#------------------------------------------------------------------------------
#$Date: 2021-02-25 11:40:25 +0200 (Thu, 25 Feb 2021) $
#$Revision: 262223 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/06/1560640.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1560640
loop_
_publ_author_name
'Ding, Ling'
'Zhong, Jie-Cen'
'Qiu, Xing-Tai'
'Sun, Yan-Qiong'
'Chen, Yi-Ping'
_publ_section_title
;
 Syntheses, structures, photoluminescence and photocatalysis of 2D layered
 lanthanide-carboxylates with 2, 2′-dithiodibenzoic acid
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              138
_journal_page_last               144
_journal_paper_doi               10.1016/j.jssc.2016.11.002
_journal_volume                  246
_journal_year                    2017
_chemical_formula_sum            'C30 H23 Dy O9 S4'
_chemical_formula_weight         818.22
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                91.025(15)
_cell_angle_beta                 99.644(19)
_cell_angle_gamma                109.028(17)
_cell_formula_units_Z            2
_cell_length_a                   9.086(4)
_cell_length_b                   11.517(4)
_cell_length_c                   15.755(7)
_cell_measurement_reflns_used    3.11
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      6957
_cell_measurement_theta_min      27.48
_cell_volume                     1531.9(11)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0177
_diffrn_reflns_av_sigmaI/netI    0.0229
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            15152
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.11
_exptl_absorpt_coefficient_mu    2.765
_exptl_absorpt_correction_T_max  0.9
_exptl_absorpt_correction_T_min  0.811
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.774
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             810
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.18
_refine_diff_density_max         0.796
_refine_diff_density_min         -0.792
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.158
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     402
_refine_ls_number_reflns         6957
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.158
_refine_ls_R_factor_all          0.0209
_refine_ls_R_factor_gt           0.0190
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0118P)²+2.7055P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0450
_refine_ls_wR_factor_ref         0.0524
_reflns_number_gt                6609
_reflns_number_total             6957
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2017-246-138.cif
_cod_data_source_block           1b
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the built-in table derived from the
CIF Core dictionary named 'cif_core.dic' version 2.4.5 last updated
on 2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_cell_volume        1532.0(11)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               1560640
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.203421(13) 0.481976(10) 0.505684(8) 0.01370(4) Uani 1 1 d . . .
S1 S 0.67021(9) 0.64226(7) 0.25428(5) 0.02961(16) Uani 1 1 d . . .
S2 S 0.74391(9) 0.72281(7) 0.14778(5) 0.02858(15) Uani 1 1 d . . .
S3 S 0.06763(9) 0.07306(6) 0.61449(5) 0.02753(15) Uani 1 1 d . . .
S4 S 0.01626(10) -0.11355(6) 0.61856(5) 0.03148(17) Uani 1 1 d . . .
O1 O 0.4233(2) 0.66715(18) 0.49913(15) 0.0288(5) Uani 1 1 d D . .
H1 H 0.501(2) 0.650(2) 0.486(2) 0.043 Uiso 1 1 d D . .
O2 O 0.3318(2) 0.4395(2) 0.40317(13) 0.0291(5) Uani 1 1 d . . .
O3 O 0.5817(2) 0.55013(17) 0.40130(12) 0.0199(4) Uani 1 1 d . . .
O4 O 0.8947(3) 0.8827(2) 0.04244(17) 0.0425(6) Uani 1 1 d . . .
O5 O 1.1368(4) 0.9115(3) 0.0185(3) 0.0700(10) Uani 1 1 d . . .
H5 H 1.1332 0.9800 0.0078 0.105 Uiso 1 1 calc R . .
O6 O 0.0995(2) 0.29936(17) 0.57131(13) 0.0234(4) Uani 1 1 d . . .
O7 O -0.0769(2) 0.39266(17) 0.56041(13) 0.0254(4) Uani 1 1 d . . .
O8 O 0.2159(2) -0.39841(17) 0.62711(13) 0.0232(4) Uani 1 1 d . . .
