#------------------------------------------------------------------------------
#$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $
#$Revision: 176729 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/88/1518876.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1518876
loop_
_publ_author_name
'Kubisiak, Marcin'
'Zelga, Karolina'
'Bury, Wojciech'
'Justyniak, Iwona'
'Budny-Godlewski, Krzysztof'
'Ochal, Zbigniew'
'Lewiński, Janusz'
_publ_section_title
;
 Development of zinc alkyl/air systems as radical initiators for organic
 reactions
;
_journal_issue                   5
_journal_name_full               'Chem. Sci.'
_journal_page_first              3102
_journal_paper_doi               10.1039/C5SC00600G
_journal_volume                  6
_journal_year                    2015
_chemical_formula_sum            'C38 H64 O26 Zn8'
_chemical_formula_weight         1460.01
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2009-11-10 deposited with the CCDC.
2015-03-19 downloaded from the CCDC.
;
_cell_angle_alpha                77.371(2)
_cell_angle_beta                 83.044(3)
_cell_angle_gamma                80.914(3)
_cell_formula_units_Z            1
_cell_length_a                   9.5731(4)
_cell_length_b                   10.8542(6)
_cell_length_c                   13.0771(7)
_cell_measurement_reflns_used    4813
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      26.373
_cell_measurement_theta_min      1.018
_cell_volume                     1304.01(12)
_computing_cell_refinement       'Denzo & Scalepak (Otwinowski, Minor, 1997)'
_computing_data_collection       'Collect (Nonius B.V. 1998)'
_computing_data_reduction        'Denzo & Scalepak (Otwinowski, Minor, 1997)'
_computing_molecular_graphics
;
DIAMOND v2.1 (Brandenburg, 1999)
Ortep-3 for Windows, L.J.Farrugia (1997) J.Appl.Cryst. 30, 565,
ORTEP III (Burnett, Johnson, 1996)
;
_computing_publication_material
;
SHELXL-97 (Sheldrick, 1997),
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_details
;
363 frames, ω rotation 1° per frame (145s per frame)
53 frames, ω rotation 1° per frame (145s per frame)
32 frames, ω rotation 1° per frame (145s per frame)
43 frames, ω rotation 1° per frame (145s per frame)
;
_diffrn_measurement_device       'κ-geometry diffractometr'
_diffrn_measurement_device_type  'Nonius Kappa-CCD'
_diffrn_measurement_method       'area detector ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0302
_diffrn_reflns_av_sigmaI/netI    0.0441
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            8314
_diffrn_reflns_theta_full        24.71
_diffrn_reflns_theta_max         24.71
_diffrn_reflns_theta_min         2.57
_exptl_absorpt_coefficient_mu    3.696
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Scalepak (Otwinowski, Minor, 1997)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.859
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             740
_exptl_crystal_size_max          0.52
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.511
_refine_diff_density_min         -0.560
_refine_diff_density_rms         0.107
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.134
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     330
_refine_ls_number_reflns         4450
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.134
_refine_ls_R_factor_all          0.0535
_refine_ls_R_factor_gt           0.0391
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0255P)²+3.1958P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0774
_refine_ls_wR_factor_ref         0.0831
_reflns_number_gt                3685
_reflns_number_total             4450
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            c5sc00600g2.cif
_cod_data_source_block           comp3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3105 2015-03-04 15:46:00Z robertas 

 Adding full bibliography for 1518875--1518876.cif.
;
_cod_database_code               1518876
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.3454(5) 0.3092(4) 0.7840(4) 0.0200(10) Uani 1 1 d .
C2 C -0.4826(5) 0.3989(5) 0.7753(4) 0.0238(11) Uani 1 1 d .
H2A H -0.5135 0.4218 0.8446 0.029 Uiso 1 1 calc R
H2B H -0.5562 0.3537 0.7585 0.029 Uiso 1 1 calc R
C3 C -0.4746(6) 0.5204(5) 0.6932(5) 0.0455(16) Uani 1 1 d .
