#------------------------------------------------------------------------------
#$Date: 2025-08-19 00:06:14 +0300 (Tue, 19 Aug 2025) $
#$Revision: 301780 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/15/1551534.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1551534
loop_
_publ_author_name
'KIWADA, Tatsuto'
'HIRASAKI, Aika'
'ODANI, Akira'
_publ_section_title
;
 Crystal Structure of
 (2,2′-Bipyridine)(N-(1-naphthyl)methyl-1,3-propanediamine)platinum(II)
 Chloride
;
_journal_issue                   0
_journal_name_full               'X-ray Structure Analysis Online'
_journal_page_first              35
_journal_paper_doi               10.2116/xraystruct.35.35
_journal_volume                  35
_journal_year                    2019
_chemical_formula_sum            'C24 H26 Cl2 N4 Pt'
_chemical_formula_weight         636.48
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                90
_cell_angle_beta                 109.032(8)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   23.3026(14)
_cell_length_b                   17.4118(12)
_cell_length_c                   12.3816(7)
_cell_measurement_reflns_used    18937
_cell_measurement_temperature    93(2)
_cell_measurement_theta_max      27.47
_cell_measurement_theta_min      1.74
_cell_volume                     4749.1(6)
_computing_cell_refinement       'RAPID AUTO (Rigaku)'
_computing_data_collection       'RAPID AUTO (Rigaku)'
_computing_data_reduction        'RAPID AUTO (Rigaku)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 2012)'
_computing_publication_material  'WinGX publication routines (Farrugia, 2012'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_diffrn_ambient_temperature      93(2)
_diffrn_detector_area_resol_mean 10
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Rigaku CCD Diffractometer'
_diffrn_measurement_method       'phi or omega oscillation scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0407
_diffrn_reflns_av_unetI/netI     0.0310
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            22044
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.467
_diffrn_reflns_theta_min         2.050
_diffrn_source                   'sealed x-ray tube'
_exptl_absorpt_coefficient_mu    6.153
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.780
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             2480
_exptl_crystal_size_max          0.450
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_transmission_factor_max   1.0000
_exptl_transmission_factor_min   0.3567
_refine_diff_density_max         0.937
_refine_diff_density_min         -0.734
_refine_diff_density_rms         0.097
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     299
_refine_ls_number_reflns         5435
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0335
_refine_ls_R_factor_gt           0.0242
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0222P)²+4.7442P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0466
_refine_ls_wR_factor_ref         0.0490
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4657
_reflns_number_total             5435
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            35_35_1.txt
_cod_data_source_block           shelx
_cod_database_code               1551534
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.168
_shelx_estimated_absorpt_t_max   0.372
_shelx_res_file
;
TITL SIR2014 run in space group C 2/c
    shelx.res
    created by SHELXL-2018/3 at 20:23:12 on 05-Mar-2019
CELL  0.71073  23.3026  17.4118  12.3816   90.000  109.032   90.000
ZERR     8.00   0.0014   0.0012   0.0007    0.000    0.008    0.000
LATT   7
SYMM  - X,   Y, 1/2 - Z
SFAC  C    H    N    CL   PT
UNIT  192 208 32 16 8
MERG   2
ABIN
RIGU 0.02 C17 C18
SADI 0.01 N4 C13A N4 C13B
FMAP   2
PLAN   25
SIZE     0.200   0.200   0.450
ACTA
BOND   $H
CONF
L.S.   5    0    9
TEMP  -180.00
WGHT    0.022200    4.744200
FVAR       0.85565   0.53992
C10   1    0.338548    0.215519    0.667769    11.00000    0.03939    0.04448 =
         0.02805   -0.00391    0.01185   -0.00443
AFIX  43
H1    2    0.358882    0.258434    0.710844    11.00000   -1.20000
AFIX   0
C9    1    0.321101    0.156228    0.723519    11.00000    0.04961    0.05277 =
         0.02964    0.00462    0.01467   -0.00303
AFIX  43
H2    2    0.329016    0.158766    0.803716    11.00000   -1.20000
AFIX   0
C8    1    0.292138    0.093196    0.662818    11.00000    0.05148    0.04659 =
         0.03575    0.00742    0.01669   -0.00885
AFIX  43
H3    2    0.280553    0.051374    0.700465    11.00000   -1.20000
AFIX   0
C7    1    0.280261    0.092022    0.545924    11.00000    0.04230    0.03442 =
         0.03952    0.00219    0.01245   -0.00795
AFIX  43
H4    2    0.260245    0.049204    0.502123    11.00000   -1.20000
AFIX   0
C6    1    0.297661    0.153468    0.493130    11.00000    0.02957    0.03067 =
         0.02763    0.00052    0.00569    0.00025
C5    1    0.282349    0.160573    0.368880    11.00000    0.03214    0.02738 =
         0.02963    0.00102    0.00918   -0.00040
C4    1    0.248450    0.106822    0.291530    11.00000    0.05324    0.03407 =
         0.03668   -0.00103    0.01219   -0.01310
AFIX  43
H7    2    0.235817    0.060687    0.318020    11.00000   -1.20000
AFIX   0
C3    1    0.233234    0.120716    0.176239    11.00000    0.05851    0.04031 =
         0.03412   -0.00883    0.00488   -0.01516
AFIX  43
H8    2    0.210541    0.084120    0.122206    11.00000   -1.20000
AFIX   0
C2    1    0.251466    0.188578    0.140527    11.00000    0.04742    0.04116 =
         0.02543    0.00051    0.00309   -0.00686
AFIX  43
H9    2    0.240716    0.199734    0.061300    11.00000   -1.20000
AFIX   0
C1    1    0.285323    0.240183    0.220060    11.00000    0.03820    0.03372 =
         0.02818    0.00264    0.00722   -0.00352
AFIX  43
H10   2    0.297367    0.287031    0.194473    11.00000   -1.20000
AFIX   0
C11   1    0.406307    0.434186    0.599777    11.00000    0.05896    0.03367 =
         0.04049   -0.01149    0.01376   -0.00526
PART    1
AFIX  23
H11A  2    0.445120    0.459013    0.643742    21.00000   -1.20000
H11B  2    0.376519    0.444768    0.639487    21.00000   -1.20000
PART    2
AFIX  23
H11C  2    0.430313    0.455272    0.675254   -21.00000   -1.20000
H11D  2    0.362906    0.445960    0.585656   -21.00000   -1.20000
AFIX   0
PART    1
C12A  1    0.382800    0.469426    0.476709    21.00000    0.04587    0.02592 =
         0.04377   -0.00224    0.01079    0.00271
AFIX  23
H12A  2    0.339340    0.456710    0.440300    21.00000   -1.20000
H12B  2    0.386787    0.526038    0.481394    21.00000   -1.20000
AFIX   0
C13A  1    0.418691    0.438199    0.406127    21.00000    0.03502    0.03253 =
         0.03887   -0.00517    0.01212   -0.01026
AFIX  23
H13A  2    0.461553    0.430349    0.453786    21.00000   -1.20000
H13B  2    0.417475    0.474141    0.343462    21.00000   -1.20000
AFIX   0
PART    2
C12B  1    0.427405    0.468395    0.506325   -21.00000    0.04615    0.02763 =
         0.04971   -0.00079    0.00541   -0.01188
AFIX  23
H12C  2    0.429891    0.524974    0.514420   -21.00000   -1.20000
H12D  2    0.468386    0.448757    0.513747   -21.00000   -1.20000
AFIX   0
C13B  1    0.383891    0.447526    0.390857   -21.00000    0.04444    0.02900 =
         0.03912    0.00076    0.00485   -0.01377
AFIX  23
H13C  2    0.391567    0.481127    0.332529   -21.00000   -1.20000
H13D  2    0.341923    0.457312    0.390169   -21.00000   -1.20000
AFIX   0
PART    0
C14   1    0.442524    0.328761    0.330587    11.00000    0.04511    0.07509 =
         0.04294    0.00817    0.01086   -0.02447
AFIX  23
H14A  2    0.473509    0.312138    0.402591    11.00000   -1.20000
H14B  2    0.460795    0.369580    0.296618    11.00000   -1.20000
AFIX   0
C15   1    0.426407    0.261710    0.249716    11.00000    0.02980    0.07014 =
         0.04598    0.00425    0.01490   -0.00244
C16   1    0.407318    0.276519    0.134138    11.00000    0.04551    0.08550 =
         0.04009    0.00677    0.01636   -0.00663
AFIX  43
H16   2    0.406096    0.328171    0.108767    11.00000   -1.20000
AFIX   0
C17   1    0.389835    0.218231    0.053749    11.00000    0.06071    0.08503 =
         0.05159    0.00100    0.02138   -0.00062
AFIX  43
H17   2    0.378056    0.230665   -0.025188    11.00000   -1.20000
AFIX   0
C18   1    0.389235    0.144569    0.085325    11.00000    0.06061    0.10403 =