O9 O -0.0084(2) -0.35320(17) 0.60418(13) 0.0230(4) Uani 1 1 d . . .
C1 C 0.4755(4) 0.7902(3) 0.5401(3) 0.0414(8) Uani 1 1 d D . .
H1A H 0.5157 0.7887 0.6010 0.050 Uiso 1 1 calc R . .
H1B H 0.3861 0.8197 0.5353 0.050 Uiso 1 1 calc R . .
C2 C 0.6021(5) 0.8765(4) 0.4999(3) 0.0586(11) Uani 1 1 d . . .
H2A H 0.5610 0.8813 0.4403 0.088 Uiso 1 1 calc R . .
H2B H 0.6901 0.8469 0.5038 0.088 Uiso 1 1 calc R . .
H2C H 0.6366 0.9569 0.5298 0.088 Uiso 1 1 calc R . .
C3 C 0.4468(3) 0.4783(2) 0.36508(17) 0.0181(5) Uani 1 1 d . . .
C4 C 0.4202(3) 0.4367(2) 0.27177(17) 0.0211(5) Uani 1 1 d . . .
C5 C 0.2954(4) 0.3296(3) 0.2410(2) 0.0307(7) Uani 1 1 d . . .
H5A H 0.2287 0.2894 0.2779 0.037 Uiso 1 1 calc R . .
C6 C 0.2684(4) 0.2817(3) 0.1569(2) 0.0393(8) Uani 1 1 d . . .
H6 H 0.1867 0.2081 0.1378 0.047 Uiso 1 1 calc R . .
C7 C 0.3637(4) 0.3440(3) 0.1009(2) 0.0359(7) Uani 1 1 d . . .
H7 H 0.3456 0.3124 0.0439 0.043 Uiso 1 1 calc R . .
C8 C 0.4856(4) 0.4531(3) 0.12938(18) 0.0291(6) Uani 1 1 d . . .
H8 H 0.5484 0.4947 0.0912 0.035 Uiso 1 1 calc R . .
C9 C 0.5155(3) 0.5012(2) 0.21475(17) 0.0213(5) Uani 1 1 d . . .
C10 C 0.8990(4) 0.6663(3) 0.1307(2) 0.0303(6) Uani 1 1 d . . .
C11 C 0.9112(5) 0.5589(3) 0.1651(3) 0.0462(9) Uani 1 1 d . . .
H11 H 0.8391 0.5164 0.1987 0.055 Uiso 1 1 calc R . .
C12 C 1.0286(6) 0.5146(4) 0.1501(4) 0.0655(13) Uani 1 1 d . . .
H12 H 1.0347 0.4423 0.1732 0.079 Uiso 1 1 calc R . .
C13 C 1.1363(6) 0.5760(5) 0.1014(4) 0.0725(15) Uani 1 1 d . . .
H13 H 1.2145 0.5448 0.0910 0.087 Uiso 1 1 calc R . .
C14 C 1.1294(5) 0.6834(4) 0.0679(3) 0.0585(11) Uani 1 1 d . . .
H14 H 1.2044 0.7253 0.0356 0.070 Uiso 1 1 calc R . .
C15 C 1.0115(4) 0.7311(3) 0.0815(2) 0.0374(7) Uani 1 1 d . . .
C16 C 1.0066(4) 0.8472(3) 0.0462(2) 0.0382(8) Uani 1 1 d . . .
C17 C -0.0277(3) 0.3065(2) 0.58776(17) 0.0185(5) Uani 1 1 d . . .
C18 C -0.1173(3) 0.2150(2) 0.64150(18) 0.0208(5) Uani 1 1 d . . .
C19 C -0.2373(4) 0.2371(3) 0.6759(2) 0.0343(7) Uani 1 1 d . . .
H19 H -0.2603 0.3087 0.6639 0.041 Uiso 1 1 calc R . .
C20 C -0.3239(4) 0.1558(4) 0.7274(3) 0.0482(9) Uani 1 1 d . . .
