#------------------------------------------------------------------------------
#$Date: 2021-04-09 11:26:17 +0300 (Fri, 09 Apr 2021) $
#$Revision: 264011 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/16/1561605.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1561605
loop_
_publ_author_name
'Jin, Jing'
'Chen, Chong'
'Gao, Yan'
'Zhao, Ran'
'Wang, Xiuyan'
'Lü, Chunxin'
'Chi, Yuxian'
'Niu, Shuyun'
_publ_section_title
;
 Synthesis, structure, and luminescence property of a series of Ag--Ln
 coordination polymers with the N-heterocyclic carboxylato ligand
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              193
_journal_page_last               201
_journal_paper_doi               10.1016/j.jssc.2016.01.001
_journal_volume                  235
_journal_year                    2016
_chemical_formula_sum            'C24 H30 Ag2 Ho N5 O18'
_chemical_formula_weight         1057.20
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.569(8)
_cell_angle_beta                 91.174(9)
_cell_angle_gamma                100.378(9)
_cell_formula_units_Z            2
_cell_length_a                   7.443(5)
_cell_length_b                   12.944(8)
_cell_length_c                   17.427(11)
_cell_measurement_temperature    293(2)
_cell_volume                     1635.4(18)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.970
_diffrn_measured_fraction_theta_max 0.970
_diffrn_measurement_device_type  'Bruker Apex2 CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0334
_diffrn_reflns_av_sigmaI/netI    0.0878
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            8707
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    3.669
_exptl_absorpt_correction_T_max  0.7105
_exptl_absorpt_correction_T_min  0.7105
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.147
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1028
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         4.869
_refine_diff_density_min         -1.772
_refine_diff_density_rms         0.213
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.059
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         6219
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.059
_refine_ls_R_factor_all          0.1001
_refine_ls_R_factor_gt           0.0627
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0842P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1497
_refine_ls_wR_factor_ref         0.1688
_reflns_number_gt                4294
_reflns_number_total             6219
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2016-235-193.CIF
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the built-in table derived from the
CIF Core dictionary named 'cif_core.dic' version 2.4.5 last updated
on 2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               1561605
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ho1 Ho 0.37678(7) 0.79631(3) -0.01885(3) 0.03006(17) Uani 1 1 d . . .
Ag1 Ag 0.26972(19) 0.94423(10) 0.47343(6) 0.0759(4) Uani 1 1 d . . .
Ag2 Ag 0.70967(17) 0.50930(10) -0.46198(6) 0.0697(4) Uani 1 1 d . . .
N1 N 0.3602(15) 0.9625(8) 0.3593(6) 0.055(3) Uani 1 1 d . . .
N2 N 0.1507(17) 0.9422(9) 0.5841(6) 0.064(3) Uani 1 1 d . . .
N3 N 0.6230(15) 0.5226(8) -0.3451(5) 0.051(3) Uani 1 1 d . . .
N4 N 0.8282(16) 0.5250(9) -0.5716(6) 0.057(3) Uani 1 1 d . . .
N5 N 0.487(2) 0.7465(9) 0.4916(7) 0.060(3) Uani 1 1 d . . .
O1 O 0.5103(12) 0.9250(5) 0.0814(4) 0.047(2) Uani 1 1 d . . .
O2 O 0.5505(12) 1.0978(5) 0.1145(4) 0.042(2) Uani 1 1 d . . .
O3 O -0.1131(12) 0.8575(6) 0.8338(5) 0.051(2) Uani 1 1 d . . .
O4 O -0.0187(15) 1.0340(7) 0.8593(5) 0.074(3) Uani 1 1 d . . .
O5 O 0.4030(12) 0.6433(6) -0.0886(4) 0.052(2) Uani 1 1 d . . .
O6 O 0.3880(15) 0.4734(6) -0.0828(5) 0.067(3) Uani 1 1 d . . .
O7 O 1.0379(12) 0.4685(6) -0.8413(5) 0.055(2) Uani 1 1 d . . .
O8 O 1.0918(12) 0.6448(6) -0.8139(4) 0.050(2) Uani 1 1 d . . .
