24 +0300 (Mon, 18 Aug 2025) $
#$Revision: 301776 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/51/56/1515664.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1515664
loop_
_publ_author_name
'Arnold, Polly L.'
'Turner, Zoë R.'
'Bellabarba, Ronan M.'
'Tooze, Robert P.'
_publ_section_title
;
 Carbon monoxide coupling and functionalisation at a simple uranium
 coordination complex
;
_journal_issue                   1
_journal_name_full               'Chemical Science'
_journal_page_first              77
_journal_paper_doi               10.1039/c0sc00452a
_journal_volume                  2
_journal_year                    2011
_chemical_formula_moiety         'C57 H162 N9 O3 Si18 U3'
_chemical_formula_sum            'C57 H162 N9 O3 Si18 U3'
_chemical_formula_weight         2241.67
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.691(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   30.0251(6)
_cell_length_b                   15.6531(3)
_cell_length_c                   22.4759(4)
_cell_measurement_reflns_used    20552
_cell_measurement_temperature    170(2)
_cell_measurement_theta_max      29.1301
_cell_measurement_theta_min      2.9477
_cell_volume                     10263.2(3)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;
_computing_molecular_graphics    'ORTEP-III (Farrugia, 2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR-92 (Giacovazzo, 1994)'
_diffrn_ambient_temperature      170(2)
_diffrn_detector_area_resol_mean 16.1042
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.860
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Enhance (Mo) X-ray Source'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.0324
_diffrn_reflns_av_sigmaI/netI    0.0872
_diffrn_reflns_limit_h_max       37
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            57493
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         2.95
_exptl_absorpt_coefficient_mu    4.970
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.81130
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            gold
_exptl_crystal_density_diffrn    1.451
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4476
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         8.542
_refine_diff_density_min         -4.670
_refine_diff_density_rms         0.194
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     863
_refine_ls_number_reflns         23909
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.076
_refine_ls_R_factor_all          0.1118
_refine_ls_R_factor_gt           0.0654
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0905P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1640
_refine_ls_wR_factor_ref         0.1752
_reflns_number_gt                14064
_reflns_number_total             22833
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            c0sc00452a.txt
_cod_data_source_block           p10006_N3UOCHCROUN2andN3UOCCOUN3inasymunit
_cod_original_sg_symbol_H-M      P21/c
_cod_database_code               1515664
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.5044(5) 0.6220(9) 0.2710(5) 0.089(5) Uani 1 1 d .
H1A H 0.5284 0.6642 0.2866 0.133 Uiso 1 1 calc R
H1B H 0.5135 0.5665 0.2903 0.133 Uiso 1 1 calc R
H1C H 0.4756 0.6405 0.2805 0.133 Uiso 1 1 calc R
C2 C 0.4568(4) 0.5195(7) 0.1634(7) 0.082(5) Uani 1 1 d .
H2A H 0.4290 0.5273 0.1787 0.123 Uiso 1 1 calc R
H2B H 0.4722 0.4667 0.1802 0.123 Uiso 1 1 calc R
H2C H 0.4484 0.5161 0.1186 0.123 Uiso 1 1 calc R
C3 C 0.5524(4) 0.5850(7) 0.1722(6) 0.063(3) Uani 1 1 d .
H3A H 0.5497 0.5842 0.1279 0.094 Uiso 1 1 calc R
H3B H 0.5621 0.5286 0.1893 0.094 Uiso 1 1 calc R
H3C H 0.5751 0.6278 0.1912 0.094 Uiso 1 1 calc R
C4 C 0.4526(4) 0.8301(7) 0.2377(5) 0.062(4) Uani 1 1 d .
H4A H 0.4193 0.8268 0.2220 0.093 Uiso 1 1 calc R
H4B H 0.4611 0.8880 0.2529 0.093 Uiso 1 1 calc R
H4C H 0.4622 0.7891 0.2712 0.093 Uiso 1 1 calc R
C5 C 0.5441(4) 0.8283(9) 0.2052(7) 0.090(5) Uani 1 1 d .
H5A H 0.5527 0.8187 0.2496 0.136 Uiso 1 1 calc R
H5B H 0.5500 0.8880 0.1965 0.136 Uiso 1 1 calc R
H5C H 0.5622 0.7907 0.1852 0.136 Uiso 1 1 calc R
C6 C 0.4556(4) 0.8808(6) 0.1113(5) 0.051(3) Uani 1 1 d .
H6A H 0.4703 0.8724 0.0771 0.077 Uiso 1 1 calc R
H6B H 0.4606 0.9397 0.1261 0.077 Uiso 1 1 calc R
H6C H 0.4226 0.8699 0.0973 0.077 Uiso 1 1 calc R
C7 C 0.5411(4) 0.7590(10) 0.0368(5) 0.085(5) Uani 1 1 d .
H7A H 0.5365 0.7969 0.0696 0.127 Uiso 1 1 calc R
H7B H 0.5717 0.7686 0.0297 0.127 Uiso 1 1 calc R
H7C H 0.5383 0.6994 0.0488 0.127 Uiso 1 1 calc R
C8 C 0.5113(5) 0.8919(8) -0.0606(7) 0.083(4) Uani 1 1 d .
H8A H 0.4935 0.9017 -0.1026 0.125 Uiso 1 1 calc R
H8B H 0.5441 0.8952 -0.0594 0.125 Uiso 1 1 calc R
H8C H 0.5035 0.9356 -0.0335 0.125 Uiso 1 1 calc R
C9 C 0.5036(4) 0.7040(7) -0.0913(5) 0.062(3) Uani 1 1 d .
H9A H 0.5132 0.6491 -0.0713 0.093 Uiso 1 1 calc R
H9B H 0.5267 0.7239 -0.1123 0.093 Uiso 1 1 calc R
H9C H 0.4742 0.6969 -0.1211 0.093 Uiso 1 1 calc R
C10 C 0.4055(5) 0.9563(8) -0.0508(8) 0.097(5) Uani 1 1 d .
H10A H 0.4278 0.9769 -0.0730 0.146 Uiso 1 1 calc R
H10B H 0.4166 0.9689 -0.0070 0.146 Uiso 1 1 calc R
H10C H 0.3760 0.9849 -0.0665 0.146 Uiso 1 1 calc R
C11 C 0.3859(5) 0.8149(11) -0.1457(6) 0.102(6) Uani 1 1 d .
H11A H 0.4099 0.8408 -0.1627 0.153 Uiso 1 1 calc R
H11B H 0.3561 0.8392 -0.1660 0.153 Uiso 1 1 calc R
H11C H 0.3854 0.7530 -0.1524 0.153 Uiso 1 1 calc R
C12 C 0.3463(4) 0.8061(7) -0.0347(6) 0.056(3) Uani 1 1 d .
H12A H 0.3368 0.7484 -0.0492 0.084 Uiso 1 1 calc R
H12B H 0.3214 0.8465 -0.0507 0.084 Uiso 1 1 calc R
H12C H 0.3536 0.8071 0.0102 0.084 Uiso 1 1 calc R
C13 C 0.3761(5) 0.5655(9) -0.0847(7) 0.105(6) Uani 1 1 d .
H13A H 0.3609 0.6180 -0.1026 0.157 Uiso 1 1 calc R
H13B H 0.3714 0.5205 -0.1159 0.157 Uiso 1 1 calc R
H13C H 0.4091 0.5761 -0.0697 0.157 Uiso 1 1 calc R
C14 C 0.2888(4) 0.5126(8) -0.0505(7) 0.088(5) Uani 1 1 d .
H14A H 0.2762 0.4849 -0.0189 0.132 Uiso 1 1 calc R
H14B H 0.2839 0.4757 -0.0867 0.132 Uiso 1 1 calc R
H14C H 0.2734 0.5674 -0.0617 0.132 Uiso 1 1 calc R
C15 C 0.3783(5) 0.4260(7) 0.0076(8) 0.107(6) Uani 1 1 d .
H15A H 0.4117 0.4321 0.0194 0.160 Uiso 1 1 calc R
H15B H 0.3699 0.3835 -0.0252 0.160 Uiso 1 1 calc R
H15C H 0.3672 0.4073 0.0431 0.160 Uiso 1 1 calc R
C16 C 0.2699(4) 0.6687(7) 0.0466(7) 0.072(4) Uani 1 1 d .
H16A H 0.2741 0.7200 0.0236 0.108 Uiso 1 1 calc R
H16B H 0.2526 0.6833 0.0771 0.108 Uiso 1 1 calc R
H16C H 0.2530 0.6257 0.0184 0.108 Uiso 1 1 calc R
C17 C 0.3532(4) 0.7063(7) 0.1430(6) 0.065(3) Uani 1 1 d .
H17A H 0.3844 0.6883 0.1632 0.097 Uiso 1 1 calc R
H17B H 0.3350 0.7124 0.1737 0.097 Uiso 1 1 calc R
H17C H 0.3544 0.7613 0.1226 0.097 Uiso 1 1 calc R
C18 C 0.3179(5) 0.5263(9) 0.1284(8) 0.104(6) Uani 1 1 d .
H18A H 0.2968 0.4878 0.1009 0.156 Uiso 1 1 calc R
H18B H 0.3048 0.5416 0.1631 0.156 Uiso 1 1 calc R
H18C H 0.3474 0.4976 0.1436 0.156 Uiso 1 1 calc R
C19 C 0.4914(4) 0.5253(7) 0.0097(6) 0.055(3) Uani 1 1 d .
C20 C 0.1424(3) 0.2060(6) 0.2251(5) 0.044(3) Uani 1 1 d .
