#------------------------------------------------------------------------------
#$Date: 2021-04-28 12:19:43 +0300 (Wed, 28 Apr 2021) $
#$Revision: 264635 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/22/1562207.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1562207
loop_
_publ_author_name
'Zhang, Ren-Chun'
'Zhang, You-Juan'
'Yuan, Bai-Qing'
'Miao, Jun-Peng'
'Pei, Bao-Hua'
'Liu, Pan-Pan'
'Wang, Jun-Jie'
'Zhang, Dao-Jun'
_publ_section_title
;
 Transformation of dense AgI into a silver-rich framework iodide using
 thiophenol as mineralizer
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              185
_journal_page_last               190
_journal_paper_doi               10.1016/j.jssc.2014.08.036
_journal_volume                  220
_journal_year                    2014
_chemical_formula_sum            'C24 H50 Ag14 I16 N8'
_chemical_formula_weight         3991.30
_space_group_IT_number           167
_space_group_name_Hall           '-R 3 2"c'
_space_group_name_H-M_alt        'R -3 c :H'
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_H-M   'R -3 c :H'
_atom_sites_solution_hydrogens   none
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            6
_cell_length_a                   13.4452(2)
_cell_length_b                   13.4452(2)
_cell_length_c                   63.725(2)
_cell_measurement_temperature    296(2)
_cell_volume                     9976.4(4)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0284
_diffrn_reflns_av_sigmaI/netI    0.0128
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       79
_diffrn_reflns_limit_l_min       -78
_diffrn_reflns_number            26642
_diffrn_reflns_theta_full        26.40
_diffrn_reflns_theta_max         26.40
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    11.474
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.986
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             10536
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.18
_refine_diff_density_max         2.803
_refine_diff_density_min         -3.989
_refine_diff_density_rms         0.332
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.086
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     104
_refine_ls_number_reflns         2276
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.086
_refine_ls_R_factor_all          0.0592
_refine_ls_R_factor_gt           0.0541
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1116P)²+360.1229P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1738
_refine_ls_wR_factor_ref         0.1801
_reflns_number_gt                2000
_reflns_number_total             2276
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            JSSC-2014-220-185.cif
_cod_data_source_block           1
_cod_original_cell_volume        9976.5(4)
_cod_original_sg_symbol_H-M      R-3c
_cod_database_code               1562207
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+5/6'
'x-y+2/3, -y+1/3, -z+5/6'
'-x+2/3, -x+y+1/3, -z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+7/6'
'x-y+1/3, -y+2/3, -z+7/6'
'-x+1/3, -x+y+2/3, -z+7/6'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-y+2/3, -x+1/3, z-1/6'
'-x+y+2/3, y+1/3, z-1/6'
'x+2/3, x-y+1/3, z-1/6'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-y+1/3, -x+2/3, z+1/6'
'-x+y+1/3, y+2/3, z+1/6'
'x+1/3, x-y+2/3, z+1/6'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
I3 I 0.33222(6) -0.00085(6) -0.154232(12) 0.0402(3) Uani 1 1 d . . .
I2 I 0.66840(6) 0.12337(7) -0.111658(13) 0.0459(3) Uani 1 1 d . . .
I1 I 0.3333 -0.02563(9) -0.0833 0.0611(4) Uani 1 2 d S . .
Ag1 Ag 0.44819(11) 0.11883(10) -0.11666(2) 0.0651(4) Uani 1 1 d . . .
Ag2 Ag 0.6667 0.3333 -0.10037(3) 0.0650(5) Uani 1 3 d S . .
I4 I 0.6667 0.3333 -0.1667 0.0571(5) Uani 1 6 d S . .
Ag3' Ag 0.5792(2) 0.0994(2) -0.15236(4) 0.0628(6) Uani 0.50 1 d P . .
Ag3 Ag 0.5197(3) 0.0982(3) -0.18037(6) 0.1031(11) Uani 0.50 1 d P . .