O9 O 0.1775(12) 0.9249(6) -0.0010(4) 0.053(2) Uani 1 1 d . . .
H9A H 0.2203 0.9905 -0.0001 0.063 Uiso 1 1 d R . .
H9B H 0.0642 0.9041 0.0046 0.063 Uiso 1 1 d R . .
O10 O 0.1392(11) 0.7101(6) 0.0466(4) 0.053(2) Uani 1 1 d . . .
H10A H 0.0500 0.7404 0.0597 0.063 Uiso 1 1 d R . .
H10B H 0.1415 0.6483 0.0575 0.063 Uiso 1 1 d R . .
O11 O 0.1324(12) 0.7418(6) -0.1145(4) 0.049(2) Uani 1 1 d . . .
H11B H 0.0483 0.7781 -0.1164 0.058 Uiso 1 1 d R . .
H11C H 0.1293 0.6861 -0.1467 0.058 Uiso 1 1 d R . .
O12 O 0.7013(11) 0.8108(6) -0.0378(4) 0.047(2) Uani 1 1 d . . .
H12B H 0.7672 0.8715 -0.0385 0.056 Uiso 1 1 d R . .
H12C H 0.7494 0.7557 -0.0435 0.056 Uiso 1 1 d R . .
O13 O 0.5018(11) 0.7111(5) 0.0762(4) 0.047(2) Uani 1 1 d . . .
H13A H 0.4775 0.7248 0.1235 0.056 Uiso 1 1 d R . .
H13B H 0.5714 0.6670 0.0630 0.056 Uiso 1 1 d R . .
O14 O 0.539(2) 0.6863(9) 0.5275(8) 0.124(5) Uani 1 1 d . . .
O15 O 0.318(2) 0.7242(10) 0.4722(7) 0.101(4) Uani 1 1 d . . .
O16 O 0.578(2) 0.8254(8) 0.4760(7) 0.104(4) Uani 1 1 d . . .
O17 O 0.8155(13) 0.7726(6) 0.1579(6) 0.070(3) Uani 1 1 d . . .
H17B H 0.8156 0.7145 0.1756 0.084 Uiso 1 1 d R . .
H17C H 0.8978 0.8264 0.1735 0.084 Uiso 1 1 d R . .
O18 O 0.1794(12) 0.3926(7) 0.0263(5) 0.063(2) Uani 1 1 d . . .
H18B H 0.2413 0.3668 0.0581 0.075 Uiso 1 1 d R . .
H18C H 0.0859 0.3540 0.0019 0.075 Uiso 1 1 d R . .
C1 C 0.5111(14) 1.0050(7) 0.1281(6) 0.030(2) Uani 1 1 d . . .
C2 C 0.4611(15) 0.9888(8) 0.2108(6) 0.033(2) Uani 1 1 d . . .
C3 C 0.4067(18) 0.8903(8) 0.2315(6) 0.048(3) Uani 1 1 d . . .
H3A H 0.4058 0.8302 0.1956 0.057 Uiso 1 1 calc R . .
C4 C 0.3533(19) 0.8801(9) 0.3053(7) 0.051(3) Uani 1 1 d . . .
H4A H 0.3106 0.8126 0.3178 0.062 Uiso 1 1 calc R . .
C5 C 0.414(2) 1.0584(10) 0.3383(7) 0.058(4) Uani 1 1 d . . .
H5A H 0.4165 1.1173 0.3754 0.070 Uiso 1 1 calc R . .
C6 C 0.4675(18) 1.0755(8) 0.2650(6) 0.045(3) Uani 1 1 d . . .
H6A H 0.5062 1.1437 0.2530 0.054 Uiso 1 1 calc R . .
C7 C 0.082(2) 0.8537(11) 0.6131(8) 0.067(4) Uani 1 1 d . . .
H7A H 0.0726 0.7894 0.5811 0.080 Uiso 1 1 calc R . .
C8 C 0.0254(19) 0.8519(10) 0.6872(7) 0.059(4) Uani 1 1 d . . .
H8A H -0.0132 0.7874 0.7053 0.071 Uiso 1 1 calc R . .
C9 C 0.0252(17) 0.9456(9) 0.7350(7) 0.045(3) Uani 1 1 d . . .
