#------------------------------------------------------------------------------
#$Date: 2017-04-05 12:30:58 +0300 (Wed, 05 Apr 2017) $
#$Revision: 195015 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/54/50/1545045.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1545045
loop_
_publ_author_name
'Hu, Ji-Yun'
'Ning, Yingying'
'Meng, Yin-Shan'
'Zhang, Jing'
'Wu, Zhuo-Yan'
'Gao, Song'
'Zhang, Jun-Long'
_publ_section_title
;
 Highly near-IR emissive ytterbium(iii) complexes with unprecedented
 quantum yields
;
_journal_issue                   4
_journal_name_full               'Chem. Sci.'
_journal_page_first              2702
_journal_paper_doi               10.1039/C6SC05021B
_journal_volume                  8
_journal_year                    2017
_chemical_formula_sum            'C55 H23 Co F28 N4 O9 P3 Yb'
_chemical_formula_weight         1740.65
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2016-08-27 deposited with the CCDC.
2017-01-05 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 92.11(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   24.588(5)
_cell_length_b                   10.147(2)
_cell_length_c                   24.582(5)
_cell_measurement_reflns_used    23454
_cell_measurement_temperature    180(2)
_cell_measurement_theta_max      30.1190
_cell_measurement_theta_min      3.1940
_cell_volume                     6129(2)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      180(2)
_diffrn_detector_area_resol_mean 10.3914
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0390
_diffrn_reflns_av_sigmaI/netI    0.0249
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            50103
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.75
_exptl_absorpt_coefficient_mu    2.010
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.99612
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.886
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3388
_exptl_crystal_size_max          0.201
_exptl_crystal_size_mid          0.178
_exptl_crystal_size_min          0.105
_refine_diff_density_max         1.207
_refine_diff_density_min         -0.793
_refine_diff_density_rms         0.086
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.052
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     479
_refine_ls_number_reflns         7019
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.052
_refine_ls_R_factor_all          0.0335
_refine_ls_R_factor_gt           0.0286
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0315P)²+19.5215P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0681
_refine_ls_wR_factor_ref         0.0719
_reflns_number_gt                6490
_reflns_number_total             7019
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c6sc05021b2.cif
_cod_data_source_block           1
_cod_depositor_comments
'Adding full bibliography for 1545045--1545047.cif.'
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               1545045
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Yb1 Yb 0.0000 0.514004(14) 0.2500 0.01877(5) Uani 1 2 d S . .
Co1B Co -0.0042(9) 0.10303(7) 0.2462(9) 0.0411(19) Uani 0.50 1 d P . .
P1 P 0.05338(9) 0.22622(17) 0.30534(9) 0.0521(5) Uani 0.50 1 d P . 1
O1 O 0.04829(18) 0.3737(4) 0.3018(2) 0.0379(11) Uani 0.50 1 d P A 1
O2 O 0.06262(16) 0.3693(4) 0.22869(18) 0.0310(9) Uani 0.50 1 d P . 2
P2 P 0.06767(8) 0.22327(16) 0.22995(9) 0.0461(5) Uani 0.50 1 d P . 2
O3 O -0.0164(2) 0.3651(4) 0.31441(19) 0.0486(14) Uani 0.50 1 d P . 3
P3 P -0.01767(9) 0.21635(15) 0.31734(8) 0.0452(5) Uani 0.50 1 d P . 3
F4 F 0.19749(8) 0.7095(2) 0.35663(8) 0.0508(6) Uani 1 1 d . . .
F3 F 0.22107(8) 0.7049(3) 0.24313(8) 0.0550(6) Uani 1 1 d . A .
F2 F 0.10058(8) 0.6221(2) 0.05214(7) 0.0496(5) Uani 1 1 d . A .
F1 F -0.01471(8) 0.6371(2) 0.02527(7) 0.0448(5) Uani 1 1 d . . .
F5 F 0.20113(9) 0.4465(2) 0.16958(11) 0.0580(6) Uani 1 1 d . A .
F6 F 0.29153(9) 0.4823(2) 0.11247(13) 0.0651(7) Uani 1 1 d . . .
F7 F 0.30694(9) 0.7095(3) 0.05835(10) 0.0612(6) Uani 1 1 d . A .
F8 F 0.23246(10) 0.9052(3) 0.06331(12) 0.0790(9) Uani 1 1 d . . .
F9 F 0.14169(9) 0.8703(2) 0.11934(11) 0.0638(7) Uani 1 1 d . A .
F10 F 0.07845(10) 0.9027(2) 0.41875(9) 0.0581(6) Uani 1 1 d . . .
F11 F 0.14172(13) 0.9667(3) 0.50583(11) 0.0779(8) Uani 1 1 d . A .
F13 F 0.20743(11) 0.5330(3) 0.51480(10) 0.0752(8) Uani 1 1 d . A .
F14 F 0.14387(10) 0.4687(2) 0.42686(9) 0.0587(6) Uani 1 1 d . . .
F12 F 0.20849(9) 0.7821(3) 0.55298(9) 0.0736(8) Uani 1 1 d . . .
N1 N 0.08234(9) 0.6308(2) 0.26961(9) 0.0211(4) Uani 1 1 d . A .
N2 N 0.01739(9) 0.6297(2) 0.16843(9) 0.0215(4) Uani 1 1 d . A .
C9 C 0.10452(11) 0.6532(3) 0.32087(11) 0.0226(5) Uani 1 1 d . . .
C8 C 0.16166(12) 0.6827(3) 0.31605(13) 0.0324(6) Uani 1 1 d . A .
C7 C 0.17240(12) 0.6791(3) 0.26361(13) 0.0325(7) Uani 1 1 d . . .
C6 C 0.12295(11) 0.6467(3) 0.23349(11) 0.0236(5) Uani 1 1 d . A .
C5 C 0.11740(11) 0.6392(3) 0.17648(11) 0.0249(5) Uani 1 1 d . . .
C4 C 0.06796(11) 0.6295(3) 0.14672(11) 0.0239(5) Uani 1 1 d . A .
C3 C 0.06110(12) 0.6281(3) 0.08817(12) 0.0321(6) Uani 1 1 d . . .
C2 C 0.00788(12) 0.6345(3) 0.07583(11) 0.0298(6) Uani 1 1 d . A .
C1 C -0.02031(11) 0.6374(3) 0.12588(11) 0.0229(5) Uani 1 1 d . . .
C10 C 0.07645(11) 0.6523(3) 0.36941(11) 0.0228(5) Uani 1 1 d . . .
C11 C 0.16804(11) 0.6558(3) 0.14516(11) 0.0271(6) Uani 1 1 d . A .
C12 C 0.20742(13) 0.5601(3) 0.14289(13) 0.0338(7) Uani 1 1 d . . .
C13 C 0.25452(12) 0.5773(3) 0.11400(15) 0.0388(7) Uani 1 1 d . A .
C14 C 0.26219(13) 0.6929(4) 0.08697(14) 0.0412(8) Uani 1 1 d . . .
C15 C 0.22456(14) 0.7916(4) 0.08908(15) 0.0445(8) Uani 1 1 d . A .
C16 C 0.17801(13) 0.7725(3) 0.11794(14) 0.0380(7) Uani 1 1 d . . .
C17 C 0.10939(11) 0.6836(3) 0.42033(12) 0.0277(6) Uani 1 1 d . . .
C18 C 0.10991(13) 0.8095(3) 0.44191(13) 0.0361(7) Uani 1 1 d . A .
C19 C 0.14250(15) 0.8439(4) 0.48663(14) 0.0468(9) Uani 1 1 d . . .
C20 C 0.17547(14) 0.7501(5) 0.51041(14) 0.0485(10) Uani 1 1 d . A .
C21 C 0.17523(14) 0.6244(4) 0.49103(13) 0.0464(9) Uani 1 1 d . . .
C22 C 0.14242(13) 0.5919(3) 0.44613(13) 0.0371(7) Uani 1 1 d . A .
C23 C 0.0499(2) 0.2403(5) 0.4094(2) 0.0819(15) Uani 1 1 d . . .
H23A H 0.0832 0.1962 0.4227 0.123 Uiso 1 1 calc R . .
H23B H 0.0231 0.2397 0.4380 0.123 Uiso 1 1 calc R . .
H23C H 0.0582 0.3316 0.3996 0.123 Uiso 1 1 calc R . .
C24 C 0.1555(3) 0.2714(10) 0.2899(3) 0.138(4) Uani 1 1 d . . .
H24A H 0.1816 0.2402 0.3181 0.208 Uiso 1 1 calc R . .
H24B H 0.1435 0.3607 0.2989 0.208 Uiso 1 1 calc R . .
H24C H 0.1729 0.2724 0.2547 0.208 Uiso 1 1 calc R . .
C25 C 0.1071(3) 0.2298(7) 0.1315(2) 0.102(2) Uani 1 1 d . A .
H25A H 0.0989 0.1820 0.0976 0.153 Uiso 1 1 calc R . .
H25B H 0.1464 0.2280 0.1396 0.153 Uiso 1 1 calc R . .
H25C H 0.0949 0.3214 0.1276 0.153 Uiso 1 1 calc R . .
O4 O 0.0830(3) 0.1763(4) 0.1695(3) 0.213(4) Uani 1 1 d . . .
O5 O 0.0300(3) 0.1785(3) 0.36667(17) 0.153(3) Uani 1 1 d . . .
O6 O 0.1140(2) 0.1938(5) 0.2873(4) 0.217(4) Uani 1 1 d . . .
C26 C 0.0153(4) -0.0684(6) 0.2916(3) 0.0750(15) Uani 0.50 1 d PG . .
H26B H 0.0073 -0.1478 0.2724 0.090 Uiso 0.50 1 calc PR . .
C27 C -0.0415(4) -0.0645(7) 0.2760(4) 0.0750(15) Uani 0.50 1 d PG . .
H27A H -0.0739 -0.0613 0.2959 0.090 Uiso 0.50 1 calc PR . .
C28 C -0.0459(3) -0.0604(7) 0.2180(4) 0.0750(15) Uani 0.50 1 d PG . .
H28A H -0.0771 -0.0469 0.1947 0.090 Uiso 0.50 1 calc PR . .
C29 C 0.0080(4) -0.0618(7) 0.1976(3) 0.0750(15) Uani 0.50 1 d PG . .
H29A H 0.0113 -0.0503 0.1595 0.090 Uiso 0.50 1 calc PR . .
C26A C 0.0459(3) -0.0668(7) 0.2431(4) 0.0750(15) Uani 0.50 1 d PG . .
H26A H 0.0800 -0.1097 0.2406 0.090 Uiso 0.50 1 calc PR . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Yb1 O2 96.5(2) 2 .
O2 Yb1 O1 49.21(18) 2 2
O2 Yb1 O1 78.49(15) . 2
O2 Yb1 O1 78.49(15) 2 .
O2 Yb1 O1 49.21(18) . .
O1 Yb1 O1 100.4(2) 2 .
O2 Yb1 O3 82.18(17) 2 2
O2 Yb1 O3 40.16(19) . 2
O1 Yb1 O3 43.01(19) 2 2
O1 Yb1 O3 82.30(18) . 2
O2 Yb1 O3 40.16(19) 2 .
O2 Yb1 O3 82.18(17) . .
O1 Yb1 O3 82.30(18) 2 .
O1 Yb1 O3 43.00(19) . .
O3 Yb1 O3 95.0(2) 2 .
O2 Yb1 N2 88.84(13) 2 2
O2 Yb1 N2 132.74(13) . 2
O1 Yb1 N2 133.67(14) 2 2
O1 Yb1 N2 86.69(14) . 2
O3 Yb1 N2 166.98(12) 2 2
O3 Yb1 N2 72.16(12) . 2
O2 Yb1 N2 132.74(13) 2 .
O2 Yb1 N2 88.84(13) . .
O1 Yb1 N2 86.69(14) 2 .
O1 Yb1 N2 133.67(14) . .
O3 Yb1 N2 72.16(12) 2 .
O3 Yb1 N2 166.98(12) . .
N2 Yb1 N2 120.77(10) 2 .
O2 Yb1 N1 77.49(12) 2 2
O2 Yb1 N1 151.62(13) . 2
O1 Yb1 N1 76.73(12) 2 2
O1 Yb1 N1 150.11(14) . 2
O3 Yb1 N1 111.56(17) 2 2
O3 Yb1 N1 107.78(16) . 2
N2 Yb1 N1 75.33(8) 2 2
N2 Yb1 N1 76.19(8) . 2
O2 Yb1 N1 151.62(13) 2 .