N4 N 0.6667 0.3333 0.0615(2) 0.033(3) Uani 1 3 d S . .
N1 N 0.6667 0.3333 -0.0628(2) 0.036(3) Uani 1 3 d S . .
N3 N 0.6667 0.3333 0.0214(2) 0.034(3) Uani 1 3 d S . .
H1 H 0.6667 0.3333 0.0079 0.041 Uiso 1 3 d SR . .
N2 N 0.6667 0.3333 -0.0226(2) 0.034(3) Uani 1 3 d S . .
C3 C 0.6662(10) 0.4372(9) 0.02948(16) 0.040(2) Uani 1 1 d . . .
H3A H 0.5983 0.4376 0.0245 0.048 Uiso 1 1 calc R . .
H3B H 0.7332 0.5059 0.0243 0.048 Uiso 1 1 calc R . .
C4 C 0.6671(11) 0.4371(9) 0.05332(17) 0.040(2) Uani 1 1 d . . .
H4A H 0.7350 0.5054 0.0583 0.048 Uiso 1 1 calc R . .
H4B H 0.6002 0.4388 0.0585 0.048 Uiso 1 1 calc R . .
C2 C 0.7718(9) 0.4378(9) -0.03111(16) 0.039(2) Uani 1 1 d . . .
H2A H 0.7761 0.5068 -0.0254 0.047 Uiso 1 1 calc R . .
H2B H 0.8403 0.4363 -0.0268 0.047 Uiso 1 1 calc R . .
C1 C 0.7668(11) 0.4399(11) -0.0544(2) 0.052(3) Uani 1 1 d . . .
H1A H 0.8371 0.4477 -0.0602 0.063 Uiso 1 1 calc R . .
H1B H 0.7613 0.5060 -0.0588 0.063 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ag3 I3 Ag3' 43.49(10) . 32_554
Ag3 I3 Ag3 70.99(15) . 32_554
Ag3' I3 Ag3 40.32(9) 32_554 32_554
Ag3 I3 Ag1 97.14(9) . .
Ag3' I3 Ag1 96.96(6) 32_554 .
Ag3 I3 Ag1 61.54(8) 32_554 .
Ag3 I3 Ag3' 40.40(10) . .
Ag3' I3 Ag3' 71.20(9) 32_554 .
Ag3 I3 Ag3' 72.48(10) 32_554 .
Ag1 I3 Ag3' 61.93(5) . .
Ag3' I2 Ag1 99.95(6) . 2_655
Ag3' I2 Ag3 42.54(9) . 33_544
Ag1 I2 Ag3 62.63(8) 2_655 33_544
Ag3' I2 Ag2 97.38(7) . .
Ag1 I2 Ag2 64.90(3) 2_655 .
Ag3 I2 Ag2 98.05(9) 33_544 .
Ag3' I2 Ag1 61.99(5) . .
Ag1 I2 Ag1 121.37(5) 2_655 .
Ag3 I2 Ag1 99.39(9) 33_544 .
Ag2 I2 Ag1 63.51(3) . .
Ag1 I1 Ag1 130.01(7) . 12_554
I1 Ag1 I2 110.29(5) . 3_665
I1 Ag1 I3 106.88(4) . .
I2 Ag1 I3 113.20(5) 3_665 .
I1 Ag1 Ag3 146.18(9) . 32_554
I2 Ag1 Ag3 58.62(9) 3_665 32_554
I3 Ag1 Ag3 59.45(9) . 32_554
I1 Ag1 I2 97.68(4) . .
I2 Ag1 I2 116.22(5) 3_665 .
I3 Ag1 I2 111.11(5) . .
Ag3 Ag1 I2 116.00(9) 32_554 .
I1 Ag1 Ag3' 132.36(7) . .
I2 Ag1 Ag3' 117.00(7) 3_665 .
I3 Ag1 Ag3' 59.42(5) . .
Ag3 Ag1 Ag3' 70.60(10) 32_554 .
I2 Ag1 Ag3' 56.68(5) . .