H20A H 0.1387 0.2495 0.1929 0.065 Uiso 1 1 calc R
H20B H 0.1182 0.2125 0.2473 0.065 Uiso 1 1 calc R
H20C H 0.1403 0.1490 0.2064 0.065 Uiso 1 1 calc R
C21 C 0.2110(4) 0.1313(7) 0.3358(5) 0.061(3) Uani 1 1 d .
H21A H 0.2219 0.0810 0.3174 0.091 Uiso 1 1 calc R
H21B H 0.1828 0.1170 0.3483 0.091 Uiso 1 1 calc R
H21C H 0.2345 0.1494 0.3717 0.091 Uiso 1 1 calc R
C22 C 0.1943(5) 0.3173(7) 0.3246(7) 0.083(5) Uani 1 1 d .
H22A H 0.2181 0.3169 0.3628 0.125 Uiso 1 1 calc R
H22B H 0.1640 0.3184 0.3340 0.125 Uiso 1 1 calc R
H22C H 0.1979 0.3681 0.3007 0.125 Uiso 1 1 calc R
C23 C 0.3255(4) 0.2136(7) 0.3400(5) 0.064(3) Uani 1 1 d .
H23A H 0.3086 0.2194 0.3722 0.097 Uiso 1 1 calc R
H23B H 0.3562 0.2384 0.3542 0.097 Uiso 1 1 calc R
H23C H 0.3282 0.1530 0.3306 0.097 Uiso 1 1 calc R
C24 C 0.2931(5) 0.3866(7) 0.2910(6) 0.080(4) Uani 1 1 d .
H24A H 0.2822 0.4207 0.2538 0.120 Uiso 1 1 calc R
H24B H 0.3241 0.4049 0.3117 0.120 Uiso 1 1 calc R
H24C H 0.2724 0.3946 0.3184 0.120 Uiso 1 1 calc R
C25 C 0.3288(4) 0.2682(8) 0.2131(6) 0.067(4) Uani 1 1 d .
H25A H 0.3367 0.2089 0.2060 0.101 Uiso 1 1 calc R
H25B H 0.3569 0.3012 0.2281 0.101 Uiso 1 1 calc R
H25C H 0.3113 0.2931 0.1746 0.101 Uiso 1 1 calc R
C26 C 0.2951(5) 0.0842(10) -0.0194(6) 0.105(6) Uani 1 1 d .
H26A H 0.3134 0.0326 -0.0069 0.158 Uiso 1 1 calc R
H26B H 0.3056 0.1128 -0.0524 0.158 Uiso 1 1 calc R
H26C H 0.2627 0.0684 -0.0339 0.158 Uiso 1 1 calc R
C27 C 0.2706(4) 0.2606(7) 0.0208(6) 0.066(4) Uani 1 1 d .
H27A H 0.2383 0.2480 0.0028 0.100 Uiso 1 1 calc R
H27B H 0.2843 0.2872 -0.0102 0.100 Uiso 1 1 calc R
H27C H 0.2731 0.2998 0.0554 0.100 Uiso 1 1 calc R
C28 C 0.3640(4) 0.1901(8) 0.0731(6) 0.071(4) Uiso 1 1 d .
H28A H 0.3682 0.2294 0.1079 0.106 Uiso 1 1 calc R
H28B H 0.3734 0.2183 0.0391 0.106 Uiso 1 1 calc R
H28C H 0.3827 0.1389 0.0852 0.106 Uiso 1 1 calc R
C29 C 0.3622(4) 0.0009(8) 0.1477(7) 0.085(5) Uani 1 1 d .
H29A H 0.3694 0.0028 0.1074 0.127 Uiso 1 1 calc R
H29B H 0.3711 -0.0548 0.1667 0.127 Uiso 1 1 calc R
H29C H 0.3792 0.0461 0.1737 0.127 Uiso 1 1 calc R
C30 C 0.2693(4) -0.0739(7) 0.0936(5) 0.063(3) Uani 1 1 d .
H30A H 0.2361 -0.0648 0.0851 0.095 Uiso 1 1 calc R
H30B H 0.2772 -0.1268 0.1170 0.095 Uiso 1 1 calc R
H30C H 0.2788 -0.0782 0.0549 0.095 Uiso 1 1 calc R
C31 C 0.2890(4) 0.0088(7) 0.2169(5) 0.052(3) Uani 1 1 d .
H31A H 0.3081 0.0506 0.2439 0.078 Uiso 1 1 calc R
H31B H 0.2969 -0.0489 0.2328 0.078 Uiso 1 1 calc R
H31C H 0.2566 0.0201 0.2152 0.078 Uiso 1 1 calc R
C32 C 0.1101(4) 0.2466(8) -0.0585(5) 0.063(3) Uani 1 1 d .
H32A H 0.0911 0.2945 -0.0512 0.094 Uiso 1 1 calc R
H32B H 0.0915 0.2070 -0.0879 0.094 Uiso 1 1 calc R
H32C H 0.1354 0.2683 -0.0750 0.094 Uiso 1 1 calc R
C33 C 0.1650(4) 0.0977(7) -0.0086(5) 0.051(3) Uani 1 1 d .
H33A H 0.1863 0.1187 -0.0323 0.077 Uiso 1 1 calc R
H33B H 0.1429 0.0585 -0.0339 0.077 Uiso 1 1 calc R
H33C H 0.1822 0.0676 0.0279 0.077 Uiso 1 1 calc R
C34 C 0.0844(3) 0.1478(7) 0.0437(5) 0.051(3) Uani 1 1 d .
H34A H 0.0959 0.1132 0.0805 0.077 Uiso 1 1 calc R
H34B H 0.0648 0.1126 0.0119 0.077 Uiso 1 1 calc R
H34C H 0.0665 0.1959 0.0537 0.077 Uiso 1 1 calc R
C35 C 0.1025(3) 0.3848(6) 0.0793(5) 0.051(3) Uani 1 1 d .
H35A H 0.0807 0.3539 0.0472 0.076 Uiso 1 1 calc R
H35B H 0.0973 0.4464 0.0738 0.076 Uiso 1 1 calc R
H35C H 0.0982 0.3677 0.1195 0.076 Uiso 1 1 calc R
C36 C 0.1750(4) 0.4195(7) 0.0091(6) 0.064(4) Uani 1 1 d .
H36A H 0.2068 0.4095 0.0073 0.096 Uiso 1 1 calc R
H36B H 0.1702 0.4806 0.0147 0.096 Uiso 1 1 calc R
H36C H 0.1544 0.4002 -0.0292 0.096 Uiso 1 1 calc R
C37 C 0.2037(4) 0.4027(6) 0.1444(5) 0.058(3) Uani 1 1 d .
H37A H 0.2007 0.3706 0.1806 0.087 Uiso 1 1 calc R
H37B H 0.1967 0.4631 0.1494 0.087 Uiso 1 1 calc R
H37C H 0.2351 0.3973 0.1393 0.087 Uiso 1 1 calc R
C38 C 0.1611(3) -0.0100(6) 0.1574(4) 0.039(2) Uani 1 1 d .
C39 C 0.1613(3) -0.0286(6) 0.2143(4) 0.035(2) Uani 1 1 d D
C40 C 0.2529(4) -0.1869(7) 0.3252(6) 0.066(4) Uani 1 1 d .
H40A H 0.2343 -0.1349 0.3227 0.099 Uiso 1 1 calc R
H40B H 0.2810 -0.1743 0.3119 0.099 Uiso 1 1 calc R
H40C H 0.2608 -0.2075 0.3676 0.099 Uiso 1 1 calc R
C41 C 0.2548(4) -0.3717(8) 0.2841(8) 0.087(5) Uani 1 1 d .
H41A H 0.2543 -0.3987 0.3233 0.131 Uiso 1 1 calc R
H41B H 0.2865 -0.3581 0.2832 0.131 Uiso 1 1 calc R
H41C H 0.2417 -0.4109 0.2506 0.131 Uiso 1 1 calc R
C42 C 0.2141(4) -0.2375(8) 0.1950(5) 0.064(3) Uani 1 1 d .
H42A H 0.1932 -0.2767 0.1679 0.096 Uiso 1 1 calc R
H42B H 0.2442 -0.2393 0.1854 0.096 Uiso 1 1 calc R
H42C H 0.2018 -0.1793 0.1891 0.096 Uiso 1 1 calc R
C43 C 0.1937(5) -0.3323(8) 0.4238(5) 0.075(4) Uani 1 1 d .
H43A H 0.2260 -0.3387 0.4232 0.112 Uiso 1 1 calc R
H43B H 0.1861 -0.3727 0.4532 0.112 Uiso 1 1 calc R
H43C H 0.1882 -0.2739 0.4360 0.112 Uiso 1 1 calc R
C44 C 0.1644(5) -0.4701(7) 0.3278(7) 0.078(4) Uani 1 1 d .
H44A H 0.1503 -0.4804 0.2844 0.118 Uiso 1 1 calc R
H44B H 0.1494 -0.5061 0.3530 0.118 Uiso 1 1 calc R
H44C H 0.1971 -0.4842 0.3362 0.118 Uiso 1 1 calc R
C45 C 0.0959(4) -0.3447(7) 0.3518(5) 0.057(3) Uani 1 1 d .
H45A H 0.0910 -0.2886 0.3686 0.085 Uiso 1 1 calc R
H45B H 0.0891 -0.3896 0.3787 0.085 Uiso 1 1 calc R
H45C H 0.0756 -0.3509 0.3109 0.085 Uiso 1 1 calc R
C46 C 0.0776(4) 0.0417(6) 0.3067(5) 0.055(3) Uani 1 1 d .