O2 Yb1 N1 77.49(12) . .
O1 Yb1 N1 150.11(14) 2 .
O1 Yb1 N1 76.73(12) . .
O3 Yb1 N1 107.78(16) 2 .
O3 Yb1 N1 111.56(17) . .
N2 Yb1 N1 76.19(8) 2 .
N2 Yb1 N1 75.33(8) . .
N1 Yb1 N1 120.29(10) 2 .
O2 Yb1 P2 17.57(11) 2 2
O2 Yb1 P2 78.93(11) . 2
O1 Yb1 P2 43.97(13) 2 2
O1 Yb1 P2 67.60(11) . 2
O3 Yb1 P2 67.79(12) 2 2
O3 Yb1 P2 38.39(15) . 2
N2 Yb1 P2 101.56(6) 2 2
N2 Yb1 P2 130.49(7) . 2
N1 Yb1 P2 92.50(6) 2 2
N1 Yb1 P2 144.33(7) . 2
O2 Yb1 P2 78.93(11) 2 .
O2 Yb1 P2 17.57(11) . .
O1 Yb1 P2 67.60(11) 2 .
O1 Yb1 P2 43.97(13) . .
O3 Yb1 P2 38.39(14) 2 .
O3 Yb1 P2 67.79(12) . .
N2 Yb1 P2 130.49(6) 2 .
N2 Yb1 P2 101.56(6) . .
N1 Yb1 P2 144.33(7) 2 .
N1 Yb1 P2 92.50(6) . .
P2 Yb1 P2 61.43(7) 2 .
Co1B Co1B C26 114(3) 2 2
Co1B Co1B P3 108(9) 2 2
C26 Co1B P3 100.0(10) 2 2
Co1B Co1B C26A 106(5) 2 2
C26 Co1B C26A 41.8(4) 2 2
P3 Co1B C26A 137.1(9) 2 2
Co1B Co1B C28 125.8(13) 2 .
C26 Co1B C28 22.8(3) 2 .
P3 Co1B C28 110.0(9) 2 .
C26A Co1B C28 27.1(5) 2 .
Co1B Co1B P2 111(9) 2 2
C26 Co1B P2 123.6(11) 2 2
P3 Co1B P2 96.2(4) 2 2
C26A Co1B P2 94.2(10) 2 2
C28 Co1B P2 101.4(10) . 2
Co1B Co1B C29 106(6) 2 .
C26 Co1B C29 18.0(4) 2 .
P3 Co1B C29 88.1(9) 2 .
C26A Co1B C29 58.4(4) 2 .
C28 Co1B C29 40.6(2) . .
P2 Co1B C29 139.2(10) 2 .
Co1B Co1B C27 95(6) 2 .
C26 Co1B C27 52.7(4) 2 .
P3 Co1B C27 150.4(9) 2 .
C26A Co1B C27 13.3(6) 2 .
C28 Co1B C27 40.4(3) . .
P2 Co1B C27 92.0(10) 2 .
C29 Co1B C27 67.7(2) . .
Co1B Co1B C26 59(3) 2 .
C26 Co1B C26 63.2(4) 2 .
P3 Co1B C26 144.3(13) 2 .
C26A Co1B C26 48.5(5) 2 .
C28 Co1B C26 67.3(2) . .
P2 Co1B C26 119.4(12) 2 .
C29 Co1B C26 66.8(2) . .
C27 Co1B C26 40.0(2) . .
Co1B Co1B P1 143.8(13) 2 2
C26 Co1B P1 99.9(8) 2 2
P3 Co1B P1 50.9(4) 2 2
C26A Co1B P1 107.4(9) 2 2
C28 Co1B P1 90.4(7) . 2
P2 Co1B P1 53.7(4) 2 2
C29 Co1B P1 102.8(8) . 2
C27 Co1B P1 116.3(10) . 2
C26 Co1B P1 155.8(10) . 2
Co1B Co1B C26A 67(5) 2 .
C26 Co1B C26A 48.8(5) 2 .
P3 Co1B C26A 105.2(12) 2 .
C26A Co1B C26A 67.1(3) 2 .
C28 Co1B C26A 67.4(3) . .
P2 Co1B C26A 158.2(11) 2 .
C29 Co1B C26A 39.7(3) . .
C27 Co1B C26A 67.2(2) . .
C26 Co1B C26A 39.6(2) . .
P1 Co1B C26A 140.8(11) 2 .
Co1B Co1B P3 65(9) 2 .
C26 Co1B P3 146.5(12) 2 .
P3 Co1B P3 112.34(13) 2 .
C26A Co1B P3 104.9(11) 2 .
C28 Co1B P3 128.4(13) . .
P2 Co1B P3 46.5(5) 2 .
C29 Co1B P3 159.1(8) . .
C27 Co1B P3 93.8(10) . .
C26 Co1B P3 92.8(8) . .
P1 Co1B P3 94.0(6) 2 .
C26A Co1B P3 125.2(9) . .
O1 P1 O6 105.3(3) . .
O1 P1 O5 107.7(3) . .
O6 P1 O5 122.2(4) . .
O1 P1 Co1B 120.4(3) . 2
O6 P1 Co1B 103.2(7) . 2
O5 P1 Co1B 99.0(7) . 2
O1 P1 Co1B 116.5(3) . .
O6 P1 Co1B 105.3(7) . .
O5 P1 Co1B 100.5(6) . .
Co1B P1 Co1B 4.0(5) 2 .
O1 P1 Yb1 26.84(17) . .
O6 P1 Yb1 114.0(3) . .
O5 P1 Yb1 116.92(19) . .
Co1B P1 Yb1 93.6(3) 2 .
Co1B P1 Yb1 89.7(2) . .
P1 O1 Yb1 135.4(3) . .
P2 O2 Yb1 135.8(3) . .
O2 P2 O4 107.2(3) . .
O2 P2 O6 103.4(3) . .
O4 P2 O6 120.5(4) . .
O2 P2 Co1B 121.8(4) . 2
O4 P2 Co1B 106.8(6) . 2
O6 P2 Co1B 98.1(5) . 2
O2 P2 Co1B 119.4(4) . .
O4 P2 Co1B 102.6(6) . .
O6 P2 Co1B 104.8(5) . .
Co1B P2 Co1B 6.7(9) 2 .
O2 P2 Yb1 26.60(16) . .
O4 P2 Yb1 121.0(2) . .
O6 P2 Yb1 109.0(2) . .
Co1B P2 Yb1 95.2(4) 2 .
Co1B P2 Yb1 93.1(4) . .
P3 O3 Yb1 135.5(3) . .
O3 P3 O4 105.6(3) . 2
O3 P3 O5 104.2(3) . .
O4 P3 O5 116.2(4) 2 .
O3 P3 Co1B 121.5(4) . 2
O4 P3 Co1B 106.9(6) 2 2
O5 P3 Co1B 103.0(5) . 2
O3 P3 Co1B 119.7(4) . .
O4 P3 Co1B 101.8(6) 2 .
O5 P3 Co1B 109.9(5) . .
Co1B P3 Co1B 7.0(10) 2 .
O3 P3 Yb1 26.78(17) . .
O4 P3 Yb1 115.7(2) 2 .
O5 P3 Yb1 116.2(2) . .
Co1B P3 Yb1 94.9(4) 2 .
Co1B P3 Yb1 93.0(3) . .
C6 N1 C9 107.5(2) . .
C6 N1 Yb1 124.23(17) . .
C9 N1 Yb1 125.06(17) . .
C4 N2 C1 107.5(2) . .
C4 N2 Yb1 121.45(17) . .
C1 N2 Yb1 122.21(17) . .
N1 C9 C10 126.1(2) . .
N1 C9 C8 108.3(2) . .
C10 C9 C8 125.6(3) . .
C7 C8 F4 125.7(3) . .
C7 C8 C9 107.6(3) . .
F4 C8 C9 126.7(3) . .
C8 C7 F3 124.9(3) . .
C8 C7 C6 108.2(3) . .
F3 C7 C6 126.9(3) . .
N1 C6 C5 126.4(2) . .
N1 C6 C7 108.4(2) . .
C5 C6 C7 125.1(3) . .
C4 C5 C6 125.2(3) . .
C4 C5 C11 117.5(2) . .
C6 C5 C11 117.0(2) . .
N2 C4 C5 125.4(2) . .
N2 C4 C3 108.3(2) . .
C5 C4 C3 126.1(3) . .
C2 C3 F2 125.5(3) . .
C2 C3 C4 107.7(3) . .
F2 C3 C4 126.8(3) . .
C3 C2 F1 125.5(3) . .
C3 C2 C1 107.9(3) . .
F1 C2 C1 126.6(3) . .
N2 C1 C10 125.7(2) . 2
N2 C1 C2 108.5(2) . .
C10 C1 C2 125.7(3) 2 .
C1 C10 C9 126.2(2) 2 .
C1 C10 C17 117.3(2) 2 .
C9 C10 C17 116.2(2) . .
C12 C11 C16 116.5(3) . .
C12 C11 C5 122.8(3) . .
C16 C11 C5 120.6(3) . .
F5 C12 C11 119.6(3) . .
F5 C12 C13 118.1(3) . .
C11 C12 C13 122.2(3) . .
F6 C13 C14 120.2(3) . .
F6 C13 C12 120.5(3) . .
C14 C13 C12 119.3(3) . .
F7 C14 C13 119.7(3) . .
F7 C14 C15 119.9(3) . .
C13 C14 C15 120.4(3) . .
F8 C15 C14 120.4(3) . .
F8 C15 C16 120.2(3) . .
C14 C15 C16 119.4(3) . .
F9 C16 C15 118.4(3) . .
F9 C16 C11 119.5(3) . .
C15 C16 C11 122.1(3) . .
C22 C17 C18 116.8(3) . .
C22 C17 C10 122.2(3) . .
C18 C17 C10 120.9(3) . .
F10 C18 C19 118.0(3) . .
F10 C18 C17 119.6(3) . .
C19 C18 C17 122.4(3) . .
F11 C19 C20 121.0(3) . .
F11 C19 C18 120.2(4) . .
C20 C19 C18 118.8(3) . .
F12 C20 C21 119.6(4) . .
F12 C20 C19 119.9(4) . .
C21 C20 C19 120.5(3) . .
F13 C21 C20 120.1(3) . .
F13 C21 C22 120.1(4) . .
C20 C21 C22 119.8(3) . .
F14 C22 C17 119.5(3) . .
F14 C22 C21 118.9(3) . .
C17 C22 C21 121.6(3) . .
O5 C23 H23A 109.5 . .
O5 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
O5 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
O6 C24 H24A 109.5 . .
O6 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
O6 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
O4 C25 H25A 109.5 . .
O4 C25 H25B 109.5 . .
H25A C25 H25B 109.5 . .
O4 C25 H25C 109.5 . .
H25A C25 H25C 109.5 . .
H25B C25 H25C 109.5 . .
C25 O4 P2 133.8(5) . .
C25 O4 P3 121.1(6) . 2
P2 O4 P3 60.09(17) . 2
C23 O5 P3 134.0(4) . .
C23 O5 P1 116.6(5) . .
P3 O5 P1 63.29(17) . .
C24 O6 P1 127.1(6) . .
C24 O6 P2 114.4(6) . .
P1 O6 P2 67.4(2) . .
C29 C26 C28 166.1(12) 2 2
C29 C26 C26A 147.6(15) 2 .
C28 C26 C26A 39.4(13) 2 .
C29 C26 C27 40.0(16) 2 .
C28 C26 C27 146.7(13) 2 .
C26A C26 C27 108.3 . .
C29 C26 C26A 54.7(13) 2 2
C28 C26 C26A 132.5(13) 2 2
C26A C26 C26A 93.7(5) . 2
C27 C26 C26A 14.7(5) . 2
C29 C26 C27 136.9(17) 2 2
C28 C26 C27 50.0(8) 2 2
C26A C26 C27 10.8(6) . 2
C27 C26 C27 97.5(6) . 2
C26A C26 C27 83.0(6) 2 2
C29 C26 Co1B 89.6(11) 2 2
C28 C26 Co1B 83.6(10) 2 2
C26A C26 Co1B 70.6(8) . 2
C27 C26 Co1B 74.7(7) . 2
C26A C26 Co1B 69.8(7) 2 2
C27 C26 Co1B 66.3(8) 2 2
C29 C26 Co1B 86.8(11) 2 .