H20 H -0.4052 0.1716 0.7491 0.058 Uiso 1 1 calc R . .
C21 C -0.2872(5) 0.0511(4) 0.7458(3) 0.0462(9) Uani 1 1 d . . .
H21 H -0.3442 -0.0040 0.7806 0.055 Uiso 1 1 calc R . .
C22 C -0.1678(4) 0.0263(3) 0.7139(2) 0.0366(7) Uani 1 1 d . . .
H22 H -0.1447 -0.0448 0.7277 0.044 Uiso 1 1 calc R . .
C23 C -0.0807(3) 0.1067(2) 0.66081(18) 0.0220(5) Uani 1 1 d . . .
C24 C 0.1494(3) -0.1297(2) 0.71117(18) 0.0230(6) Uani 1 1 d . . .
C25 C 0.2115(4) -0.0397(3) 0.7798(2) 0.0346(7) Uani 1 1 d . . .
H25 H 0.1789 0.0289 0.7794 0.042 Uiso 1 1 calc R . .
C26 C 0.3207(4) -0.0510(3) 0.8481(2) 0.0397(8) Uani 1 1 d . . .
H26 H 0.3591 0.0090 0.8942 0.048 Uiso 1 1 calc R . .
C27 C 0.3743(4) -0.1514(3) 0.8489(2) 0.0378(8) Uani 1 1 d . . .
H27 H 0.4498 -0.1582 0.8945 0.045 Uiso 1 1 calc R . .
C28 C 0.3134(4) -0.2404(3) 0.7809(2) 0.0284(6) Uani 1 1 d . . .
H28 H 0.3499 -0.3070 0.7806 0.034 Uiso 1 1 calc R . .
C29 C 0.1986(3) -0.2333(2) 0.71259(17) 0.0198(5) Uani 1 1 d . . .
C30 C 0.1309(3) -0.3361(2) 0.64269(17) 0.0174(5) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Dy1 O7 103.03(8) . 2_566
O2 Dy1 O8 147.56(7) . 1_565
O7 Dy1 O8 82.42(7) 2_566 1_565
O2 Dy1 O6 107.47(8) . .
O7 Dy1 O6 129.42(7) 2_566 .
O8 Dy1 O6 92.07(8) 1_565 .
O2 Dy1 O9 73.28(8) . 2_556
O7 Dy1 O9 75.40(7) 2_566 2_556
O8 Dy1 O9 137.94(7) 1_565 2_556
O6 Dy1 O9 76.04(8) . 2_556
O2 Dy1 O3 81.61(8) . 2_666
O7 Dy1 O3 151.91(7) 2_566 2_666
O8 Dy1 O3 79.71(7) 1_565 2_666
O6 Dy1 O3 72.96(7) . 2_666
O9 Dy1 O3 131.53(7) 2_556 2_666
O2 Dy1 O1 73.30(8) . .
O7 Dy1 O1 78.33(8) 2_566 .
O8 Dy1 O1 76.69(8) 1_565 .
O6 Dy1 O1 148.97(7) . .
O9 Dy1 O1 130.90(8) 2_556 .
O3 Dy1 O1 76.58(7) 2_666 .
O2 Dy1 O7 140.39(7) . .
O7 Dy1 O7 80.35(7) 2_566 .
O8 Dy1 O7 71.90(7) 1_565 .
O6 Dy1 O7 50.68(6) . .
O9 Dy1 O7 69.47(7) 2_556 .
O3 Dy1 O7 113.90(7) 2_666 .
O1 Dy1 O7 143.92(7) . .
O2 Dy1 Dy1 132.86(6) . 2_566
O7 Dy1 Dy1 44.27(5) 2_566 2_566
O8 Dy1 Dy1 72.62(5) 1_565 2_566
O6 Dy1 Dy1 86.02(5) . 2_566
O9 Dy1 Dy1 66.49(5) 2_556 2_566
O3 Dy1 Dy1 144.47(5) 2_666 2_566
O1 Dy1 Dy1 116.83(6) . 2_566
O7 Dy1 Dy1 36.07(4) . 2_566
C9 S1 S2 105.76(10) . .