H3A H -0.4024 0.5665 0.7091 0.068 Uiso 1 1 calc R
H3B H -0.5671 0.5740 0.6938 0.068 Uiso 1 1 calc R
H3C H -0.4491 0.4993 0.6236 0.068 Uiso 1 1 calc R
C4 C -0.0937(4) -0.0406(4) 0.6503(3) 0.0186(10) Uani 1 1 d .
C5 C -0.1485(5) -0.1163(5) 0.5850(4) 0.0255(11) Uani 1 1 d .
H5A H -0.0710 -0.1405 0.5327 0.031 Uiso 1 1 calc R
H5B H -0.2256 -0.0617 0.5458 0.031 Uiso 1 1 calc R
C6 C -0.2049(6) -0.2370(5) 0.6481(4) 0.0354(13) Uani 1 1 d .
H6A H -0.1345 -0.2858 0.6951 0.053 Uiso 1 1 calc R
H6B H -0.2231 -0.2889 0.5998 0.053 Uiso 1 1 calc R
H6C H -0.2934 -0.2136 0.6898 0.053 Uiso 1 1 calc R
C7 C 0.3442(5) 0.0741(5) 0.7068(4) 0.0255(11) Uani 1 1 d .
C8 C 0.4794(5) 0.0667(5) 0.6351(4) 0.0312(12) Uani 1 1 d .
H8A H 0.4803 -0.0022 0.5962 0.037 Uiso 1 1 calc R
H8B H 0.5609 0.0431 0.6787 0.037 Uiso 1 1 calc R
C9 C 0.4996(5) 0.1887(5) 0.5566(4) 0.0359(13) Uani 1 1 d .
H9A H 0.4191 0.2134 0.5132 0.054 Uiso 1 1 calc R
H9B H 0.5878 0.1755 0.5114 0.054 Uiso 1 1 calc R
H9C H 0.5049 0.2564 0.5942 0.054 Uiso 1 1 calc R
C10 C 0.2713(4) 0.1258(4) 1.0158(3) 0.0195(10) Uani 1 1 d .
C11 C 0.3665(5) 0.0922(4) 1.1042(4) 0.0218(10) Uani 1 1 d .
H11A H 0.4316 0.0136 1.0968 0.026 Uiso 1 1 calc R
H11B H 0.3071 0.0735 1.1717 0.026 Uiso 1 1 calc R
C12 C 0.4547(5) 0.1959(5) 1.1088(4) 0.0283(12) Uani 1 1 d .
H12A H 0.5134 0.2158 1.0421 0.042 Uiso 1 1 calc R
H12B H 0.5160 0.1659 1.1665 0.042 Uiso 1 1 calc R
H12C H 0.3913 0.2727 1.1206 0.042 Uiso 1 1 calc R
C13 C 0.1165(5) 0.3965(4) 0.6408(4) 0.0228(11) Uani 1 1 d .
C14 C 0.1941(6) 0.4908(5) 0.5620(4) 0.0296(12) Uani 1 1 d .
H14A H 0.1652 0.4938 0.4912 0.035 Uiso 1 1 calc R
H14B H 0.2972 0.4606 0.5611 0.035 Uiso 1 1 calc R
C15 C 0.1674(6) 0.6242(5) 0.5837(4) 0.0359(13) Uani 1 1 d .
H15A H 0.0674 0.6591 0.5763 0.054 Uiso 1 1 calc R
H15B H 0.2279 0.6784 0.5333 0.054 Uiso 1 1 calc R
H15C H 0.1896 0.6216 0.6554 0.054 Uiso 1 1 calc R
C16 C -0.0822(5) 0.2877(4) 1.0607(3) 0.0214(10) Uani 1 1 d .
H16 H 0.0051 0.2759 1.0987 0.026 Uiso 1 1 calc R
C17 C -0.1954(5) 0.3844(4) 1.1009(4) 0.0225(11) Uani 1 1 d .
H17A H -0.1523 0.4454 1.1294 0.027 Uiso 1 1 calc R
H17B H -0.2619 0.3418 1.1565 0.027 Uiso 1 1 calc R
C18 C -0.2713(5) 0.4516(5) 1.0033(4) 0.0265(11) Uani 1 1 d .
