#------------------------------------------------------------------------------
#$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $
#$Revision: 176729 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/80/1518022.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1518022
loop_
_publ_author_name
'Braunschweig, Holger'
'Celik, Mehmet Ali'
'Dewhurst, Rian D.'
'Heid, Magdalena'
'Hupp, Florian'
'Sen, Sakya S.'
_publ_section_title
;
 Stepwise isolation of low-valent, low-coordinate Sn and Pb mono- and
 dications in the coordination sphere of platinum
;
_journal_issue                   1
_journal_name_full               'Chem. Sci.'
_journal_page_first              425
_journal_paper_doi               10.1039/C4SC02948H
_journal_volume                  6
_journal_year                    2015
_chemical_formula_moiety         'C36 H66 Al2 Cl8 P2 Pb Pt'
_chemical_formula_sum            'C36 H66 Al2 Cl8 P2 Pb Pt'
_chemical_formula_weight         1300.67
_chemical_name_common
;
?
;
_chemical_name_systematic
; 
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 111.311(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.719(2)
_cell_length_b                   10.6901(9)
_cell_length_c                   23.859(2)
_cell_measurement_reflns_used    3296
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.86
_cell_measurement_theta_min      3.52
_cell_volume                     4923.1(8)
_computing_cell_refinement       'Saint+ ver. 7.68A (Bruker AXS)'
_computing_data_collection       'APEX2 ver. 2010.3 (Bruker AXS)'
_computing_data_reduction        'Saint+ ver. 7.68A (Bruker AXS)'
_computing_molecular_graphics    'XP ver. 5.1 (Bruker AXS, 1998)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 8.333
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker X8-APEX II'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'multi-layer mirror'
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0321
_diffrn_reflns_av_sigmaI/netI    0.0306
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            20613
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         2.11
_exptl_absorpt_coefficient_mu    6.813
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5233
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Sadabs 2008/1 (Bruker 2008)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.755
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2536
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.09
_refine_diff_density_max         1.359
_refine_diff_density_min         -1.004
_refine_diff_density_rms         0.106
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.009
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     227
_refine_ls_number_reflns         5044
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.009
_refine_ls_R_factor_all          0.0265
_refine_ls_R_factor_gt           0.0213
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0134P)²+13.8384P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0417
_refine_ls_wR_factor_ref         0.0431
_reflns_number_gt                4510
_reflns_number_total             5044
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4sc02948h2.cif
_cod_data_source_block           7
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2827 2014-09-09 07:05:25Z andrius 

 Adding full bibliography for 1518019--1518027.cif.
;
_cod_original_cell_volume        4923.2(8)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               1518022
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.0000 0.760310(15) 0.7500 0.00896(5) Uani 1 2 d S
Pb1 Pb 0.0000 1.000127(15) 0.7500 0.01600(5) Uani 1 2 d S
Al4 Al -0.11482(6) 1.15357(10) 0.84165(5) 0.0224(2) Uani 1 1 d .
P1 P 0.04518(4) 0.72676(7) 0.85323(4) 0.00979(16) Uani 1 1 d .
Cl1 Cl -0.12782(5) 0.99499(9) 0.78123(4) 0.0293(2) Uani 1 1 d .
Cl2 Cl -0.09385(7) 1.07808(10) 0.92904(5) 0.0458(3) Uani 1 1 d .
Cl3 Cl -0.20542(6) 1.26396(11) 0.81094(7) 0.0566(4) Uani 1 1 d .
Cl4 Cl -0.02577(5) 1.25271(8) 0.83894(4) 0.0284(2) Uani 1 1 d .
C11 C 0.08584(16) 0.5689(3) 0.86069(14) 0.0122(6) Uani 1 1 d .
H11A H 0.0489 0.5067 0.8581 0.015 Uiso 1 1 calc R
C12 C 0.14632(16) 0.5443(3) 0.92100(15) 0.0161(7) Uani 1 1 d .