C28 C26 Co1B 87.7(10) 2 .
C26A C26 Co1B 70.5(7) . .
C27 C26 Co1B 68.7(7) . .
C26A C26 Co1B 63.1(6) 2 .
C27 C26 Co1B 65.0(8) 2 .
Co1B C26 Co1B 6.8(9) 2 .
C29 C26 H26B 96.9 2 .
C28 C26 H26B 96.9 2 .
C26A C26 H26B 72.8 . .
C27 C26 H26B 73.2 . .
C26A C26 H26B 66.2 2 .
C27 C26 H26B 68.7 2 .
Co1B C26 H26B 119.3 2 .
Co1B C26 H26B 113.5 . .
C26A C27 C29 140(2) 2 2
C26A C27 C28 9.7(14) 2 .
C29 C27 C28 131.2(9) 2 .
C26A C27 C26 116.2(16) 2 .
C29 C27 C26 23.8(9) 2 .
C28 C27 C26 107.8 . .
C26A C27 C26 33.9(13) 2 2
C29 C27 C26 106.0(11) 2 2
C28 C27 C26 25.5(4) . 2
C26 C27 C26 82.4(4) . 2
C26A C27 Co1B 77.3(10) 2 .
C29 C27 Co1B 81.3(8) 2 .
C28 C27 Co1B 69.0(6) . .
C26 C27 Co1B 71.3(6) . .
C26 C27 Co1B 61.0(6) 2 .
C26A C27 Co1B 83.6(11) 2 2
C29 C27 Co1B 73.9(7) 2 2
C28 C27 Co1B 75.0(6) . 2
C26 C27 Co1B 64.6(6) . 2
C26 C27 Co1B 64.5(6) 2 2
Co1B C27 Co1B 7.4(9) . 2
C26A C27 H27A 110.0 2 .
C29 C27 H27A 110.0 2 .
C28 C27 H27A 118.5 . .
C26 C27 H27A 133.7 . .
C26 C27 H27A 143.9 2 .
Co1B C27 H27A 122.9 . .
Co1B C27 H27A 124.6 2 .
C26 C28 C26A 108.6(14) 2 2
C26 C28 C27 104.6(8) 2 .
C26A C28 C27 4.8(8) 2 .
C26 C28 C29 6.2(8) 2 .
C26A C28 C29 112.3(9) 2 .
C27 C28 C29 108.1 . .
C26 C28 Co1B 73.6(11) 2 .
C26A C28 Co1B 74.7(8) 2 .
C27 C28 Co1B 70.6(7) . .
C29 C28 Co1B 70.7(8) . .
C26 C28 Co1B 71.3(11) 2 2
C26A C28 Co1B 71.0(8) 2 2
C27 C28 Co1B 66.7(6) . 2
C29 C28 Co1B 68.9(7) . 2
Co1B C28 Co1B 5.7(7) . 2
C26 C28 H28A 125.7 2 .
C26A C28 H28A 125.7 2 .
C27 C28 H28A 129.7 . .
C29 C28 H28A 121.8 . .
Co1B C28 H28A 117.9 . .
Co1B C28 H28A 123.6 2 .
C26 C29 C27 116.2(14) 2 2
C26 C29 C26A 103.7(11) 2 .
C27 C29 C26A 12.5(8) 2 .
C26 C29 C28 7.7(10) 2 .
C27 C29 C28 120.6(8) 2 .
C26A C29 C28 108.1 . .
C26 C29 C26A 22.5(9) 2 2
C27 C29 C26A 94.4(8) 2 2
C26A C29 C26A 81.9(5) . 2
C28 C29 C26A 26.2(5) . 2
C26 C29 Co1B 72.4(12) 2 .
C27 C29 Co1B 77.8(7) 2 .
C26A C29 Co1B 71.6(5) . .
C28 C29 Co1B 68.7(7) . .
C26A C29 Co1B 59.4(7) 2 .
C26 C29 Co1B 76.0(12) 2 2
C27 C29 Co1B 70.9(7) 2 2
C26A C29 Co1B 64.7(5) . 2
C28 C29 Co1B 73.0(7) . 2
C26A C29 Co1B 60.8(7) 2 2
Co1B C29 Co1B 7.0(10) . 2
C26 C29 H29A 121.9 2 .
C27 C29 H29A 121.9 2 .
C26A C29 H29A 134.3 . .
C28 C29 H29A 117.1 . .
C26A C29 H29A 143.3 2 .
Co1B C29 H29A 119.0 . .
Co1B C29 H29A 122.6 2 .
C27 C26A C28 165(2) 2 2
C27 C26A C29 27.6(18) 2 .
C28 C26A C29 139.1(12) 2 .
C27 C26A C26 135.3(17) 2 .
C28 C26A C26 32.1(12) 2 .
C29 C26A C26 107.7 . .
C27 C26A C26 49.1(17) 2 2
C28 C26A C26 118.0(13) 2 2
C29 C26A C26 21.6(3) . 2
C26 C26A C26 86.3(3) . 2
C27 C26A C29 125(2) 2 2
C28 C26A C29 41.5(6) 2 2
C29 C26A C29 98.0(6) . 2
C26 C26A C29 9.9(6) . 2
C26 C26A C29 76.6(7) 2 2
C27 C26A Co1B 89.4(11) 2 2
C28 C26A Co1B 78.2(8) 2 2
C29 C26A Co1B 75.8(6) . 2
C26 C26A Co1B 67.5(7) . 2
C26 C26A Co1B 68.4(6) 2 2
C29 C26A Co1B 62.2(8) 2 2
C27 C26A Co1B 83.4(12) 2 .
C28 C26A Co1B 83.7(9) 2 .
C29 C26A Co1B 68.7(5) . .
C26 C26A Co1B 69.9(7) . .
C26 C26A Co1B 61.4(5) 2 .
C29 C26A Co1B 63.5(8) 2 .
Co1B C26A Co1B 7.1(9) 2 .
C27 C26A H26A 97.3 2 .
C28 C26A H26A 97.3 2 .
C29 C26A H26A 121.1 . .
C26 C26A H26A 122.8 . .
C26 C26A H26A 136.9 2 .
C29 C26A H26A 131.9 2 .
Co1B C26A H26A 148.3 2 .
Co1B C26A H26A 153.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Yb1 O2 2.205(4) 2
Yb1 O2 2.205(4) .
Yb1 O1 2.224(4) 2
Yb1 O1 2.224(4) .
Yb1 O3 2.236(4) 2
Yb1 O3 2.236(4) .
Yb1 N2 2.376(2) 2
Yb1 N2 2.376(2) .
Yb1 N1 2.380(2) 2
Yb1 N1 2.380(2) .
Yb1 P2 3.4314(16) 2
Yb1 P2 3.4314(16) .
Co1B Co1B 0.27(4) 2
Co1B C26 1.985(12) 2
Co1B P3 2.03(2) 2
Co1B C26A 2.027(15) 2
Co1B C28 2.057(13) .
Co1B P2 2.08(2) 2
Co1B C29 2.083(16) .
Co1B C27 2.078(17) .
Co1B C26 2.112(12) .
Co1B P1 2.125(14) 2
Co1B C26A 2.120(16) .
Co1B P3 2.13(2) .
P1 O1 1.504(4) .
P1 O6 1.606(7) .
P1 O5 1.703(6) .
P1 Co1B 2.125(14) 2
O2 P2 1.487(4) .
P2 O4 1.618(6) .
P2 O6 1.805(8) .
P2 Co1B 2.08(2) 2
O3 P3 1.511(4) .
P3 O4 1.699(7) 2
P3 O5 1.700(6) .
P3 Co1B 2.03(2) 2
F4 C8 1.334(3) .
F3 C7 1.341(3) .
F2 C3 1.339(3) .
F1 C2 1.343(3) .
F5 C12 1.339(4) .
F6 C13 1.327(4) .
F7 C14 1.338(4) .
F8 C15 1.333(4) .
F9 C16 1.337(4) .
F10 C18 1.336(4) .
F11 C19 1.334(4) .
F13 C21 1.340(4) .
F14 C22 1.338(4) .
F12 C20 1.340(4) .
N1 C6 1.370(3) .
N1 C9 1.374(3) .
N2 C4 1.371(3) .
N2 C1 1.374(3) .
C9 C10 1.400(4) .
C9 C8 1.446(4) .
C8 C7 1.326(4) .
C7 C6 1.438(4) .
C6 C5 1.405(4) .
C5 C4 1.399(4) .
C5 C11 1.497(4) .
C4 C3 1.443(4) .
C3 C2 1.334(4) .
C2 C1 1.435(4) .
C1 C10 1.398(4) 2
C10 C1 1.398(4) 2
C10 C17 1.500(4) .
C11 C12 1.374(4) .
C11 C16 1.386(4) .
C12 C13 1.392(4) .
C13 C14 1.364(5) .
C14 C15 1.366(5) .
C15 C16 1.382(5) .
C17 C22 1.375(4) .
C17 C18 1.383(4) .
C18 C19 1.381(5) .
C19 C20 1.367(6) .
C20 C21 1.362(6) .
C21 C22 1.383(5) .
C23 O5 1.303(6) .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
C24 O6 1.287(9) .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
C25 O4 1.248(7) .
C25 H25A 0.9800 .
C25 H25B 0.9800 .
C25 H25C 0.9800 .
O4 P3 1.699(7) 2
C26 C29 0.64(2) 2
C26 C28 0.80(2) 2
C26 C26A 1.432(4) .
C26 C27 1.433(4) .
C26 C26A 1.701(18) 2
C26 C27 1.805(15) 2
C26 Co1B 1.985(12) 2
C26 H26B 0.9500 .
C27 C26A 0.480(19) 2
C27 C29 1.03(2) 2
C27 C28 1.428(4) .
C27 C26 1.805(11) 2
C27 Co1B 2.119(17) 2
C27 H27A 0.9500 .
C28 C26 0.802(12) 2
C28 C26A 0.959(18) 2
C28 C29 1.435(4) .
C28 Co1B 2.228(14) 2
C28 H28A 0.9500 .
C29 C26 0.644(12) 2
C29 C27 1.03(2) 2
C29 C26A 1.428(4) .
C29 C26A 2.006(13) 2
C29 Co1B 2.174(16) 2
C29 H29A 0.9500 .
C26A C27 0.48(2) 2
C26A C28 0.96(2) 2
C26A C26 1.701(15) 2
C26A C29 2.006(16) 2
C26A Co1B 2.027(15) 2
C26A H26A 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Co1B Co1B P1 O1 175(19) 2 .
C26 Co1B P1 O1 157.1(18) 2 .
P3 Co1B P1 O1 49.0(9) 2 .
C26A Co1B P1 O1 -140.5(11) 2 .
C28 Co1B P1 O1 -160(3) . .
P2 Co1B P1 O1 -47.2(8) 2 .
C29 Co1B P1 O1 136.6(9) . .
C27 Co1B P1 O1 -138.0(7) . .
C26 Co1B P1 O1 -166.6(5) . .
P1 Co1B P1 O1 1.7(14) 2 .
C26A Co1B P1 O1 154.4(5) . .
P3 Co1B P1 O1 -72.3(5) . .
Co1B Co1B P1 O6 58(20) 2 .
C26 Co1B P1 O6 41(2) 2 .
P3 Co1B P1 O6 -67.2(6) 2 .
C26A Co1B P1 O6 103.3(14) 2 .
C28 Co1B P1 O6 83(3) . .
P2 Co1B P1 O6 -163.4(5) 2 .
C29 Co1B P1 O6 20.3(13) . .
C27 Co1B P1 O6 105.8(11) . .
C26 Co1B P1 O6 77.1(9) . .
P1 Co1B P1 O6 -114.5(10) 2 .
C26A Co1B P1 O6 38.1(9) . .
P3 Co1B P1 O6 171.5(3) . .
Co1B Co1B P1 O5 -69(20) 2 .
C26 Co1B P1 O5 -87(2) 2 .
P3 Co1B P1 O5 165.0(5) 2 .
