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#$Date: 2015-10-13 18:40:25 +0300 (Tue, 13 Oct 2015) $
#$Revision: 167302 $
#$URL: svn://www.crystallography.net/cod/cif/1/53/86/1538634.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1538634
loop_
_publ_author_name
'Kanishcheva, A.S.'
'Kargin, V.F.'
'Mikhailov, Yu.N.'
'Kargin, Yu.F.'
'Skorikov, V.M.'
_publ_section_title
;
 Synthese und Strukturuntersuchung von dem Doppelphosphat Pb11 Nb (P O4)9.
;
_journal_name_full
'Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy'
_journal_page_first              994
_journal_page_last               997
_journal_volume                  24
_journal_year                    1988
_chemical_formula_sum            'Nb0.332 O12 P3 Pb3.668'
_chemical_name_systematic        '(Pb.917 Nb.083)4 (P O4)3'
_space_group_IT_number           220
_symmetry_space_group_name_Hall  'I -4bd 2c 3'
_symmetry_space_group_name_H-M   'I -4 3 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.396
_cell_length_b                   10.396
_cell_length_c                   10.396
_cell_volume                     1123.567
_citation_journal_id_ASTM        IVNMAW
_cod_data_source_file            Kanishcheva_IVNMAW_1988_1028.cif
_cod_data_source_block           Nb0.332O12P3Pb3.668
_cod_database_code               1538634
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
y+1/4,-x+3/4,-z+1/4
-x,-y+1/2,z
-y+3/4,x+3/4,-z+1/4
x,-y,-z+1/2
-y+1/4,-x+3/4,z+3/4
-x,y+1/2,-z+1/2
y+3/4,x+3/4,z+3/4
z,x,y
x+1/4,-z+3/4,-y+1/4
-z,-x+1/2,y
-x+3/4,z+3/4,-y+1/4
z,-x,-y+1/2
-x+1/4,-z+3/4,y+3/4
-z,x+1/2,-y+1/2
x+3/4,z+3/4,y+3/4
y,z,x
y,-z,-x+1/2
-z+1/4,-y+3/4,x+3/4
-y,z+1/2,-x+1/2
z+1/4,y+1/4,x+1/4
-y+1/2,-z,x+1/2
-z+1/4,y+1/4,-x+3/4
z+3/4,-y+1/4,-x+3/4
x+1/2,y+1/2,z+1/2
y+3/4,-x+5/4,-z+3/4
-x+1/2,-y+1,z+1/2
-y+5/4,x+5/4,-z+3/4
x+1/2,-y+1/2,-z+1
-y+3/4,-x+5/4,z+5/4
-x+1/2,y+1,-z+1
y+5/4,x+5/4,z+5/4
z+1/2,x+1/2,y+1/2
x+3/4,-z+5/4,-y+3/4
-z+1/2,-x+1,y+1/2
-x+5/4,z+5/4,-y+3/4
z+1/2,-x+1/2,-y+1
-x+3/4,-z+5/4,y+5/4
-z+1/2,x+1,-y+1
x+5/4,z+5/4,y+5/4
y+1/2,z+1/2,x+1/2
y+1/2,-z+1/2,-x+1
-z+3/4,-y+5/4,x+5/4
-y+1/2,z+1,-x+1
z+3/4,y+3/4,x+3/4
-y+1,-z+1/2,x+1
-z+3/4,y+3/4,-x+5/4
z+5/4,-y+3/4,-x+5/4
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Nb1 Nb+5 0.07453 0.07453 0.07453 0.083 0.0
P1 P+5 0.375 0 0.25 1 0.0
O1 O-2 0.0468 0.1374 0.2885 1 0.0
Pb1 Pb+2 0.07453 0.07453 0.07453 0.917 0.0