C10 S2 S1 104.58(11) . .
C23 S3 S4 105.01(9) . .
C24 S4 S3 104.33(10) . .
C1 O1 Dy1 134.00(19) . .
C1 O1 H1 110.7(17) . .
Dy1 O1 H1 110.9(18) . .
C3 O2 Dy1 146.39(19) . .
C3 O3 Dy1 132.80(17) . 2_666
C16 O5 H5 109.5 . .
C17 O6 Dy1 103.15(15) . .
C17 O7 Dy1 168.87(18) . 2_566
C17 O7 Dy1 85.39(16) . .
Dy1 O7 Dy1 99.65(7) 2_566 .
C30 O8 Dy1 130.94(17) . 1_545
C30 O9 Dy1 140.85(17) . 2_556
O1 C1 C2 111.6(3) . .
O1 C1 H1A 109.3 . .
C2 C1 H1A 109.3 . .
O1 C1 H1B 109.3 . .
C2 C1 H1B 109.3 . .
H1A C1 H1B 108.0 . .
C1 C2 H2A 109.5 . .
C1 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C1 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
O2 C3 O3 123.6(2) . .
O2 C3 C4 117.2(2) . .
O3 C3 C4 119.3(2) . .
C5 C4 C9 119.3(3) . .
C5 C4 C3 117.9(2) . .
C9 C4 C3 122.8(2) . .
C6 C5 C4 121.3(3) . .
C6 C5 H5A 119.3 . .
C4 C5 H5A 119.3 . .
C5 C6 C7 119.5(3) . .
C5 C6 H6 120.3 . .
C7 C6 H6 120.3 . .
C8 C7 C6 120.2(3) . .
C8 C7 H7 119.9 . .
C6 C7 H7 119.9 . .
C7 C8 C9 120.7(3) . .
C7 C8 H8 119.6 . .
C9 C8 H8 119.6 . .
C8 C9 C4 118.9(3) . .
C8 C9 S1 122.4(2) . .
C4 C9 S1 118.7(2) . .
C11 C10 C15 118.9(3) . .
C11 C10 S2 121.2(3) . .
C15 C10 S2 120.0(3) . .
C12 C11 C10 120.8(4) . .
C12 C11 H11 119.6 . .
C10 C11 H11 119.6 . .
C13 C12 C11 120.6(4) . .
C13 C12 H12 119.7 . .
C11 C12 H12 119.7 . .
C12 C13 C14 120.2(4) . .
C12 C13 H13 119.9 . .
C14 C13 H13 119.9 . .
C13 C14 C15 121.0(4) . .
C13 C14 H14 119.5 . .
C15 C14 H14 119.5 . .
C14 C15 C10 118.7(3) . .
C14 C15 C16 120.5(3) . .
C10 C15 C16 120.9(3) . .
O4 C16 O5 122.0(3) . .
O4 C16 C15 123.8(3) . .
O5 C16 C15 114.3(3) . .
O6 C17 O7 120.4(2) . .
O6 C17 C18 119.0(2) . .
O7 C17 C18 120.6(2) . .
C19 C18 C23 118.9(3) . .
C19 C18 C17 119.3(3) . .
C23 C18 C17 121.8(2) . .
C20 C19 C18 122.0(3) . .
C20 C19 H19 119.0 . .
C18 C19 H19 119.0 . .
C21 C20 C19 118.5(3) . .
C21 C20 H20 120.7 . .
C19 C20 H20 120.7 . .
C20 C21 C22 121.4(3) . .
C20 C21 H21 119.3 . .
C22 C21 H21 119.3 . .
C21 C22 C23 120.7(3) . .
C21 C22 H22 119.6 . .
C23 C22 H22 119.6 . .
C22 C23 C18 118.4(3) . .