C26A Co1B P1 O5 -24.5(14) 2 .
C28 Co1B P1 O5 -44(3) . .
P2 Co1B P1 O5 68.8(5) 2 .
C29 Co1B P1 O5 -107.4(12) . .
C27 Co1B P1 O5 -22.0(11) . .
C26 Co1B P1 O5 -50.7(8) . .
P1 Co1B P1 O5 117.7(10) 2 .
C26A Co1B P1 O5 -89.7(8) . .
P3 Co1B P1 O5 43.7(3) . .
C26 Co1B P1 Co1B -18(18) 2 2
P3 Co1B P1 Co1B -126(20) 2 2
C26A Co1B P1 Co1B 45(18) 2 2
C28 Co1B P1 Co1B 25(16) . 2
P2 Co1B P1 Co1B 138(20) 2 2
C29 Co1B P1 Co1B -38(18) . 2
C27 Co1B P1 Co1B 47(19) . 2
C26 Co1B P1 Co1B 19(19) . 2
P1 Co1B P1 Co1B -173(21) 2 2
C26A Co1B P1 Co1B -20(19) . 2
P3 Co1B P1 Co1B 113(20) . 2
Co1B Co1B P1 Yb1 173(20) 2 .
C26 Co1B P1 Yb1 156(2) 2 .
P3 Co1B P1 Yb1 47.6(6) 2 .
C26A Co1B P1 Yb1 -141.9(13) 2 .
C28 Co1B P1 Yb1 -162(3) . .
P2 Co1B P1 Yb1 -48.5(5) 2 .
C29 Co1B P1 Yb1 135.2(12) . .
C27 Co1B P1 Yb1 -139.4(10) . .
C26 Co1B P1 Yb1 -168.0(8) . .
P1 Co1B P1 Yb1 0.3(10) 2 .
C26A Co1B P1 Yb1 153.0(7) . .
P3 Co1B P1 Yb1 -73.64(17) . .
O2 Yb1 P1 O1 -129.7(5) 2 .
O2 Yb1 P1 O1 100.7(5) . .
O1 Yb1 P1 O1 -178.3(3) 2 .
O3 Yb1 P1 O1 139.6(5) 2 .
O3 Yb1 P1 O1 -91.4(5) . .
N2 Yb1 P1 O1 -45.1(4) 2 .
N2 Yb1 P1 O1 103.1(4) . .
N1 Yb1 P1 O1 -123.0(4) 2 .
N1 Yb1 P1 O1 31.2(4) . .
P2 Yb1 P1 O1 -142.5(5) 2 .
P2 Yb1 P1 O1 122.9(5) . .
O2 Yb1 P1 O6 154.3(4) 2 .
O2 Yb1 P1 O6 24.7(4) . .
O1 Yb1 P1 O6 105.7(4) 2 .
O1 Yb1 P1 O6 -76.1(6) . .
O3 Yb1 P1 O6 63.6(4) 2 .
O3 Yb1 P1 O6 -167.5(4) . .
N2 Yb1 P1 O6 -121.1(4) 2 .
N2 Yb1 P1 O6 27.0(4) . .
N1 Yb1 P1 O6 161.0(3) 2 .
N1 Yb1 P1 O6 -44.8(4) . .
P2 Yb1 P1 O6 141.4(4) 2 .
P2 Yb1 P1 O6 46.9(3) . .
O2 Yb1 P1 O5 -54.0(3) 2 .
O2 Yb1 P1 O5 176.4(3) . .
O1 Yb1 P1 O5 -102.6(3) 2 .
O1 Yb1 P1 O5 75.7(5) . .
O3 Yb1 P1 O5 -144.7(3) 2 .
O3 Yb1 P1 O5 -15.7(3) . .
N2 Yb1 P1 O5 30.6(3) 2 .
N2 Yb1 P1 O5 178.7(3) . .
N1 Yb1 P1 O5 -47.3(3) 2 .
N1 Yb1 P1 O5 106.9(3) . .
P2 Yb1 P1 O5 -66.8(3) 2 .
P2 Yb1 P1 O5 -161.4(3) . .
O2 Yb1 P1 Co1B 48.0(7) 2 2
O2 Yb1 P1 Co1B -81.6(7) . 2
O1 Yb1 P1 Co1B -0.5(7) 2 2
O1 Yb1 P1 Co1B 177.7(8) . 2
O3 Yb1 P1 Co1B -42.7(7) 2 2
O3 Yb1 P1 Co1B 86.3(7) . 2
N2 Yb1 P1 Co1B 132.6(7) 2 2
N2 Yb1 P1 Co1B -79.2(7) . 2
N1 Yb1 P1 Co1B 54.7(7) 2 2
N1 Yb1 P1 Co1B -151.0(7) . 2
P2 Yb1 P1 Co1B 35.2(7) 2 2
P2 Yb1 P1 Co1B -59.3(7) . 2
O2 Yb1 P1 Co1B 47.6(7) 2 .
O2 Yb1 P1 Co1B -82.0(7) . .
O1 Yb1 P1 Co1B -1.0(7) 2 .
O1 Yb1 P1 Co1B 177.3(8) . .
O3 Yb1 P1 Co1B -43.1(7) 2 .
O3 Yb1 P1 Co1B 85.9(7) . .
N2 Yb1 P1 Co1B 132.2(6) 2 .
N2 Yb1 P1 Co1B -79.7(6) . .
N1 Yb1 P1 Co1B 54.3(7) 2 .
N1 Yb1 P1 Co1B -151.5(6) . .
P2 Yb1 P1 Co1B 34.7(6) 2 .
P2 Yb1 P1 Co1B -59.8(6) . .
O6 P1 O1 Yb1 113.2(5) . .
O5 P1 O1 Yb1 -114.9(5) . .
Co1B P1 O1 Yb1 -2.6(10) 2 .
Co1B P1 O1 Yb1 -3.1(9) . .
O2 Yb1 O1 P1 46.1(4) 2 .
O2 Yb1 O1 P1 -63.0(4) . .
O1 Yb1 O1 P1 1.8(3) 2 .
O3 Yb1 O1 P1 -37.4(4) 2 .
O3 Yb1 O1 P1 68.4(4) . .
N2 Yb1 O1 P1 135.6(4) 2 .
N2 Yb1 O1 P1 -93.6(4) . .
N1 Yb1 O1 P1 83.2(5) 2 .
N1 Yb1 O1 P1 -147.8(5) . .
P2 Yb1 O1 P1 31.7(4) 2 .
P2 Yb1 O1 P1 -39.8(4) . .
O2 Yb1 O2 P2 -3.8(3) 2 .
O1 Yb1 O2 P2 -49.8(4) 2 .
O1 Yb1 O2 P2 64.9(4) . .
O3 Yb1 O2 P2 -73.5(4) 2 .
O3 Yb1 O2 P2 33.8(4) . .
N2 Yb1 O2 P2 90.6(4) 2 .
N2 Yb1 O2 P2 -136.7(4) . .
N1 Yb1 O2 P2 -79.4(5) 2 .
N1 Yb1 O2 P2 148.1(4) . .
P2 Yb1 O2 P2 -5.0(4) 2 .
Yb1 O2 P2 O4 125.8(5) . .
Yb1 O2 P2 O6 -105.9(4) . .
Yb1 O2 P2 Co1B 2.7(8) . 2
Yb1 O2 P2 Co1B 9.9(8) . .
Co1B Co1B P2 O2 -113(7) 2 .
C26 Co1B P2 O2 143.7(6) 2 .
P3 Co1B P2 O2 69.8(5) 2 .
C26A Co1B P2 O2 180(2) 2 .
C28 Co1B P2 O2 133.3(10) . .
P2 Co1B P2 O2 -9.2(10) 2 .
C29 Co1B P2 O2 145.2(5) . .
C27 Co1B P2 O2 -150(2) . .
C26 Co1B P2 O2 -145.1(6) . .
P1 Co1B P2 O2 41.9(8) 2 .
C26A Co1B P2 O2 -177.2(4) . .
P3 Co1B P2 O2 -52.0(6) . .
Co1B Co1B P2 O4 129(8) 2 .
C26 Co1B P2 O4 25.4(9) 2 .
P3 Co1B P2 O4 -48.5(4) 2 .
C26A Co1B P2 O4 61(3) 2 .
C28 Co1B P2 O4 15.0(12) . .
P2 Co1B P2 O4 -127.5(7) 2 .
C29 Co1B P2 O4 26.9(7) . .
C27 Co1B P2 O4 91(2) . .
C26 Co1B P2 O4 96.6(9) . .
P1 Co1B P2 O4 -76.4(6) 2 .
C26A Co1B P2 O4 64.5(7) . .
P3 Co1B P2 O4 -170.4(4) . .
Co1B Co1B P2 O6 2(8) 2 .
C26 Co1B P2 O6 -101.3(9) 2 .
P3 Co1B P2 O6 -175.2(3) 2 .
C26A Co1B P2 O6 -65(3) 2 .
C28 Co1B P2 O6 -111.7(12) . .
P2 Co1B P2 O6 105.8(7) 2 .
C29 Co1B P2 O6 -99.8(7) . .
C27 Co1B P2 O6 -35(2) . .
C26 Co1B P2 O6 -30.1(10) . .
P1 Co1B P2 O6 157.0(5) 2 .
C26A Co1B P2 O6 -62.2(7) . .
P3 Co1B P2 O6 63.0(5) . .
C26 Co1B P2 Co1B -103(7) 2 2
P3 Co1B P2 Co1B -177(8) 2 2
C26A Co1B P2 Co1B -67(6) 2 2
C28 Co1B P2 Co1B -114(8) . 2
P2 Co1B P2 Co1B 104(8) 2 2
C29 Co1B P2 Co1B -102(7) . 2
C27 Co1B P2 Co1B -37(6) . 2
C26 Co1B P2 Co1B -32(7) . 2
P1 Co1B P2 Co1B 155(8) 2 2
C26A Co1B P2 Co1B -64(7) . 2
P3 Co1B P2 Co1B 61(8) . 2
Co1B Co1B P2 Yb1 -109(8) 2 .
C26 Co1B P2 Yb1 148.1(8) 2 .
P3 Co1B P2 Yb1 74.2(3) 2 .
C26A Co1B P2 Yb1 -176(3) 2 .
C28 Co1B P2 Yb1 137.7(11) . .
P2 Co1B P2 Yb1 -4.8(8) 2 .
C29 Co1B P2 Yb1 149.6(6) . .
C27 Co1B P2 Yb1 -146(2) . .
C26 Co1B P2 Yb1 -140.7(8) . .
P1 Co1B P2 Yb1 46.4(6) 2 .
C26A Co1B P2 Yb1 -172.8(6) . .
P3 Co1B P2 Yb1 -47.6(4) . .
O2 Yb1 P2 O2 176.2(3) 2 .
O1 Yb1 P2 O2 125.9(4) 2 .
O1 Yb1 P2 O2 -99.0(4) . .
O3 Yb1 P2 O2 84.8(4) 2 .
O3 Yb1 P2 O2 -143.4(4) . .
N2 Yb1 P2 O2 -105.0(4) 2 .
N2 Yb1 P2 O2 44.4(4) . .
N1 Yb1 P2 O2 126.8(4) 2 .
N1 Yb1 P2 O2 -31.1(4) . .
P2 Yb1 P2 O2 174.5(4) 2 .
O2 Yb1 P2 O4 111.6(4) 2 .
O2 Yb1 P2 O4 -64.6(5) . .
O1 Yb1 P2 O4 61.3(4) 2 .
O1 Yb1 P2 O4 -163.6(4) . .
O3 Yb1 P2 O4 20.2(4) 2 .
O3 Yb1 P2 O4 152.0(4) . .
N2 Yb1 P2 O4 -169.6(3) 2 .
N2 Yb1 P2 O4 -20.2(3) . .
N1 Yb1 P2 O4 62.2(4) 2 .
N1 Yb1 P2 O4 -95.7(3) . .
P2 Yb1 P2 O4 109.8(4) 2 .
O2 Yb1 P2 O6 -102.0(3) 2 .
O2 Yb1 P2 O6 81.8(5) . .
O1 Yb1 P2 O6 -152.3(3) 2 .
O1 Yb1 P2 O6 -17.2(3) . .
O3 Yb1 P2 O6 166.6(4) 2 .
O3 Yb1 P2 O6 -61.6(3) . .