C10 C -0.0401(18) 0.9450(10) 0.8166(8) 0.053(3) Uani 1 1 d . . .
C11 C 0.093(2) 1.0367(10) 0.7035(8) 0.064(4) Uani 1 1 d . . .
H11A H 0.0993 1.1024 0.7333 0.077 Uiso 1 1 calc R . .
C12 C 0.153(2) 1.0325(11) 0.6285(7) 0.071(5) Uani 1 1 d . . .
H12A H 0.1957 1.0955 0.6091 0.085 Uiso 1 1 calc R . .
C13 C 0.4266(16) 0.5526(8) -0.1155(6) 0.039(3) Uani 1 1 d . . .
C14 C 0.5021(15) 0.5415(8) -0.1949(6) 0.036(2) Uani 1 1 d . . .
C15 C 0.5724(18) 0.6290(8) -0.2298(7) 0.048(3) Uani 1 1 d . . .
H15A H 0.5792 0.6969 -0.2032 0.058 Uiso 1 1 calc R . .
C16 C 0.6319(19) 0.6158(9) -0.3036(7) 0.053(3) Uani 1 1 d . . .
H16A H 0.6812 0.6759 -0.3254 0.064 Uiso 1 1 calc R . .
C17 C 0.5579(19) 0.4354(9) -0.3097(7) 0.052(3) Uani 1 1 d . . .
H17A H 0.5556 0.3684 -0.3370 0.062 Uiso 1 1 calc R . .
C18 C 0.4972(16) 0.4429(8) -0.2371(6) 0.040(3) Uani 1 1 d . . .
H18A H 0.4523 0.3818 -0.2156 0.048 Uiso 1 1 calc R . .
C19 C 0.891(2) 0.6181(11) -0.5937(7) 0.065(4) Uani 1 1 d . . .
H19A H 0.8901 0.6786 -0.5586 0.078 Uiso 1 1 calc R . .
C20 C 0.9584(19) 0.6310(10) -0.6651(7) 0.058(4) Uani 1 1 d . . .
H20A H 0.9996 0.6986 -0.6778 0.069 Uiso 1 1 calc R . .
C21 C 0.9642(16) 0.5420(9) -0.7184(6) 0.040(3) Uani 1 1 d . . .
C22 C 1.0383(17) 0.5519(9) -0.7976(7) 0.046(3) Uani 1 1 d . . .
C23 C 0.8965(17) 0.4455(9) -0.6964(7) 0.048(3) Uani 1 1 d . . .
H23A H 0.8957 0.3839 -0.7307 0.058 Uiso 1 1 calc R . .
C24 C 0.8280(19) 0.4390(11) -0.6224(8) 0.061(4) Uani 1 1 d . . .
H24A H 0.7812 0.3728 -0.6086 0.073 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ho Ho -0.2175 4.6783 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O5 Ho1 O2 97.1(3) . 2_675
O5 Ho1 O10 90.5(3) . .
O2 Ho1 O10 144.7(3) 2_675 .
O5 Ho1 O1 144.3(3) . .
O2 Ho1 O1 94.6(3) 2_675 .
O10 Ho1 O1 99.1(3) . .
O5 Ho1 O13 79.1(3) . .
O2 Ho1 O13 144.0(3) 2_675 .
O10 Ho1 O13 71.4(3) . .
O1 Ho1 O13 71.7(3) . .
O5 Ho1 O11 69.5(3) . .
O2 Ho1 O11 74.7(3) 2_675 .
O10 Ho1 O11 75.8(3) . .
O1 Ho1 O11 146.2(3) . .
O13 Ho1 O11 133.8(3) . .
O5 Ho1 O9 142.1(3) . .
O2 Ho1 O9 75.2(3) 2_675 .
O10 Ho1 O9 77.7(3) . .
O1 Ho1 O9 73.6(3) . .
O13 Ho1 O9 128.3(3) . .
O11 Ho1 O9 72.7(3) . .
O5 Ho1 O12 75.4(3) . .
O2 Ho1 O12 72.4(3) 2_675 .
O10 Ho1 O12 142.5(3) . .