H18A H -0.3424 0.4015 0.9896 0.032 Uiso 1 1 calc R
H18B H -0.3183 0.5379 1.0099 0.032 Uiso 1 1 calc R
C19 C -0.1487(5) 0.4571(4) 0.9192(4) 0.0254(11) Uani 1 1 d .
H19A H -0.1819 0.4611 0.8496 0.030 Uiso 1 1 calc R
H19B H -0.1013 0.5330 0.9156 0.030 Uiso 1 1 calc R
O1 O -0.3323(3) 0.2283(3) 0.8691(2) 0.0235(7) Uani 1 1 d .
O2 O -0.2536(3) 0.3196(3) 0.7061(2) 0.0247(7) Uani 1 1 d .
O3 O -0.1099(3) 0.0799(3) 0.6202(2) 0.0230(7) Uani 1 1 d .
O4 O -0.0297(3) -0.0998(3) 0.7293(2) 0.0248(7) Uani 1 1 d .
O5 O 0.2716(3) -0.0172(3) 0.7182(3) 0.0268(8) Uani 1 1 d .
O6 O 0.3133(3) 0.1658(3) 0.7526(3) 0.0262(8) Uani 1 1 d .
O7 O 0.2030(3) 0.0410(3) 0.9992(2) 0.0235(7) Uani 1 1 d .
O8 O 0.2566(3) 0.2363(3) 0.9605(2) 0.0201(7) Uani 1 1 d .
O9 O 0.1154(3) 0.3975(3) 0.7375(2) 0.0255(8) Uani 1 1 d .
O10 O 0.0597(3) 0.3186(3) 0.6050(2) 0.0236(7) Uani 1 1 d .
O11 O -0.0020(3) 0.1312(3) 0.8280(2) 0.0177(7) Uani 1 1 d .
O12 O -0.1294(3) 0.1700(3) 1.0668(2) 0.0190(7) Uani 1 1 d .
O13 O -0.0521(3) 0.3408(3) 0.9500(2) 0.0213(7) Uani 1 1 d .
Zn1 Zn -0.16142(5) 0.13225(5) 0.93349(4) 0.01823(14) Uani 1 1 d .
Zn2 Zn -0.07242(5) 0.20979(5) 0.69189(4) 0.01796(14) Uani 1 1 d .
Zn3 Zn 0.09658(5) -0.03552(5) 0.81062(4) 0.01873(14) Uani 1 1 d .
Zn4 Zn 0.13942(5) 0.23597(5) 0.84484(4) 0.02013(14) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 C1 O1 125.1(4) . .
O2 C1 C2 117.8(4) . .
O1 C1 C2 117.0(4) . .
C1 C2 C3 114.7(4) . .
C1 C2 H2A 108.6 . .
C3 C2 H2A 108.6 . .
C1 C2 H2B 108.6 . .
C3 C2 H2B 108.6 . .
H2A C2 H2B 107.6 . .
C2 C3 H3A 109.5 . .
C2 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C2 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
O4 C4 O3 124.0(4) . .
O4 C4 C5 118.3(4) . .
O3 C4 C5 117.6(4) . .
C4 C5 C6 114.2(4) . .
C4 C5 H5A 108.7 . .
C6 C5 H5A 108.7 . .
C4 C5 H5B 108.7 . .
C6 C5 H5B 108.7 . .
H5A C5 H5B 107.6 . .
C5 C6 H6A 109.5 . .
C5 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
O6 C7 O5 124.8(4) . .
O6 C7 C8 118.8(4) . .
O5 C7 C8 116.4(4) . .
C7 C8 C9 114.4(4) . .
C7 C8 H8A 108.7 . .
C9 C8 H8A 108.7 . .
C7 C8 H8B 108.7 . .
C9 C8 H8B 108.7 . .
H8A C8 H8B 107.6 . .
C8 C9 H9A 109.5 . .
C8 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C8 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
O8 C10 O7 120.2(4) . .
O8 C10 C11 120.6(4) . .
O7 C10 C11 119.2(4) . .
C10 C11 C12 114.3(4) . .
C10 C11 H11A 108.7 . .
C12 C11 H11A 108.7 . .