H46A H 0.0950 0.0401 0.2749 0.083 Uiso 1 1 calc R
H46B H 0.0905 0.0857 0.3370 0.083 Uiso 1 1 calc R
H46C H 0.0455 0.0551 0.2880 0.083 Uiso 1 1 calc R
C47 C 0.1429(3) -0.0906(6) 0.3829(5) 0.045(3) Uani 1 1 d .
H47A H 0.1442 -0.1401 0.4099 0.068 Uiso 1 1 calc R
H47B H 0.1571 -0.0413 0.4069 0.068 Uiso 1 1 calc R
H47C H 0.1595 -0.1035 0.3513 0.068 Uiso 1 1 calc R
C48 C 0.0501(4) -0.0557(7) 0.4079(5) 0.060(3) Uani 1 1 d .
H48A H 0.0179 -0.0417 0.3901 0.090 Uiso 1 1 calc R
H48B H 0.0641 -0.0103 0.4363 0.090 Uiso 1 1 calc R
H48C H 0.0519 -0.1100 0.4301 0.090 Uiso 1 1 calc R
C49 C -0.0142(4) -0.2334(8) 0.3406(6) 0.060(3) Uani 1 1 d .
H49A H -0.0001 -0.2903 0.3455 0.090 Uiso 1 1 calc R
H49B H -0.0476 -0.2391 0.3315 0.090 Uiso 1 1 calc R
H49C H -0.0037 -0.2009 0.3786 0.090 Uiso 1 1 calc R
C50 C -0.0391(4) -0.0862(7) 0.2513(6) 0.068(4) Uani 1 1 d .
H50A H -0.0344 -0.0422 0.2833 0.101 Uiso 1 1 calc R
H50B H -0.0705 -0.1080 0.2440 0.101 Uiso 1 1 calc R
H50C H -0.0340 -0.0613 0.2134 0.101 Uiso 1 1 calc R
C51 C -0.0054(3) -0.2533(7) 0.2118(5) 0.052(3) Uani 1 1 d .
H51A H 0.0060 -0.2277 0.1784 0.077 Uiso 1 1 calc R
H51B H -0.0381 -0.2665 0.1971 0.077 Uiso 1 1 calc R
H51C H 0.0116 -0.3059 0.2255 0.077 Uiso 1 1 calc R
C52 C 0.0950(4) -0.3902(7) 0.1670(5) 0.068(4) Uani 1 1 d .
H52A H 0.1265 -0.3803 0.1903 0.102 Uiso 1 1 calc R
H52B H 0.0922 -0.4486 0.1507 0.102 Uiso 1 1 calc R
H52C H 0.0740 -0.3827 0.1940 0.102 Uiso 1 1 calc R
C53 C 0.0210(4) -0.3390(8) 0.0573(6) 0.072(4) Uani 1 1 d .
H53A H -0.0009 -0.3296 0.0827 0.107 Uiso 1 1 calc R
H53B H 0.0198 -0.3989 0.0444 0.107 Uiso 1 1 calc R
H53C H 0.0131 -0.3021 0.0211 0.107 Uiso 1 1 calc R
C54 C 0.1216(4) -0.3337(9) 0.0533(6) 0.073(4) Uani 1 1 d .
H54A H 0.1204 -0.2864 0.0244 0.110 Uiso 1 1 calc R
H54B H 0.1132 -0.3870 0.0305 0.110 Uiso 1 1 calc R
H54C H 0.1527 -0.3386 0.0792 0.110 Uiso 1 1 calc R
C55 C 0.0539(4) -0.1262(9) 0.0140(5) 0.075(4) Uani 1 1 d .
H55A H 0.0748 -0.1578 -0.0054 0.113 Uiso 1 1 calc R
H55B H 0.0487 -0.0690 -0.0041 0.113 Uiso 1 1 calc R
H55C H 0.0246 -0.1567 0.0074 0.113 Uiso 1 1 calc R
C56 C 0.1363(3) -0.0616(6) 0.1000(4) 0.039(2) Uani 1 1 d .
H56A H 0.1579 -0.1061 0.0930 0.046 Uiso 1 1 calc R
H56B H 0.1314 -0.0222 0.0646 0.046 Uiso 1 1 calc R
N1 N 0.4723(3) 0.7006(4) 0.1476(3) 0.0336(18) Uani 1 1 d .
N2 N 0.4433(3) 0.7746(6) -0.0200(3) 0.050(2) Uani 1 1 d .
N3 N 0.3623(3) 0.6071(5) 0.0371(4) 0.045(2) Uani 1 1 d .
N4 N 0.2408(3) 0.2265(4) 0.2378(4) 0.0328(18) Uani 1 1 d .
N5 N 0.2796(3) 0.1173(5) 0.1058(3) 0.0376(19) Uani 1 1 d .
N6 N 0.1699(2) 0.2485(5) 0.0705(3) 0.0325(17) Uani 1 1 d .
N7 N 0.1669(3) -0.2845(4) 0.2898(3) 0.0358(19) Uani 1 1 d .
N8 N 0.0593(2) -0.1440(4) 0.2938(3) 0.0293(17) Uani 1 1 d .
N9 N 0.0846(3) -0.2141(5) 0.1354(4) 0.042(2) Uani 1 1 d .
O1 O 0.4679(3) 0.5880(5) 0.0289(4) 0.067(2) Uani 1 1 d .
O2 O 0.1846(2) 0.0629(4) 0.1453(3) 0.0404(16) Uani 1 1 d .
O3 O 0.1401(2) -0.0979(4) 0.2300(3) 0.0343(15) Uani 1 1 d .
Si1 Si 0.49608(10) 0.61204(18) 0.18760(13) 0.0453(7) Uani 1 1 d .
Si2 Si 0.48133(10) 0.80444(17) 0.17535(13) 0.0397(7) Uani 1 1 d .
Si3 Si 0.49732(11) 0.7819(2) -0.03407(14) 0.0544(8) Uani 1 1 d .
Si4 Si 0.39788(11) 0.8373(3) -0.06193(15) 0.0619(10) Uani 1 1 d .
Si5 Si 0.35177(11) 0.5310(2) -0.02008(19) 0.0650(11) Uani 1 1 d .
Si6 Si 0.32656(11) 0.6254(2) 0.08578(17) 0.0559(9) Uani 1 1 d .
Si7 Si 0.19953(10) 0.21888(18) 0.27923(13) 0.0424(7) Uani 1 1 d .
Si8 Si 0.29414(10) 0.27078(19) 0.26989(14) 0.0464(7) Uani 1 1 d .
Si9 Si 0.30184(11) 0.1589(2) 0.04819(16) 0.0564(9) Uani 1 1 d .
Si10 Si 0.29927(10) 0.01754(18) 0.13875(14) 0.0454(7) Uani 1 1 d .
Si11 Si 0.13390(10) 0.18962(17) 0.01502(12) 0.0387(6) Uani 1 1 d .
Si12 Si 0.16241(9) 0.35877(17) 0.07454(13) 0.0383(6) Uani 1 1 d .
Si13 Si 0.21971(9) -0.26987(18) 0.27510(15) 0.0449(7) Uani 1 1 d .
Si14 Si 0.15730(11) -0.35415(18) 0.34636(14) 0.0466(7) Uani 1 1 d .
Si15 Si 0.08129(10) -0.06534(16) 0.34554(13) 0.0373(6) Uani 1 1 d .
Si16 Si 0.00268(9) -0.17662(18) 0.27680(14) 0.0401(7) Uani 1 1 d .
Si17 Si 0.08025(11) -0.3127(2) 0.10261(14) 0.0496(8) Uani 1 1 d .
Si18 Si 0.07949(10) -0.11674(19) 0.09724(13) 0.0432(7) Uani 1 1 d .
U1 U 0.428425(13) 0.68485(2) 0.051062(16) 0.04055(11) Uani 1 1 d .
U2 U 0.222359(12) 0.17420(2) 0.141087(16) 0.03292(10) Uani 1 1 d .
U3 U 0.105101(12) -0.20813(2) 0.239304(15) 0.03005(10) Uani 1 1 d .
C57 C 0.0422(4) -0.0500(10) 0.1277(6) 0.098(6) Uani 1 1 d .
H57A H 0.0127 -0.0789 0.1240 0.147 Uiso 1 1 calc R
H57B H 0.0373 0.0039 0.1049 0.147 Uiso 1 1 calc R
H57C H 0.0560 -0.0382 0.1710 0.147 Uiso 1 1 calc R
H39 H 0.181(4) 0.008(7) 0.245(5) 0.118 Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
C19 C19 O1 175.4(18) 3_665
C39 C38 O2 119.0(9) .
C39 C38 C56 125.8(9) .
O2 C38 C56 115.2(8) .
C38 C39 O3 122.7(9) .
C38 C56 Si18 120.9(7) .
Si1 N1 Si2 123.9(4) .
Si1 N1 U1 119.3(4) .
Si2 N1 U1 116.8(4) .
Si3 N2 Si4 120.5(5) .
Si3 N2 U1 121.5(5) .
Si4 N2 U1 118.0(4) .
Si5 N3 Si6 123.7(5) .
Si5 N3 U1 118.0(5) .
Si6 N3 U1 118.3(4) .
Si7 N4 Si8 121.0(5) .
Si7 N4 U2 116.7(4) .
Si8 N4 U2 122.3(4) .
Si9 N5 Si10 120.0(4) .
Si9 N5 U2 125.7(4) .