H12A H 0.1829 0.6079 0.9268 0.019 Uiso 1 1 calc R
H12B H 0.1293 0.5520 0.9546 0.019 Uiso 1 1 calc R
C13 C 0.17697(18) 0.4132(3) 0.92179(15) 0.0192(7) Uani 1 1 d .
H13A H 0.2165 0.4007 0.9601 0.023 Uiso 1 1 calc R
H13B H 0.1414 0.3493 0.9193 0.023 Uiso 1 1 calc R
C14 C 0.20149(18) 0.3969(3) 0.86916(16) 0.0209(8) Uani 1 1 d .
H14A H 0.2380 0.4592 0.8722 0.025 Uiso 1 1 calc R
H14B H 0.2216 0.3124 0.8707 0.025 Uiso 1 1 calc R
C15 C 0.14090(19) 0.4140(3) 0.80965(16) 0.0214(8) Uani 1 1 d .
H15A H 0.1057 0.3486 0.8056 0.026 Uiso 1 1 calc R
H15B H 0.1575 0.4044 0.7759 0.026 Uiso 1 1 calc R
C16 C 0.10798(17) 0.5436(3) 0.80647(14) 0.0165(7) Uani 1 1 d .
H16A H 0.0669 0.5500 0.7688 0.020 Uiso 1 1 calc R
H16B H 0.1416 0.6083 0.8053 0.020 Uiso 1 1 calc R
C21 C -0.02199(15) 0.7205(3) 0.88663(14) 0.0110(6) Uani 1 1 d .
H21A H -0.0369 0.8089 0.8884 0.013 Uiso 1 1 calc R
C22 C -0.08724(16) 0.6494(3) 0.84712(15) 0.0158(7) Uani 1 1 d .
H22A H -0.1041 0.6846 0.8059 0.019 Uiso 1 1 calc R
H22B H -0.0757 0.5603 0.8446 0.019 Uiso 1 1 calc R
C23 C -0.14434(17) 0.6600(3) 0.87368(15) 0.0214(8) Uani 1 1 d .
H23A H -0.1595 0.7482 0.8719 0.026 Uiso 1 1 calc R
H23B H -0.1848 0.6091 0.8494 0.026 Uiso 1 1 calc R
C24 C -0.11831(18) 0.6148(4) 0.93913(16) 0.0243(8) Uani 1 1 d .
H24A H -0.1551 0.6275 0.9559 0.029 Uiso 1 1 calc R
H24B H -0.1082 0.5241 0.9403 0.029 Uiso 1 1 calc R
C25 C -0.05332(17) 0.6845(3) 0.97779(15) 0.0204(8) Uani 1 1 d .
H25A H -0.0369 0.6505 1.0192 0.024 Uiso 1 1 calc R
H25B H -0.0644 0.7741 0.9798 0.024 Uiso 1 1 calc R
C26 C 0.00400(16) 0.6716(3) 0.95194(14) 0.0155(7) Uani 1 1 d .
H26A H 0.0177 0.5827 0.9527 0.019 Uiso 1 1 calc R
H26B H 0.0452 0.7200 0.9768 0.019 Uiso 1 1 calc R
C31 C 0.11210(15) 0.8350(3) 0.90153(14) 0.0110(6) Uani 1 1 d .
H31A H 0.1345 0.7942 0.9417 0.013 Uiso 1 1 calc R
C32 C 0.07989(16) 0.9589(3) 0.91147(14) 0.0145(7) Uani 1 1 d .
H32A H 0.0503 0.9935 0.8720 0.017 Uiso 1 1 calc R
H32B H 0.0501 0.9424 0.9350 0.017 Uiso 1 1 calc R
C33 C 0.13481(17) 1.0557(3) 0.94465(15) 0.0175(7) Uani 1 1 d .
H33A H 0.1119 1.1363 0.9461 0.021 Uiso 1 1 calc R
H33B H 0.1595 1.0274 0.9865 0.021 Uiso 1 1 calc R
C34 C 0.18696(18) 1.0749(3) 0.91375(16) 0.0194(7) Uani 1 1 d .