C10 C11 H11B 108.7 . .
C12 C11 H11B 108.7 . .
H11A C11 H11B 107.6 . .
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
O9 C13 O10 124.7(4) . .
O9 C13 C14 118.4(4) . .
O10 C13 C14 116.9(4) . .
C13 C14 C15 114.0(4) . .
C13 C14 H14A 108.8 . .
C15 C14 H14A 108.8 . .
C13 C14 H14B 108.8 . .
C15 C14 H14B 108.8 . .
H14A C14 H14B 107.6 . .
C14 C15 H15A 109.5 . .
C14 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C14 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
O12 C16 O13 106.7(3) . .
O12 C16 C17 113.1(4) . .
O13 C16 C17 105.2(4) . .
O12 C16 H16 110.5 . .
O13 C16 H16 110.5 . .
C17 C16 H16 110.5 . .
C16 C17 C18 103.7(4) . .
C16 C17 H17A 111.0 . .
C18 C17 H17A 111.0 . .
C16 C17 H17B 111.0 . .
C18 C17 H17B 111.0 . .
H17A C17 H17B 109.0 . .
C19 C18 C17 101.1(4) . .
C19 C18 H18A 111.5 . .
C17 C18 H18A 111.5 . .
C19 C18 H18B 111.5 . .
C17 C18 H18B 111.5 . .
H18A C18 H18B 109.4 . .
O13 C19 C18 105.5(4) . .
O13 C19 H19A 110.6 . .
C18 C19 H19A 110.6 . .
O13 C19 H19B 110.6 . .
C18 C19 H19B 110.6 . .
H19A C19 H19B 108.8 . .
C1 O1 Zn1 130.8(3) . .
C1 O2 Zn2 126.6(3) . .
C4 O3 Zn2 129.3(3) . .
C4 O4 Zn3 128.7(3) . .
C7 O5 Zn3 125.1(3) . .
C7 O6 Zn4 136.2(3) . .
C10 O7 Zn1 139.0(3) . 2_557
C10 O8 Zn4 107.8(3) . .
C13 O9 Zn4 121.2(3) . .
C13 O10 Zn2 122.5(3) . .
Zn1 O11 Zn2 107.89(14) . .
Zn1 O11 Zn3 116.56(14) . .
Zn2 O11 Zn3 104.90(14) . .
Zn1 O11 Zn4 113.26(14) . .
Zn2 O11 Zn4 104.94(13) . .
Zn3 O11 Zn4 108.34(14) . .
C16 O12 Zn3 119.4(3) . 2_557
C16 O12 Zn1 115.7(2) . .
Zn3 O12 Zn1 121.28(15) 2_557 .
C16 O13 C19 109.8(3) . .
C16 O13 Zn4 120.5(3) . .
C19 O13 Zn4 129.6(3) . .
O11 Zn1 O12 116.93(12) . .
O11 Zn1 O1 109.80(13) . .
O12 Zn1 O1 115.53(13) . .
O11 Zn1 O7 112.51(13) . 2_557
O12 Zn1 O7 92.44(12) . 2_557
O1 Zn1 O7 108.25(13) . 2_557
O11 Zn1 Zn2 36.26(9) . .
O12 Zn1 Zn2 140.52(9) . .
O1 Zn1 Zn2 73.73(9) . .
O7 Zn1 Zn2 122.27(9) 2_557 .
O11 Zn2 O3 110.59(13) . .
O11 Zn2 O10 111.09(12) . .
O3 Zn2 O10 111.31(13) . .
O11 Zn2 O2 111.91(13) . .
O3 Zn2 O2 105.60(13) . .
O10 Zn2 O2 106.14(13) . .
O11 Zn2 Zn3 37.58(9) . .
O3 Zn2 Zn3 77.33(9) . .
O10 Zn2 Zn3 109.47(10) . .
O2 Zn2 Zn3 140.24(9) . .
O11 Zn2 Zn4 37.66(8) . .
O3 Zn2 Zn4 137.50(9) . .
O10 Zn2 Zn4 75.32(9) . .
O2 Zn2 Zn4 112.72(10) . .