O1 Ho1 O12 76.3(3) . .
O13 Ho1 O12 71.9(3) . .
O11 Ho1 O12 127.6(3) . .
O9 Ho1 O12 133.2(3) . .
N2 Ag1 N1 171.0(4) . .
N4 Ag2 N3 169.0(4) . .
N4 Ag2 Ag2 92.0(3) . 2_664
N3 Ag2 Ag2 93.6(3) . 2_664
C4 N1 C5 117.1(10) . .
C4 N1 Ag1 121.5(8) . .
C5 N1 Ag1 121.3(8) . .
C12 N2 C7 117.1(11) . .
C12 N2 Ag1 118.8(9) . .
C7 N2 Ag1 124.0(9) . .
C16 N3 C17 116.8(10) . .
C16 N3 Ag2 120.8(8) . .
C17 N3 Ag2 122.3(8) . .
C19 N4 C24 117.6(11) . .
C19 N4 Ag2 122.7(9) . .
C24 N4 Ag2 119.6(8) . .
O14 N5 O16 125.0(17) . .
O14 N5 O15 114.8(15) . .
O16 N5 O15 120.2(14) . .
C1 O1 Ho1 152.7(8) . .
C1 O2 Ho1 144.6(6) . 2_675
C13 O5 Ho1 168.9(8) . .
Ho1 O9 H9A 120.4 . .
Ho1 O9 H9B 119.6 . .
H9A O9 H9B 120.0 . .
Ho1 O10 H10A 120.1 . .
Ho1 O10 H10B 119.9 . .
H10A O10 H10B 120.0 . .
Ho1 O11 H11B 120.0 . .
Ho1 O11 H11C 120.0 . .
H11B O11 H11C 120.0 . .
Ho1 O12 H12B 119.6 . .
Ho1 O12 H12C 120.4 . .
H12B O12 H12C 120.0 . .
Ho1 O13 H13A 120.0 . .
Ho1 O13 H13B 120.0 . .
H13A O13 H13B 120.0 . .
H17B O17 H17C 120.0 . .
H18B O18 H18C 120.0 . .
O1 C1 O2 126.1(9) . .
O1 C1 C2 117.1(8) . .
O2 C1 C2 116.9(8) . .
C6 C2 C3 119.1(10) . .
C6 C2 C1 118.9(9) . .
C3 C2 C1 122.0(9) . .
C2 C3 C4 119.7(11) . .
C2 C3 H3A 120.1 . .
C4 C3 H3A 120.1 . .
N1 C4 C3 122.4(11) . .
N1 C4 H4A 118.8 . .
C3 C4 H4A 118.8 . .
N1 C5 C6 124.0(11) . .
N1 C5 H5A 118.0 . .
C6 C5 H5A 118.0 . .
C2 C6 C5 117.5(10) . .
C2 C6 H6A 121.2 . .
C5 C6 H6A 121.2 . .
N2 C7 C8 124.0(13) . .
N2 C7 H7A 118.0 . .
C8 C7 H7A 118.0 . .
C7 C8 C9 120.0(12) . .
C7 C8 H8A 120.0 . .
C9 C8 H8A 120.0 . .
C8 C9 C11 115.1(11) . .
C8 C9 C10 120.7(11) . .
C11 C9 C10 124.2(11) . .
O3 C10 O4 127.1(12) . .
O3 C10 C9 116.3(11) . .
O4 C10 C9 116.6(11) . .
C9 C11 C12 121.7(12) . .
C9 C11 H11A 119.2 . .
C12 C11 H11A 119.2 . .
N2 C12 C11 121.9(12) . .
N2 C12 H12A 119.0 . .
C11 C12 H12A 119.0 . .
O6 C13 O5 124.8(11) . .
O6 C13 C14 119.1(9) . .
O5 C13 C14 116.1(10) . .
C15 C14 C18 117.3(10) . .
C15 C14 C13 121.7(10) . .
C18 C14 C13 121.0(9) . .
C16 C15 C14 119.9(10) . .
C16 C15 H15A 120.0 . .
C14 C15 H15A 120.0 . .
N3 C16 C15 123.3(11) . .