Si10 N5 U2 114.2(4) .
Si11 N6 Si12 120.2(4) .
Si11 N6 U2 116.5(4) .
Si12 N6 U2 123.1(4) .
Si13 N7 Si14 123.0(4) .
Si13 N7 U3 121.2(4) .
Si14 N7 U3 115.8(4) .
Si15 N8 Si16 124.2(4) .
Si15 N8 U3 119.8(4) .
Si16 N8 U3 115.9(4) .
Si17 N9 Si18 126.3(5) .
Si17 N9 U3 117.2(4) .
Si18 N9 U3 116.3(4) .
C19 O1 U1 175.2(8) .
C38 O2 U2 171.6(6) .
C39 O3 U3 170.9(6) .
N1 Si1 C1 114.0(5) .
N1 Si1 C3 111.8(5) .
C1 Si1 C3 107.5(6) .
N1 Si1 C2 108.6(5) .
C1 Si1 C2 106.7(7) .
C3 Si1 C2 108.1(6) .
C1 Si1 U1 142.1(4) .
C3 Si1 U1 106.3(4) .
C2 Si1 U1 78.4(4) .
N1 Si2 C4 114.4(5) .
N1 Si2 C5 111.8(5) .
C4 Si2 C5 107.0(6) .
N1 Si2 C6 108.5(4) .
C4 Si2 C6 105.0(5) .
C5 Si2 C6 109.9(6) .
C4 Si2 U1 121.7(4) .
C5 Si2 U1 129.2(5) .
C6 Si2 U1 72.4(3) .
N2 Si3 C9 110.2(5) .
N2 Si3 C7 109.7(5) .
C9 Si3 C7 108.1(6) .
N2 Si3 C8 113.7(5) .
C9 Si3 C8 108.6(6) .
C7 Si3 C8 106.4(7) .
N2 Si4 C12 106.1(5) .
N2 Si4 C11 112.1(6) .
C12 Si4 C11 107.9(6) .
N2 Si4 C10 115.1(5) .
C12 Si4 C10 107.4(6) .
C11 Si4 C10 107.9(7) .
C12 Si4 U1 70.9(4) .
C11 Si4 U1 124.6(5) .
C10 Si4 U1 125.7(5) .
N3 Si5 C13 110.2(5) .
N3 Si5 C15 111.8(6) .
C13 Si5 C15 107.5(8) .
N3 Si5 C14 111.6(5) .
C13 Si5 C14 108.1(7) .
C15 Si5 C14 107.4(6) .
C13 Si5 U1 79.4(4) .
C15 Si5 U1 105.9(4) .
C14 Si5 U1 141.4(4) .
N3 Si6 C16 113.5(6) .
N3 Si6 C17 108.8(5) .
C16 Si6 C17 106.2(6) .
N3 Si6 C18 111.7(6) .
C16 Si6 C18 108.8(6) .
C17 Si6 C18 107.5(7) .
C16 Si6 U1 123.9(4) .
C17 Si6 U1 73.3(4) .
C18 Si6 U1 125.2(5) .
N4 Si7 C21 112.5(5) .
N4 Si7 C20 108.9(4) .
C21 Si7 C20 111.3(5) .
N4 Si7 C22 113.7(5) .
C21 Si7 C22 105.2(6) .
C20 Si7 C22 105.2(6) .
C21 Si7 U2 115.5(4) .
C20 Si7 U2 74.6(3) .
C22 Si7 U2 136.5(4) .
N4 Si8 C25 108.8(5) .
N4 Si8 C23 113.0(5) .
C25 Si8 C23 108.9(6) .
N4 Si8 C24 114.9(5) .
C25 Si8 C24 104.1(6) .
C23 Si8 C24 106.6(6) .
N5 Si9 C27 108.4(4) .
N5 Si9 C28 114.1(5) .
C27 Si9 C28 105.1(6) .
N5 Si9 C26 112.6(6) .
C27 Si9 C26 108.1(6) .
C28 Si9 C26 108.1(7) .
N5 Si10 C31 110.4(4) .
N5 Si10 C30 112.3(5) .
C31 Si10 C30 107.0(5) .
N5 Si10 C29 113.3(5) .
C31 Si10 C29 106.1(6) .
C30 Si10 C29 107.3(6) .
C31 Si10 U2 76.8(3) .
C30 Si10 U2 108.9(4) .
C29 Si10 U2 140.9(5) .
N6 Si11 C33 110.5(4) .
N6 Si11 C32 115.5(5) .
C33 Si11 C32 103.3(5) .
N6 Si11 C34 110.7(4) .
C33 Si11 C34 108.8(5) .
C32 Si11 C34 107.7(5) .
C33 Si11 U2 80.6(3) .
C32 Si11 U2 146.2(4) .
C34 Si11 U2 102.4(4) .
N6 Si12 C36 114.2(5) .
N6 Si12 C35 110.9(4) .
C36 Si12 C35 108.1(5) .
N6 Si12 C37 109.7(4) .
C36 Si12 C37 104.8(5) .
C35 Si12 C37 108.9(5) .
N7 Si13 C42 110.6(5) .
N7 Si13 C40 111.5(5) .
C42 Si13 C40 108.3(6) .
N7 Si13 C41 112.6(5) .
C42 Si13 C41 104.9(6) .
C40 Si13 C41 108.7(6) .
N7 Si14 C43 113.9(5) .
N7 Si14 C45 109.3(4) .
C43 Si14 C45 107.0(6) .
N7 Si14 C44 113.1(5) .
C43 Si14 C44 108.3(6) .
C45 Si14 C44 104.7(5) .
C43 Si14 U3 127.4(4) .
C45 Si14 U3 72.6(3) .
C44 Si14 U3 123.0(5) .
N8 Si15 C48 112.8(5) .
N8 Si15 C46 110.7(4) .
C48 Si15 C46 107.0(5) .
N8 Si15 C47 109.3(4) .
C48 Si15 C47 107.3(5) .
C46 Si15 C47 109.7(5) .
C48 Si15 U3 142.3(4) .
C46 Si15 U3 104.7(4) .
C47 Si15 U3 80.3(3) .
N8 Si16 C49 113.8(5) .
N8 Si16 C51 107.6(4) .
C49 Si16 C51 106.8(5) .
N8 Si16 C50 113.1(5) .
C49 Si16 C50 108.1(5) .
C51 Si16 C50 106.9(6) .
C49 Si16 U3 123.2(4) .
C51 Si16 U3 70.8(3) .
C50 Si16 U3 127.3(4) .
N9 Si17 C52 105.9(4) .
N9 Si17 C53 113.6(5) .
C52 Si17 C53 107.5(6) .
N9 Si17 C54 114.9(5) .
C52 Si17 C54 106.1(6) .
C53 Si17 C54 108.4(5) .
C52 Si17 U3 69.5(3) .
C53 Si17 U3 124.9(4) .
C54 Si17 U3 125.6(4) .
N9 Si18 C57 108.3(5) .
N9 Si18 C55 113.3(5) .
C57 Si18 C55 106.7(6) .
N9 Si18 C56 114.1(4) .
C57 Si18 C56 111.2(6) .
C55 Si18 C56 103.0(5) .
C57 Si18 U3 84.8(4) .
C55 Si18 U3 149.1(4) .
C56 Si18 U3 99.1(3) .
O1 U1 N2 93.8(3) .
O1 U1 N1 94.3(3) .
N2 U1 N1 116.3(3) .
O1 U1 N3 96.1(3) .
N2 U1 N3 123.1(3) .
N1 U1 N3 118.5(3) .
O1 U1 Si2 114.7(2) .
N2 U1 Si2 96.1(2) .
N1 U1 Si2 26.97(18) .
N3 U1 Si2 128.5(2) .
O1 U1 Si4 113.5(3) .
N2 U1 Si4 26.8(2) .
N1 U1 Si4 128.48(19) .
N3 U1 Si4 101.3(2) .
Si2 U1 Si4 102.34(8) .
O1 U1 Si1 73.8(2) .
N2 U1 Si1 131.6(2) .
N1 U1 Si1 25.67(18) .
N3 U1 Si1 104.8(2) .
Si2 U1 Si1 52.63(7) .
Si4 U1 Si1 151.93(8) .
O1 U1 Si5 74.5(2) .
N2 U1 Si5 109.2(2) .
N1 U1 Si5 133.7(2) .
N3 U1 Si5 26.2(2) .
Si2 U1 Si5 152.74(9) .
Si4 U1 Si5 96.29(9) .
Si1 U1 Si5 111.69(8) .
O1 U1 Si6 116.6(2) .
N2 U1 Si6 131.5(2) .
N1 U1 Si6 99.1(2) .
N3 U1 Si6 26.1(2) .
Si2 U1 Si6 103.13(8) .
Si4 U1 Si6 104.90(8) .
Si1 U1 Si6 94.38(8) .
Si5 U1 Si6 52.29(9) .
O2 U2 N5 98.9(3) .
O2 U2 N4 105.6(2) .
N5 U2 N4 116.7(3) .
O2 U2 N6 99.5(2) .
N5 U2 N6 114.7(3) .
N4 U2 N6 117.2(3) .
O2 U2 Si10 77.05(17) .
N5 U2 Si10 28.5(2) .
N4 U2 Si10 105.32(18) .
N6 U2 Si10 136.38(19) .
O2 U2 Si11 76.84(17) .
N5 U2 Si11 104.2(2) .
N4 U2 Si11 137.64(18) .
N6 U2 Si11 26.8(2) .
Si10 U2 Si11 116.13(7) .
O2 U2 Si7 84.36(18) .