         0.05985   -0.01496    0.02334   -0.00106
AFIX  43
H18   2    0.375148    0.105752    0.028938    11.00000   -1.20000
AFIX   0
C19   1    0.409653    0.124613    0.203016    11.00000    0.04257    0.07465 =
         0.07923   -0.00072    0.02537    0.00619
C20   1    0.410007    0.048143    0.240812    11.00000    0.07426    0.07221 =
         0.11114    0.00434    0.03021    0.00914
AFIX  43
H20   2    0.396704    0.008217    0.186017    11.00000   -1.20000
AFIX   0
C21   1    0.428620    0.030582    0.351897    11.00000    0.07929    0.07478 =
         0.12263    0.02590    0.03035    0.01665
AFIX  43
H21   2    0.428311   -0.021540    0.374386    11.00000   -1.20000
AFIX   0
C22   1    0.448584    0.087404    0.435916    11.00000    0.06332    0.09932 =
         0.07518    0.03435    0.01811    0.02671
AFIX  43
H22   2    0.461378    0.073734    0.514475    11.00000   -1.20000
AFIX   0
C23   1    0.449633    0.162834    0.404580    11.00000    0.04523    0.07988 =
         0.06575    0.02197    0.02193    0.01789
AFIX  43
H23   2    0.464447    0.201091    0.461609    11.00000   -1.20000
AFIX   0
C24   1    0.428691    0.184129    0.287294    11.00000    0.03078    0.07157 =
         0.05654    0.01106    0.01884    0.00829
N2    3    0.327763    0.214736    0.554233    11.00000    0.02981    0.03057 =
         0.02728   -0.00003    0.01016    0.00004
N1    3    0.301823    0.226362    0.332512    11.00000    0.03255    0.02629 =
         0.02580   -0.00082    0.00500   -0.00166
N3    3    0.415661    0.349788    0.596361    11.00000    0.03520    0.03433 =
         0.02688   -0.00220    0.00535   -0.00325
AFIX  23
H3NA  2    0.412702    0.329117    0.661843    11.00000   -1.20000
H3NB  2    0.454234    0.341469    0.596475    11.00000   -1.20000
AFIX   0
N4    3    0.389241    0.361639    0.357773    11.00000    0.06315    0.03038 =
         0.02566   -0.00029    0.00988   -0.01439
PART    1
AFIX  13
H4NA  2    0.355537    0.371420    0.284763    21.00000   -1.20000
PART    2
AFIX  13
H4NB  2    0.356063    0.357512    0.282595   -21.00000   -1.20000
AFIX   0
PART    0
CL1   4    0.440953    0.341547    0.869128    11.00000    0.04245    0.06676 =
         0.03398   -0.00574    0.00875   -0.00758
CL2   4    0.291229    0.425256    0.125618    11.00000    0.08343    0.03309 =
         0.04125    0.00585    0.01990    0.00906
PT1   5    0.357564    0.291342    0.460930    11.00000    0.03043    0.02382 =
         0.02318   -0.00032    0.00498   -0.00208
HKLF    4




REM  SIR2014 run in space group C 2/c
REM wR2 = 0.0490, GooF = S = 1.034, Restrained GooF = 1.035 for all data
REM R1 = 0.0242 for 4657 Fo > 4sig(Fo) and 0.0335 for all 5435 data
REM 299 parameters refined using 4 restraints

END

WGHT      0.0222      4.7441

REM Highest difference peak  0.937,  deepest hole -0.734,  1-sigma level  0.097
Q1    1   0.3557  0.3438  0.4620  11.00000  0.05    0.94
Q2    1   0.3573  0.2406  0.4629  11.00000  0.05    0.90
Q3    1   0.4574  0.2998  0.8748  11.00000  0.05    0.61
Q4    1   0.4048  0.2950  0.5490  11.00000  0.05    0.44
Q5    1   0.4184  0.2975  0.4667  11.00000  0.05    0.41
Q6    1   0.3421  0.2811  0.5573  11.00000  0.05    0.39
Q7    1   0.2956  0.1537  0.4288  11.00000  0.05    0.39
Q8    1   0.3310  0.2506  0.5164  11.00000  0.05    0.37
Q9    1   0.4576  0.2132  0.1181  11.00000  0.05    0.37
Q10   1   0.2700  0.0612  0.4364  11.00000  0.05    0.37
Q11   1   0.3568  0.3702  0.3886  11.00000  0.05    0.36
Q12   1   0.4305  0.3788  0.7959  11.00000  0.05    0.36
Q13   1   0.3288  0.1898  0.6959  11.00000  0.05    0.36
Q14   1   0.3945  0.2894  0.6108  11.00000  0.05    0.35
Q15   1   0.3095  0.4003  0.1206  11.00000  0.05    0.35
Q16   1   0.4580  0.1012  0.5023  11.00000  0.05    0.35
Q17   1   0.3091  0.2787  0.3717  11.00000  0.05    0.34
Q18   1   0.3891  0.3339  0.4055  11.00000  0.05    0.34
Q19   1   0.2616  0.4124  0.1125  11.00000  0.05    0.33
Q20   1   0.3012  0.4401  0.1743  11.00000  0.05    0.33
Q21   1   0.3185  0.2893  0.3043  11.00000  0.05    0.33
Q22   1   0.3740  0.3235  0.6781  11.00000  0.05    0.32
Q23   1   0.4255  0.0731  0.4043  11.00000  0.05    0.32
Q24   1   0.2889  0.1181  0.3146  11.00000  0.05    0.32
Q25   1   0.3675  0.2684  0.3746  11.00000  0.05    0.32
;
_shelx_res_checksum              17470
_shelx_hkl_file
;
   0   0   1-19.1455  7.2594   1
   0   0  -290966.80 2095.86   1
   0   0  -2101139.0 1797.21   1
   0   0  -3 -145.46 211.953   1
   0   0  -3 35.9823 18.2911   1
   0   0  -4 1165.30  167.37   1
   0   0  -4 908.877 25.0859   1
   0   0  -5 452.289 181.513   1
   0   0  -5 115.604 22.5754   1
   0   0  -6 7817.79 337.639   1
   0   0  -6 6975.23 74.3226   1
   0   0  -7 463.735 239.955   1
   0   0  -8 2038.66 309.622   1
   0   0  -9 329.742 313.819   1
   0   0 -1046860.90 1707.75   1
   0   0 -11-547.733 675.302   1
   0   0 -1253090.70 2190.32   1
   0   0 -13 149.219 492.759   1
   0   0 -1415857.70 1799.74   1
   0   0 -15-180.812 627.709   1
   0  -2   1 1213.32 74.9258   1
   0   2   1 1091.51 47.5027   1
   0   2  -1 1222.95 71.1823   1
   0  -2  -1 1110.89 43.5005   1
   0   2  -1 1109.42 55.4643   1
   0  -2   267018.80 1453.93   1
   0  -2   272823.70 1195.23   1
   0   2   270970.70 1310.59   1
   0   2  -267667.60 1454.47   1
   0  -2  -269808.40 1212.33   1
   0   2  -274117.00 1189.86   1
   0  -2   3 6464.85 227.818   1
   0  -2   3 6054.41 60.1482   1
   0   2   3 5967.65 96.0366   1
   0   2  -3 6513.07 235.171   1
   0  -2  -3 6155.07 88.6151   1
   0   2  -3 6039.00 68.0241   1
   0  -2   444811.20 1040.30   1
   0  -2   445477.00 603.537   1
   0   2   443460.90  673.36   1
   0   2  -443952.00 1247.09   1
   0  -2  -442890.50  657.03   1
   0   2  -447275.40 572.508   1
   0  -2   531905.30 1055.94   1
   0   2   530648.00 488.228   1
   0   2  -531046.50 773.472   1
   0  -2  -530877.80 433.461   1
   0  -2   6 2084.44 255.005   1
   0   2   6 2015.69 63.3811   1
   0   2  -6 1687.15 242.766   1
   0  -2  -6 2094.30 58.6049   1
   0   2   737085.50 626.849   1
   0   2  -740073.20 1123.38   1
   0  -2  -739625.60 1110.58   1
   0  -2  -739938.80 605.537   1
   0   2  -815480.00 615.302   1
   0  -2  -814718.50 871.232   1
   0  -2  -814971.80 205.745   1
   0   2  -918970.90 791.883   1
   0  -2  -919115.70 759.052   1
   0  -2  -918711.10 287.879   1
   0   2 -1042981.30 2036.11   1
   0  -2 -1041998.70 1435.11   1
   0  -2 -1035685.50 610.919   1
   0  -2 -1037849.00 564.186   1
   0   2 -11 1278.43 464.446   1
   0  -2 -11 1057.33 430.889   1
   0   2 -1228127.50 1347.79   1
   0  -2 -1225845.50 1296.62   1
   0   2 -13 423.916  516.94   1
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 -29  -3   2 3090.24  666.87   1
 -29   3   2 2907.30 678.581   1
 -29  -3   2 2157.90 729.586   1
  29  -5  -7-370.049 604.105   1
 -29  -5   7 864.521  539.19   1
 -29   5   7  489.40 607.905   1
 -29  -5   7 694.622 615.256   1
  29  -5  -6 5513.40 838.573   1
 -29  -5   6 5311.53 737.612   1
 -29   5   6 4576.32 819.869   1
 -29  -5   6 5860.22 853.846   1
  29  -5  -5-22.5228 575.927   1
 -29  -5   5 246.239 985.282   1
 -29   5   5 1687.83 1016.72   1
 -29  -5   5 1251.26 1069.49   1
 -29  -5   4 8030.82 866.294   1
 -29   5   4 6822.03 1377.12   1
 -29  -5   4 6487.07 1441.55   1
 -29  -5   3 1068.53 614.042   1
 -29   5   3 454.366 578.363   1
 -29  -5   3 559.044 634.415   1
 -30   0   7 568.921 969.577   1
 -30   0   613333.10 1097.55   1
 -30   0   5-1005.33  584.61   1
 -30   0   4 4587.24 773.066   1
 -30  -2   6 6283.65 787.118   1
 -30   2   6 5066.73 833.091   1
 -30  -2   5 789.358 578.564   1
 -30   2   5 967.595 613.679   1
 -30  -2   4 4200.00  715.58   1
 -30   2   4 2964.16 716.366   1
   0   0   0    0.00    0.00   1

_diffrn_radiation_type                  Mok\a
_diffrn_radiation_monochromator         graphite
_diffrn_radiation_probe                 x-ray
_diffrn_radiation_wavelength            0.71073
_diffrn_source                          'sealed x-ray tube'
_diffrn_detector                        'CCD plate'
_diffrn_detector_area_resol_mean        10
_diffrn_measurement_device              'quarter \C-circle diffractometer'
_diffrn_measurement_device_type         'Rigaku CCD Diffractometer'
_diffrn_measurement_method              'phi or omega oscillation scans'
_diffrn_standards_number                0
_diffrn_standards_interval_time         .