C22 C23 S3 121.6(2) . .
C18 C23 S3 119.9(2) . .
C25 C24 C29 119.2(3) . .
C25 C24 S4 121.8(2) . .
C29 C24 S4 118.9(2) . .
C26 C25 C24 120.7(3) . .
C26 C25 H25 119.6 . .
C24 C25 H25 119.6 . .
C25 C26 C27 120.6(3) . .
C25 C26 H26 119.7 . .
C27 C26 H26 119.7 . .
C28 C27 C26 118.7(3) . .
C28 C27 H27 120.6 . .
C26 C27 H27 120.6 . .
C27 C28 C29 121.7(3) . .
C27 C28 H28 119.1 . .
C29 C28 H28 119.1 . .
C28 C29 C24 119.0(2) . .
C28 C29 C30 119.2(2) . .
C24 C29 C30 121.8(2) . .
O9 C30 O8 125.3(2) . .
O9 C30 C29 116.4(2) . .
O8 C30 C29 118.3(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O2 2.277(2) .
Dy1 O7 2.286(2) 2_566
Dy1 O8 2.303(2) 1_565
Dy1 O6 2.3440(19) .
Dy1 O9 2.346(2) 2_556
Dy1 O3 2.373(2) 2_666
Dy1 O1 2.419(2) .
Dy1 O7 2.710(2) .
Dy1 Dy1 3.8278(17) 2_566
S1 C9 1.785(3) .
S1 S2 2.0375(12) .
S2 C10 1.789(3) .
S3 C23 1.777(3) .
S3 S4 2.0499(12) .
S4 C24 1.787(3) .
O1 C1 1.441(4) .
O1 H1 0.847(10) .
O2 C3 1.252(3) .
O3 C3 1.265(3) .
O3 Dy1 2.373(2) 2_666
O4 C16 1.206(4) .
O5 C16 1.323(4) .
O5 H5 0.8200 .
O6 C17 1.254(3) .
O7 C17 1.268(3) .
O7 Dy1 2.286(2) 2_566
O8 C30 1.261(3) .
O8 Dy1 2.303(2) 1_545
O9 C30 1.259(3) .
O9 Dy1 2.346(2) 2_556
C1 C2 1.495(5) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C2 H2A 0.9600 .
C2 H2B 0.9600 .
C2 H2C 0.9600 .
C3 C4 1.493(4) .
C4 C5 1.387(4) .
C4 C9 1.405(4) .
C5 C6 1.378(4) .
C5 H5A 0.9300 .
C6 C7 1.384(5) .
C6 H6 0.9300 .
C7 C8 1.383(4) .
C7 H7 0.9300 .
C8 C9 1.394(4) .
C8 H8 0.9300 .
C10 C11 1.389(5) .
C10 C15 1.412(4) .
C11 C12 1.373(6) .
C11 H11 0.9300 .
C12 C13 1.366(7) .
C12 H12 0.9300 .
C13 C14 1.370(7) .
C13 H13 0.9300 .
C14 C15 1.397(5) .
C14 H14 0.9300 .
C15 C16 1.469(5) .
C17 C18 1.481(4) .
C18 C19 1.386(4) .
C18 C23 1.417(4) .
C19 C20 1.384(5) .
C19 H19 0.9300 .
C20 C21 1.375(6) .
C20 H20 0.9300 .
C21 C22 1.376(5) .
C21 H21 0.9300 .
C22 C23 1.398(4) .
C22 H22 0.9300 .
C24 C25 1.392(4) .
C24 C29 1.403(4) .
C25 C26 1.375(5) .
C25 H25 0.9300 .
C26 C27 1.393(5) .
C26 H26 0.9300 .
C27 C28 1.378(4) .
C27 H27 0.9300 .
C28 C29 1.391(4) .
C28 H28 0.9300 .
C29 C30 1.499(4) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
C9 S1 S2 C10 -90.43(15) . . . .
C23 S3 S4 C24 -99.60(15) . . . .