N5 U2 Si7 137.8(2) .
N4 U2 Si7 26.84(19) .
N6 U2 Si7 105.99(19) .
Si10 U2 Si7 116.68(7) .
Si11 U2 Si7 117.30(7) .
O3 U3 N9 87.2(2) .
O3 U3 N7 96.7(3) .
N9 U3 N7 118.9(3) .
O3 U3 N8 94.2(2) .
N9 U3 N8 121.3(3) .
N7 U3 N8 119.2(3) .
O3 U3 Si17 108.64(17) .
N9 U3 Si17 26.4(2) .
N7 U3 Si17 100.2(2) .
N8 U3 Si17 131.74(19) .
O3 U3 Si16 114.59(18) .
N9 U3 Si16 102.6(2) .
N7 U3 Si16 129.0(2) .
N8 U3 Si16 27.14(19) .
Si17 U3 Si16 105.94(7) .
O3 U3 Si18 63.95(17) .
N9 U3 Si18 27.1(2) .
N7 U3 Si18 131.6(2) .
N8 U3 Si18 106.67(18) .
Si17 U3 Si18 53.49(8) .
Si16 U3 Si18 98.84(7) .
O3 U3 Si14 118.20(17) .
N9 U3 Si14 131.6(2) .
N7 U3 Si14 27.4(2) .
N8 U3 Si14 98.67(18) .
Si17 U3 Si14 106.25(8) .
Si16 U3 Si14 102.28(7) .
Si18 U3 Si14 154.44(7) .
O3 U3 Si15 73.91(17) .
N9 U3 Si15 133.2(2) .
N7 U3 Si15 105.8(2) .
N8 U3 Si15 25.40(19) .
Si17 U3 Si15 153.48(7) .
Si16 U3 Si15 52.53(7) .
Si18 U3 Si15 109.65(7) .
Si14 U3 Si15 94.66(7) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 Si1 1.837(12) .
C2 Si1 1.866(12) .
C3 Si1 1.853(11) .
C4 Si2 1.855(11) .
C5 Si2 1.882(12) .
C6 Si2 1.890(10) .
C7 Si3 1.844(11) .
C8 Si3 1.902(12) .
C9 Si3 1.813(11) .
C10 Si4 1.886(14) .
C11 Si4 1.865(13) .
C12 Si4 1.859(11) .
C13 Si5 1.854(17) .
C14 Si5 1.874(12) .
C15 Si5 1.868(12) .
C16 Si6 1.850(12) .
C17 Si6 1.848(12) .
C18 Si6 1.875(12) .
C19 C19 1.09(2) 3_665
C19 O1 1.338(11) .
C20 Si7 1.864(10) .
C21 Si7 1.846(11) .
C22 Si7 1.874(11) .
C23 Si8 1.863(11) .
C24 Si8 1.875(12) .
C25 Si8 1.829(12) .
C26 Si9 1.889(14) .
C27 Si9 1.876(10) .
C28 Si9 1.881(13) .
C29 Si10 1.872(11) .
C30 Si10 1.859(11) .
C31 Si10 1.858(11) .
C32 Si11 1.864(10) .
C33 Si11 1.860(10) .
C34 Si11 1.873(11) .
C35 Si12 1.871(10) .
C36 Si12 1.864(10) .
C37 Si12 1.884(11) .
C38 C39 1.310(13) .
C38 O2 1.402(11) .
C38 C56 1.555(13) .
C39 O3 1.345(11) .
C40 Si13 1.848(11) .
C41 Si13 1.895(11) .
C42 Si13 1.838(12) .
C43 Si14 1.854(12) .
C44 Si14 1.886(11) .
C45 Si14 1.882(12) .
C46 Si15 1.881(10) .
C47 Si15 1.885(10) .
C48 Si15 1.867(11) .
C49 Si16 1.858(11) .
C50 Si16 1.888(10) .
C51 Si16 1.862(11) .
C52 Si17 1.861(12) .
C53 Si17 1.874(12) .
C54 Si17 1.879(12) .
C55 Si18 1.853(11) .
C56 Si18 1.899(9) .
N1 Si1 1.713(7) .
N1 Si2 1.740(7) .
N1 U1 2.269(7) .
N2 Si3 1.729(8) .
N2 Si4 1.761(9) .
N2 U1 2.250(8) .
N3 Si5 1.726(8) .
N3 Si6 1.728(9) .
N3 U1 2.287(8) .
N4 Si7 1.722(8) .
N4 Si8 1.736(8) .
N4 U2 2.266(8) .
N5 Si9 1.718(8) .
N5 Si10 1.769(8) .
N5 U2 2.242(7) .
N6 Si11 1.714(8) .
N6 Si12 1.745(8) .
N6 U2 2.273(7) .
N7 Si13 1.710(9) .
N7 Si14 1.749(8) .
N7 U3 2.273(7) .
N8 Si15 1.714(7) .
N8 Si16 1.730(8) .
N8 U3 2.279(7) .
N9 Si17 1.703(8) .
N9 Si18 1.738(8) .
N9 U3 2.271(8) .
O1 U1 2.058(7) .
O2 U2 2.093(7) .
O3 U3 2.057(6) .
Si1 U1 3.449(3) .
Si2 U1 3.425(3) .
Si4 U1 3.447(3) .
Si5 U1 3.451(3) .
Si6 U1 3.458(3) .
Si7 U2 3.407(3) .
Si10 U2 3.377(3) .
Si11 U2 3.403(3) .
Si14 U3 3.418(3) .
Si15 U3 3.467(3) .
Si16 U3 3.411(3) .
Si17 U3 3.405(3) .
Si18 C57 1.784(14) .
Si18 U3 3.416(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
O2 C38 C39 O3 -179.1(8)
C56 C38 C39 O3 1.4(15)
C39 C38 C56 Si18 34.7(13)
O2 C38 C56 Si18 -144.8(6)
Si2 N1 Si1 C1 32.0(9)
U1 N1 Si1 C1 -150.4(6)
Si2 N1 Si1 C3 -90.2(7)
U1 N1 Si1 C3 87.4(6)
Si2 N1 Si1 C2 150.7(7)
U1 N1 Si1 C2 -31.7(7)
Si2 N1 Si1 U1 -177.6(9)
Si1 N1 Si2 C4 -71.4(7)
U1 N1 Si2 C4 111.0(5)
Si1 N1 Si2 C5 50.4(8)
U1 N1 Si2 C5 -127.2(7)
Si1 N1 Si2 C6 171.8(5)
U1 N1 Si2 C6 -5.9(6)
Si1 N1 Si2 U1 177.6(8)
Si4 N2 Si3 C9 -91.2(7)
U1 N2 Si3 C9 88.2(6)
Si4 N2 Si3 C7 150.0(7)
U1 N2 Si3 C7 -30.7(8)
Si4 N2 Si3 C8 31.0(8)
U1 N2 Si3 C8 -149.7(6)
Si3 N2 Si4 C12 177.6(6)
U1 N2 Si4 C12 -1.8(7)
Si3 N2 Si4 C11 60.1(8)
U1 N2 Si4 C11 -119.3(6)
Si3 N2 Si4 C10 -63.8(8)
U1 N2 Si4 C10 116.9(7)
Si3 N2 Si4 U1 179.4(9)
Si6 N3 Si5 C13 149.8(7)
U1 N3 Si5 C13 -32.2(7)
Si6 N3 Si5 C15 -90.7(8)
U1 N3 Si5 C15 87.3(7)
Si6 N3 Si5 C14 29.6(8)
U1 N3 Si5 C14 -152.4(6)
Si6 N3 Si5 U1 -178.0(9)
Si5 N3 Si6 C16 -66.2(7)
U1 N3 Si6 C16 115.9(5)
Si5 N3 Si6 C17 175.9(6)
U1 N3 Si6 C17 -2.1(7)
Si5 N3 Si6 C18 57.3(8)
U1 N3 Si6 C18 -120.7(6)
Si5 N3 Si6 U1 178.0(9)
Si8 N4 Si7 C21 -76.1(6)
U2 N4 Si7 C21 102.9(5)
Si8 N4 Si7 C20 160.1(5)
U2 N4 Si7 C20 -20.9(5)
Si8 N4 Si7 C22 43.3(8)
U2 N4 Si7 C22 -137.7(6)
Si8 N4 Si7 U2 -179.0(7)
Si7 N4 Si8 C25 180.0(6)
U2 N4 Si8 C25 1.0(6)
Si7 N4 Si8 C23 58.9(7)
U2 N4 Si8 C23 -120.0(5)
Si7 N4 Si8 C24 -63.8(7)
U2 N4 Si8 C24 117.3(6)
Si10 N5 Si9 C27 176.3(6)
U2 N5 Si9 C27 0.8(7)
Si10 N5 Si9 C28 -67.0(7)
U2 N5 Si9 C28 117.5(6)
Si10 N5 Si9 C26 56.7(7)
U2 N5 Si9 C26 -118.8(6)