_diffrn_standards_interval_count        .
_diffrn_standards_decay_%               ?
_diffrn_orient_matrix_UB_11             0.008929
_diffrn_orient_matrix_UB_12             -0.054456
_diffrn_orient_matrix_UB_13             -0.014674
_diffrn_orient_matrix_UB_21             0.022287
_diffrn_orient_matrix_UB_22             0.018123
_diffrn_orient_matrix_UB_23             -0.051905
_diffrn_orient_matrix_UB_31             0.038526
_diffrn_orient_matrix_UB_32             0.002137
_diffrn_orient_matrix_UB_33             0.066254
_diffrn_reflns_limit_h_min              1000000
_diffrn_reflns_limit_h_max              -1000000
_diffrn_reflns_limit_k_min              1000000
_diffrn_reflns_limit_k_max              -1000000
_diffrn_reflns_limit_l_min              1000000
_diffrn_reflns_limit_l_max              -1000000
_diffrn_reflns_theta_min                1000
_diffrn_reflns_theta_max                0
_diffrn_reflns_number                   0
_diffrn_reflns_number_extinctions       0
_diffrn_reflns_number_accepted          22389
_diffrn_reflns_number_rejected          0
_diffrn_ambient_temperature             93
_computing_data_collection              'CrystalClear (Rigaku/MSC Inc., 2006)'
_computing_cell_refinement              'CrystalClear (Rigaku/MSC Inc., 2006)'
_computing_data_reduction               'CrystalClear (Rigaku/MSC Inc., 2006), S
_exptl_crystal_description              platelet
_exptl_crystal_colour                   yellow
_exptl_crystal_size_max                 0.45
_exptl_crystal_size_mid                 0.2
_exptl_crystal_size_min                 0.2
_exptl_crystal_density_method           'not measured'
_exptl_crystal_F000                     2480
_cell_length_a                          23.3026(14)
_cell_length_b                          17.4118(12)
_cell_length_c                          12.3816(7)
_cell_angle_alpha                       90
_cell_angle_beta                        109.032(8)
_cell_angle_gamma                       90
_cell_volume                            4749.1(5)
_cell_measurement_temperature           93
_cell_measurement_wavelength            0.71073
_cell_measurement_reflns_used           18937
_cell_measurement_theta_max             27.47
_cell_measurement_theta_min             1.74
_exptl_absorpt_coefficient_mu           6.117
_exptl_absorpt_correction_type          ?
loop_
    _atom_type_symbol
    _atom_type_number_in_cell
C 192
H 208
Cl 16
N 32
Pt 8
_cell_formula_units_Z                   8
_chemical_formula_moiety                ?
_chemical_formula_sum                  'C24 H26 N4 Cl2 Pt1'
_chemical_compound_source               ?
_space_group_crystal_system             monoclinic
_space_group_name_H-M_alt               C2/c
_space_group_name_Hall                 '-C 2yc'
_space_group_IT_number                  15
_computing_structure_solution           ?
_computing_structure_refinement        'SHELXL (Sheldrick, 2015)'
_computing_molecular_graphics          'Ortep-3 for Windows (Farrugia, 2012)'
_computing_publication_material        'WinGX publication routines (Farrugia, 20
_atom_sites_solution_primary            ?
_atom_sites_solution_secondary          ?
_refine_ls_number_constraints           0
_refine_ls_number_restraints            0
;
_shelx_hkl_checksum              77506
_shelx_fab_file
;
    4    0    0     50.35      0.00
    6    0    0     30.01      0.00
    8    0    0     13.42      0.00
   10    0    0      3.54      0.00
   12    0    0     -0.56      0.00
   14    0    0     -1.41      0.00
   16    0    0     -0.96      0.00
   18    0    0     -0.10      0.00
   20    0    0      0.75      0.00
   22    0    0      1.20      0.00
   24    0    0      1.10      0.00
   26    0    0      0.67      0.00
   28    0    0      0.30      0.00
    3    1    0    -29.74      0.00
    5    1    0    -19.90      0.00
    7    1    0    -10.45      0.00
    9    1    0     -3.89      0.00
   11    1    0     -0.53      0.00
   13    1    0      0.66      0.00
   15    1    0      0.81      0.00
   17    1    0      0.56      0.00
   19    1    0      0.21      0.00
   21    1    0      0.00      0.00
   23    1    0      0.05      0.00
   25    1    0      0.25      0.00
   27    1    0      0.35      0.00
    2    2    0    -28.37      0.00
    4    2    0    -21.13      0.00
    6    2    0    -12.47      0.00
    8    2    0     -5.32      0.00
   10    2    0     -1.09      0.00
   12    2    0      0.52      0.00
   14    2    0      0.62      0.00
   16    2    0      0.16      0.00
   18    2    0     -0.46      0.00
   20    2    0     -1.15      0.00
   22    2    0     -1.73      0.00
   24    2    0     -1.95      0.00
   26    2    0     -1.66      0.00
   28    2    0     -1.05      0.00
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    7    3    0     15.34      0.00
    9    3    0      5.14      0.00
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   13    3    0     -1.63      0.00
   15    3    0     -1.57      0.00
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   19    3    0      0.19      0.00
   21    3    0      1.09      0.00
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   25    3    0      1.25      0.00
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   26    4    0      1.08      0.00
   28    4    0      0.91      0.00
    1    5    0    -18.00      0.00
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    4    6    0     19.21      0.00
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   10    6    0      0.63      0.00
   12    6    0     -1.05      0.00
   14    6    0     -1.30      0.00
   16    6    0     -0.89      0.00
   18    6    0     -0.16      0.00
   20    6    0      0.67      0.00
   22    6    0      1.31      0.00
   24    6    0      1.48      0.00
   26    6    0      1.16      0.00
    1    7    0    -10.16      0.00
    3    7    0     -8.35      0.00
    5    7    0     -5.54      0.00
    7    7    0     -2.83      0.00
    9    7    0     -0.90      0.00
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   25    7    0      0.14      0.00
   27    7    0      0.24      0.00
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    2    8    0     -8.09      0.00
    4    8    0     -6.00      0.00
    6    8    0     -3.43      0.00
    8    8    0     -1.23      0.00
   10    8    0      0.05      0.00
   12    8    0      0.35      0.00
   14    8    0      0.03      0.00
   16    8    0     -0.43      0.00
   18    8    0     -0.74      0.00
   20    8    0     -0.83      0.00
   22    8    0     -0.78      0.00
   24    8    0     -0.68      0.00
   26    8    0     -0.57      0.00
    1    9    0     13.42      0.00
    3    9    0     11.00      0.00
    5    9    0      7.15      0.00
    7    9    0      3.33      0.00
    9    9    0      0.64      0.00
   11    9    0     -0.53      0.00
   13    9    0     -0.55      0.00
   15    9    0     -0.06      0.00
   17    9    0      0.39      0.00
   19    9    0      0.56      0.00
   21    9    0      0.46      0.00
   23    9    0      0.24      0.00
   25    9    0      0.05      0.00
    0   10    0     -6.22      0.00
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    6   10    0     -2.04      0.00
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   12   10    0      0.43      0.00
   14   10    0      0.30      0.00
   16   10    0      0.24      0.00
   18   10    0      0.30      0.00
   20   10    0      0.39      0.00
   22   10    0      0.40      0.00