O2 Dy1 O1 C1 175.0(3) . . . .
O7 Dy1 O1 C1 67.4(3) 2_566 . . .
O8 Dy1 O1 C1 -17.4(3) 1_565 . . .
O6 Dy1 O1 C1 -88.7(3) . . . .
O9 Dy1 O1 C1 126.1(3) 2_556 . . .
O3 Dy1 O1 C1 -99.8(3) 2_666 . . .
O7 Dy1 O1 C1 12.5(3) . . . .
Dy1 Dy1 O1 C1 44.9(3) 2_566 . . .
O7 Dy1 O2 C3 76.1(4) 2_566 . . .
O8 Dy1 O2 C3 -20.4(4) 1_565 . . .
O6 Dy1 O2 C3 -144.8(3) . . . .
O9 Dy1 O2 C3 146.2(4) 2_556 . . .
O3 Dy1 O2 C3 -75.7(4) 2_666 . . .
O1 Dy1 O2 C3 2.7(3) . . . .
O7 Dy1 O2 C3 166.6(3) . . . .
Dy1 Dy1 O2 C3 114.1(3) 2_566 . . .
O2 Dy1 O6 C17 -145.56(16) . . . .
O7 Dy1 O6 C17 -21.2(2) 2_566 . . .
O8 Dy1 O6 C17 60.71(17) 1_565 . . .
O9 Dy1 O6 C17 -78.45(17) 2_556 . . .
O3 Dy1 O6 C17 139.29(18) 2_666 . . .
O1 Dy1 O6 C17 127.95(18) . . . .
O7 Dy1 O6 C17 -3.72(15) . . . .
Dy1 Dy1 O6 C17 -11.70(16) 2_566 . . .
O2 Dy1 O7 C17 71.19(19) . . . .
O7 Dy1 O7 C17 170.00(19) 2_566 . . .
O8 Dy1 O7 C17 -104.88(16) 1_565 . . .
O6 Dy1 O7 C17 3.60(14) . . . .
O9 Dy1 O7 C17 92.09(16) 2_556 . . .
O3 Dy1 O7 C17 -35.39(16) 2_666 . . .
O1 Dy1 O7 C17 -135.59(16) . . . .
Dy1 Dy1 O7 C17 170.00(19) 2_566 . . .
O2 Dy1 O7 Dy1 -98.82(12) . . . 2_566
O7 Dy1 O7 Dy1 0.0 2_566 . . 2_566
O8 Dy1 O7 Dy1 85.12(8) 1_565 . . 2_566
O6 Dy1 O7 Dy1 -166.41(11) . . . 2_566
O9 Dy1 O7 Dy1 -77.92(8) 2_556 . . 2_566
O3 Dy1 O7 Dy1 154.61(7) 2_666 . . 2_566
O1 Dy1 O7 Dy1 54.41(14) . . . 2_566
Dy1 O1 C1 C2 -168.7(3) . . . .
Dy1 O2 C3 O3 34.6(5) . . . .
Dy1 O2 C3 C4 -145.1(3) . . . .
Dy1 O3 C3 O2 78.8(3) 2_666 . . .
Dy1 O3 C3 C4 -101.6(3) 2_666 . . .
O2 C3 C4 C5 -21.7(4) . . . .
O3 C3 C4 C5 158.6(3) . . . .
O2 C3 C4 C9 158.2(3) . . . .
O3 C3 C4 C9 -21.5(4) . . . .
C9 C4 C5 C6 3.6(5) . . . .
C3 C4 C5 C6 -176.5(3) . . . .
C4 C5 C6 C7 -2.5(6) . . . .
C5 C6 C7 C8 0.4(6) . . . .
C6 C7 C8 C9 0.6(5) . . . .
C7 C8 C9 C4 0.5(5) . . . .
C7 C8 C9 S1 -179.4(3) . . . .
C5 C4 C9 C8 -2.5(4) . . . .
C3 C4 C9 C8 177.6(3) . . . .