I1 Ag1 Ag2 109.47(6) . .
I2 Ag1 Ag2 58.96(3) 3_665 .
I3 Ag1 Ag2 143.09(6) . .
Ag3 Ag1 Ag2 92.08(9) 32_554 .
I2 Ag1 Ag2 57.87(3) . .
Ag3' Ag1 Ag2 90.61(6) . .
N1 Ag2 I2 104.24(4) . .
N1 Ag2 I2 104.24(4) . 2_655
I2 Ag2 I2 114.16(3) . 2_655
N1 Ag2 I2 104.24(4) . 3_665
I2 Ag2 I2 114.16(3) . 3_665
I2 Ag2 I2 114.16(3) 2_655 3_665
N1 Ag2 Ag1 109.63(4) . 2_655
I2 Ag2 Ag1 56.14(3) . 2_655
I2 Ag2 Ag1 58.62(3) 2_655 2_655
I2 Ag2 Ag1 146.11(8) 3_665 2_655
N1 Ag2 Ag1 109.63(4) . .
I2 Ag2 Ag1 58.62(3) . .
I2 Ag2 Ag1 146.11(8) 2_655 .
I2 Ag2 Ag1 56.14(3) 3_665 .
Ag1 Ag2 Ag1 109.31(4) 2_655 .
N1 Ag2 Ag1 109.63(4) . 3_665
I2 Ag2 Ag1 146.11(8) . 3_665
I2 Ag2 Ag1 56.14(3) 2_655 3_665
I2 Ag2 Ag1 58.62(3) 3_665 3_665
Ag1 Ag2 Ag1 109.31(4) 2_655 3_665
Ag1 Ag2 Ag1 109.31(4) . 3_665
Ag3 I4 Ag3 111.35(7) 32_554 31_654
Ag3 I4 Ag3 68.65(7) 32_554 .
Ag3 I4 Ag3 180.0 31_654 .
Ag3 I4 Ag3 180.0 32_554 2_655
Ag3 I4 Ag3 68.65(7) 31_654 2_655
Ag3 I4 Ag3 111.34(7) . 2_655
Ag3 I4 Ag3 68.66(7) 32_554 3_665
Ag3 I4 Ag3 68.66(7) 31_654 3_665
Ag3 I4 Ag3 111.34(7) . 3_665
Ag3 I4 Ag3 111.34(7) 2_655 3_665
Ag3 I4 Ag3 111.35(7) 32_554 33_544
Ag3 I4 Ag3 111.35(7) 31_654 33_544
Ag3 I4 Ag3 68.65(7) . 33_544
Ag3 I4 Ag3 68.65(7) 2_655 33_544
Ag3 I4 Ag3 179.996(1) 3_665 33_544
Ag3 I4 Ag3' 140.65(9) 32_554 2_655
Ag3 I4 Ag3' 41.31(10) 31_654 2_655
Ag3 I4 Ag3' 138.69(10) . 2_655
Ag3 I4 Ag3' 39.35(9) 2_655 2_655
Ag3 I4 Ag3' 107.83(9) 3_665 2_655
Ag3 I4 Ag3' 72.17(9) 33_544 2_655
Ag3 I4 Ag3' 72.17(9) 32_554 .
Ag3 I4 Ag3' 140.65(9) 31_654 .
Ag3 I4 Ag3' 39.35(9) . .
Ag3 I4 Ag3' 107.83(9) 2_655 .
Ag3 I4 Ag3' 138.69(10) 3_665 .
Ag3 I4 Ag3' 41.31(10) 33_544 .
Ag3' I4 Ag3' 110.59(4) 2_655 .