   24   10    0      0.36      0.00
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    5   11    0     -2.07      0.00
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   13   11    0     -0.01      0.00
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   19   11    0     -0.75      0.00
   21   11    0     -0.43      0.00
   23   11    0      0.05      0.00
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    2   12    0      6.90      0.00
    4   12    0      4.93      0.00
    6   12    0      2.61      0.00
    8   12    0      0.73      0.00
   10   12    0     -0.32      0.00
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    0   22    0     -1.09      0.00
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    3    1    1    -45.63      0.00
    5    1    1    -31.56      0.00
    7    1    1    -17.40      0.00
    9    1    1     -7.08      0.00
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   13    1    1      0.63      0.00
   15    1    1      1.02      0.00
   17    1    1      0.72      0.00
   19    1    1      0.15      0.00
   21    1    1     -0.40      0.00
   23    1    1     -0.66      0.00
   25    1    1     -0.56      0.00
   27    1    1     -0.28      0.00
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  -10    2    1      1.74      0.00
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    0    2    1     51.41      0.00
    2    2    1     47.68      0.00
    4    2    1     36.52      0.00
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   15    3    1      0.07      0.00
   17    3    1      0.39      0.00
   19    3    1      0.69      0.00
   21    3    1      1.04      0.00
   23    3    1      1.36      0.00
   25    3    1      1.41      0.00
   27    3    1      1.06      0.00
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    6    4    1    -16.29      0.00
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  -21    5   13      0.19      0.00
  -19    5   13      0.24      0.00
  -17    5   13      0.06      0.00
  -15    5   13     -0.37      0.00
  -13    5   13     -0.92      0.00
  -11    5   13     -1.38      0.00
   -9    5   13     -1.48      0.00
   -7    5   13     -1.06      0.00
   -5    5   13     -0.21      0.00
   -3    5   13      0.78      0.00
   -1    5   13      1.50      0.00
    1    5   13      1.66      0.00
    3    5   13      1.27      0.00
    5    5   13      0.60      0.00
    7    5   13      0.03      0.00
  -22    6   13      0.10      0.00
  -20    6   13     -0.21      0.00
  -18    6   13     -0.56      0.00
  -16    6   13     -0.75      0.00
  -14    6   13     -0.63      0.00
  -12    6   13     -0.24      0.00
  -10    6   13      0.25      0.00
   -8    6   13      0.60      0.00
   -6    6   13      0.65      0.00
   -4    6   13      0.44      0.00
   -2    6   13      0.10      0.00
    0    6   13     -0.20      0.00
    2    6   13     -0.32      0.00
    4    6   13     -0.20      0.00
    6    6   13      0.09      0.00
  -21    7   13      0.21      0.00
  -19    7   13      0.66      0.00
  -17    7   13      1.12      0.00
  -15    7   13      1.43      0.00
  -13    7   13      1.46      0.00
  -11    7   13      1.23      0.00
   -9    7   13      0.78      0.00
   -7    7   13      0.19      0.00
   -5    7   13     -0.50      0.00
   -3    7   13     -1.13      0.00
   -1    7   13     -1.47      0.00
    1    7   13     -1.34      0.00
    3    7   13     -0.82      0.00
    5    7   13     -0.22      0.00
  -20    8   13     -0.24      0.00
  -18    8   13     -0.42      0.00
  -16    8   13     -0.67      0.00
  -14    8   13     -0.84      0.00
  -12    8   13     -0.82      0.00
  -10    8   13     -0.63      0.00
   -8    8   13     -0.29      0.00
   -6    8   13      0.16      0.00
   -4    8   13      0.72      0.00
   -2    8   13      1.23      0.00
    0    8   13      1.43      0.00
    2    8   13      1.13      0.00
    4    8   13      0.40      0.00
  -19    9   13     -0.45      0.00
  -17    9   13     -0.37      0.00
  -15    9   13     -0.20      0.00
  -13    9   13     -0.18      0.00
  -11    9   13     -0.38      0.00
   -9    9   13     -0.64      0.00
   -7    9   13     -0.73      0.00
   -5    9   13     -0.57      0.00
   -3    9   13     -0.29      0.00
   -1    9   13     -0.07      0.00
    1    9   13      0.04      0.00
    3    9   13      0.14      0.00
  -18   10   13      0.70      0.00
  -16   10   13      0.50      0.00
  -14   10   13      0.25      0.00
  -12   10   13      0.16      0.00
  -10   10   13      0.28      0.00
   -8   10   13      0.43      0.00
   -6   10   13      0.36      0.00
   -4   10   13     -0.05      0.00
   -2   10   13     -0.64      0.00
    0   10   13     -1.05      0.00
    2   10   13     -1.06      0.00
  -17   11   13     -0.35      0.00
  -15   11   13     -0.17      0.00
  -13   11   13      0.34      0.00
  -11   11   13      0.97      0.00
   -9   11   13      1.34      0.00
   -7   11   13      1.27      0.00
   -5   11   13      0.94      0.00
   -3   11   13      0.70      0.00
   -1   11   13      0.73      0.00
    1   11   13      0.87      0.00
  -14   12   13      0.17      0.00
  -12   12   13     -0.66      0.00
  -10   12   13     -1.69      0.00
   -8   12   13     -2.25      0.00
   -6   12   13     -1.96      0.00
   -4   12   13     -1.09      0.00
   -2   12   13     -0.25      0.00
  -11   13   13      0.02      0.00
   -9   13   13      0.59      0.00
   -7   13   13      0.90      0.00
   -5   13   13      0.73      0.00
  -22    0   14      1.46      0.00
  -20    0   14      1.01      0.00
  -18    0   14      0.52      0.00
  -16    0   14      0.31      0.00
  -14    0   14      0.59      0.00
  -12    0   14      1.27      0.00
  -10    0   14      1.99      0.00
   -8    0   14      2.37      0.00
   -6    0   14      2.25      0.00
   -4    0   14      1.77      0.00
   -2    0   14      1.20      0.00
    0    0   14      0.68      0.00
    2    0   14      0.27      0.00
    4    0   14      0.00      0.00
  -21    1   14     -1.05      0.00
  -19    1   14     -0.86      0.00
  -17    1   14     -0.59      0.00
  -15    1   14     -0.46      0.00
  -13    1   14     -0.64      0.00
  -11    1   14     -1.05      0.00
   -9    1   14     -1.43      0.00
   -7    1   14     -1.54      0.00
   -5    1   14     -1.34      0.00
   -3    1   14     -0.95      0.00
   -1    1   14     -0.56      0.00
    1    1   14     -0.25      0.00
    3    1   14     -0.03      0.00
    5    1   14      0.07      0.00
  -22    2   14      0.24      0.00
  -20    2   14      0.64      0.00
  -18    2   14      0.71      0.00
  -16    2   14      0.42      0.00
  -14    2   14     -0.05      0.00
  -12    2   14     -0.44      0.00
  -10    2   14     -0.57      0.00
   -8    2   14     -0.47      0.00
   -6    2   14     -0.25      0.00
   -4    2   14     -0.04      0.00
   -2    2   14      0.09      0.00
    0    2   14      0.12      0.00
    2    2   14      0.10      0.00
    4    2   14      0.06      0.00
  -21    3   14      0.22      0.00
  -19    3   14     -0.02      0.00
  -17    3   14      0.03      0.00
  -15    3   14      0.48      0.00
  -13    3   14      1.22      0.00
  -11    3   14      1.90      0.00
   -9    3   14      2.17      0.00
   -7    3   14      1.85      0.00
   -5    3   14      1.09      0.00
   -3    3   14      0.27      0.00
   -1    3   14     -0.31      0.00
    1    3   14     -0.53      0.00