Si9 N5 Si10 C31 156.8(6)
U2 N5 Si10 C31 -27.2(6)
Si9 N5 Si10 C30 -83.9(7)
U2 N5 Si10 C30 92.1(6)
Si9 N5 Si10 C29 38.0(8)
U2 N5 Si10 C29 -146.0(6)
Si9 N5 Si10 U2 -176.0(8)
Si12 N6 Si11 C33 147.5(5)
U2 N6 Si11 C33 -37.5(5)
Si12 N6 Si11 C32 30.8(7)
U2 N6 Si11 C32 -154.3(5)
Si12 N6 Si11 C34 -91.9(6)
U2 N6 Si11 C34 83.0(5)
Si12 N6 Si11 U2 -174.9(7)
Si11 N6 Si12 C36 -68.0(7)
U2 N6 Si12 C36 117.4(6)
Si11 N6 Si12 C35 54.5(6)
U2 N6 Si12 C35 -120.1(5)
Si11 N6 Si12 C37 174.7(5)
U2 N6 Si12 C37 0.2(6)
Si14 N7 Si13 C42 152.8(6)
U3 N7 Si13 C42 -30.4(6)
Si14 N7 Si13 C40 -86.6(6)
U3 N7 Si13 C40 90.3(6)
Si14 N7 Si13 C41 35.8(8)
U3 N7 Si13 C41 -147.3(6)
Si13 N7 Si14 C43 55.9(7)
U3 N7 Si14 C43 -121.1(6)
Si13 N7 Si14 C45 175.5(5)
U3 N7 Si14 C45 -1.5(6)
Si13 N7 Si14 C44 -68.3(7)
U3 N7 Si14 C44 114.7(6)
Si13 N7 Si14 U3 177.0(8)
Si16 N8 Si15 C48 28.7(7)
U3 N8 Si15 C48 -154.2(5)
Si16 N8 Si15 C46 -91.2(6)
U3 N8 Si15 C46 86.0(5)
Si16 N8 Si15 C47 147.9(5)
U3 N8 Si15 C47 -35.0(6)
Si16 N8 Si15 U3 -177.2(8)
Si15 N8 Si16 C49 -68.6(7)
U3 N8 Si16 C49 114.2(5)
Si15 N8 Si16 C51 173.2(5)
U3 N8 Si16 C51 -4.0(5)
Si15 N8 Si16 C50 55.4(7)
U3 N8 Si16 C50 -121.9(5)
Si15 N8 Si16 U3 177.3(7)
Si18 N9 Si17 C52 174.1(6)
U3 N9 Si17 C52 -0.2(6)
Si18 N9 Si17 C53 -68.2(8)
U3 N9 Si17 C53 117.5(6)
Si18 N9 Si17 C54 57.4(8)
U3 N9 Si17 C54 -116.9(6)
Si18 N9 Si17 U3 174.3(9)
Si17 N9 Si18 C57 133.0(7)
U3 N9 Si18 C57 -52.7(7)
Si17 N9 Si18 C55 14.8(8)
U3 N9 Si18 C55 -170.8(5)
Si17 N9 Si18 C56 -102.6(6)
U3 N9 Si18 C56 71.7(6)
Si17 N9 Si18 U3 -174.3(9)
C38 C56 Si18 N9 -80.2(8)
C38 C56 Si18 C57 42.6(9)
C38 C56 Si18 C55 156.5(8)
C38 C56 Si18 U3 -45.3(7)
Si3 N2 U1 O1 -40.1(5)
Si4 N2 U1 O1 139.2(5)
Si3 N2 U1 N1 56.5(6)
Si4 N2 U1 N1 -124.1(4)
Si3 N2 U1 N3 -139.9(4)
Si4 N2 U1 N3 39.5(6)
Si3 N2 U1 Si2 75.2(5)
Si4 N2 U1 Si2 -105.4(5)
Si3 N2 U1 Si4 -179.4(9)
Si3 N2 U1 Si1 31.4(7)
Si4 N2 U1 Si1 -149.2(3)
Si3 N2 U1 Si5 -115.0(5)
Si4 N2 U1 Si5 64.3(5)
Si3 N2 U1 Si6 -171.2(3)
Si4 N2 U1 Si6 8.1(7)
Si1 N1 U1 O1 -36.7(5)
Si2 N1 U1 O1 141.1(5)
Si1 N1 U1 N2 -133.0(5)
Si2 N1 U1 N2 44.7(5)
Si1 N1 U1 N3 62.6(5)
Si2 N1 U1 N3 -119.6(4)
Si1 N1 U1 Si2 -177.7(8)
Si1 N1 U1 Si4 -161.5(3)
Si2 N1 U1 Si4 16.3(5)
Si2 N1 U1 Si1 177.7(8)
Si1 N1 U1 Si5 35.9(6)
Si2 N1 U1 Si5 -146.4(3)
Si1 N1 U1 Si6 81.1(4)
Si2 N1 U1 Si6 -101.1(4)
Si5 N3 U1 O1 -34.4(5)
Si6 N3 U1 O1 143.7(5)
Si5 N3 U1 N2 64.1(6)
Si6 N3 U1 N2 -117.8(5)
Si5 N3 U1 N1 -132.6(4)
Si6 N3 U1 N1 45.4(5)
Si5 N3 U1 Si2 -162.9(3)
Si6 N3 U1 Si2 15.2(6)
Si5 N3 U1 Si4 81.1(4)
Si6 N3 U1 Si4 -100.8(4)
Si5 N3 U1 Si1 -109.2(4)
Si6 N3 U1 Si1 68.9(4)
Si6 N3 U1 Si5 178.1(8)
Si5 N3 U1 Si6 -178.1(8)
N1 Si2 U1 O1 -43.6(5)
C4 Si2 U1 O1 -132.4(5)
C5 Si2 U1 O1 28.9(7)
C6 Si2 U1 O1 130.5(5)
N1 Si2 U1 N2 -140.6(5)
C4 Si2 U1 N2 130.6(5)
C5 Si2 U1 N2 -68.1(7)
C6 Si2 U1 N2 33.5(4)
C4 Si2 U1 N1 -88.7(6)
C5 Si2 U1 N1 72.5(8)
C6 Si2 U1 N1 174.2(6)
N1 Si2 U1 N3 77.4(5)
C4 Si2 U1 N3 -11.3(5)
C5 Si2 U1 N3 149.9(7)
C6 Si2 U1 N3 -108.4(4)
N1 Si2 U1 Si4 -167.0(4)
C4 Si2 U1 Si4 104.2(4)
C5 Si2 U1 Si4 -94.5(7)
C6 Si2 U1 Si4 7.1(4)
N1 Si2 U1 Si1 -1.2(4)
C4 Si2 U1 Si1 -90.0(4)
C5 Si2 U1 Si1 71.3(7)
C6 Si2 U1 Si1 172.9(4)
N1 Si2 U1 Si5 60.9(5)
C4 Si2 U1 Si5 -27.8(5)
C5 Si2 U1 Si5 133.4(7)
C6 Si2 U1 Si5 -124.9(4)
N1 Si2 U1 Si6 84.2(4)
C4 Si2 U1 Si6 -4.5(4)
C5 Si2 U1 Si6 156.7(7)
C6 Si2 U1 Si6 -101.6(4)
N2 Si4 U1 O1 -45.3(6)
C12 Si4 U1 O1 132.9(5)
C11 Si4 U1 O1 33.9(6)
C10 Si4 U1 O1 -129.0(6)
C12 Si4 U1 N2 178.2(7)
C11 Si4 U1 N2 79.2(8)
C10 Si4 U1 N2 -83.7(8)
N2 Si4 U1 N1 71.4(6)
C12 Si4 U1 N1 -110.4(5)
C11 Si4 U1 N1 150.7(6)
C10 Si4 U1 N1 -12.2(6)
N2 Si4 U1 N3 -147.1(5)
C12 Si4 U1 N3 31.0(5)
C11 Si4 U1 N3 -67.9(6)
C10 Si4 U1 N3 129.2(6)
N2 Si4 U1 Si2 78.9(5)
C12 Si4 U1 Si2 -102.9(4)
C11 Si4 U1 Si2 158.1(6)
C10 Si4 U1 Si2 -4.8(6)
N2 Si4 U1 Si1 54.5(6)
C12 Si4 U1 Si1 -127.4(4)
C11 Si4 U1 Si1 133.7(6)
C10 Si4 U1 Si1 -29.2(6)
N2 Si4 U1 Si5 -121.1(5)
C12 Si4 U1 Si5 57.1(4)
C11 Si4 U1 Si5 -41.9(6)
C10 Si4 U1 Si5 155.2(6)
N2 Si4 U1 Si6 -173.7(5)
C12 Si4 U1 Si6 4.5(4)
C11 Si4 U1 Si6 -94.5(6)
C10 Si4 U1 Si6 102.6(6)
N1 Si1 U1 O1 141.7(5)
C1 Si1 U1 O1 -171.2(9)
C3 Si1 U1 O1 36.7(5)
C2 Si1 U1 O1 -69.0(5)
N1 Si1 U1 N2 61.3(6)
C1 Si1 U1 N2 108.4(9)
C3 Si1 U1 N2 -43.7(5)
C2 Si1 U1 N2 -149.3(6)
C1 Si1 U1 N1 47.2(10)
C3 Si1 U1 N1 -105.0(6)
C2 Si1 U1 N1 149.4(7)
N1 Si1 U1 N3 -126.2(5)
C1 Si1 U1 N3 -79.0(9)
C3 Si1 U1 N3 128.8(4)
C2 Si1 U1 N3 23.2(5)
N1 Si1 U1 Si2 1.3(5)
C1 Si1 U1 Si2 48.5(9)
C3 Si1 U1 Si2 -103.7(4)
C2 Si1 U1 Si2 150.7(5)
N1 Si1 U1 Si4 31.9(5)
C1 Si1 U1 Si4 79.1(9)
C3 Si1 U1 Si4 -73.1(4)
