#------------------------------------------------------------------------------
#$Date: 2023-12-22 17:07:40 +0200 (Fri, 22 Dec 2023) $
#$Revision: 288505 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/20/1562003.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1562003
loop_
_publ_author_name
'Hasegawa, Toru'
'Yamane, Hisanori'
_publ_section_title
;
 Synthesis and crystal structure analysis of Li2NaBP2O8 and LiNa2B5P2O14
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              65
_journal_page_last               71
_journal_paper_doi               10.1016/j.jssc.2014.11.024
_journal_volume                  225
_journal_year                    2015
_chemical_formula_moiety         'B5 O14 P2, Na2, (Li)'
_chemical_formula_sum            'B5 Li Na2 O14 P2'
_chemical_formula_weight         392.91
_chemical_name_common
;
lithium sodium boron phosphorous oxide
;
_chemical_name_systematic
; 
 monolithium disodium pentaboron diphosphorous oxide  
;
_space_group_IT_number           11
_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.709(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   8.208(3)
_cell_length_b                   9.151(3)
_cell_length_c                   8.349(3)
_cell_measurement_reflns_used    2744
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.51
_cell_volume                     565.0(3)
_computing_cell_refinement       'PROCESS-AUTO	"(Rigaku/MSC,"	2005)'
_computing_data_collection       'PROCESS-AUTO	"(Rigaku/MSC,"	2005)'
_computing_data_reduction        'PROCESS-AUTO	"(Rigaku/MSC,"	2005)'
_computing_molecular_graphics    'VESTA	(Momma	&"Izumi,"2008)'
_computing_publication_material  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  'Rigaku	RAXIS-RAPID	II'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0639
_diffrn_reflns_av_unetI/netI     0.0589
_diffrn_reflns_Laue_measured_fraction_full 0.985
_diffrn_reflns_Laue_measured_fraction_max 0.980
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            5358
_diffrn_reflns_point_group_measured_fraction_full 0.985
_diffrn_reflns_point_group_measured_fraction_max 0.980
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.476
_diffrn_reflns_theta_min         3.506
_exptl_absorpt_coefficient_mu    0.546
_exptl_absorpt_correction_T_max  0.951068
_exptl_absorpt_correction_T_min  0.904336
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
;
(NUMABS;Higashi,1999)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.309
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             384
_exptl_crystal_size_max          0.149
_exptl_crystal_size_mid          0.126
_exptl_crystal_size_min          0.123
_refine_diff_density_max         0.422
_refine_diff_density_min         -0.588
_refine_diff_density_rms         0.106
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.059
_refine_ls_matrix_type           full
_refine_ls_number_parameters     130
_refine_ls_number_reflns         1350
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.059
_refine_ls_R_factor_all          0.0548
_refine_ls_R_factor_gt           0.0424
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0398P)²+0.4367P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0896
_refine_ls_wR_factor_ref         0.0985
_reflns_Friedel_coverage         0.000
_reflns_number_gt                1098
_reflns_number_total             1350
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            LiNa2B5P2O14.cif
_cod_data_source_block           shelxl
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Numerical' was
changed to 'numerical' in accordance with the built-in table derived
from the CIF Core dictionary named 'cif_core.dic' version 2.4.5 last
updated on 2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 

The following automatic conversions were performed:

data name '_iucr_refine_instruction_details' was replaced with
'_iucr_refine_instructions_details' as specified in the replacement
file 'data/replacement-values/replacement_tags.lst'.

Automatic conversion script
Id: cif_correct_tags 9268 2022-04-12 08:56:07Z antanas 
;
_cod_original_sg_symbol_H-M      P21/m
_cod_database_code               1562003
_cod_database_fobs_code          1562003
_shelxl_version_number           2014-3
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.15342(8) 0.05756(7) 0.27310(8) 0.0120(2) Uani 1 1 d . . . . .
B1 B 0.2656(5) 0.2500 0.5453(5) 0.0124(8) Uani 1 2 d S T P . .
B2 B 0.2806(5) 0.2500 0.0982(5) 0.0123(8) Uani 1 2 d S T P . .
B3 B 0.9490(5) 0.2500 0.3494(5) 0.0120(8) Uani 1 2 d S T P . .
B4 B 0.4151(5) 0.2500 0.8845(5) 0.0147(8) Uani 1 2 d S T P . .
B5 B 0.6105(5) 0.2500 0.1995(5) 0.0157(8) Uani 1 2 d S T P . .