N2 Yb1 P2 O6 -23.2(3) 2 .
N2 Yb1 P2 O6 126.2(3) . .
N1 Yb1 P2 O6 -151.4(3) 2 .
N1 Yb1 P2 O6 50.7(3) . .
P2 Yb1 P2 O6 -103.7(3) 2 .
O2 Yb1 P2 Co1B -1.6(5) 2 2
O2 Yb1 P2 Co1B -177.7(7) . 2
O1 Yb1 P2 Co1B -51.8(5) 2 2
O1 Yb1 P2 Co1B 83.3(5) . 2
O3 Yb1 P2 Co1B -92.9(6) 2 2
O3 Yb1 P2 Co1B 38.8(5) . 2
N2 Yb1 P2 Co1B 77.2(5) 2 2
N2 Yb1 P2 Co1B -133.3(5) . 2
N1 Yb1 P2 Co1B -51.0(5) 2 2
N1 Yb1 P2 Co1B 151.2(5) . 2
P2 Yb1 P2 Co1B -3.3(5) 2 2
O2 Yb1 P2 Co1B 4.8(5) 2 .
O2 Yb1 P2 Co1B -171.4(7) . .
O1 Yb1 P2 Co1B -45.5(5) 2 .
O1 Yb1 P2 Co1B 89.6(5) . .
O3 Yb1 P2 Co1B -86.6(6) 2 .
O3 Yb1 P2 Co1B 45.2(5) . .
N2 Yb1 P2 Co1B 83.6(5) 2 .
N2 Yb1 P2 Co1B -126.9(5) . .
N1 Yb1 P2 Co1B -44.6(5) 2 .
N1 Yb1 P2 Co1B 157.5(5) . .
P2 Yb1 P2 Co1B 3.1(5) 2 .
O2 Yb1 O3 P3 71.0(5) 2 .
O2 Yb1 O3 P3 -38.8(5) . .
O1 Yb1 O3 P3 40.6(5) 2 .
O1 Yb1 O3 P3 -73.8(5) . .
O3 Yb1 O3 P3 -0.6(4) 2 .
N2 Yb1 O3 P3 -178.6(6) 2 .
N2 Yb1 O3 P3 8.0(12) . .
N1 Yb1 O3 P3 113.9(5) 2 .
N1 Yb1 O3 P3 -112.0(5) . .
P2 Yb1 O3 P3 43.2(4) 2 .
P2 Yb1 O3 P3 -28.3(5) . .
Yb1 O3 P3 O4 -116.5(5) . 2
Yb1 O3 P3 O5 120.5(5) . .
Yb1 O3 P3 Co1B 5.2(9) . 2
Yb1 O3 P3 Co1B -2.7(9) . .
Co1B Co1B P3 O3 107(7) 2 .
C26 Co1B P3 O3 -157.2(15) 2 .
P3 Co1B P3 O3 6.5(12) 2 .
C26A Co1B P3 O3 -151.7(5) 2 .
C28 Co1B P3 O3 -136.3(7) . .
P2 Co1B P3 O3 -70.2(6) 2 .
C29 Co1B P3 O3 174(3) . .
C27 Co1B P3 O3 -159.3(5) . .
C26 Co1B P3 O3 160.7(5) . .
P1 Co1B P3 O3 -42.5(10) 2 .
C26A Co1B P3 O3 136.1(9) . .
Co1B Co1B P3 O4 -137(7) 2 2
C26 Co1B P3 O4 -41.4(19) 2 2
P3 Co1B P3 O4 122.3(9) 2 2
C26A Co1B P3 O4 -35.9(8) 2 2
C28 Co1B P3 O4 -20.5(9) . 2
P2 Co1B P3 O4 45.6(3) 2 2
C29 Co1B P3 O4 -71(3) . 2
C27 Co1B P3 O4 -43.5(7) . 2
C26 Co1B P3 O4 -83.5(7) . 2
P1 Co1B P3 O4 73.3(6) 2 2
C26A Co1B P3 O4 -108.1(11) . 2
Co1B Co1B P3 O5 -13(7) 2 .
C26 Co1B P3 O5 82.4(19) 2 .
P3 Co1B P3 O5 -113.9(8) 2 .
C26A Co1B P3 O5 87.9(8) 2 .
C28 Co1B P3 O5 103.3(10) . .
P2 Co1B P3 O5 169.4(3) 2 .
C29 Co1B P3 O5 53(3) . .
C27 Co1B P3 O5 80.3(8) . .
C26 Co1B P3 O5 40.2(9) . .
P1 Co1B P3 O5 -163.0(5) 2 .
C26A Co1B P3 O5 15.6(13) . .
C26 Co1B P3 Co1B 96(6) 2 2
P3 Co1B P3 Co1B -100(8) 2 2
C26A Co1B P3 Co1B 101(7) 2 2
C28 Co1B P3 Co1B 117(7) . 2
P2 Co1B P3 Co1B -177(7) 2 2
C29 Co1B P3 Co1B 67(5) . 2
C27 Co1B P3 Co1B 94(7) . 2
C26 Co1B P3 Co1B 54(7) . 2
P1 Co1B P3 Co1B -150(8) 2 2
C26A Co1B P3 Co1B 29(6) . 2
Co1B Co1B P3 Yb1 106(7) 2 .
C26 Co1B P3 Yb1 -158.4(18) 2 .
P3 Co1B P3 Yb1 5.3(9) 2 .
C26A Co1B P3 Yb1 -152.9(7) 2 .
C28 Co1B P3 Yb1 -137.5(8) . .
P2 Co1B P3 Yb1 -71.4(2) 2 .
C29 Co1B P3 Yb1 172(3) . .
C27 Co1B P3 Yb1 -160.5(6) . .
C26 Co1B P3 Yb1 159.4(7) . .
P1 Co1B P3 Yb1 -43.8(6) 2 .
C26A Co1B P3 Yb1 134.8(11) . .
O2 Yb1 P3 O3 -86.9(6) 2 .
O2 Yb1 P3 O3 138.2(5) . .
O1 Yb1 P3 O3 -136.4(5) 2 .
O1 Yb1 P3 O3 86.4(6) . .
O3 Yb1 P3 O3 179.4(4) 2 .
N2 Yb1 P3 O3 1.3(5) 2 .
N2 Yb1 P3 O3 -176.5(5) . .
N1 Yb1 P3 O3 -72.5(5) 2 .
N1 Yb1 P3 O3 75.7(5) . .
P2 Yb1 P3 O3 -114.3(5) 2 .
P2 Yb1 P3 O3 146.4(5) . .
O2 Yb1 P3 O4 -13.9(3) 2 2
O2 Yb1 P3 O4 -148.8(3) . 2
O1 Yb1 P3 O4 -63.4(3) 2 2
O1 Yb1 P3 O4 159.5(3) . 2
O3 Yb1 P3 O4 -107.6(3) 2 2
O3 Yb1 P3 O4 73.0(6) . 2
N2 Yb1 P3 O4 74.4(3) 2 2
N2 Yb1 P3 O4 -103.4(3) . 2
N1 Yb1 P3 O4 0.5(3) 2 2
N1 Yb1 P3 O4 148.7(3) . 2
P2 Yb1 P3 O4 -41.3(3) 2 2
P2 Yb1 P3 O4 -140.6(3) . 2
O2 Yb1 P3 O5 -155.4(3) 2 .
O2 Yb1 P3 O5 69.7(3) . .
O1 Yb1 P3 O5 155.1(3) 2 .
O1 Yb1 P3 O5 17.9(3) . .
O3 Yb1 P3 O5 110.9(3) 2 .
O3 Yb1 P3 O5 -68.5(6) . .
N2 Yb1 P3 O5 -67.2(2) 2 .
N2 Yb1 P3 O5 115.0(2) . .
N1 Yb1 P3 O5 -141.0(2) 2 .
N1 Yb1 P3 O5 7.2(2) . .
P2 Yb1 P3 O5 177.2(3) 2 .
P2 Yb1 P3 O5 77.9(2) . .
O2 Yb1 P3 Co1B 97.5(6) 2 2
O2 Yb1 P3 Co1B -37.4(6) . 2
O1 Yb1 P3 Co1B 48.0(6) 2 2
O1 Yb1 P3 Co1B -89.2(6) . 2
O3 Yb1 P3 Co1B 3.8(6) 2 2
O3 Yb1 P3 Co1B -175.6(8) . 2
N2 Yb1 P3 Co1B -174.2(6) 2 2
N2 Yb1 P3 Co1B 8.0(6) . 2
N1 Yb1 P3 Co1B 111.9(6) 2 2
N1 Yb1 P3 Co1B -99.9(6) . 2
P2 Yb1 P3 Co1B 70.1(6) 2 2
P2 Yb1 P3 Co1B -29.2(6) . 2
O2 Yb1 P3 Co1B 90.7(6) 2 .
O2 Yb1 P3 Co1B -44.2(6) . .
O1 Yb1 P3 Co1B 41.3(6) 2 .
O1 Yb1 P3 Co1B -95.9(6) . .
O3 Yb1 P3 Co1B -3.0(6) 2 .
O3 Yb1 P3 Co1B 177.6(8) . .
N2 Yb1 P3 Co1B 179.0(6) 2 .
N2 Yb1 P3 Co1B 1.2(6) . .
N1 Yb1 P3 Co1B 105.1(6) 2 .
N1 Yb1 P3 Co1B -106.6(6) . .
P2 Yb1 P3 Co1B 63.3(6) 2 .
P2 Yb1 P3 Co1B -36.0(6) . .
O2 Yb1 N1 C6 133.3(3) 2 .
O2 Yb1 N1 C6 53.0(2) . .
O1 Yb1 N1 C6 15.8(3) 2 .
O1 Yb1 N1 C6 103.6(2) . .
O3 Yb1 N1 C6 26.3(2) 2 .
O3 Yb1 N1 C6 129.3(2) . .
N2 Yb1 N1 C6 -166.6(2) 2 .
N2 Yb1 N1 C6 -39.1(2) . .
N1 Yb1 N1 C6 -103.1(2) 2 .
P2 Yb1 N1 C6 102.8(2) 2 .
P2 Yb1 N1 C6 62.2(2) . .
O2 Yb1 N1 C9 -23.9(4) 2 .
O2 Yb1 N1 C9 -104.2(2) . .
O1 Yb1 N1 C9 -141.4(3) 2 .
O1 Yb1 N1 C9 -53.6(2) . .
O3 Yb1 N1 C9 -130.9(2) 2 .
O3 Yb1 N1 C9 -27.9(2) . .
N2 Yb1 N1 C9 36.2(2) 2 .
N2 Yb1 N1 C9 163.7(2) . .
N1 Yb1 N1 C9 99.7(2) 2 .
P2 Yb1 N1 C9 -54.5(2) 2 .
P2 Yb1 N1 C9 -95.0(2) . .
O2 Yb1 N2 C4 -128.3(2) 2 .
O2 Yb1 N2 C4 -30.6(2) . .
O1 Yb1 N2 C4 -109.1(2) 2 .
O1 Yb1 N2 C4 -7.9(3) . .
O3 Yb1 N2 C4 -67.8(3) 2 .
O3 Yb1 N2 C4 -76.9(8) . .
N2 Yb1 N2 C4 110.5(2) 2 .
N1 Yb1 N2 C4 173.7(2) 2 .
N1 Yb1 N2 C4 46.77(19) . .
P2 Yb1 N2 C4 -104.95(19) 2 .
P2 Yb1 N2 C4 -42.8(2) . .
O2 Yb1 N2 C1 14.9(3) 2 .
O2 Yb1 N2 C1 112.6(2) . .
O1 Yb1 N2 C1 34.1(2) 2 .
O1 Yb1 N2 C1 135.3(2) . .
O3 Yb1 N2 C1 75.4(3) 2 .
O3 Yb1 N2 C1 66.3(8) . .
N2 Yb1 N2 C1 -106.3(2) 2 .
N1 Yb1 N2 C1 -43.09(19) 2 .
N1 Yb1 N2 C1 -170.0(2) . .
P2 Yb1 N2 C1 38.2(2) 2 .
P2 Yb1 N2 C1 100.39(19) . .
C6 N1 C9 C10 177.2(3) . .
Yb1 N1 C9 C10 -22.4(4) . .
C6 N1 C9 C8 -0.8(3) . .
