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#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/1/54/03/1540333.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1540333
loop_
_publ_author_name
'Kryuchkov, S.V.'
'Grigor'ev, M.S.'
'Kuzina, A.F.'
'Spitsyn, V.I.'
_publ_section_title
;
 Crystal and molecular structure of potassium hexaiodotechnetate(IV)
;
_journal_name_full               'Zhurnal Neorganicheskoi Khimii'
_journal_page_first              2944
_journal_page_last               2947
_journal_volume                  32
_journal_year                    1987
_chemical_formula_sum            'I6 K2 Tc'
_chemical_name_systematic        'K2 (Tc I6)'
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 145.63
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.352
_cell_length_b                   7.846
_cell_length_c                   13.817
_cell_volume                     694.745
_citation_journal_id_ASTM        ZNOKAQ
_cod_data_source_file            Kryuchkov_ZNOKAQ_1987_466.cif
_cod_data_source_block           I6K2Tc1
_cod_original_cell_volume        694.7446
_cod_original_formula_sum        'I6 K2 Tc1'
_cod_database_code               1540333
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,y+1/2,-z+1/2
-x,-y,-z
x,-y-1/2,z-1/2
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
I2 I-1 0.25604 0.20264 0.28121 1 0.0
I3 I-1 -0.18259 0.2177 0.29874 1 0.0
K1 K+1 0.764 0.4595 0.0153 1 0.0
I1 I-1 0.28597 0.00278 0.04802 1 0.0
Tc1 Tc+4 0 0 0 1 0.0