    3    3   14     -0.49      0.00
  -20    4   14     -0.49      0.00
  -18    4   14     -0.36      0.00
  -16    4   14     -0.28      0.00
  -14    4   14     -0.50      0.00
  -12    4   14     -1.03      0.00
  -10    4   14     -1.57      0.00
   -8    4   14     -1.70      0.00
   -6    4   14     -1.25      0.00
   -4    4   14     -0.46      0.00
   -2    4   14      0.26      0.00
    0    4   14      0.64      0.00
    2    4   14      0.66      0.00
    4    4   14      0.51      0.00
  -21    5   14      0.23      0.00
  -19    5   14      0.11      0.00
  -17    5   14     -0.32      0.00
  -15    5   14     -0.80      0.00
  -13    5   14     -1.02      0.00
  -11    5   14     -0.87      0.00
   -9    5   14     -0.52      0.00
   -7    5   14     -0.18      0.00
   -5    5   14      0.02      0.00
   -3    5   14      0.12      0.00
   -1    5   14      0.16      0.00
    1    5   14      0.12      0.00
    3    5   14      0.01      0.00
  -20    6   14      0.04      0.00
  -18    6   14      0.33      0.00
  -16    6   14      0.86      0.00
  -14    6   14      1.48      0.00
  -12    6   14      1.94      0.00
  -10    6   14      2.03      0.00
   -8    6   14      1.63      0.00
   -6    6   14      0.82      0.00
   -4    6   14     -0.15      0.00
   -2    6   14     -0.92      0.00
    0    6   14     -1.18      0.00
    2    6   14     -0.92      0.00
  -19    7   14      0.37      0.00
  -17    7   14      0.33      0.00
  -15    7   14      0.05      0.00
  -13    7   14     -0.41      0.00
  -11    7   14     -0.83      0.00
   -9    7   14     -0.92      0.00
   -7    7   14     -0.52      0.00
   -5    7   14      0.20      0.00
   -3    7   14      0.89      0.00
   -1    7   14      1.19      0.00
    1    7   14      1.01      0.00
  -18    8   14     -1.03      0.00
  -16    8   14     -1.16      0.00
  -14    8   14     -1.08      0.00
  -12    8   14     -0.86      0.00
  -10    8   14     -0.69      0.00
   -8    8   14     -0.67      0.00
   -6    8   14     -0.72      0.00
   -4    8   14     -0.65      0.00
   -2    8   14     -0.39      0.00
    0    8   14     -0.06      0.00
  -15    9   14      0.70      0.00
  -13    9   14      0.62      0.00
  -11    9   14      0.53      0.00
   -9    9   14      0.47      0.00
   -7    9   14      0.40      0.00
   -5    9   14      0.18      0.00
   -3    9   14     -0.24      0.00
   -1    9   14     -0.68      0.00
  -14   10   14      0.31      0.00
  -12   10   14      0.57      0.00
  -10   10   14      0.84      0.00
   -8   10   14      0.98      0.00
   -6   10   14      0.95      0.00
   -4   10   14      0.81      0.00
   -9   11   14     -1.18      0.00
   -7   11   14     -1.30      0.00
  -19    1   15      0.11      0.00
  -17    1   15      0.30      0.00
  -15    1   15      0.07      0.00
  -13    1   15     -0.59      0.00
  -11    1   15     -1.40      0.00
   -9    1   15     -1.95      0.00
   -7    1   15     -1.99      0.00
   -5    1   15     -1.58      0.00
   -3    1   15     -1.00      0.00
   -1    1   15     -0.51      0.00
  -18    2   15      0.34      0.00
  -16    2   15      0.21      0.00
  -14    2   15      0.55      0.00
  -12    2   15      1.33      0.00
  -10    2   15      2.13      0.00
   -8    2   15      2.45      0.00
   -6    2   15      2.15      0.00
   -4    2   15      1.47      0.00
   -2    2   15      0.78      0.00
    0    2   15      0.33      0.00
  -17    3   15     -0.69      0.00
  -15    3   15     -0.34      0.00
  -13    3   15     -0.24      0.00
  -11    3   15     -0.44      0.00
   -9    3   15     -0.71      0.00
   -7    3   15     -0.78      0.00
   -5    3   15     -0.64      0.00
   -3    3   15     -0.42      0.00
   -1    3   15     -0.28      0.00
  -18    4   15      0.51      0.00
  -16    4   15      0.03      0.00
  -14    4   15     -0.67      0.00
  -12    4   15     -1.29      0.00
  -10    4   15     -1.58      0.00
   -8    4   15     -1.46      0.00
   -6    4   15     -1.00      0.00
   -4    4   15     -0.38      0.00
   -2    4   15      0.16      0.00
  -17    5   15     -0.02      0.00
  -15    5   15      0.41      0.00
  -13    5   15      1.14      0.00
  -11    5   15      1.84      0.00
   -9    5   15      2.07      0.00
   -7    5   15      1.62      0.00
   -5    5   15      0.71      0.00
   -3    5   15     -0.20      0.00
  -16    6   15      0.49      0.00
  -14    6   15      0.33      0.00
  -12    6   15     -0.07      0.00
  -10    6   15     -0.39      0.00
   -8    6   15     -0.32      0.00
   -6    6   15      0.14      0.00
   -4    6   15      0.64      0.00
  -13    7   15     -1.00      0.00
  -11    7   15     -1.08      0.00
   -9    7   15     -1.15      0.00
   -7    7   15     -1.18      0.00
   -5    7   15     -1.06      0.00
  -10    8   15      0.87      0.00
   -8    8   15      0.87      0.00
  -12    0   16     -0.49      0.00
  -10    0   16     -1.38      0.00
   -8    0   16     -1.90      0.00
  -11    1   16      0.62      0.00
   -9    1   16      1.08      0.00
    2    0    0     67.58      0.00
    1    1    0    -36.13      0.00
    0    2    0    -31.20      0.00
   25   11    0      0.34      0.00
   19   17    0      0.48      0.00
   11   21    0     -0.54      0.00
   28    2    1     -0.27      0.00
  -29    3    1      1.15      0.00
   -4    8    1      7.78      0.00
  -27    9    1     -0.06      0.00
   22   14    1     -1.60      0.00
  -18   18    1      0.24      0.00
   15   19    1      0.47      0.00
  -14   20    1     -0.76      0.00
    6   22    1     -0.46      0.00
   27    3    2      0.07      0.00
  -29    5    2      0.57      0.00
   16   18    2      0.40      0.00
   12   20    2     -0.08      0.00
    9   21    2      0.01      0.00
  -30    2    3      1.32      0.00
   26    4    3      0.41      0.00
   25    7    3      0.74      0.00
   22   12    3     -0.72      0.00
   21   13    3      0.41      0.00
   20   14    3      0.14      0.00
   19   15    3     -0.05      0.00
   13   19    3      0.78      0.00
  -11   21    3      0.16      0.00
   -6   22    3      0.07      0.00
    2   22    3      0.15      0.00
   25    3    4      0.40      0.00
   23    9    4     -0.10      0.00
  -25   13    4     -0.39      0.00
  -24   14    4      0.27      0.00
   15   17    4     -0.06      0.00
  -14   20    4     -0.47      0.00
  -11   21    4      0.68      0.00
   -4   22    4     -0.15      0.00
   -2   22    4     -0.04      0.00
   24    2    5      0.37      0.00
  -30    4    5     -0.06      0.00
  -29    7    5     -0.46      0.00
  -18   18    5      0.30      0.00
   12   18    5      0.55      0.00
   -9   21    5      0.27      0.00
    3   21    5     -0.25      0.00
   23    1    6      0.21      0.00
   19   11    6     -0.18      0.00
   15   15    6      0.17      0.00
   10   18    6      0.09      0.00
  -15   19    6     -0.13      0.00
  -12   20    6      0.27      0.00
   -5   21    6      1.57      0.00
   -3   21    6      1.54      0.00
   -1   21    6      1.10      0.00
  -30    2    7      1.12      0.00
  -28    8    7      0.25      0.00
   19    9    7     -0.82      0.00
    8   18    7     -0.53      0.00
    5   19    7      0.68      0.00
  -10   20    7      0.27      0.00
   20    0    8     -0.22      0.00
   20    2    8     -0.12      0.00
  -29    5    8     -0.06      0.00
   18    8    8     -1.58      0.00
  -27    9    8     -0.93      0.00