Na1 Na 0.6034(2) 0.2500 0.53499(19) 0.0260(4) Uani 1 2 d S T P . .
Na2 Na 0.8341(2) 0.2500 0.95832(19) 0.0255(4) Uani 1 2 d S T P . .
Li1 Li 0.0144(8) 0.2500 0.7154(8) 0.0183(13) Uani 1 2 d S T P . .
O1 O 0.2981(2) 0.11792(19) 0.4514(2) 0.0136(4) Uani 1 1 d . . . . .
O2 O 0.0322(2) 0.6182(2) 0.7508(2) 0.0196(4) Uani 1 1 d . . . . .
O3 O 0.1859(3) 0.1187(2) 0.1168(2) 0.0266(5) Uani 1 1 d . . . . .
O4 O 0.1555(2) 0.6040(2) 0.2673(2) 0.0176(4) Uani 1 1 d . . . . .
O5 O 0.4104(3) 0.2500 0.7209(3) 0.0158(5) Uani 1 2 d S T P . .
O6 O 0.0849(3) 0.2500 0.5273(3) 0.0127(5) Uani 1 2 d S T P . .
O7 O 0.2656(3) 0.2500 0.9166(3) 0.0127(5) Uani 1 2 d S T P . .
O8 O 0.4630(3) 0.2500 0.2318(3) 0.0233(7) Uani 1 2 d S T P . .
O9 O 0.7726(3) 0.2500 0.3418(3) 0.0184(6) Uani 1 2 d S T P . .
O10 O 0.5881(3) 0.2500 0.0243(3) 0.0194(6) Uani 1 2 d S T P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 P1 O3 108.99(11) 4_565 .
O4 P1 O1 111.89(10) 4_565 .
O3 P1 O1 109.95(10) . .
O4 P1 O2 112.22(10) 4_565 2_546
O3 P1 O2 106.36(12) . 2_546
O1 P1 O2 107.27(10) . 2_546
O4 P1 Na2 121.57(7) 4_565 1_454
O3 P1 Na2 60.21(9) . 1_454
O1 P1 Na2 126.01(7) . 1_454
O2 P1 Na2 46.40(8) 2_546 1_454
O4 P1 Na1 34.94(7) 4_565 3_656
O3 P1 Na1 114.45(9) . 3_656
O1 P1 Na1 78.16(7) . 3_656
O2 P1 Na1 134.10(8) 2_546 3_656
Na2 P1 Na1 155.81(3) 1_454 3_656
O4 P1 Na2 32.93(7) 4_565 3_656
O3 P1 Na2 76.35(8) . 3_656
O1 P1 Na2 129.39(7) . 3_656
O2 P1 Na2 119.17(7) 2_546 3_656
Na2 P1 Na2 101.30(3) 1_454 3_656
Na1 P1 Na2 55.70(4) 3_656 3_656
O6 B1 O5 118.2(3) . .
O6 B1 O1 110.61(19) . .
O5 B1 O1 105.87(19) . .
O6 B1 O1 110.61(19) . 4_565
O5 B1 O1 105.87(19) . 4_565
O1 B1 O1 104.8(3) . 4_565
O6 B1 Na1 173.0(2) . .
O5 B1 Na1 68.86(17) . .
O1 B1 Na1 65.77(15) . .
O1 B1 Na1 65.77(15) 4_565 .
O8 B2 O7 113.4(3) . 1_554
O8 B2 O3 109.84(19) . .
O7 B2 O3 107.29(19) 1_554 .
O8 B2 O3 109.84(19) . 4_565
O7 B2 O3 107.29(19) 1_554 4_565
O3 B2 O3 109.1(3) . 4_565
O6 B3 O9 111.7(3) 1_655 .
O6 B3 O2 110.88(18) 1_655 2_646
O9 B3 O2 108.74(18) . 2_646
O6 B3 O2 110.88(18) 1_655 3_666
O9 B3 O2 108.74(18) . 3_666
O2 B3 O2 105.7(3) 2_646 3_666
O6 B3 Na2 151.4(2) 1_655 1_554
O9 B3 Na2 96.81(19) . 1_554
O2 B3 Na2 56.89(14) 2_646 1_554
O2 B3 Na2 56.89(14) 3_666 1_554
O5 B4 O7 124.4(3) . .
O5 B4 O10 114.8(3) . 1_556
O7 B4 O10 120.8(3) . 1_556
O9 B5 O8 117.0(3) . .
O9 B5 O10 123.8(3) . .
O8 B5 O10 119.2(3) . .