Yb1 N1 C9 C8 159.63(18) . .
N1 C9 C8 C7 0.7(3) . .
C10 C9 C8 C7 -177.3(3) . .
N1 C9 C8 F4 -179.6(3) . .
C10 C9 C8 F4 2.4(5) . .
F4 C8 C7 F3 -1.6(6) . .
C9 C8 C7 F3 178.2(3) . .
F4 C8 C7 C6 179.9(3) . .
C9 C8 C7 C6 -0.3(4) . .
C9 N1 C6 C5 -176.7(3) . .
Yb1 N1 C6 C5 22.8(4) . .
C9 N1 C6 C7 0.6(3) . .
Yb1 N1 C6 C7 -160.03(19) . .
C8 C7 C6 N1 -0.1(3) . .
F3 C7 C6 N1 -178.6(3) . .
C8 C7 C6 C5 177.1(3) . .
F3 C7 C6 C5 -1.3(5) . .
N1 C6 C5 C4 8.0(4) . .
C7 C6 C5 C4 -168.7(3) . .
N1 C6 C5 C11 -178.1(3) . .
C7 C6 C5 C11 5.1(4) . .
C1 N2 C4 C5 171.6(3) . .
Yb1 N2 C4 C5 -40.5(3) . .
C1 N2 C4 C3 -4.0(3) . .
Yb1 N2 C4 C3 143.95(19) . .
C6 C5 C4 N2 2.0(4) . .
C11 C5 C4 N2 -171.8(2) . .
C6 C5 C4 C3 176.8(3) . .
C11 C5 C4 C3 3.0(4) . .
N2 C4 C3 C2 3.2(3) . .
C5 C4 C3 C2 -172.3(3) . .
N2 C4 C3 F2 -177.1(3) . .
C5 C4 C3 F2 7.4(5) . .
F2 C3 C2 F1 -0.6(5) . .
C4 C3 C2 F1 179.1(3) . .
F2 C3 C2 C1 179.1(3) . .
C4 C3 C2 C1 -1.2(3) . .
C4 N2 C1 C10 -173.7(3) . 2
Yb1 N2 C1 C10 38.7(3) . 2
C4 N2 C1 C2 3.2(3) . .
Yb1 N2 C1 C2 -144.36(19) . .
C3 C2 C1 N2 -1.2(3) . .
F1 C2 C1 N2 178.5(3) . .
C3 C2 C1 C10 175.7(3) . 2
F1 C2 C1 C10 -4.6(5) . 2
N1 C9 C10 C1 -4.7(4) . 2
C8 C9 C10 C1 173.0(3) . 2
N1 C9 C10 C17 -178.3(2) . .
C8 C9 C10 C17 -0.6(4) . .
C4 C5 C11 C12 -112.0(3) . .
C6 C5 C11 C12 73.7(4) . .
C4 C5 C11 C16 69.9(4) . .
C6 C5 C11 C16 -104.4(3) . .
C16 C11 C12 F5 178.1(3) . .
C5 C11 C12 F5 -0.1(5) . .
C16 C11 C12 C13 -1.2(5) . .
C5 C11 C12 C13 -179.4(3) . .
F5 C12 C13 F6 1.0(5) . .
C11 C12 C13 F6 -179.6(3) . .
F5 C12 C13 C14 -179.3(3) . .
C11 C12 C13 C14 0.1(5) . .
F6 C13 C14 F7 0.8(5) . .
C12 C13 C14 F7 -178.9(3) . .
F6 C13 C14 C15 -179.1(3) . .
C12 C13 C14 C15 1.2(5) . .
F7 C14 C15 F8 -0.8(6) . .
C13 C14 C15 F8 179.0(3) . .
F7 C14 C15 C16 178.8(3) . .
C13 C14 C15 C16 -1.3(6) . .
F8 C15 C16 F9 -0.2(6) . .
C14 C15 C16 F9 -179.9(3) . .
F8 C15 C16 C11 179.8(3) . .
C14 C15 C16 C11 0.1(6) . .
C12 C11 C16 F9 -178.9(3) . .
C5 C11 C16 F9 -0.6(5) . .
C12 C11 C16 C15 1.1(5) . .
C5 C11 C16 C15 179.4(3) . .
C1 C10 C17 C22 106.4(3) 2 .
C9 C10 C17 C22 -79.4(4) . .
C1 C10 C17 C18 -77.0(4) 2 .
C9 C10 C17 C18 97.2(3) . .
C22 C17 C18 F10 -179.7(3) . .
C10 C17 C18 F10 3.5(5) . .
C22 C17 C18 C19 1.2(5) . .
C10 C17 C18 C19 -175.6(3) . .
F10 C18 C19 F11 0.5(5) . .
C17 C18 C19 F11 179.7(3) . .
F10 C18 C19 C20 -179.2(3) . .
C17 C18 C19 C20 0.0(5) . .
F11 C19 C20 F12 -1.5(5) . .
C18 C19 C20 F12 178.3(3) . .
F11 C19 C20 C21 178.9(3) . .
C18 C19 C20 C21 -1.4(5) . .
F12 C20 C21 F13 0.7(5) . .
C19 C20 C21 F13 -179.6(3) . .
F12 C20 C21 C22 -178.1(3) . .
C19 C20 C21 C22 1.6(5) . .
C18 C17 C22 F14 -179.6(3) . .
C10 C17 C22 F14 -2.8(5) . .
C18 C17 C22 C21 -1.0(5) . .
C10 C17 C22 C21 175.8(3) . .
F13 C21 C22 F14 -0.6(5) . .
C20 C21 C22 F14 178.2(3) . .
F13 C21 C22 C17 -179.2(3) . .
C20 C21 C22 C17 -0.4(5) . .
O2 P2 O4 C25 27.5(11) . .
O6 P2 O4 C25 -90.1(10) . .
Co1B P2 O4 C25 159.5(10) 2 .
Co1B P2 O4 C25 154.0(10) . .
Yb1 P2 O4 C25 52.5(11) . .
O2 P2 O4 P3 -78.5(2) . 2
O6 P2 O4 P3 163.9(3) . 2
Co1B P2 O4 P3 53.5(4) 2 2
Co1B P2 O4 P3 48.1(4) . 2
Yb1 P2 O4 P3 -53.4(2) . 2
O3 P3 O5 C23 27.2(8) . .
O4 P3 O5 C23 -88.5(8) 2 .
Co1B P3 O5 C23 155.0(9) 2 .
Co1B P3 O5 C23 156.7(8) . .
Yb1 P3 O5 C23 52.8(8) . .
O3 P3 O5 P1 -75.0(2) . .
O4 P3 O5 P1 169.3(2) 2 .
Co1B P3 O5 P1 52.8(5) 2 .
Co1B P3 O5 P1 54.4(5) . .
Yb1 P3 O5 P1 -49.38(16) . .
O1 P1 O5 C23 -50.6(6) . .
O6 P1 O5 C23 71.4(5) . .
Co1B P1 O5 C23 -176.7(6) 2 .
Co1B P1 O5 C23 -172.9(6) . .
Yb1 P1 O5 C23 -77.9(5) . .
O1 P1 O5 P3 77.6(2) . .
O6 P1 O5 P3 -160.5(3) . .
Co1B P1 O5 P3 -48.5(4) 2 .
Co1B P1 O5 P3 -44.8(4) . .
Yb1 P1 O5 P3 50.22(18) . .
O1 P1 O6 C24 24.5(10) . .
O5 P1 O6 C24 -98.6(9) . .
Co1B P1 O6 C24 151.6(9) 2 .
Co1B P1 O6 C24 148.1(9) . .
Yb1 P1 O6 C24 51.5(10) . .
O1 P1 O6 P2 -79.8(3) . .
O5 P1 O6 P2 157.1(3) . .
Co1B P1 O6 P2 47.3(4) 2 .
Co1B P1 O6 P2 43.9(4) . .
Yb1 P1 O6 P2 -52.8(2) . .
O2 P2 O6 C24 -43.9(7) . .
O4 P2 O6 C24 75.7(7) . .
Co1B P2 O6 C24 -169.4(8) 2 .
Co1B P2 O6 C24 -169.6(8) . .
Yb1 P2 O6 C24 -71.0(7) . .
O2 P2 O6 P1 78.0(3) . .
O4 P2 O6 P1 -162.5(2) . .
Co1B P2 O6 P1 -47.5(5) 2 .
Co1B P2 O6 P1 -47.8(5) . .
Yb1 P2 O6 P1 50.9(2) . .
Co1B Co1B C26 C29 114(12) 2 2
C26 Co1B C26 C29 -99.7(16) 2 2
P3 Co1B C26 C29 -167.9(16) 2 2
C26A Co1B C26 C29 -51.6(11) 2 2
C28 Co1B C26 C29 -74.9(15) . 2
P2 Co1B C26 C29 15.7(14) 2 2
C29 Co1B C26 C29 -119.1(14) . 2
C27 Co1B C26 C29 -36.7(14) . 2
P1 Co1B C26 C29 -50(3) 2 2
C26A Co1B C26 C29 -156.4(13) . 2
P3 Co1B C26 C29 55.9(13) . 2
Co1B Co1B C26 C28 -53(12) 2 2
C26 Co1B C26 C28 93.1(12) 2 2
P3 Co1B C26 C28 24.8(16) 2 2
C26A Co1B C26 C28 141.1(11) 2 2
C28 Co1B C26 C28 117.8(12) . 2
P2 Co1B C26 C28 -151.6(11) 2 2
C29 Co1B C26 C28 73.6(12) . 2
C27 Co1B C26 C28 156.0(11) . 2
P1 Co1B C26 C28 142(3) 2 2
C26A Co1B C26 C28 36.3(12) . 2
P3 Co1B C26 C28 -111.4(11) . 2
Co1B Co1B C26 C26A -90(12) 2 .
C26 Co1B C26 C26A 56.8(5) 2 .
P3 Co1B C26 C26A -11.5(13) 2 .
C26A Co1B C26 C26A 104.8(6) 2 .
C28 Co1B C26 C26A 81.5(5) . .
P2 Co1B C26 C26A 172.1(9) 2 .
C29 Co1B C26 C26A 37.3(3) . .
C27 Co1B C26 C26A 119.7(3) . .
P1 Co1B C26 C26A 106(3) 2 .
P3 Co1B C26 C26A -147.7(8) . .
Co1B Co1B C26 C27 151(12) 2 .
C26 Co1B C26 C27 -62.9(5) 2 .
P3 Co1B C26 C27 -131.2(15) 2 .
C26A Co1B C26 C27 -14.9(5) 2 .
C28 Co1B C26 C27 -38.2(3) . .
P2 Co1B C26 C27 52.4(8) 2 .
C29 Co1B C26 C27 -82.4(4) . .
P1 Co1B C26 C27 -14(3) 2 .
C26A Co1B C26 C27 -119.7(3) . .
P3 Co1B C26 C27 92.6(8) . .
Co1B Co1B C26 C26A 165(12) 2 2
C26 Co1B C26 C26A -48.1(6) 2 2
P3 Co1B C26 C26A -116.3(14) 2 2
C28 Co1B C26 C26A -23.3(6) . 2
P2 Co1B C26 C26A 67.2(9) 2 2
C29 Co1B C26 C26A -67.6(6) . 2
C27 Co1B C26 C26A 14.9(5) . 2
P1 Co1B C26 C26A 1(3) 2 2
C26A Co1B C26 C26A -104.8(6) . 2
P3 Co1B C26 C26A 107.5(9) . 2
Co1B Co1B C26 C27 -100(12) 2 2
C26 Co1B C26 C27 46.8(6) 2 2
P3 Co1B C26 C27 -21.4(12) 2 2
C26A Co1B C26 C27 94.9(6) 2 2
C28 Co1B C26 C27 71.5(7) . 2
P2 Co1B C26 C27 162.1(10) 2 2
C29 Co1B C26 C27 27.3(7) . 2
C27 Co1B C26 C27 109.7(6) . 2
P1 Co1B C26 C27 96(3) 2 2
C26A Co1B C26 C27 -10.0(6) . 2
P3 Co1B C26 C27 -157.7(9) . 2
C26 Co1B C26 Co1B 147(12) 2 2
P3 Co1B C26 Co1B 78(12) 2 2
C26A Co1B C26 Co1B -165(12) 2 2
C28 Co1B C26 Co1B 171(12) . 2
P2 Co1B C26 Co1B -98(12) 2 2
C29 Co1B C26 Co1B 127(12) . 2
C27 Co1B C26 Co1B -151(12) . 2
P1 Co1B C26 Co1B -164(15) 2 2
C26A Co1B C26 Co1B 90(12) . 2
P3 Co1B C26 Co1B -58(11) . 2
C29 C26 C27 C26A 176.6(3) 2 2
C28 C26 C27 C26A 17.0(6) 2 2
C26A C26 C27 C26A 5.13(14) . 2
C27 C26 C27 C26A 5.39(13) 2 2
Co1B C26 C27 C26A 68.2(7) 2 2
Co1B C26 C27 C26A 64.8(7) . 2
C28 C26 C27 C29 -159.6(5) 2 2
C26A C26 C27 C29 -171.4(3) . 2
C26A C26 C27 C29 -176.6(3) 2 2
C27 C26 C27 C29 -171.2(3) 2 2
Co1B C26 C27 C29 -108.3(7) 2 2
Co1B C26 C27 C29 -111.8(7) . 2
C29 C26 C27 C28 171.4(3) 2 .