  -21   15    8      0.62      0.00
  -29    3    9      1.00      0.00
  -28    6    9      0.51      0.00
   16    8    9     -0.74      0.00
  -25   11    9     -1.09      0.00
  -24   12    9      0.72      0.00
    9   15    9     -0.49      0.00
  -18   16    9     -0.38      0.00
    5   17    9     -0.22      0.00
  -28    4   10     -0.57      0.00
   14    8   10     -0.40      0.00
  -20   14   10     -0.42      0.00
    8   14   10     -0.56      0.00
  -16   16   10      0.31      0.00
    4   16   10     -0.21      0.00
  -13   17   10      0.05      0.00
    1   17   10      0.44      0.00
   14    2   11     -0.07      0.00
   11    9   11      0.07      0.00
   10   10   11     -0.45      0.00
    9   11   11     -0.35      0.00
  -18   14   11     -0.58      0.00
  -12   16   11      0.65      0.00
  -26    4   12      0.21      0.00
  -23    9   12     -0.32      0.00
  -22   10   12      0.15      0.00
  -17   13   12      0.11      0.00
    0   14   12      0.00      0.00
  -11   15   12      0.80      0.00
   -9   15   12      0.52      0.00
   -5   15   12     -0.31      0.00
  -25    1   13      1.20      0.00
    9    1   13     -0.18      0.00
    8    4   13     -0.31      0.00
  -16   12   13      0.35      0.00
    0   12   13      0.13      0.00
  -23    1   14     -1.02      0.00
    5    3   14     -0.33      0.00
  -22    4   14     -0.44      0.00
  -17    9   14      0.68      0.00
   -2   10   14      0.67      0.00
  -11   11   14     -0.84      0.00
   -5   11   14     -1.03      0.00
    1    1   15     -0.21      0.00
  -19    3   15     -0.98      0.00
    0    4   15      0.44      0.00
   -1    5   15     -0.69      0.00
   -2    6   15      0.82      0.00
  -15    7   15     -0.84      0.00
   -3    7   15     -0.71      0.00
  -12    8   15      0.61      0.00
   -6    8   15      0.55      0.00
  -14    0   16      0.28      0.00
   -6    0   16     -1.85      0.00
  -13    1   16      0.12      0.00
   -7    1   16      1.26      0.00
  -12    2   16      0.13      0.00
  -10    2   16      0.33      0.00
   -8    2   16      0.35      0.00
  -11    3   16     -0.99      0.00
   -9    3   16     -1.43      0.00
    0    0    0      0.00      0.00
# SQUEEZE RESULTS (Version =  60119)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
  _platon_squeeze_void_nr
  _platon_squeeze_void_average_x
  _platon_squeeze_void_average_y
  _platon_squeeze_void_average_z
  _platon_squeeze_void_volume
  _platon_squeeze_void_count_electrons
  _platon_squeeze_void_content
   1  0.000  0.343  0.250        65        17 ' '
   2  0.500  0.843  0.250        65        17 ' '
   3  0.500  0.157  0.750        65        17 ' '
   4  0.000  0.657  0.750        65        17 ' '
# Missing Reflections Below sin(th)/lambda = 0.25
loop_
  _platon_missing_refln_index_h
  _platon_missing_refln_index_k
  _platon_missing_refln_index_l
  _platon_missing_refln_theta
    2    0    0     1.849
    1    1    0     1.491
    0    2    0     2.339
   -4    8    1    10.052
_platon_squeeze_void_probe_radius                  1.20
_platon_squeeze_details
)
TITL shelx            C 2/c        R = 0.03
CELL   23.3026   17.4118   12.3816     90.00    109.03     90.00
SPGR C2/c
# Solvent Accessible Volume =       251
# Electrons Found in S.A.V. =        66
# Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others
C101 1.000 0.344 0.245 !       3.77 eA-3
C102 0.030 0.330 0.182 !       2.26 eA-3
Q103 0.626 0.249 0.031 !       1.18 eA-3
Q104 0.353 0.346 0.452 !       1.02 eA-3
Q105 0.375 0.336 0.459 !       0.87 eA-3
Q106 0.671 0.267 0.034 !       0.73 eA-3
Q107 0.688 0.273 0.128 !       0.73 eA-3
Q108 0.164 0.314 0.297 !       0.71 eA-3
Q109 0.826 0.169 0.006 !       0.68 eA-3
Q110 0.094 0.200 0.449 !       0.66 eA-3
Q111 0.414 0.298 0.458 !       0.66 eA-3
Q112 0.914 0.798 0.458 !       0.66 eA-3
Q113 0.469 0.232 0.870 !       0.66 eA-3
Q114 0.773 0.147 0.321 !       0.64 eA-3
Q115 0.273 0.647 0.321 !       0.64 eA-3
Q116 0.052 0.482 0.236 !       0.62 eA-3
Q117 0.959 0.205 0.374 !       0.62 eA-3
Q118 0.070 0.189 0.204 !       0.60 eA-3
Q119 0.969 0.345 0.462 !       0.59 eA-3
Q120 0.007 0.096 0.529 !       0.59 eA-3
Q121 0.358 0.448 0.470 !       0.58 eA-3
Q122 0.679 0.391 0.377 !       0.58 eA-3
Q123 0.072 0.437 0.594 !       0.57 eA-3
Q124 0.072 0.121 0.196 !       0.56 eA-3
Q125 0.568 0.184 0.455 !       0.56 eA-3
Q126 0.670 0.424 0.437 !       0.56 eA-3
Q127 0.820 0.329 0.305 !       0.55 eA-3
Q128 0.711 0.466 0.374 !       0.54 eA-3
Q129 0.077 0.270 0.137 !       0.54 eA-3
Q130 0.119 0.469 0.653 !       0.53 eA-3
Q131 0.072 0.109 0.266 !       0.53 eA-3
Q132 0.127 0.170 0.335 !       0.53 eA-3
Q133 0.571 0.013 0.155 !       0.51 eA-3
Q134 0.566 0.128 0.073 !       0.51 eA-3
Q135 0.346 0.291 0.581 !       0.51 eA-3
Q136 0.357 0.423 0.187 !       0.51 eA-3
Q137 0.400 0.468 0.436 !       0.50 eA-3
Q138 0.697 0.108-0.004 !       0.50 eA-3
)
;
_shelx_fab_checksum              76018
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C10 C 0.33855(15) 0.21552(18) 0.6678(3) 0.0371(7) Uani 1 1 d . . . . .
H1 H 0.358882 0.258434 0.710844 0.045 Uiso 1 1 calc R U . . .
C9 C 0.32110(17) 0.1562(2) 0.7235(3) 0.0436(8) Uani 1 1 d . . . . .
H2 H 0.329016 0.158766 0.803716 0.052 Uiso 1 1 calc R U . . .
C8 C 0.29214(17) 0.0932(2) 0.6628(3) 0.0440(8) Uani 1 1 d . . . . .
H3 H 0.280553 0.051374 0.700465 0.053 Uiso 1 1 calc R U . . .
C7 C 0.28026(15) 0.09202(18) 0.5459(3) 0.0390(7) Uani 1 1 d . . . . .
H4 H 0.260245 0.049204 0.502123 0.047 Uiso 1 1 calc R U . . .
C6 C 0.29766(14) 0.15347(16) 0.4931(2) 0.0302(6) Uani 1 1 d . . . . .
C5 C 0.28235(14) 0.16057(16) 0.3689(2) 0.0299(6) Uani 1 1 d . . . . .
C4 C 0.24845(16) 0.10682(18) 0.2915(3) 0.0419(8) Uani 1 1 d . . . . .
H7 H 0.235817 0.060687 0.318020 0.050 Uiso 1 1 calc R U . . .
C3 C 0.23323(17) 0.12072(19) 0.1762(3) 0.0468(9) Uani 1 1 d . . . . .
H8 H 0.210541 0.084120 0.122206 0.056 Uiso 1 1 calc R U . . .
C2 C 0.25147(16) 0.18858(18) 0.1405(3) 0.0401(8) Uani 1 1 d . . . . .
H9 H 0.240716 0.199734 0.061300 0.048 Uiso 1 1 calc R U . . .
C1 C 0.28532(15) 0.24018(18) 0.2201(2) 0.0342(7) Uani 1 1 d . . . . .
H10 H 0.297367 0.287031 0.194473 0.041 Uiso 1 1 calc R U . . .
C11 C 0.40631(18) 0.43419(18) 0.5998(3) 0.0450(8) Uani 1 1 d . . . . .
H11A H 0.445120 0.459013 0.643742 0.054 Uiso 0.540(12) 1 calc R U P A 1
H11B H 0.376519 0.444768 0.639487 0.054 Uiso 0.540(12) 1 calc R U P A 1
H11C H 0.430313 0.455272 0.675254 0.054 Uiso 0.460(12) 1 calc R U P A 2
H11D H 0.362906 0.445960 0.585656 0.054 Uiso 0.460(12) 1 calc R U P A 2
C12A C 0.3828(4) 0.4694(3) 0.4767(6) 0.039(2) Uani 0.540(12) 1 d . . P A 1
H12A H 0.339340 0.456710 0.440300 0.047 Uiso 0.540(12) 1 calc R U P A 1
H12B H 0.386787 0.526038 0.481394 0.047 Uiso 0.540(12) 1 calc R U P A 1
C13A C 0.4187(4) 0.4382(4) 0.4061(6) 0.0355(18) Uani 0.540(12) 1 d D . P A 1
H13A H 0.461553 0.430349 0.453786 0.043 Uiso 0.540(12) 1 calc R U P A 1
H13B H 0.417475 0.474141 0.343462 0.043 Uiso 0.540(12) 1 calc R U P A 1
C12B C 0.4274(5) 0.4684(4) 0.5063(7) 0.044(3) Uani 0.460(12) 1 d . . P A 2
H12C H 0.429891 0.524974 0.514420 0.052 Uiso 0.460(12) 1 calc R U P A 2
H12D H 0.468386 0.448757 0.513747 0.052 Uiso 0.460(12) 1 calc R U P A 2
C13B C 0.3839(5) 0.4475(4) 0.3909(7) 0.040(2) Uani 0.460(12) 1 d D . P A 2
H13C H 0.391567 0.481127 0.332529 0.048 Uiso 0.460(12) 1 calc R U P A 2
H13D H 0.341923 0.457312 0.390169 0.048 Uiso 0.460(12) 1 calc R U P A 2
C14 C 0.44252(18) 0.3288(2) 0.3306(3) 0.0552(10) Uani 1 1 d . . . . .