C2 Si1 U1 Si4 -178.7(5)
N1 Si1 U1 Si5 -152.9(5)
C1 Si1 U1 Si5 -105.7(9)
C3 Si1 U1 Si5 102.2(4)
C2 Si1 U1 Si5 -3.5(5)
N1 Si1 U1 Si6 -101.9(5)
C1 Si1 U1 Si6 -54.7(9)
C3 Si1 U1 Si6 153.1(4)
C2 Si1 U1 Si6 47.5(5)
N3 Si5 U1 O1 144.3(5)
C13 Si5 U1 O1 -66.2(6)
C15 Si5 U1 O1 39.1(7)
C14 Si5 U1 O1 -172.1(9)
N3 Si5 U1 N2 -127.1(5)
C13 Si5 U1 N2 22.4(5)
C15 Si5 U1 N2 127.7(7)
C14 Si5 U1 N2 -83.5(9)
N3 Si5 U1 N1 63.5(5)
C13 Si5 U1 N1 -147.1(5)
C15 Si5 U1 N1 -41.8(7)
C14 Si5 U1 N1 107.1(9)
C13 Si5 U1 N3 149.4(7)
C15 Si5 U1 N3 -105.3(8)
C14 Si5 U1 N3 43.6(10)
N3 Si5 U1 Si2 30.2(5)
C13 Si5 U1 Si2 179.6(5)
C15 Si5 U1 Si2 -75.1(7)
C14 Si5 U1 Si2 73.8(9)
N3 Si5 U1 Si4 -102.9(5)
C13 Si5 U1 Si4 46.5(5)
C15 Si5 U1 Si4 151.8(6)
C14 Si5 U1 Si4 -59.3(9)
N3 Si5 U1 Si1 79.3(5)
C13 Si5 U1 Si1 -131.3(5)
C15 Si5 U1 Si1 -25.9(6)
C14 Si5 U1 Si1 122.9(9)
N3 Si5 U1 Si6 1.1(5)
C13 Si5 U1 Si6 150.5(5)
C15 Si5 U1 Si6 -104.2(6)
C14 Si5 U1 Si6 44.7(9)
N3 Si6 U1 O1 -41.2(5)
C16 Si6 U1 O1 -124.7(6)
C17 Si6 U1 O1 136.7(5)
C18 Si6 U1 O1 36.8(8)
N3 Si6 U1 N2 81.6(6)
C16 Si6 U1 N2 -2.0(6)
C17 Si6 U1 N2 -100.5(5)
C18 Si6 U1 N2 159.5(8)
N3 Si6 U1 N1 -140.7(5)
C16 Si6 U1 N1 135.8(5)
C17 Si6 U1 N1 37.3(5)
C18 Si6 U1 N1 -62.7(7)
C16 Si6 U1 N3 -83.5(7)
C17 Si6 U1 N3 177.9(6)
C18 Si6 U1 N3 78.0(8)
N3 Si6 U1 Si2 -167.8(5)
C16 Si6 U1 Si2 108.6(5)
C17 Si6 U1 Si2 10.1(4)
C18 Si6 U1 Si2 -89.9(7)
N3 Si6 U1 Si4 85.3(5)
C16 Si6 U1 Si4 1.8(5)
C17 Si6 U1 Si4 -96.7(4)
C18 Si6 U1 Si4 163.3(7)
N3 Si6 U1 Si1 -115.2(5)
C16 Si6 U1 Si1 161.2(5)
C17 Si6 U1 Si1 62.7(4)
C18 Si6 U1 Si1 -37.3(7)
N3 Si6 U1 Si5 -1.1(5)
C16 Si6 U1 Si5 -84.6(5)
C17 Si6 U1 Si5 176.8(4)
C18 Si6 U1 Si5 76.9(7)
Si9 N5 U2 O2 135.3(5)
Si10 N5 U2 O2 -40.4(5)
Si9 N5 U2 N4 -112.1(5)
Si10 N5 U2 N4 72.2(5)
Si9 N5 U2 N6 30.5(6)
Si10 N5 U2 N6 -145.2(4)
Si9 N5 U2 Si10 175.7(9)
Si9 N5 U2 Si11 56.7(5)
Si10 N5 U2 Si11 -119.0(4)
Si9 N5 U2 Si7 -133.3(4)
Si10 N5 U2 Si7 51.0(6)
Si7 N4 U2 O2 -38.8(4)
Si8 N4 U2 O2 140.2(4)
Si7 N4 U2 N5 -147.5(4)
Si8 N4 U2 N5 31.5(5)
Si7 N4 U2 N6 70.8(4)
Si8 N4 U2 N6 -110.2(4)
Si7 N4 U2 Si10 -119.3(3)
Si8 N4 U2 Si10 59.7(4)
Si7 N4 U2 Si11 48.7(5)
Si8 N4 U2 Si11 -132.3(3)
Si8 N4 U2 Si7 179.0(7)
Si11 N6 U2 O2 -32.6(4)
Si12 N6 U2 O2 142.2(4)
Si11 N6 U2 N5 71.8(5)
Si12 N6 U2 N5 -113.4(4)
Si11 N6 U2 N4 -145.7(4)
Si12 N6 U2 N4 29.0(5)
Si11 N6 U2 Si10 48.6(5)
Si12 N6 U2 Si10 -136.7(3)
Si12 N6 U2 Si11 174.8(8)
Si11 N6 U2 Si7 -119.4(3)
Si12 N6 U2 Si7 55.4(4)
N5 Si10 U2 O2 138.9(5)
C31 Si10 U2 O2 -67.2(4)
C30 Si10 U2 O2 36.5(4)
C29 Si10 U2 O2 -166.6(8)
C31 Si10 U2 N5 153.9(6)
C30 Si10 U2 N5 -102.4(6)
C29 Si10 U2 N5 54.5(9)
N5 Si10 U2 N4 -118.1(5)
C31 Si10 U2 N4 35.7(4)
C30 Si10 U2 N4 139.5(5)
C29 Si10 U2 N4 -63.6(8)
N5 Si10 U2 N6 48.7(5)
C31 Si10 U2 N6 -157.4(5)
C30 Si10 U2 N6 -53.7(5)
C29 Si10 U2 N6 103.2(8)
N5 Si10 U2 Si11 70.8(4)
C31 Si10 U2 Si11 -135.3(4)
C30 Si10 U2 Si11 -31.6(4)
C29 Si10 U2 Si11 125.3(8)
N5 Si10 U2 Si7 -144.3(4)
C31 Si10 U2 Si7 9.6(4)
C30 Si10 U2 Si7 113.3(4)
C29 Si10 U2 Si7 -89.8(8)
N6 Si11 U2 O2 146.9(4)
C33 Si11 U2 O2 -68.4(4)
C32 Si11 U2 O2 -168.3(7)
C34 Si11 U2 O2 38.9(4)
N6 Si11 U2 N5 -117.1(4)
C33 Si11 U2 N5 27.6(4)
C32 Si11 U2 N5 -72.3(7)
C34 Si11 U2 N5 134.9(4)
N6 Si11 U2 N4 48.0(5)
C33 Si11 U2 N4 -167.3(4)
C32 Si11 U2 N4 92.8(7)
C34 Si11 U2 N4 -60.0(4)
C33 Si11 U2 N6 144.7(5)
C32 Si11 U2 N6 44.8(8)
C34 Si11 U2 N6 -108.0(5)
N6 Si11 U2 Si10 -144.8(4)
C33 Si11 U2 Si10 -0.2(4)
C32 Si11 U2 Si10 -100.1(7)
C34 Si11 U2 Si10 107.1(3)
N6 Si11 U2 Si7 70.5(4)
C33 Si11 U2 Si7 -144.8(4)
C32 Si11 U2 Si7 115.3(7)
C34 Si11 U2 Si7 -37.5(4)
N4 Si7 U2 O2 142.7(4)
C21 Si7 U2 O2 48.8(4)
C20 Si7 U2 O2 -57.8(3)
C22 Si7 U2 O2 -153.8(8)
N4 Si7 U2 N5 45.7(5)
C21 Si7 U2 N5 -48.2(5)
C20 Si7 U2 N5 -154.8(4)
C22 Si7 U2 N5 109.2(8)
C21 Si7 U2 N4 -93.9(6)
C20 Si7 U2 N4 159.5(5)
C22 Si7 U2 N4 63.5(8)
N4 Si7 U2 N6 -119.0(4)
C21 Si7 U2 N6 147.0(5)
C20 Si7 U2 N6 40.5(4)
C22 Si7 U2 N6 -55.5(8)
N4 Si7 U2 Si10 70.2(4)
C21 Si7 U2 Si10 -23.7(4)
C20 Si7 U2 Si10 -130.3(3)
C22 Si7 U2 Si10 133.8(8)
N4 Si7 U2 Si11 -145.3(4)
C21 Si7 U2 Si11 120.8(4)
C20 Si7 U2 Si11 14.2(3)
C22 Si7 U2 Si11 -81.8(8)
Si17 N9 U3 O3 145.0(5)
Si18 N9 U3 O3 -29.9(4)
Si17 N9 U3 N7 49.0(5)
Si18 N9 U3 N7 -125.9(4)
Si17 N9 U3 N8 -121.9(4)
Si18 N9 U3 N8 63.3(5)
Si18 N9 U3 Si17 -174.9(8)
Si17 N9 U3 Si16 -100.4(4)
Si18 N9 U3 Si16 84.7(4)
Si17 N9 U3 Si18 174.9(8)
Si17 N9 U3 Si14 18.9(6)
Si18 N9 U3 Si14 -155.9(3)
Si17 N9 U3 Si15 -150.3(3)
Si18 N9 U3 Si15 34.8(6)
Si13 N7 U3 O3 -33.2(5)
Si14 N7 U3 O3 143.9(4)
Si13 N7 U3 N9 57.3(5)
Si14 N7 U3 N9 -125.7(4)