O9 B5 Na1 64.11(19) . .
O8 B5 Na1 52.88(17) . .
O10 B5 Na1 172.1(3) . .
O8 Na1 O4 129.90(8) . 3_666
O8 Na1 O4 129.90(8) . 2_646
O4 Na1 O4 68.80(10) 3_666 2_646
O8 Na1 O9 56.54(9) . .
O4 Na1 O9 85.46(8) 3_666 .
O4 Na1 O9 85.46(8) 2_646 .
O8 Na1 O1 74.76(7) . 4_565
O4 Na1 O1 110.08(7) 3_666 4_565
O4 Na1 O1 150.52(9) 2_646 4_565
O9 Na1 O1 124.02(7) . 4_565
O8 Na1 O1 74.76(7) . .
O4 Na1 O1 150.52(9) 3_666 .
O4 Na1 O1 110.08(7) 2_646 .
O9 Na1 O1 124.02(7) . .
O1 Na1 O1 55.62(8) 4_565 .
O8 Na1 O5 120.42(10) . .
O4 Na1 O5 97.05(8) 3_666 .
O4 Na1 O5 97.05(8) 2_646 .
O9 Na1 O5 176.96(9) . .
O1 Na1 O5 53.48(6) 4_565 .
O1 Na1 O5 53.48(6) . .
O8 Na1 B1 90.22(11) . .
O4 Na1 B1 121.10(9) 3_666 .
O4 Na1 B1 121.10(9) 2_646 .
O9 Na1 B1 146.76(11) . .
O1 Na1 B1 32.49(6) 4_565 .
O1 Na1 B1 32.49(6) . .
O5 Na1 B1 30.20(9) . .
O8 Na1 B5 28.14(10) . .
O4 Na1 B5 108.72(9) 3_666 .
O4 Na1 B5 108.72(9) 2_646 .
O9 Na1 B5 28.40(10) . .
O1 Na1 B5 99.58(9) 4_565 .
O1 Na1 B5 99.58(9) . .
O5 Na1 B5 148.56(11) . .
B1 Na1 B5 118.36(12) . .
O8 Na1 Li1 117.88(14) . 1_655
O4 Na1 Li1 40.65(8) 3_666 1_655
O4 Na1 Li1 40.65(8) 2_646 1_655
O9 Na1 Li1 61.34(13) . 1_655
O1 Na1 Li1 150.39(6) 4_565 1_655
O1 Na1 Li1 150.39(6) . 1_655
O5 Na1 Li1 121.70(14) . 1_655
B1 Na1 Li1 151.90(15) . 1_655
B5 Na1 Li1 89.74(15) . 1_655
O8 Na1 Na2 174.90(9) . .
O4 Na1 Na2 46.76(5) 3_666 .
O4 Na1 Na2 46.76(5) 2_646 .
O9 Na1 Na2 118.37(8) . .
O1 Na1 Na2 109.69(6) 4_565 .
O1 Na1 Na2 109.69(6) . .
O5 Na1 Na2 64.67(7) . .
B1 Na1 Na2 94.88(9) . .
B5 Na1 Na2 146.77(10) . .
Li1 Na1 Na2 57.03(12) 1_655 .