Ag3 I4 Ag3' 41.31(10) 32_554 3_665
Ag3 I4 Ag3' 72.17(9) 31_654 3_665
Ag3 I4 Ag3' 107.83(9) . 3_665
Ag3 I4 Ag3' 138.69(10) 2_655 3_665
Ag3 I4 Ag3' 39.35(9) 3_665 3_665
Ag3 I4 Ag3' 140.65(9) 33_544 3_665
Ag3' I4 Ag3' 110.59(4) 2_655 3_665
Ag3' I4 Ag3' 110.59(4) . 3_665
Ag3 I4 Ag3' 107.83(9) 32_554 31_654
Ag3 I4 Ag3' 39.35(9) 31_654 31_654
Ag3 I4 Ag3' 140.64(9) . 31_654
Ag3 I4 Ag3' 72.17(9) 2_655 31_654
Ag3 I4 Ag3' 41.31(10) 3_665 31_654
Ag3 I4 Ag3' 138.69(10) 33_544 31_654
Ag3' I4 Ag3' 69.41(4) 2_655 31_654
Ag3' I4 Ag3' 179.997(1) . 31_654
Ag3' I4 Ag3' 69.42(4) 3_665 31_654
Ag3 I4 Ag3' 39.35(9) 32_554 32_554
Ag3 I4 Ag3' 138.70(10) 31_654 32_554
Ag3 I4 Ag3' 41.30(10) . 32_554
Ag3 I4 Ag3' 140.64(9) 2_655 32_554
Ag3 I4 Ag3' 72.17(9) 3_665 32_554
Ag3 I4 Ag3' 107.83(9) 33_544 32_554
Ag3' I4 Ag3' 180.0 2_655 32_554
Ag3' I4 Ag3' 69.41(4) . 32_554
Ag3' I4 Ag3' 69.42(4) 3_665 32_554
Ag3' I4 Ag3' 110.59(4) 31_654 32_554
Ag3 I4 Ag3' 138.69(10) 32_554 33_544
Ag3 I4 Ag3' 107.83(9) 31_654 33_544
Ag3 I4 Ag3' 72.17(9) . 33_544
Ag3 I4 Ag3' 41.31(10) 2_655 33_544
Ag3 I4 Ag3' 140.64(9) 3_665 33_544
Ag3 I4 Ag3' 39.35(9) 33_544 33_544
Ag3' I4 Ag3' 69.41(4) 2_655 33_544
Ag3' I4 Ag3' 69.41(4) . 33_544
Ag3' I4 Ag3' 179.997(1) 3_665 33_544
Ag3' I4 Ag3' 110.58(4) 31_654 33_544
Ag3' I4 Ag3' 110.58(4) 32_554 33_544
Ag3 Ag3' Ag3 109.78(19) . 33_544
Ag3 Ag3' I3 72.87(13) . 33_544
Ag3 Ag3' I3 67.55(12) 33_544 33_544
Ag3 Ag3' I2 174.33(17) . .
Ag3 Ag3' I2 69.31(13) 33_544 .
I3 Ag3' I2 111.26(9) 33_544 .
Ag3 Ag3' I3 65.73(13) . .
Ag3 Ag3' I3 173.22(17) 33_544 .
I3 Ag3' I3 114.44(8) 33_544 .
I2 Ag3' I3 114.61(8) . .
Ag3 Ag3' I4 70.36(14) . .
Ag3 Ag3' I4 69.38(13) 33_544 .
I3 Ag3' I4 107.11(7) 33_544 .
I2 Ag3' I4 104.35(8) . .
I3 Ag3' I4 103.96(8) . .
Ag3 Ag3' Ag1 116.31(16) . .
Ag3 Ag3' Ag1 122.05(14) 33_544 .
I3 Ag3' Ag1 158.14(10) 33_544 .
I2 Ag3' Ag1 61.32(5) . .
I3 Ag3' Ag1 58.64(5) . .
I4 Ag3' Ag1 94.74(7) . .