H14A H 0.473509 0.312138 0.402591 0.066 Uiso 1 1 calc R U . . .
H14B H 0.460795 0.369580 0.296618 0.066 Uiso 1 1 calc R U . . .
C15 C 0.42641(16) 0.2617(2) 0.2497(3) 0.0480(9) Uani 1 1 d . . . . .
C16 C 0.40732(18) 0.2765(3) 0.1341(3) 0.0564(10) Uani 1 1 d . . . . .
H16 H 0.406096 0.328171 0.108767 0.068 Uiso 1 1 calc R U . . .
C17 C 0.3898(2) 0.2182(3) 0.0537(4) 0.0650(12) Uani 1 1 d . . . . .
H17 H 0.378056 0.230665 -0.025188 0.078 Uiso 1 1 calc R U . . .
C18 C 0.3892(2) 0.1446(3) 0.0853(4) 0.0739(13) Uani 1 1 d . . . . .
H18 H 0.375148 0.105752 0.028938 0.089 Uiso 1 1 calc R U . . .
C19 C 0.40965(19) 0.1246(3) 0.2030(4) 0.0641(11) Uani 1 1 d . . . . .
C20 C 0.4100(2) 0.0481(3) 0.2408(5) 0.0859(15) Uani 1 1 d . . . . .
H20 H 0.396704 0.008217 0.186017 0.103 Uiso 1 1 calc R U . . .
C21 C 0.4286(3) 0.0306(3) 0.3519(6) 0.0929(17) Uani 1 1 d . . . . .
H21 H 0.428311 -0.021540 0.374386 0.111 Uiso 1 1 calc R U . . .
C22 C 0.4486(2) 0.0874(3) 0.4359(4) 0.0804(15) Uani 1 1 d . . . . .
H22 H 0.461378 0.073734 0.514475 0.096 Uiso 1 1 calc R U . . .
C23 C 0.44963(19) 0.1628(3) 0.4046(4) 0.0627(11) Uani 1 1 d . . . . .
H23 H 0.464447 0.201091 0.461609 0.075 Uiso 1 1 calc R U . . .
C24 C 0.42869(17) 0.1841(2) 0.2873(3) 0.0518(9) Uani 1 1 d . . . . .
N2 N 0.32776(11) 0.21474(13) 0.5542(2) 0.0290(5) Uani 1 1 d . . . . .
N1 N 0.30182(12) 0.22636(13) 0.3325(2) 0.0293(5) Uani 1 1 d . . . . .
N3 N 0.41566(12) 0.34979(13) 0.5964(2) 0.0333(6) Uani 1 1 d . . . . .
H3NA H 0.412702 0.329117 0.661843 0.040 Uiso 1 1 calc R U . . .
H3NB H 0.454234 0.341469 0.596475 0.040 Uiso 1 1 calc R U . . .
N4 N 0.38924(14) 0.36164(14) 0.3578(2) 0.0408(7) Uani 1 1 d D . . . .
H4NA H 0.355537 0.371420 0.284763 0.049 Uiso 0.540(12) 1 calc R U P A 1
H4NB H 0.356063 0.357512 0.282595 0.049 Uiso 0.460(12) 1 calc R U P A 2
Cl1 Cl 0.44095(4) 0.34155(6) 0.86913(7) 0.0486(2) Uani 1 1 d . . . . .
Cl2 Cl 0.29123(5) 0.42526(5) 0.12562(7) 0.0527(2) Uani 1 1 d . . . . .
Pt1 Pt 0.35756(2) 0.29134(2) 0.46093(2) 0.02673(4) Uani 1 1 d . . . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
C10 0.0394(19) 0.0445(18) 0.0281(17) -0.0039(12) 0.0118(13) -0.0044(15)
C9 0.050(2) 0.053(2) 0.0296(18) 0.0046(14) 0.0147(14) -0.0030(17)
C8 0.051(2) 0.0466(19) 0.0357(19) 0.0074(14) 0.0167(15) -0.0088(16)
C7 0.042(2) 0.0344(16) 0.0395(18) 0.0022(13) 0.0124(14) -0.0080(14)
C6 0.0296(16) 0.0307(14) 0.0276(15) 0.0005(11) 0.0057(11) 0.0003(12)
C5 0.0321(17) 0.0274(14) 0.0296(16) 0.0010(11) 0.0092(12) -0.0004(12)
C4 0.053(2) 0.0341(17) 0.0367(18) -0.0010(13) 0.0122(15) -0.0131(15)
C3 0.059(2) 0.0403(18) 0.0341(18) -0.0088(14) 0.0049(15) -0.0152(17)
C2 0.047(2) 0.0412(18) 0.0254(16) 0.0005(12) 0.0031(13) -0.0069(15)
C1 0.0382(19) 0.0337(15) 0.0282(16) 0.0026(12) 0.0072(13) -0.0035(14)
C11 0.059(2) 0.0337(17) 0.0405(19) -0.0115(13) 0.0138(16) -0.0053(16)
C12A 0.046(5) 0.026(3) 0.044(4) -0.002(2) 0.011(3) 0.003(3)
C13A 0.035(4) 0.033(3) 0.039(4) -0.005(2) 0.012(3) -0.010(3)
C12B 0.046(7) 0.028(4) 0.050(5) -0.001(3) 0.005(4) -0.012(4)
C13B 0.044(6) 0.029(4) 0.039(5) 0.001(3) 0.005(4) -0.014(4)
C14 0.045(2) 0.075(3) 0.043(2) 0.0082(18) 0.0109(17) -0.024(2)
C15 0.0298(19) 0.070(2) 0.046(2) 0.0042(17) 0.0149(15) -0.0024(17)
C16 0.046(2) 0.085(3) 0.040(2) 0.0068(19) 0.0164(16) -0.007(2)
C17 0.061(3) 0.085(3) 0.052(3) 0.001(2) 0.021(2) -0.001(2)
C18 0.061(3) 0.104(4) 0.060(3) -0.015(3) 0.023(2) -0.001(3)
C19 0.043(2) 0.075(3) 0.079(3) -0.001(2) 0.025(2) 0.006(2)
C20 0.074(4) 0.072(3) 0.111(4) 0.004(3) 0.030(3) 0.009(3)
C21 0.079(4) 0.075(4) 0.123(5) 0.026(3) 0.030(3) 0.017(3)
C22 0.063(3) 0.099(4) 0.075(3) 0.034(3) 0.018(2) 0.027(3)
C23 0.045(2) 0.080(3) 0.066(3) 0.022(2) 0.022(2) 0.018(2)
C24 0.031(2) 0.072(3) 0.057(2) 0.0111(19) 0.0188(16) 0.0083(18)
N2 0.0298(14) 0.0306(12) 0.0273(13) 0.0000(9) 0.0102(10) 0.0000(10)
N1 0.0326(14) 0.0263(12) 0.0258(13) -0.0008(9) 0.0050(10) -0.0017(10)
N3 0.0352(15) 0.0343(13) 0.0269(13) -0.0022(10) 0.0054(10) -0.0032(11)
N4 0.063(2) 0.0304(13) 0.0257(13) -0.0003(10) 0.0099(12) -0.0144(13)
Cl1 0.0425(5) 0.0668(6) 0.0340(4) -0.0057(4) 0.0088(3) -0.0076(4)
Cl2 0.0834(7) 0.0331(4) 0.0413(5) 0.0058(3) 0.0199(4) 0.0091(4)
Pt1 0.03043(7) 0.02382(6) 0.02318(7) -0.00032(4) 0.00498(4) -0.00208(5)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N2 C10 C9 122.1(3)
N2 C10 H1 118.9
C9 C10 H1 118.9
C10 C9 C8 119.8(3)
C10 C9 H2 120.1
C8 C9 H2 120.1
C9 C8 C7 118.6(3)
C9 C8 H3 120.7
C7 C8 H3 120.7
C6 C7 C8 119.6(3)
C6 C7 H4 120.2
C8 C7 H4 120.2
N2 C6 C7 121.4(3)
N2 C6 C5 114.9(3)
C7 C6 C5 123.6(3)
N1 C5 C4 121.0(3)
N1 C5 C6 115.1(2)
C4 C5 C6 123.8(3)
C3 C4 C5 119.6(3)
C3 C4 H7 120.2
C5 C4 H7 120.2
C4 C3 C2 118.8(3)
C4 C3 H8 120.6
C2 C3 H8 120.6
C1 C2 C3 119.7(3)
C1 C2 H9 120.1
C3 C2 H9 120.1
N1 C1 C2 122.0(3)
N1 C1 H10 119.0