O8 Na1 P1 115.53(4) . 2_656
O4 Na1 P1 21.01(4) 3_666 2_656
O4 Na1 P1 89.78(6) 2_646 2_656
O9 Na1 P1 85.92(5) . 2_656
O1 Na1 P1 92.41(5) 4_565 2_656
O1 Na1 P1 144.09(6) . 2_656
O5 Na1 P1 95.80(5) . 2_656
B1 Na1 P1 111.63(5) . 2_656
B5 Na1 P1 101.86(6) . 2_656
Li1 Na1 P1 58.07(4) 1_655 2_656
Na2 Na1 P1 62.47(3) . 2_656
O10 Na2 O4 122.15(8) 1_556 2_646
O10 Na2 O4 122.15(8) 1_556 3_666
O4 Na2 O4 69.59(10) 2_646 3_666
O10 Na2 O2 80.16(8) 1_556 3_667
O4 Na2 O2 154.64(9) 2_646 3_667
O4 Na2 O2 110.66(7) 3_666 3_667
O10 Na2 O2 80.16(8) 1_556 2_647
O4 Na2 O2 110.66(7) 2_646 2_647
O4 Na2 O2 154.64(9) 3_666 2_647
O2 Na2 O2 57.71(9) 3_667 2_647
O10 Na2 O3 134.34(8) 1_556 4_666
O4 Na2 O3 103.28(8) 2_646 4_666
O4 Na2 O3 75.60(7) 3_666 4_666
O2 Na2 O3 54.51(6) 3_667 4_666
O2 Na2 O3 79.86(7) 2_647 4_666
O10 Na2 O3 134.34(8) 1_556 1_656
O4 Na2 O3 75.60(7) 2_646 1_656
O4 Na2 O3 103.28(8) 3_666 1_656
O2 Na2 O3 79.86(7) 3_667 1_656
O2 Na2 O3 54.51(6) 2_647 1_656
O3 Na2 O3 49.56(8) 4_666 1_656
O10 Na2 B3 68.46(10) 1_556 1_556
O4 Na2 B3 141.00(6) 2_646 1_556
O4 Na2 B3 141.00(6) 3_666 1_556
O2 Na2 B3 30.48(5) 3_667 1_556
O2 Na2 B3 30.48(5) 2_647 1_556
O3 Na2 B3 73.60(8) 4_666 1_556
O3 Na2 B3 73.60(8) 1_656 1_556
O10 Na2 Li1 154.64(14) 1_556 1_655
O4 Na2 Li1 41.52(8) 2_646 1_655
O4 Na2 Li1 41.52(8) 3_666 1_655
O2 Na2 Li1 121.49(12) 3_667 1_655
O2 Na2 Li1 121.49(12) 2_647 1_655
O3 Na2 Li1 67.46(12) 4_666 1_655
O3 Na2 Li1 67.46(12) 1_656 1_655
B3 Na2 Li1 136.90(15) 1_556 1_655
O10 Na2 Na1 95.94(8) 1_556 .
O4 Na2 Na1 47.38(6) 2_646 .
O4 Na2 Na1 47.38(6) 3_666 .
O2 Na2 Na1 150.70(5) 3_667 .
O2 Na2 Na1 150.70(5) 2_647 .
O3 Na2 Na1 120.27(6) 4_666 .
O3 Na2 Na1 120.27(6) 1_656 .
B3 Na2 Na1 164.40(10) 1_556 .
Li1 Na2 Na1 58.70(12) 1_655 .
O10 Na2 P1 106.50(7) 1_556 4_666
O4 Na2 P1 130.66(8) 2_646 4_666
O4 Na2 P1 92.46(6) 3_666 4_666
O2 Na2 P1 26.71(4) 3_667 4_666
O2 Na2 P1 67.76(6) 2_647 4_666
O3 Na2 P1 27.89(4) 4_666 4_666
O3 Na2 P1 64.10(5) 1_656 4_666
B3 Na2 P1 50.45(6) 1_556 4_666
Li1 Na2 P1 94.85(11) 1_655 4_666
Na1 Na2 P1 139.74(4) . 4_666
O10 Na2 P1 106.50(7) 1_556 1_656
O4 Na2 P1 92.46(6) 2_646 1_656
O4 Na2 P1 130.66(8) 3_666 1_656
O2 Na2 P1 67.76(6) 3_667 1_656
O2 Na2 P1 26.71(4) 2_647 1_656
O3 Na2 P1 64.10(5) 4_666 1_656
O3 Na2 P1 27.89(4) 1_656 1_656
B3 Na2 P1 50.45(6) 1_556 1_656
Li1 Na2 P1 94.85(11) 1_655 1_656
Na1 Na2 P1 139.74(4) . 1_656
P1 Na2 P1 64.46(4) 4_666 1_656
O6 Li1 O4 122.6(2) . 2_546
O6 Li1 O4 122.6(2) . 3_566
O4 Li1 O4 84.8(3) 2_546 3_566
O6 Li1 O7 96.9(3) . .
O4 Li1 O7 115.9(2) 2_546 .
O4 Li1 O7 115.9(2) 3_566 .
O6 Li1 Na2 169.5(3) . 1_455
O4 Li1 Na2 51.56(15) 2_546 1_455
O4 Li1 Na2 51.56(15) 3_566 1_455
O7 Li1 Na2 93.6(2) . 1_455
O6 Li1 Na1 105.2(3) . 1_455
O4 Li1 Na1 51.03(14) 2_546 1_455
O4 Li1 Na1 51.03(14) 3_566 1_455
O7 Li1 Na1 157.9(3) . 1_455
Na2 Li1 Na1 64.27(13) 1_455 1_455
B1 O1 P1 123.00(18) . .
B1 O1 Na1 81.74(15) . .
P1 O1 Na1 132.39(10) . .