H34A H 0.1629 1.1092 0.8729 0.023 Uiso 1 1 calc R
H34B H 0.2225 1.1361 0.9369 0.023 Uiso 1 1 calc R
C35 C 0.22176(16) 0.9521(3) 0.90936(15) 0.0183(7) Uani 1 1 d .
H35A H 0.2480 0.9202 0.9503 0.022 Uiso 1 1 calc R
H35B H 0.2550 0.9663 0.8889 0.022 Uiso 1 1 calc R
C36 C 0.16815(16) 0.8547(3) 0.87442(14) 0.0145(7) Uani 1 1 d .
H36A H 0.1918 0.7742 0.8746 0.017 Uiso 1 1 calc R
H36B H 0.1460 0.8823 0.8321 0.017 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P1 Pt1 P1 162.23(4) 2_556 .
P1 Pt1 Pb1 98.88(2) 2_556 .
P1 Pt1 Pb1 98.88(2) . .
Pt1 Pb1 Cl1 88.952(18) . .
Pt1 Pb1 Cl1 88.953(18) . 2_556
Cl1 Pb1 Cl1 177.90(4) . 2_556
Cl3 Al4 Cl2 113.03(6) . .
Cl3 Al4 Cl4 112.27(6) . .
Cl2 Al4 Cl4 110.17(7) . .
Cl3 Al4 Cl1 108.97(7) . .
Cl2 Al4 Cl1 106.59(6) . .
Cl4 Al4 Cl1 105.37(5) . .
C21 P1 C31 105.46(14) . .
C21 P1 C11 108.20(14) . .
C31 P1 C11 107.22(14) . .
C21 P1 Pt1 112.84(10) . .
C31 P1 Pt1 119.04(10) . .
C11 P1 Pt1 103.59(10) . .
Al4 Cl1 Pb1 104.01(4) . .
C12 C11 C16 111.2(3) . .
C12 C11 P1 115.3(2) . .
C16 C11 P1 109.9(2) . .
C12 C11 H11A 106.7 . .
C16 C11 H11A 106.7 . .
P1 C11 H11A 106.7 . .
C13 C12 C11 111.0(3) . .
C13 C12 H12A 109.4 . .
C11 C12 H12A 109.4 . .
C13 C12 H12B 109.4 . .
C11 C12 H12B 109.4 . .
H12A C12 H12B 108.0 . .
C14 C13 C12 110.7(3) . .
C14 C13 H13A 109.5 . .
C12 C13 H13A 109.5 . .
C14 C13 H13B 109.5 . .
C12 C13 H13B 109.5 . .
H13A C13 H13B 108.1 . .
C15 C14 C13 110.2(3) . .
C15 C14 H14A 109.6 . .
C13 C14 H14A 109.6 . .
C15 C14 H14B 109.6 . .
C13 C14 H14B 109.6 . .
H14A C14 H14B 108.1 . .
C14 C15 C16 110.8(3) . .
C14 C15 H15A 109.5 . .
C16 C15 H15A 109.5 . .
C14 C15 H15B 109.5 . .
C16 C15 H15B 109.5 . .
H15A C15 H15B 108.1 . .
C15 C16 C11 112.3(3) . .
C15 C16 H16A 109.1 . .
C11 C16 H16A 109.1 . .
C15 C16 H16B 109.1 . .
C11 C16 H16B 109.1 . .
H16A C16 H16B 107.9 . .
C22 C21 C26 111.0(2) . .
C22 C21 P1 112.8(2) . .
C26 C21 P1 114.1(2) . .
C22 C21 H21A 106.1 . .
C26 C21 H21A 106.1 . .
P1 C21 H21A 106.1 . .
C23 C22 C21 110.4(3) . .
C23 C22 H22A 109.6 . .
C21 C22 H22A 109.6 . .
C23 C22 H22B 109.6 . .
C21 C22 H22B 109.6 . .
H22A C22 H22B 108.1 . .
C24 C23 C22 111.0(3) . .
C24 C23 H23A 109.4 . .
C22 C23 H23A 109.4 . .
C24 C23 H23B 109.4 . .