N3 C16 H16A 118.3 . .
C15 C16 H16A 118.3 . .
C18 C17 N3 122.8(10) . .
C18 C17 H17A 118.6 . .
N3 C17 H17A 118.6 . .
C17 C18 C14 119.7(10) . .
C17 C18 H18A 120.1 . .
C14 C18 H18A 120.1 . .
N4 C19 C20 124.1(12) . .
N4 C19 H19A 117.9 . .
C20 C19 H19A 117.9 . .
C19 C20 C21 119.2(11) . .
C19 C20 H20A 120.4 . .
C21 C20 H20A 120.4 . .
C23 C21 C20 117.0(11) . .
C23 C21 C22 121.7(11) . .
C20 C21 C22 121.3(10) . .
O7 C22 O8 125.9(11) . .
O7 C22 C21 116.9(10) . .
O8 C22 C21 117.2(10) . .
C21 C23 C24 120.3(12) . .
C21 C23 H23A 119.9 . .
C24 C23 H23A 119.9 . .
N4 C24 C23 121.8(12) . .
N4 C24 H24A 119.1 . .
C23 C24 H24A 119.1 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ho1 O5 2.226(7) .
Ho1 O2 2.307(6) 2_675
Ho1 O10 2.319(8) .
Ho1 O1 2.320(7) .
Ho1 O13 2.370(7) .
Ho1 O11 2.385(8) .
Ho1 O9 2.416(7) .
Ho1 O12 2.421(8) .
Ag1 N2 2.140(11) .
Ag1 N1 2.142(10) .
Ag2 N4 2.139(10) .
Ag2 N3 2.144(10) .
Ag2 Ag2 3.321(3) 2_664
N1 C4 1.319(14) .
N1 C5 1.335(15) .
N2 C12 1.312(16) .
N2 C7 1.334(16) .
N3 C16 1.312(14) .
N3 C17 1.373(14) .
N4 C19 1.322(16) .
N4 C24 1.327(16) .
N5 O14 1.173(14) .
N5 O16 1.186(14) .
N5 O15 1.262(16) .
O1 C1 1.229(11) .
O2 C1 1.239(11) .
O2 Ho1 2.307(6) 2_675
O3 C10 1.241(14) .
O4 C10 1.269(15) .
O5 C13 1.250(12) .
O6 C13 1.229(12) .
O7 C22 1.236(13) .
O8 C22 1.268(13) .
O9 H9A 0.8500 .
O9 H9B 0.8500 .
O10 H10A 0.8500 .
O10 H10B 0.8501 .
O11 H11B 0.8500 .
O11 H11C 0.8501 .
O12 H12B 0.8500 .
O12 H12C 0.8500 .
O13 H13A 0.8499 .
O13 H13B 0.8502 .
O17 H17B 0.8500 .
O17 H17C 0.8500 .
O18 H18B 0.8500 .
O18 H18C 0.8500 .
C1 C2 1.528(13) .
C2 C6 1.361(14) .
C2 C3 1.364(14) .
C3 C4 1.370(15) .
C3 H3A 0.9300 .
C4 H4A 0.9300 .
C5 C6 1.378(15) .
C5 H5A 0.9300 .
C6 H6A 0.9300 .
C7 C8 1.368(17) .
C7 H7A 0.9300 .
C8 C9 1.379(16) .
C8 H8A 0.9300 .
C9 C11 1.385(16) .
C9 C10 1.512(16) .
C11 C12 1.385(17) .
C11 H11A 0.9300 .
C12 H12A 0.9300 .
C13 C14 1.503(15) .
C14 C15 1.381(14) .
C14 C18 1.382(14) .
C15 C16 1.368(16) .
C15 H15A 0.9300 .
C16 H16A 0.9300 .
C17 C18 1.350(15) .
C17 H17A 0.9300 .
C18 H18A 0.9300 .
C19 C20 1.369(17) .
C19 H19A 0.9300 .
C20 C21 1.390(16) .
C20 H20A 0.9300 .
C21 C23 1.366(15) .
C21 C22 1.510(15) .
C23 C24 1.404(16) .
C23 H23A 0.9300 .
C24 H24A 0.9300 .