C5 C4 C9 S1 177.4(2) . . . .
C3 C4 C9 S1 -2.6(4) . . . .
S2 S1 C9 C8 12.2(3) . . . .
S2 S1 C9 C4 -167.7(2) . . . .
S1 S2 C10 C11 20.9(3) . . . .
S1 S2 C10 C15 -159.2(3) . . . .
C15 C10 C11 C12 -1.4(6) . . . .
S2 C10 C11 C12 178.5(4) . . . .
C10 C11 C12 C13 0.4(8) . . . .
C11 C12 C13 C14 0.8(9) . . . .
C12 C13 C14 C15 -1.1(8) . . . .
C13 C14 C15 C10 0.1(7) . . . .
C13 C14 C15 C16 179.2(4) . . . .
C11 C10 C15 C14 1.1(5) . . . .
S2 C10 C15 C14 -178.8(3) . . . .
C11 C10 C15 C16 -178.0(3) . . . .
S2 C10 C15 C16 2.2(5) . . . .
C14 C15 C16 O4 166.8(4) . . . .
C10 C15 C16 O4 -14.2(6) . . . .
C14 C15 C16 O5 -13.4(5) . . . .
C10 C15 C16 O5 165.6(3) . . . .
Dy1 O6 C17 O7 7.1(3) . . . .
Dy1 O6 C17 C18 -171.21(19) . . . .
Dy1 O7 C17 O6 111.5(10) 2_566 . . .
Dy1 O7 C17 O6 -6.0(2) . . . .
Dy1 O7 C17 C18 -70.2(11) 2_566 . . .
Dy1 O7 C17 C18 172.3(2) . . . .
O6 C17 C18 C19 165.8(3) . . . .
O7 C17 C18 C19 -12.5(4) . . . .
O6 C17 C18 C23 -12.4(4) . . . .
O7 C17 C18 C23 169.2(3) . . . .
C23 C18 C19 C20 -0.9(5) . . . .
C17 C18 C19 C20 -179.2(3) . . . .
C18 C19 C20 C21 1.1(6) . . . .
C19 C20 C21 C22 -0.3(6) . . . .
C20 C21 C22 C23 -0.6(6) . . . .
C21 C22 C23 C18 0.7(5) . . . .
C21 C22 C23 S3 -176.9(3) . . . .
C19 C18 C23 C22 0.1(4) . . . .
C17 C18 C23 C22 178.3(3) . . . .
C19 C18 C23 S3 177.7(2) . . . .
C17 C18 C23 S3 -4.1(4) . . . .
S4 S3 C23 C22 20.1(3) . . . .
S4 S3 C23 C18 -157.5(2) . . . .
S3 S4 C24 C25 25.3(3) . . . .
S3 S4 C24 C29 -151.5(2) . . . .
C29 C24 C25 C26 0.4(5) . . . .
S4 C24 C25 C26 -176.3(3) . . . .
C24 C25 C26 C27 1.6(6) . . . .
C25 C26 C27 C28 -1.4(6) . . . .
C26 C27 C28 C29 -1.0(5) . . . .
C27 C28 C29 C24 3.0(5) . . . .
C27 C28 C29 C30 -176.9(3) . . . .
C25 C24 C29 C28 -2.7(4) . . . .
S4 C24 C29 C28 174.1(2) . . . .
C25 C24 C29 C30 177.2(3) . . . .
S4 C24 C29 C30 -6.0(4) . . . .
Dy1 O9 C30 O8 0.2(4) 2_556 . . .
Dy1 O9 C30 C29 -179.62(18) 2_556 . . .
Dy1 O8 C30 O9 22.0(4) 1_545 . . .
Dy1 O8 C30 C29 -158.15(17) 1_545 . . .
C28 C29 C30 O9 151.8(3) . . . .
C24 C29 C30 O9 -28.2(4) . . . .
C28 C29 C30 O8 -28.0(4) . . . .
C24 C29 C30 O8 152.0(3) . . . .