C22 C23 H23B 109.4 . .
H23A C23 H23B 108.0 . .
C25 C24 C23 111.7(3) . .
C25 C24 H24A 109.3 . .
C23 C24 H24A 109.3 . .
C25 C24 H24B 109.3 . .
C23 C24 H24B 109.3 . .
H24A C24 H24B 107.9 . .
C24 C25 C26 110.9(3) . .
C24 C25 H25A 109.5 . .
C26 C25 H25A 109.5 . .
C24 C25 H25B 109.5 . .
C26 C25 H25B 109.5 . .
H25A C25 H25B 108.0 . .
C25 C26 C21 109.8(3) . .
C25 C26 H26A 109.7 . .
C21 C26 H26A 109.7 . .
C25 C26 H26B 109.7 . .
C21 C26 H26B 109.7 . .
H26A C26 H26B 108.2 . .
C36 C31 C32 112.6(3) . .
C36 C31 P1 109.5(2) . .
C32 C31 P1 111.4(2) . .
C36 C31 H31A 107.7 . .
C32 C31 H31A 107.7 . .
P1 C31 H31A 107.7 . .
C33 C32 C31 112.3(3) . .
C33 C32 H32A 109.2 . .
C31 C32 H32A 109.2 . .
C33 C32 H32B 109.2 . .
C31 C32 H32B 109.2 . .
H32A C32 H32B 107.9 . .
C34 C33 C32 111.4(3) . .
C34 C33 H33A 109.3 . .
C32 C33 H33A 109.3 . .
C34 C33 H33B 109.3 . .
C32 C33 H33B 109.3 . .
H33A C33 H33B 108.0 . .
C35 C34 C33 110.7(3) . .
C35 C34 H34A 109.5 . .
C33 C34 H34A 109.5 . .
C35 C34 H34B 109.5 . .
C33 C34 H34B 109.5 . .
H34A C34 H34B 108.1 . .
C34 C35 C36 110.9(3) . .
C34 C35 H35A 109.5 . .
C36 C35 H35A 109.5 . .
C34 C35 H35B 109.5 . .
C36 C35 H35B 109.5 . .
H35A C35 H35B 108.0 . .
C35 C36 C31 112.0(2) . .
C35 C36 H36A 109.2 . .
C31 C36 H36A 109.2 . .
C35 C36 H36B 109.2 . .
C31 C36 H36B 109.2 . .
H36A C36 H36B 107.9 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 P1 2.3226(8) 2_556
Pt1 P1 2.3227(8) .
Pt1 Pb1 2.5637(3) .
Pb1 Cl1 3.0010(9) .
Pb1 Cl1 3.0010(9) 2_556
Al4 Cl3 2.1105(16) .
Al4 Cl2 2.1281(15) .
Al4 Cl4 2.1489(14) .
Al4 Cl1 2.1777(13) .
P1 C21 1.839(3) .
P1 C31 1.852(3) .
P1 C11 1.865(3) .
C11 C12 1.549(4) .
C11 C16 1.545(4) .
C11 H11A 1.0000 .
C12 C13 1.536(4) .
C12 H12A 0.9900 .
C12 H12B 0.9900 .
C13 C14 1.526(5) .
C13 H13A 0.9900 .
C13 H13B 0.9900 .
C14 C15 1.526(5) .
C14 H14A 0.9900 .
C14 H14B 0.9900 .
C15 C16 1.534(4) .
C15 H15A 0.9900 .
C15 H15B 0.9900 .
C16 H16A 0.9900 .
C16 H16B 0.9900 .
C21 C22 1.538(4) .
C21 C26 1.543(4) .
C21 H21A 1.0000 .
C22 C23 1.536(4) .
C22 H22A 0.9900 .
C22 H22B 0.9900 .
C23 C24 1.533(5) .
C23 H23A 0.9900 .
C23 H23B 0.9900 .
C24 C25 1.522(5) .
C24 H24A 0.9900 .
C24 H24B 0.9900 .
C25 C26 1.531(4) .
C25 H25A 0.9900 .