C2 C1 H10 119.0
N3 C11 C12B 106.2(4)
N3 C11 C12A 111.5(3)
N3 C11 H11A 109.3
C12A C11 H11A 109.3
N3 C11 H11B 109.3
C12A C11 H11B 109.3
H11A C11 H11B 108.0
N3 C11 H11C 110.5
C12B C11 H11C 110.5
N3 C11 H11D 110.5
C12B C11 H11D 110.5
H11C C11 H11D 108.7
C13A C12A C11 110.0(7)
C13A C12A H12A 109.7
C11 C12A H12A 109.7
C13A C12A H12B 109.7
C11 C12A H12B 109.7
H12A C12A H12B 108.2
C12A C13A N4 106.3(6)
C12A C13A H13A 110.5
N4 C13A H13A 110.5
C12A C13A H13B 110.5
N4 C13A H13B 110.5
H13A C13A H13B 108.7
C13B C12B C11 110.1(8)
C13B C12B H12C 109.6
C11 C12B H12C 109.6
C13B C12B H12D 109.6
C11 C12B H12D 109.6
H12C C12B H12D 108.1
C12B C13B N4 113.1(7)
C12B C13B H13C 108.9
N4 C13B H13C 108.9
C12B C13B H13D 108.9
N4 C13B H13D 108.9
H13C C13B H13D 107.8
N4 C14 C15 113.6(3)
N4 C14 H14A 108.9
C15 C14 H14A 108.9
N4 C14 H14B 108.9
C15 C14 H14B 108.9
H14A C14 H14B 107.7
C16 C15 C24 118.8(4)
C16 C15 C14 118.2(4)
C24 C15 C14 123.0(3)
C15 C16 C17 121.9(4)
C15 C16 H16 119.0
C17 C16 H16 119.0
C18 C17 C16 121.3(4)
C18 C17 H17 119.4
C16 C17 H17 119.4
C17 C18 C19 120.0(5)
C17 C18 H18 120.0
C19 C18 H18 120.0
C20 C19 C18 122.3(5)
C20 C19 C24 118.3(5)
C18 C19 C24 119.4(4)
C21 C20 C19 121.5(6)
C21 C20 H20 119.2
C19 C20 H20 119.2
C20 C21 C22 121.4(5)
C20 C21 H21 119.3
C22 C21 H21 119.3
C23 C22 C21 119.9(5)
C23 C22 H22 120.1
C21 C22 H22 120.1
C22 C23 C24 120.4(5)
C22 C23 H23 119.8
C24 C23 H23 119.8
C23 C24 C15 123.0(4)
C23 C24 C19 118.4(4)
C15 C24 C19 118.5(4)
C10 N2 C6 118.4(3)
C10 N2 Pt1 127.3(2)
C6 N2 Pt1 114.10(19)
C1 N1 C5 118.8(2)
C1 N1 Pt1 127.3(2)
C5 N1 Pt1 113.93(18)
C11 N3 Pt1 116.7(2)
C11 N3 H3NA 108.1
Pt1 N3 H3NA 108.1
C11 N3 H3NB 108.1
Pt1 N3 H3NB 108.1
H3NA N3 H3NB 107.3
C14 N4 C13A 97.0(4)
C14 N4 C13B 124.4(5)
C14 N4 Pt1 113.6(2)
C13A N4 Pt1 118.6(3)
C13B N4 Pt1 109.2(4)
C14 N4 H4NA 109.0
C13A N4 H4NA 109.0
Pt1 N4 H4NA 109.0
C14 N4 H4NB 102.0
C13B N4 H4NB 102.0
Pt1 N4 H4NB 102.0
N2 Pt1 N1 80.20(10)
N2 Pt1 N3 96.77(10)
N1 Pt1 N3 176.01(9)
N2 Pt1 N4 175.11(10)
N1 Pt1 N4 96.41(10)
N3 Pt1 N4 86.44(10)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
C10 N2 1.345(4)
C10 C9 1.375(4)
C10 H1 0.9500
C9 C8 1.376(5)
C9 H2 0.9500
C8 C7 1.382(5)
C8 H3 0.9500
C7 C6 1.382(4)
C7 H4 0.9500
C6 N2 1.362(4)
C6 C5 1.467(4)
C5 N1 1.362(4)
C5 C4 1.387(4)
C4 C3 1.375(5)
C4 H7 0.9500
C3 C2 1.376(5)
C3 H8 0.9500
C2 C1 1.376(4)
C2 H9 0.9500
C1 N1 1.340(4)
C1 H10 0.9500
C11 N3 1.488(4)
C11 C12B 1.519(9)
C11 C12A 1.567(8)
C11 H11A 0.9900
C11 H11B 0.9900
C11 H11C 0.9900
C11 H11D 0.9900
C12A C13A 1.495(12)
C12A H12A 0.9900
C12A H12B 0.9900
C13A N4 1.529(6)
C13A H13A 0.9900
C13A H13B 0.9900
C12B C13B 1.503(13)
C12B H12C 0.9900
C12B H12D 0.9900
C13B N4 1.566(7)
C13B H13C 0.9900
C13B H13D 0.9900
C14 N4 1.502(5)
C14 C15 1.504(6)
C14 H14A 0.9900
C14 H14B 0.9900
C15 C16 1.377(5)
C15 C24 1.424(6)
C16 C17 1.386(6)
C16 H16 0.9500
C17 C18 1.342(6)
C17 H17 0.9500
C18 C19 1.421(6)
C18 H18 0.9500
C19 C20 1.410(7)
C19 C24 1.434(6)
C20 C21 1.336(8)
C20 H20 0.9500
C21 C22 1.401(8)
C21 H21 0.9500
C22 C23 1.372(6)
C22 H22 0.9500
C23 C24 1.422(5)
C23 H23 0.9500
N2 Pt1 2.030(2)
N1 Pt1 2.037(2)
N3 Pt1 2.049(2)
N3 H3NA 0.9100
N3 H3NB 0.9100
N4 Pt1 2.071(3)
N4 H4NA 1.0000
N4 H4NB 1.0000
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
N2 C10 C9 C8 0.7(6)
C10 C9 C8 C7 -1.3(6)
C9 C8 C7 C6 0.1(6)
C8 C7 C6 N2 1.6(5)
C8 C7 C6 C5 -174.4(3)
N2 C6 C5 N1 1.7(4)
C7 C6 C5 N1 178.0(3)
N2 C6 C5 C4 -175.7(3)
C7 C6 C5 C4 0.6(5)
N1 C5 C4 C3 -1.2(5)
C6 C5 C4 C3 176.0(3)
C5 C4 C3 C2 -0.9(6)
C4 C3 C2 C1 1.3(6)
C3 C2 C1 N1 0.5(6)
N3 C11 C12A C13A -45.2(7)
C11 C12A C13A N4 84.5(8)
N3 C11 C12B C13B 70.4(8)
C11 C12B C13B N4 -74.0(11)
N4 C14 C15 C16 87.3(4)
N4 C14 C15 C24 -91.2(4)
C24 C15 C16 C17 0.6(6)
C14 C15 C16 C17 -178.0(4)
C15 C16 C17 C18 1.8(7)
C16 C17 C18 C19 -3.2(7)
C17 C18 C19 C20 -180.0(5)
C17 C18 C19 C24 2.3(7)
C18 C19 C20 C21 -179.1(5)
C24 C19 C20 C21 -1.3(7)
C19 C20 C21 C22 0.1(9)
C20 C21 C22 C23 -0.4(8)
C21 C22 C23 C24 2.1(7)
C22 C23 C24 C15 177.4(4)
C22 C23 C24 C19 -3.3(6)
C16 C15 C24 C23 177.9(4)
C14 C15 C24 C23 -3.6(6)
C16 C15 C24 C19 -1.4(5)
C14 C15 C24 C19 177.1(4)
C20 C19 C24 C23 2.9(6)
C18 C19 C24 C23 -179.3(4)
C20 C19 C24 C15 -177.8(4)
C18 C19 C24 C15 0.0(6)
C9 C10 N2 C6 1.1(5)
C9 C10 N2 Pt1 -173.3(3)
C7 C6 N2 C10 -2.2(5)
C5 C6 N2 C10 174.1(3)
C7 C6 N2 Pt1 172.8(2)
C5 C6 N2 Pt1 -10.8(3)
C2 C1 N1 C5 -2.7(5)
C2 C1 N1 Pt1 174.3(3)
C4 C5 N1 C1 3.0(5)
C6 C5 N1 C1 -174.5(3)
C4 C5 N1 Pt1 -174.3(3)
C6 C5 N1 Pt1 8.2(3)
C12B C11 N3 Pt1 -72.2(5)
C12A C11 N3 Pt1 -33.3(5)
C15 C14 N4 C13A -163.3(4)
C15 C14 N4 C13B -151.6(5)
C15 C14 N4 Pt1 71.3(3)
C12A C13A N4 C14 -160.2(6)
C12A C13A N4 Pt1 -38.5(8)
C12B C13B N4 C14 -69.4(9)
C12B C13B N4 Pt1 69.3(9)
loop_
_cod_related_entry_id
_cod_related_entry_database
_cod_related_entry_code
1 PubChem 168302931
