#------------------------------------------------------------------------------
#$Date: 2018-09-27 07:13:35 +0300 (Thu, 27 Sep 2018) $
#$Revision: 211196 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/53/37/1533798.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1533798
loop_
_publ_author_name
'Hoch, C.'
'Wendorff, M.'
'Roehr, C.'
_publ_section_title
;
 Synthesis and crystal structure of the tetrelides A12 M17 (A = Na, K, Rb,
 Cs; M = Si, Ge, Sn) and A4 B9 (A = K, Rb)
;
_journal_name_full               'Journal of Alloys Compd.'
_journal_page_first              206
_journal_page_last               221
_journal_volume                  361
_journal_year                    2003
_chemical_formula_sum            'K4 Pb9'
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.19
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.601
_cell_length_b                   13.19
_cell_length_c                   15.823
_cell_volume                     1950.918
_citation_journal_id_ASTM        JALCEU
_cod_data_source_file            Hoch_JALCEU_2003_110.cif
_cod_data_source_block           K4Pb9
_cod_database_code               1533798
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,y+1/2,-z
-x,-y,-z
x,-y-1/2,z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Pb3 Pb 0.0039 0.2307 0.73895 0.5 0.0
Pb4 Pb 0.1928 0.06201 0.87791 1 0.0
Pb6 Pb 0.1104 0.13183 0.0509 1 0.0
Pb1 Pb 0.3292 0.25 0.80837 1 0.0
K3 K 0.4474 0.5024 0.1296 1 0.0
Pb12 Pb 0.0612 0.7289 0.57222 0.5 0.0
K2 K 0.762 0.25 0.0676 1 0.0
Pb11 Pb 0.2523 0.63147 0.47104 1 0.0
Pb10 Pb 0.7342 0.13329 0.28204 1 0.0
K4 K 0.3839 0.7302 0.2946 0.5 0.0
Pb5 Pb 0.1151 0.63109 0.12135 1 0.0
Pb8 Pb 0.4328 0.25 0.25432 1 0.0
K1 K 0.1183 0.0745 0.2863 1 0.0
Pb9 Pb 0.4344 0.25 0.47136 1 0.0
K5 K 0.1761 0.0972 0.5923 1 0.0
Pb2 Pb 0.3693 0.25 0.00654 1 0.0
Pb7 Pb 0.5015 0.05777 0.37793 1 0.0