C28 C26 C27 C28 11.9(6) 2 .
C26A C26 C27 C28 0.0 . .
C26A C26 C27 C28 -5.13(14) 2 .
C27 C26 C27 C28 0.3 2 .
Co1B C26 C27 C28 63.1(7) 2 .
Co1B C26 C27 C28 59.6(7) . .
C29 C26 C27 C26 173.7(4) 2 2
C28 C26 C27 C26 14.2(7) 2 2
C26A C26 C27 C26 2.3(4) . 2
C26A C26 C27 C26 -2.8(4) 2 2
C27 C26 C27 C26 2.6(4) 2 2
Co1B C26 C27 C26 65.4(7) 2 2
Co1B C26 C27 C26 61.9(6) . 2
C29 C26 C27 Co1B 111.8(7) 2 .
C28 C26 C27 Co1B -47.8(9) 2 .
C26A C26 C27 Co1B -59.6(7) . .
C26A C26 C27 Co1B -64.8(7) 2 .
C27 C26 C27 Co1B -59.4(7) 2 .
Co1B C26 C27 Co1B 3.5(12) 2 .
C29 C26 C27 Co1B 108.3(7) 2 2
C28 C26 C27 Co1B -51.2(9) 2 2
C26A C26 C27 Co1B -63.1(7) . 2
C26A C26 C27 Co1B -68.2(7) 2 2
C27 C26 C27 Co1B -62.8(7) 2 2
Co1B C26 C27 Co1B -3.5(12) . 2
Co1B Co1B C27 C26A -149(9) 2 2
C26 Co1B C27 C26A -32.1(12) 2 2
P3 Co1B C27 C26A -6(3) 2 2
C28 Co1B C27 C26A -5.4(15) . 2
P2 Co1B C27 C26A 100.0(16) 2 2
C29 Co1B C27 C26A -43.7(15) . 2
C26 Co1B C27 C26A -123.7(14) . 2
P1 Co1B C27 C26A 50.1(17) 2 2
C26A Co1B C27 C26A -86.8(15) . 2
P3 Co1B C27 C26A 146.5(16) . 2
Co1B Co1B C27 C29 -3(9) 2 2
C26 Co1B C27 C29 113.8(10) 2 2
P3 Co1B C27 C29 140(2) 2 2
C26A Co1B C27 C29 146(2) 2 2
C28 Co1B C27 C29 140.6(8) . 2
P2 Co1B C27 C29 -114.1(8) 2 2
C29 Co1B C27 C29 102.3(8) . 2
C26 Co1B C27 C29 22.3(8) . 2
P1 Co1B C27 C29 -164.0(12) 2 2
C26A Co1B C27 C29 59.1(8) . 2
P3 Co1B C27 C29 -67.6(8) . 2
Co1B Co1B C27 C28 -143(9) 2 .
C26 Co1B C27 C28 -26.8(5) 2 .
P3 Co1B C27 C28 -1(2) 2 .
C26A Co1B C27 C28 5.4(15) 2 .
P2 Co1B C27 C28 105.3(7) 2 .
C29 Co1B C27 C28 -38.3(2) . .
C26 Co1B C27 C28 -118.4(4) . .
P1 Co1B C27 C28 55.4(8) 2 .
C26A Co1B C27 C28 -81.5(4) . .
P3 Co1B C27 C28 151.8(8) . .
Co1B Co1B C27 C26 -25(9) 2 .
C26 Co1B C27 C26 91.6(6) 2 .
P3 Co1B C27 C26 117(2) 2 .
C26A Co1B C27 C26 123.7(14) 2 .
C28 Co1B C27 C26 118.4(4) . .
P2 Co1B C27 C26 -136.3(7) 2 .
C29 Co1B C27 C26 80.0(4) . .
P1 Co1B C27 C26 173.8(12) 2 .
C26A Co1B C27 C26 36.9(2) . .
P3 Co1B C27 C26 -89.8(6) . .
Co1B Co1B C27 C26 -117(9) 2 2
P3 Co1B C27 C26 26(2) 2 2
C26A Co1B C27 C26 32.1(12) 2 2
C28 Co1B C27 C26 26.8(5) . 2
P2 Co1B C27 C26 132.1(9) 2 2
C29 Co1B C27 C26 -11.5(5) . 2
C26 Co1B C27 C26 -91.6(6) . 2
P1 Co1B C27 C26 82.2(10) 2 2
C26A Co1B C27 C26 -54.7(6) . 2
P3 Co1B C27 C26 178.6(10) . 2
C26 Co1B C27 Co1B 117(9) 2 2
P3 Co1B C27 Co1B 143(11) 2 2
C26A Co1B C27 Co1B 149(9) 2 2
C28 Co1B C27 Co1B 143(9) . 2
P2 Co1B C27 Co1B -111(9) 2 2
C29 Co1B C27 Co1B 105(9) . 2
C26 Co1B C27 Co1B 25(9) . 2
P1 Co1B C27 Co1B -161(10) 2 2
C26A Co1B C27 Co1B 62(9) . 2
P3 Co1B C27 Co1B -65(9) . 2
C26A C27 C28 C26 -146(5) 2 2
C29 C27 C28 C26 9.9(8) 2 2
C26 C27 C28 C26 5.3(8) . 2
Co1B C27 C28 C26 66.4(11) . 2
Co1B C27 C28 C26 61.8(11) 2 2
C29 C27 C28 C26A 156(5) 2 2
C26 C27 C28 C26A 152(5) . 2
C26 C27 C28 C26A 146(5) 2 2
Co1B C27 C28 C26A -147(5) . 2
Co1B C27 C28 C26A -152(5) 2 2
C26A C27 C28 C29 -152(5) 2 .
C29 C27 C28 C29 4.58(10) 2 .
C26 C27 C28 C29 0.0 . .
C26 C27 C28 C29 -5.3(8) 2 .
Co1B C27 C28 C29 61.1(7) . .
Co1B C27 C28 C29 56.5(6) 2 .
C26A C27 C28 Co1B 147(5) 2 .
C29 C27 C28 Co1B -56.5(7) 2 .
C26 C27 C28 Co1B -61.1(7) . .
C26 C27 C28 Co1B -66.4(11) 2 .
Co1B C27 C28 Co1B -4.6(12) 2 .
C26A C27 C28 Co1B 152(5) 2 2
C29 C27 C28 Co1B -51.9(6) 2 2
C26 C27 C28 Co1B -56.5(6) . 2
C26 C27 C28 Co1B -61.8(11) 2 2
Co1B C27 C28 Co1B 4.6(12) . 2
Co1B Co1B C28 C26 -65(14) 2 2
P3 Co1B C28 C26 67.1(12) 2 2
C26A Co1B C28 C26 -115.1(13) 2 2
P2 Co1B C28 C26 168.1(11) 2 2
C29 Co1B C28 C26 5.7(8) . 2
C27 Co1B C28 C26 -112.4(9) . 2
C26 Co1B C28 C26 -74.6(9) . 2
P1 Co1B C28 C26 115.2(12) 2 2
C26A Co1B C28 C26 -31.6(9) . 2
P3 Co1B C28 C26 -149.4(12) . 2
Co1B Co1B C28 C26A 50(14) 2 2
C26 Co1B C28 C26A 115.1(13) 2 2
P3 Co1B C28 C26A -177.7(12) 2 2
P2 Co1B C28 C26A -76.8(10) 2 2
C29 Co1B C28 C26A 120.9(7) . 2
C27 Co1B C28 C26A 2.7(8) . 2
C26 Co1B C28 C26A 40.5(9) . 2
P1 Co1B C28 C26A -129.7(11) 2 2
C26A Co1B C28 C26A 83.5(8) . 2
P3 Co1B C28 C26A -34.3(11) . 2
Co1B Co1B C28 C27 47(14) 2 .
C26 Co1B C28 C27 112.4(9) 2 .
P3 Co1B C28 C27 179.5(11) 2 .
C26A Co1B C28 C27 -2.7(8) 2 .
P2 Co1B C28 C27 -79.5(8) 2 .
C29 Co1B C28 C27 118.2(3) . .
C26 Co1B C28 C27 37.8(3) . .
P1 Co1B C28 C27 -132.4(10) 2 .
C26A Co1B C28 C27 80.8(4) . .
P3 Co1B C28 C27 -37.0(8) . .
Co1B Co1B C28 C29 -71(14) 2 .
C26 Co1B C28 C29 -5.7(8) 2 .
P3 Co1B C28 C29 61.4(9) 2 .
C26A Co1B C28 C29 -120.9(7) 2 .
P2 Co1B C28 C29 162.3(9) 2 .
C27 Co1B C28 C29 -118.2(3) . .
C26 Co1B C28 C29 -80.3(5) . .
P1 Co1B C28 C29 109.4(9) 2 .
C26A Co1B C28 C29 -37.3(3) . .
P3 Co1B C28 C29 -155.1(10) . .
C26 Co1B C28 Co1B 65(14) 2 2
P3 Co1B C28 Co1B 132(15) 2 2
C26A Co1B C28 Co1B -50(14) 2 2
P2 Co1B C28 Co1B -127(15) 2 2
C29 Co1B C28 Co1B 71(14) . 2
C27 Co1B C28 Co1B -47(14) . 2
C26 Co1B C28 Co1B -9(14) . 2
P1 Co1B C28 Co1B -180(100) 2 2
C26A Co1B C28 Co1B 34(14) . 2
P3 Co1B C28 Co1B -84(14) . 2
C26A C28 C29 C26 54(8) 2 2
C27 C28 C29 C26 56(8) . 2
Co1B C28 C29 C26 117(8) . 2
Co1B C28 C29 C26 111(8) 2 2
C26 C28 C29 C27 -57(8) 2 2
C26A C28 C29 C27 -3.02(11) 2 2
C27 C28 C29 C27 -0.5 . 2
Co1B C28 C29 C27 60.5(5) . 2
Co1B C28 C29 C27 54.7(5) 2 2
C26 C28 C29 C26A -56(8) 2 .
C26A C28 C29 C26A -2.49(10) 2 .
C27 C28 C29 C26A 0.0 . .
Co1B C28 C29 C26A 61.0(5) . .
Co1B C28 C29 C26A 55.2(5) 2 .
C26 C28 C29 C26A -54(8) 2 2
C27 C28 C29 C26A 2.49(10) . 2
Co1B C28 C29 C26A 63.5(6) . 2
Co1B C28 C29 C26A 57.7(5) 2 2
C26 C28 C29 Co1B -117(8) 2 .
C26A C28 C29 Co1B -63.5(6) 2 .
C27 C28 C29 Co1B -61.0(5) . .
Co1B C28 C29 Co1B -5.8(9) 2 .