Si13 N7 U3 N8 -131.7(4)
Si14 N7 U3 N8 45.4(5)
Si13 N7 U3 Si17 77.2(4)
Si14 N7 U3 Si17 -105.7(4)
Si13 N7 U3 Si16 -162.5(3)
Si14 N7 U3 Si16 14.6(5)
Si13 N7 U3 Si18 27.6(6)
Si14 N7 U3 Si18 -155.3(3)
Si13 N7 U3 Si14 -177.1(8)
Si13 N7 U3 Si15 -108.3(4)
Si14 N7 U3 Si15 68.8(4)
Si15 N8 U3 O3 -36.8(4)
Si16 N8 U3 O3 140.6(4)
Si15 N8 U3 N9 -126.0(4)
Si16 N8 U3 N9 51.4(5)
Si15 N8 U3 N7 63.2(5)
Si16 N8 U3 N7 -119.4(4)
Si15 N8 U3 Si17 -156.4(3)
Si16 N8 U3 Si17 21.0(5)
Si15 N8 U3 Si16 -177.4(7)
Si15 N8 U3 Si18 -100.8(4)
Si16 N8 U3 Si18 76.6(4)
Si15 N8 U3 Si14 82.6(4)
Si16 N8 U3 Si14 -100.0(4)
Si16 N8 U3 Si15 177.4(7)
N9 Si17 U3 O3 -37.2(5)
C52 Si17 U3 O3 142.6(5)
C53 Si17 U3 O3 -119.9(6)
C54 Si17 U3 O3 47.1(6)
C52 Si17 U3 N9 179.8(7)
C53 Si17 U3 N9 -82.7(7)
C54 Si17 U3 N9 84.3(7)
N9 Si17 U3 N7 -137.9(5)
C52 Si17 U3 N7 41.9(5)
C53 Si17 U3 N7 139.4(6)
C54 Si17 U3 N7 -53.6(6)
N9 Si17 U3 N8 76.6(5)
C52 Si17 U3 N8 -103.6(5)
C53 Si17 U3 N8 -6.2(6)
C54 Si17 U3 N8 160.9(6)
N9 Si17 U3 Si16 86.4(5)
C52 Si17 U3 Si16 -93.8(4)
C53 Si17 U3 Si16 3.6(5)
C54 Si17 U3 Si16 170.7(6)
N9 Si17 U3 Si18 -2.9(5)
C52 Si17 U3 Si18 176.9(4)
C53 Si17 U3 Si18 -85.7(5)
C54 Si17 U3 Si18 81.4(6)
N9 Si17 U3 Si14 -165.4(5)
C52 Si17 U3 Si14 14.4(4)
C53 Si17 U3 Si14 111.9(5)
C54 Si17 U3 Si14 -81.1(6)
N9 Si17 U3 Si15 54.0(5)
C52 Si17 U3 Si15 -126.2(4)
C53 Si17 U3 Si15 -28.8(6)
C54 Si17 U3 Si15 138.3(6)
N8 Si16 U3 O3 -44.1(4)
C49 Si16 U3 O3 -130.3(5)
C51 Si16 U3 O3 131.8(4)
C50 Si16 U3 O3 34.8(6)
N8 Si16 U3 N9 -136.8(4)
C49 Si16 U3 N9 137.1(5)
C51 Si16 U3 N9 39.1(4)
C50 Si16 U3 N9 -57.8(6)
N8 Si16 U3 N7 78.2(5)
C49 Si16 U3 N7 -7.9(5)
C51 Si16 U3 N7 -105.8(4)
C50 Si16 U3 N7 157.2(6)
C49 Si16 U3 N8 -86.1(6)
C51 Si16 U3 N8 175.9(6)
C50 Si16 U3 N8 79.0(7)
N8 Si16 U3 Si17 -163.9(4)
C49 Si16 U3 Si17 110.0(5)
C51 Si16 U3 Si17 12.1(4)
C50 Si16 U3 Si17 -84.9(5)
N8 Si16 U3 Si18 -109.4(4)
C49 Si16 U3 Si18 164.4(5)
C51 Si16 U3 Si18 66.5(4)
C50 Si16 U3 Si18 -30.5(5)
N8 Si16 U3 Si14 85.0(4)
C49 Si16 U3 Si14 -1.1(5)
C51 Si16 U3 Si14 -99.0(4)
C50 Si16 U3 Si14 164.0(5)
N8 Si16 U3 Si15 -1.4(4)
C49 Si16 U3 Si15 -87.6(5)
C51 Si16 U3 Si15 174.5(4)
C50 Si16 U3 Si15 77.5(5)
N9 Si18 U3 O3 146.4(5)
C57 Si18 U3 O3 -83.0(5)
C55 Si18 U3 O3 162.9(9)
C56 Si18 U3 O3 27.8(4)
C57 Si18 U3 N9 130.7(7)
C55 Si18 U3 N9 16.6(10)
C56 Si18 U3 N9 -118.6(6)
N9 Si18 U3 N7 71.6(5)
C57 Si18 U3 N7 -157.8(6)
C55 Si18 U3 N7 88.1(9)
C56 Si18 U3 N7 -47.1(4)
N9 Si18 U3 N8 -127.2(5)
C57 Si18 U3 N8 3.5(5)
C55 Si18 U3 N8 -110.6(9)
C56 Si18 U3 N8 114.2(4)
N9 Si18 U3 Si17 2.8(5)
C57 Si18 U3 Si17 133.5(5)
C55 Si18 U3 Si17 19.4(9)
C56 Si18 U3 Si17 -115.8(3)
N9 Si18 U3 Si16 -100.5(5)
C57 Si18 U3 Si16 30.2(5)
C55 Si18 U3 Si16 -83.9(9)
C56 Si18 U3 Si16 140.9(3)
N9 Si18 U3 Si14 45.0(5)
C57 Si18 U3 Si14 175.7(5)
C55 Si18 U3 Si14 61.6(9)
C56 Si18 U3 Si14 -73.6(4)
N9 Si18 U3 Si15 -153.7(5)
C57 Si18 U3 Si15 -23.1(5)
C55 Si18 U3 Si15 -137.2(9)
C56 Si18 U3 Si15 87.6(3)
N7 Si14 U3 O3 -41.6(5)
C43 Si14 U3 O3 38.5(6)
C45 Si14 U3 O3 136.9(4)
C44 Si14 U3 O3 -126.6(5)
N7 Si14 U3 N9 72.0(5)
C43 Si14 U3 N9 152.1(6)
C45 Si14 U3 N9 -109.4(5)
C44 Si14 U3 N9 -13.0(6)
C43 Si14 U3 N7 80.1(7)
C45 Si14 U3 N7 178.5(6)
C44 Si14 U3 N7 -85.0(7)
N7 Si14 U3 N8 -141.1(4)
C43 Si14 U3 N8 -61.0(6)
C45 Si14 U3 N8 37.4(4)
C44 Si14 U3 N8 133.9(5)
N7 Si14 U3 Si17 80.7(4)
C43 Si14 U3 Si17 160.8(6)
C45 Si14 U3 Si17 -100.8(4)
C44 Si14 U3 Si17 -4.3(5)
N7 Si14 U3 Si16 -168.4(4)
C43 Si14 U3 Si16 -88.3(6)
C45 Si14 U3 Si16 10.1(4)
C44 Si14 U3 Si16 106.5(5)
N7 Si14 U3 Si18 46.5(5)
C43 Si14 U3 Si18 126.6(6)
C45 Si14 U3 Si18 -135.0(4)
C44 Si14 U3 Si18 -38.5(6)
N7 Si14 U3 Si15 -115.8(4)
C43 Si14 U3 Si15 -35.7(6)
C45 Si14 U3 Si15 62.7(4)
C44 Si14 U3 Si15 159.2(5)
N8 Si15 U3 O3 141.6(4)
C48 Si15 U3 O3 -177.4(7)
C46 Si15 U3 O3 36.2(4)
C47 Si15 U3 O3 -71.7(4)
N8 Si15 U3 N9 71.5(5)
C48 Si15 U3 N9 112.6(7)
C46 Si15 U3 N9 -33.8(5)
C47 Si15 U3 N9 -141.7(4)
N8 Si15 U3 N7 -125.9(5)
C48 Si15 U3 N7 -84.9(7)
C46 Si15 U3 N7 128.8(4)
C47 Si15 U3 N7 20.8(4)
C48 Si15 U3 N8 41.1(7)
C46 Si15 U3 N8 -105.3(6)
C47 Si15 U3 N8 146.7(5)
N8 Si15 U3 Si17 41.9(5)
C48 Si15 U3 Si17 83.0(7)
C46 Si15 U3 Si17 -63.4(4)
C47 Si15 U3 Si17 -171.3(3)
N8 Si15 U3 Si16 1.5(4)
C48 Si15 U3 Si16 42.6(6)
C46 Si15 U3 Si16 -103.8(4)
C47 Si15 U3 Si16 148.2(3)
N8 Si15 U3 Si18 87.6(4)
C48 Si15 U3 Si18 128.7(6)
C46 Si15 U3 Si18 -17.7(4)
C47 Si15 U3 Si18 -125.7(3)
N8 Si15 U3 Si14 -100.4(4)
C48 Si15 U3 Si14 -59.4(6)
C46 Si15 U3 Si14 154.3(4)
C47 Si15 U3 Si14 46.3(3)
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1 PubChem 139043136