C25 H25B 0.9900 .
C26 H26A 0.9900 .
C26 H26B 0.9900 .
C31 C36 1.535(4) .
C31 C32 1.540(4) .
C31 H31A 1.0000 .
C32 C33 1.528(4) .
C32 H32A 0.9900 .
C32 H32B 0.9900 .
C33 C34 1.527(4) .
C33 H33A 0.9900 .
C33 H33B 0.9900 .
C34 C35 1.520(4) .
C34 H34A 0.9900 .
C34 H34B 0.9900 .
C35 C36 1.529(4) .
C35 H35A 0.9900 .
C35 H35B 0.9900 .
C36 H36A 0.9900 .
C36 H36B 0.9900 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
P1 Pt1 Pb1 Cl1 102.35(3) 2_556 .
P1 Pt1 Pb1 Cl1 -77.65(3) . .
P1 Pt1 Pb1 Cl1 -77.65(3) 2_556 2_556
P1 Pt1 Pb1 Cl1 102.35(3) . 2_556
P1 Pt1 P1 C21 -91.48(11) 2_556 .
Pb1 Pt1 P1 C21 88.53(11) . .
P1 Pt1 P1 C31 144.14(11) 2_556 .
Pb1 Pt1 P1 C31 -35.86(11) . .
P1 Pt1 P1 C11 25.29(10) 2_556 .
Pb1 Pt1 P1 C11 -154.71(10) . .
Cl3 Al4 Cl1 Pb1 129.11(5) . .
Cl2 Al4 Cl1 Pb1 -108.61(6) . .
Cl4 Al4 Cl1 Pb1 8.45(6) . .
Cl1 Pb1 Cl1 Al4 143.81(5) 2_556 .
C21 P1 C11 C12 -86.1(2) . .
C31 P1 C11 C12 27.2(3) . .
Pt1 P1 C11 C12 153.9(2) . .
C21 P1 C11 C16 147.3(2) . .
C31 P1 C11 C16 -99.4(2) . .
Pt1 P1 C11 C16 27.3(2) . .
C16 C11 C12 C13 -52.8(3) . .
P1 C11 C12 C13 -178.7(2) . .
C11 C12 C13 C14 57.2(4) . .
C12 C13 C14 C15 -60.0(4) . .
C13 C14 C15 C16 58.4(4) . .
C14 C15 C16 C11 -54.9(4) . .
C12 C11 C16 C15 52.0(4) . .
P1 C11 C16 C15 -179.2(2) . .
C31 P1 C21 C22 171.7(2) . .
C11 P1 C21 C22 -73.9(2) . .
Pt1 P1 C21 C22 40.1(2) . .
C31 P1 C21 C26 -60.5(3) . .
C11 P1 C21 C26 54.0(3) . .
Pt1 P1 C21 C26 167.97(19) . .
C26 C21 C22 C23 56.9(3) . .
P1 C21 C22 C23 -173.6(2) . .
C21 C22 C23 C24 -55.2(4) . .
C22 C23 C24 C25 55.5(4) . .
C23 C24 C25 C26 -56.7(4) . .
C24 C25 C26 C21 57.3(4) . .
C22 C21 C26 C25 -57.8(3) . .
P1 C21 C26 C25 173.4(2) . .
C21 P1 C31 C36 -175.6(2) . .
C11 P1 C31 C36 69.2(2) . .
Pt1 P1 C31 C36 -47.7(2) . .
C21 P1 C31 C32 -50.5(2) . .
C11 P1 C31 C32 -165.6(2) . .
Pt1 P1 C31 C32 77.4(2) . .
C36 C31 C32 C33 -49.6(3) . .
P1 C31 C32 C33 -173.0(2) . .
C31 C32 C33 C34 53.0(4) . .
C32 C33 C34 C35 -57.6(4) . .
C33 C34 C35 C36 58.6(4) . .
C34 C35 C36 C31 -55.2(4) . .
C32 C31 C36 C35 50.6(4) . .
P1 C31 C36 C35 175.1(2) . .