B3 O2 P1 122.96(18) 3_666 2_556
B3 O2 Na2 92.62(15) 3_666 3_667
P1 O2 Na2 106.88(10) 2_556 3_667
B2 O3 P1 132.50(19) . .
B2 O3 Na2 94.64(17) . 1_454
P1 O3 Na2 91.90(10) . 1_454
P1 O4 Li1 130.75(16) 4_565 3_566
P1 O4 Na2 126.98(10) 4_565 3_666
Li1 O4 Na2 86.93(17) 3_566 3_666
P1 O4 Na1 124.05(10) 4_565 3_666
Li1 O4 Na1 88.31(16) 3_566 3_666
Na2 O4 Na1 85.86(8) 3_666 3_666
B4 O5 B1 133.0(3) . .
B4 O5 Na1 146.0(2) . .
B1 O5 Na1 80.93(19) . .
B3 O6 B1 114.9(3) 1_455 .
B3 O6 Li1 118.9(3) 1_455 .
B1 O6 Li1 126.2(3) . .
B4 O7 B2 121.6(3) . 1_556
B4 O7 Li1 121.2(3) . .
B2 O7 Li1 117.3(3) 1_556 .
B5 O8 B2 124.9(3) . .
B5 O8 Na1 99.0(2) . .
B2 O8 Na1 136.1(2) . .
B5 O9 B3 129.7(3) . .
B5 O9 Na1 87.5(2) . .
B3 O9 Na1 142.8(2) . .
B5 O10 B4 120.2(3) . 1_554
B5 O10 Na2 121.3(2) . 1_554
B4 O10 Na2 118.6(2) 1_554 1_554
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
P1 O4 1.480(2) 4_565
P1 O3 1.5455(19) .
P1 O1 1.5483(17) .
P1 O2 1.5511(18) 2_546
P1 Na2 3.3017(16) 1_454
P1 Na1 3.4203(13) 3_656
P1 Na2 3.4405(13) 3_656
B1 O6 1.424(4) .
B1 O5 1.432(4) .
B1 O1 1.526(3) .
B1 O1 1.526(3) 4_565
B1 Na1 2.811(4) .
B2 O8 1.427(4) .
B2 O7 1.467(4) 1_554
B2 O3 1.475(3) .
B2 O3 1.475(3) 4_565
B3 O6 1.419(4) 1_655
B3 O9 1.421(4) .
B3 O2 1.513(3) 2_646
B3 O2 1.513(3) 3_666
B3 Na2 2.980(4) 1_554
B4 O5 1.349(4) .
B4 O7 1.365(5) .
B4 O10 1.393(4) 1_556
B5 O9 1.346(5) .
B5 O8 1.349(5) .
B5 O10 1.393(5) .
B5 Na1 2.826(4) .
Na1 O8 2.282(3) .
Na1 O4 2.364(2) 3_666
Na1 O4 2.364(2) 2_646
Na1 O9 2.545(3) .
Na1 O1 2.590(2) 4_565
Na1 O1 2.590(2) .
Na1 O5 2.655(3) .
Na1 Li1 3.040(6) 1_655
Na1 Na2 3.205(2) .
Na1 P1 3.4203(13) 2_656
Na2 O10 2.312(3) 1_556
Na2 O4 2.341(2) 2_646
Na2 O4 2.341(2) 3_666
Na2 O2 2.499(2) 3_667
Na2 O2 2.499(2) 2_647
Na2 O3 2.867(3) 4_666
Na2 O3 2.867(3) 1_656
Na2 B3 2.980(4) 1_556
Na2 Li1 2.984(6) 1_655
Na2 P1 3.3017(16) 4_666
Na2 P1 3.3017(16) 1_656
Li1 O6 1.895(6) .
Li1 O4 1.981(5) 2_546
Li1 O4 1.981(5) 3_566
Li1 O7 2.017(6) .
Li1 Na2 2.984(6) 1_455
Li1 Na1 3.040(6) 1_455
O2 B3 1.513(3) 3_666
O2 P1 1.5511(18) 2_556
O2 Na2 2.499(2) 3_667
O3 Na2 2.867(3) 1_454
O4 P1 1.480(2) 4_565
O4 Li1 1.981(5) 3_566
O4 Na2 2.341(2) 3_666
O4 Na1 2.364(2) 3_666
O6 B3 1.419(4) 1_455
O7 B2 1.467(4) 1_556
O10 B4 1.393(4) 1_554
O10 Na2 2.312(3) 1_554
