#------------------------------------------------------------------------------
#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/1/53/27/1532719.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1532719
loop_
_publ_author_name
'Wickleder, M.S.'
'Pley, M.'
_publ_section_title
;
 (Ag (N H3)2) Ag (Os O3 N)2: a new nitridoosmate(VIII)
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              2073
_journal_page_last               2078
_journal_volume                  177
_journal_year                    2004
_chemical_formula_sum            'Ag2 H6 N4 O6 Os2'
_chemical_name_systematic        '(Ag (N H3)2) Ag (Os O3 N)2'
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.71
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   19.625
_cell_length_b                   6.331
_cell_length_c                   8.126
_cell_volume                     1002.706
_citation_journal_id_ASTM        JSSCBI
_cod_data_source_file            Wickleder_JSSCBI_2004_1743.cif
_cod_data_source_block           H6Ag2N4O6Os2
_cod_original_formula_sum        'H6 Ag2 N4 O6 Os2'
_cod_database_code               1532719
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,y,-z
-x,-y,-z
x,-y,z
x+1/2,y+1/2,z
-x+1/2,y+1/2,-z
-x+1/2,-y+1/2,-z
x+1/2,-y+1/2,z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Os1 Os+8 0.11117 0 0.00793 1 0.0
N2 N-3 0.1078 0 0.476 1 0.0
O2 O-2 0.895 0.7734 0.8704 1 0.0
O3 O-2 0.3569 0 0.5051 1 0.0
O1 O-2 0.049 0 0.8366 1 0.0
N3 N-3 0.8109 0 0.0597 1 0.0
N4 N-3 0.2482 0.2191 0.3191 0.5 0.0
Ag2 Ag+1 0.5 0.5 0.5 1 0.0
Ag1 Ag+1 0.5 0 0.5 1 0.0
Os2 Os+8 0.29998 0 0.32268 1 0.0
Ag3 Ag+1 0.30408 0 0.83808 1 0.0
O5 O-2 0.2482 0.2191 0.3191 0.5 0.0
O4 O-2 0.3453 0 0.1494 1 0.0
N1 N-3 0.5049 0 0.7635 1 0.0