C26 C28 C29 Co1B -111(8) 2 2
C26A C28 C29 Co1B -57.7(5) 2 2
C27 C28 C29 Co1B -55.2(5) . 2
Co1B C28 C29 Co1B 5.8(9) . 2
Co1B Co1B C29 C26 120(10) 2 2
P3 Co1B C29 C26 -131.5(13) 2 2
C26A Co1B C29 C26 20.2(9) 2 2
C28 Co1B C29 C26 -7.2(11) . 2
P2 Co1B C29 C26 -34.3(18) 2 2
C27 Co1B C29 C26 31.0(12) . 2
C26 Co1B C29 C26 74.5(12) . 2
P1 Co1B C29 C26 -82.5(14) 2 2
C26A Co1B C29 C26 111.6(12) . 2
P3 Co1B C29 C26 60(4) . 2
Co1B Co1B C29 C27 -3(10) 2 2
C26 Co1B C29 C27 -122.8(13) 2 2
P3 Co1B C29 C27 105.7(9) 2 2
C26A Co1B C29 C27 -102.6(7) 2 2
C28 Co1B C29 C27 -130.0(7) . 2
P2 Co1B C29 C27 -157.1(15) 2 2
C27 Co1B C29 C27 -91.9(8) . 2
C26 Co1B C29 C27 -48.3(8) . 2
P1 Co1B C29 C27 154.7(10) 2 2
C26A Co1B C29 C27 -11.2(7) . 2
P3 Co1B C29 C27 -62(3) . 2
Co1B Co1B C29 C26A 8(10) 2 .
C26 Co1B C29 C26A -111.6(12) 2 .
P3 Co1B C29 C26A 116.8(8) 2 .
C26A Co1B C29 C26A -91.4(6) 2 .
C28 Co1B C29 C26A -118.8(4) . .
P2 Co1B C29 C26A -145.9(16) 2 .
C27 Co1B C29 C26A -80.7(4) . .
C26 Co1B C29 C26A -37.1(3) . .
P1 Co1B C29 C26A 165.9(11) 2 .
P3 Co1B C29 C26A -51(3) . .
Co1B Co1B C29 C28 127(10) 2 .
C26 Co1B C29 C28 7.2(11) 2 .
P3 Co1B C29 C28 -124.3(7) 2 .
C26A Co1B C29 C28 27.4(6) 2 .
P2 Co1B C29 C28 -27.1(13) 2 .
C27 Co1B C29 C28 38.1(3) . .
C26 Co1B C29 C28 81.7(5) . .
P1 Co1B C29 C28 -75.3(8) 2 .
C26A Co1B C29 C28 118.8(4) . .
P3 Co1B C29 C28 68(3) . .
Co1B Co1B C29 C26A 100(10) 2 2
C26 Co1B C29 C26A -20.2(9) 2 2
P3 Co1B C29 C26A -151.7(9) 2 2
C28 Co1B C29 C26A -27.4(6) . 2
P2 Co1B C29 C26A -54.5(14) 2 2
C27 Co1B C29 C26A 10.8(6) . 2
C26 Co1B C29 C26A 54.3(7) . 2
P1 Co1B C29 C26A -102.7(10) 2 2
C26A Co1B C29 C26A 91.4(6) . 2
P3 Co1B C29 C26A 40(3) . 2
C26 Co1B C29 Co1B -120(10) 2 2
P3 Co1B C29 Co1B 109(10) 2 2
C26A Co1B C29 Co1B -100(10) 2 2
C28 Co1B C29 Co1B -127(10) . 2
P2 Co1B C29 Co1B -154(11) 2 2
C27 Co1B C29 Co1B -89(10) . 2
C26 Co1B C29 Co1B -45(9) . 2
P1 Co1B C29 Co1B 158(11) 2 2
C26A Co1B C29 Co1B -8(10) . 2
P3 Co1B C29 Co1B -60(8) . 2
C26 C29 C26A C27 175.6(11) 2 2
C28 C29 C26A C27 -177.9(2) . 2
C26A C29 C26A C27 -179.0(2) 2 2
Co1B C29 C26A C27 -118.6(7) . 2
Co1B C29 C26A C27 -117.5(7) 2 2
C26 C29 C26A C28 -14.9(11) 2 2
C27 C29 C26A C28 169.57(18) 2 2
C28 C29 C26A C28 -8.3(3) . 2
C26A C29 C26A C28 -9.4(3) 2 2
Co1B C29 C26A C28 50.9(7) . 2
Co1B C29 C26A C28 52.0(7) 2 2
C26 C29 C26A C26 -6.6(10) 2 .
C27 C29 C26A C26 177.9(2) 2 .
C28 C29 C26A C26 0.0 . .
C26A C29 C26A C26 -1.1 2 .
Co1B C29 C26A C26 59.2(7) . .
Co1B C29 C26A C26 60.3(7) 2 .
C27 C29 C26A C26 -175.6(11) 2 2
C28 C29 C26A C26 6.6(10) . 2
C26A C29 C26A C26 5.5(10) 2 2
Co1B C29 C26A C26 65.8(13) . 2
Co1B C29 C26A C26 66.9(14) 2 2
C26 C29 C26A C29 -8.3(10) 2 2
C27 C29 C26A C29 176.1(2) 2 2
C28 C29 C26A C29 -1.8 . 2
C26A C29 C26A C29 -2.9 2 2
Co1B C29 C26A C29 57.5(7) . 2
Co1B C29 C26A C29 58.6(7) 2 2
C26 C29 C26A Co1B -66.9(14) 2 2
C27 C29 C26A Co1B 117.5(7) 2 2
C28 C29 C26A Co1B -60.3(7) . 2
C26A C29 C26A Co1B -61.5(7) 2 2
Co1B C29 C26A Co1B -1.1(13) . 2
C26 C29 C26A Co1B -65.8(13) 2 .
C27 C29 C26A Co1B 118.6(7) 2 .
C28 C29 C26A Co1B -59.2(7) . .
C26A C29 C26A Co1B -60.3(7) 2 .
Co1B C29 C26A Co1B 1.1(13) 2 .
C29 C26 C26A C27 -8.9(9) 2 2
C28 C26 C26A C27 -168.3(3) 2 2
C27 C26 C26A C27 1.4(2) . 2
C26A C26 C26A C27 2.7(2) 2 2
Co1B C26 C26A C27 -64.3(6) 2 2
Co1B C26 C26A C27 -57.1(5) . 2
C29 C26 C26A C28 159.4(6) 2 2
C27 C26 C26A C28 169.7(3) . 2
C26A C26 C26A C28 171.0(3) 2 2
C27 C26 C26A C28 168.3(3) 2 2
Co1B C26 C26A C28 104.0(6) 2 2
Co1B C26 C26A C28 111.2(5) . 2
C29 C26 C26A C29 -10.3(8) 2 .
C28 C26 C26A C29 -169.7(3) 2 .
C27 C26 C26A C29 0.0 . .
C26A C26 C26A C29 1.3 2 .
C27 C26 C26A C29 -1.4(2) 2 .
Co1B C26 C26A C29 -65.7(6) 2 .
Co1B C26 C26A C29 -58.5(5) . .
C29 C26 C26A C26 -12.7(9) 2 2
C28 C26 C26A C26 -172.2(5) 2 2
C27 C26 C26A C26 -2.4(4) . 2
C26A C26 C26A C26 -1.1(4) 2 2
C27 C26 C26A C26 -3.8(4) 2 2
Co1B C26 C26A C26 -68.1(6) 2 2
Co1B C26 C26A C26 -60.9(6) . 2
C28 C26 C26A C29 -159.4(6) 2 2
C27 C26 C26A C29 10.3(8) . 2
C26A C26 C26A C29 11.6(8) 2 2
C27 C26 C26A C29 8.9(9) 2 2
Co1B C26 C26A C29 -55.4(9) 2 2
Co1B C26 C26A C29 -48.2(9) . 2
C29 C26 C26A Co1B 55.4(9) 2 2
C28 C26 C26A Co1B -104.0(6) 2 2
C27 C26 C26A Co1B 65.7(6) . 2
C26A C26 C26A Co1B 67.0(6) 2 2
C27 C26 C26A Co1B 64.3(6) 2 2
Co1B C26 C26A Co1B 7.2(10) . 2
C29 C26 C26A Co1B 48.2(9) 2 .
C28 C26 C26A Co1B -111.2(5) 2 .
C27 C26 C26A Co1B 58.5(5) . .
C26A C26 C26A Co1B 59.8(5) 2 .
C27 C26 C26A Co1B 57.1(5) 2 .
Co1B C26 C26A Co1B -7.2(10) 2 .
Co1B Co1B C26A C27 -147(11) 2 2
C26 Co1B C26A C27 46.6(15) 2 2
P3 Co1B C26A C27 -43.4(15) 2 2
C26A Co1B C26A C27 91.7(15) 2 2
C28 Co1B C26A C27 62.3(15) . 2
P2 Co1B C26A C27 125(3) 2 2
C29 Co1B C26A C27 24.1(15) . 2
C27 Co1B C26A C27 106.2(14) . 2
C26 Co1B C26A C27 143.5(14) . 2
P1 Co1B C26A C27 2(2) 2 2
P3 Co1B C26A C27 -175.7(17) . 2
Co1B Co1B C26A C28 39(10) 2 2
C26 Co1B C26A C28 -126.8(12) 2 2
P3 Co1B C26A C28 143.2(10) 2 2
C26A Co1B C26A C28 -81.6(8) 2 2
C28 Co1B C26A C28 -111.1(11) . 2
P2 Co1B C26A C28 -49(3) 2 2
C29 Co1B C26A C28 -149.2(10) . 2
C27 Co1B C26A C28 -67.1(11) . 2
C26 Co1B C26A C28 -29.9(10) . 2
P1 Co1B C26A C28 -171.3(17) 2 2
P3 Co1B C26A C28 10.9(13) . 2
Co1B Co1B C26A C29 -171(11) 2 .
C26 Co1B C26A C29 22.5(4) 2 .
P3 Co1B C26A C29 -67.5(7) 2 .
C26A Co1B C26A C29 67.6(6) 2 .
C28 Co1B C26A C29 38.1(3) . .
P2 Co1B C26A C29 101(2) 2 .
C27 Co1B C26A C29 82.1(4) . .
C26 Co1B C26A C29 119.4(4) . .
P1 Co1B C26A C29 -22.1(14) 2 .
P3 Co1B C26A C29 160.1(13) . .
Co1B Co1B C26A C26 69(10) 2 .
C26 Co1B C26A C26 -96.9(6) 2 .
P3 Co1B C26A C26 173.1(8) 2 .
C26A Co1B C26A C26 -51.8(7) 2 .
C28 Co1B C26A C26 -81.2(5) . .
P2 Co1B C26A C26 -19(2) 2 .
C29 Co1B C26A C26 -119.4(4) . .
C27 Co1B C26A C26 -37.3(3) . .
P1 Co1B C26A C26 -141.4(17) 2 .
P3 Co1B C26A C26 40.7(10) . .
Co1B Co1B C26A C26 166(11) 2 2
P3 Co1B C26A C26 -90.0(8) 2 2
C26A Co1B C26A C26 45.1(6) 2 2
C28 Co1B C26A C26 15.7(4) . 2
P2 Co1B C26A C26 78(2) 2 2
C29 Co1B C26A C26 -22.5(4) . 2
C27 Co1B C26A C26 59.6(5) . 2
C26 Co1B C26A C26 96.9(6) . 2
P1 Co1B C26A C26 -44.5(14) 2 2
P3 Co1B C26A C26 137.6(14) . 2
Co1B Co1B C26A C29 78(10) 2 2
C26 Co1B C26A C29 -88.7(8) 2 2
P3 Co1B C26A C29 -178.7(9) 2 2
C26A Co1B C26A C29 -43.5(4) 2 2
C28 Co1B C26A C29 -73.0(8) . 2
P2 Co1B C26A C29 -11(2) 2 2
C29 Co1B C26A C29 -111.1(7) . 2
C27 Co1B C26A C29 -29.0(7) . 2
C26 Co1B C26A C29 8.2(6) . 2
P1 Co1B C26A C29 -133.2(17) 2 2
P3 Co1B C26A C29 49.0(11) . 2
C26 Co1B C26A Co1B -166(11) 2 2
P3 Co1B C26A Co1B 104(10) 2 2
C26A Co1B C26A Co1B -121(11) 2 2
C28 Co1B C26A Co1B -151(11) . 2
P2 Co1B C26A Co1B -88(11) 2 2
C29 Co1B C26A Co1B 171(11) . 2
C27 Co1B C26A Co1B -107(11) . 2
C26 Co1B C26A Co1B -69(10) . 2
P1 Co1B C26A Co1B 149(12) 2 2
P3 Co1B C26A Co1B -29(9) . 2