Zn3 Zn2 Zn4 61.616(17) . .
O11 Zn2 Zn1 35.85(8) . .
O3 Zn2 Zn1 109.80(9) . .
O10 Zn2 Zn1 135.38(9) . .
O2 Zn2 Zn1 78.35(9) . .
Zn3 Zn2 Zn1 64.022(17) . .
Zn4 Zn2 Zn1 62.792(17) . .
O12 Zn3 O11 119.80(12) 2_557 .
O12 Zn3 O5 110.78(13) 2_557 .
O11 Zn3 O5 110.44(13) . .
O12 Zn3 O4 105.05(12) 2_557 .
O11 Zn3 O4 104.46(13) . .
O5 Zn3 O4 104.90(13) . .
O12 Zn3 Zn2 152.72(9) 2_557 .
O11 Zn3 Zn2 37.52(9) . .
O5 Zn3 Zn2 94.75(10) . .
O4 Zn3 Zn2 76.17(9) . .
O11 Zn4 O8 134.03(12) . .
O11 Zn4 O9 107.99(13) . .
O8 Zn4 O9 115.68(13) . .
O11 Zn4 O6 100.87(12) . .
O8 Zn4 O6 92.86(13) . .
O9 Zn4 O6 90.21(13) . .
O11 Zn4 O13 85.22(11) . .
O8 Zn4 O13 84.63(11) . .
O9 Zn4 O13 85.39(12) . .
O6 Zn4 O13 173.38(11) . .
O11 Zn4 Zn2 37.40(8) . .
O8 Zn4 Zn2 170.93(9) . .
O9 Zn4 Zn2 71.65(9) . .
O6 Zn4 Zn2 92.44(9) . .
O13 Zn4 Zn2 90.86(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O2 1.260(5) .
C1 O1 1.264(5) .
C1 C2 1.507(6) .
C2 C3 1.513(7) .
C2 H2A 0.9900 .
C2 H2B 0.9900 .
C3 H3A 0.9800 .
C3 H3B 0.9800 .
C3 H3C 0.9800 .
C4 O4 1.262(5) .
C4 O3 1.270(5) .
C4 C5 1.494(6) .
C5 C6 1.527(7) .
C5 H5A 0.9900 .
C5 H5B 0.9900 .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 O6 1.249(6) .
C7 O5 1.271(6) .
C7 C8 1.505(7) .
C8 C9 1.512(7) .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 O8 1.254(5) .
C10 O7 1.278(5) .
C10 C11 1.505(6) .
C11 C12 1.525(6) .
C11 H11A 0.9900 .
C11 H11B 0.9900 .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 O9 1.266(5) .
C13 O10 1.269(6) .
C13 C14 1.502(6) .
C14 C15 1.512(7) .
C14 H14A 0.9900 .
C14 H14B 0.9900 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 O12 1.405(5) .
C16 O13 1.449(5) .
C16 C17 1.515(6) .
C16 H16 1.0000 .
C17 C18 1.529(7) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C19 1.508(7) .
C18 H18A 0.9900 .
C18 H18B 0.9900 .
C19 O13 1.453(5) .
C19 H19A 0.9900 .
C19 H19B 0.9900 .
O1 Zn1 1.970(3) .
O2 Zn2 1.957(3) .
O3 Zn2 1.953(3) .
O4 Zn3 1.996(3) .
O5 Zn3 1.953(3) .
O6 Zn4 2.079(3) .
O7 Zn1 1.974(3) 2_557
O8 Zn4 1.990(3) .
O9 Zn4 1.993(3) .
O10 Zn2 1.955(3) .
O11 Zn1 1.929(3) .
O11 Zn2 1.948(3) .
O11 Zn3 1.951(3) .
O11 Zn4 1.960(3) .
O12 Zn3 1.937(3) 2_557
O12 Zn1 1.945(3) .
O13 Zn4 2.441(3) .
Zn1 O7 1.974(3) 2_557
Zn1 Zn2 3.1350(7) .
Zn2 Zn3 3.0916(7) .
Zn2 Zn4 3.0995(7) .
Zn3 O12 1.937(3) 2_557