Ag3 Ag3' Ag3' 35.26(14) . 32_554
Ag3 Ag3' Ag3' 120.64(14) 33_544 32_554
I3 Ag3' Ag3' 107.88(11) 33_544 32_554
I2 Ag3' Ag3' 140.01(9) . 32_554
I3 Ag3' Ag3' 52.70(7) . 32_554
I4 Ag3' Ag3' 55.29(2) . 32_554
Ag1 Ag3' Ag3' 84.63(7) . 32_554
Ag3 Ag3' Ag3' 76.34(15) . 33_544
Ag3 Ag3' Ag3' 33.44(11) 33_544 33_544
I3 Ag3' Ag3' 56.10(8) 33_544 33_544
I2 Ag3' Ag3' 102.52(8) . 33_544
I3 Ag3' Ag3' 141.60(11) . 33_544
I4 Ag3' Ag3' 55.29(2) . 33_544
Ag1 Ag3' Ag3' 143.27(8) . 33_544
Ag3' Ag3' Ag3' 92.42(9) 32_554 33_544
Ag3' Ag3 Ag3' 111.3(2) . 32_554
Ag3' Ag3 I3 73.87(13) . .
Ag3' Ag3 I3 68.96(12) 32_554 .
Ag3' Ag3 I2 173.3(2) . 32_554
Ag3' Ag3 I2 68.15(13) 32_554 32_554
I3 Ag3 I2 111.40(14) . 32_554
Ag3' Ag3 I3 66.81(14) . 33_544
Ag3' Ag3 I3 173.3(2) 32_554 33_544
I3 Ag3 I3 115.63(14) . 33_544
I2 Ag3 I3 112.93(12) 32_554 33_544
Ag3' Ag3 I4 70.29(14) . .
Ag3' Ag3 I4 69.31(13) 32_554 .
I3 Ag3 I4 107.81(12) . .
I2 Ag3 I4 103.75(13) 32_554 .
I3 Ag3 I4 104.20(13) 33_544 .
Ag3' Ag3 Ag1 117.94(19) . 33_544
Ag3' Ag3 Ag1 118.87(17) 32_554 33_544
I3 Ag3 Ag1 156.83(16) . 33_544
I2 Ag3 Ag1 58.75(8) 32_554 33_544
I3 Ag3 Ag1 59.02(8) 33_544 33_544
I4 Ag3 Ag1 95.20(11) . 33_544
Ag3' Ag3 Ag3 77.13(17) . 32_554
Ag3' Ag3 Ag3 34.18(9) 32_554 32_554
I3 Ag3 Ag3 56.46(13) . 32_554
I2 Ag3 Ag3 102.16(14) 32_554 32_554
I3 Ag3 Ag3 143.42(18) 33_544 32_554
I4 Ag3 Ag3 55.67(3) . 32_554
Ag1 Ag3 Ag3 142.54(13) 33_544 32_554
Ag3' Ag3 Ag3 36.05(16) . 33_544
Ag3' Ag3 Ag3 121.95(15) 32_554 33_544
I3 Ag3 Ag3 109.76(19) . 33_544
I2 Ag3 Ag3 138.16(15) 32_554 33_544
I3 Ag3 Ag3 52.55(11) 33_544 33_544
I4 Ag3 Ag3 55.67(3) . 33_544
Ag1 Ag3 Ag3 85.18(11) 33_544 33_544
Ag3 Ag3 Ag3 94.15(16) 32_554 33_544
C4 N4 C4 108.4(6) 3_665 2_655
C4 N4 C4 108.4(6) 3_665 .
C4 N4 C4 108.4(6) 2_655 .
C1 N1 C1 107.8(7) 3_665 .
C1 N1 C1 107.8(7) 3_665 2_655
C1 N1 C1 107.8(7) . 2_655
C1 N1 Ag2 111.1(7) 3_665 .
C1 N1 Ag2 111.1(7) . .
C1 N1 Ag2 111.1(7) 2_655 .
C3 N3 C3 108.6(7) 3_665 2_655
C3 N3 C3 108.6(7) 3_665 .
C3 N3 C3 108.6(7) 2_655 .
C2 N2 C2 107.8(7) 3_665 .
C2 N2 C2 107.8(7) 3_665 2_655
C2 N2 C2 107.8(7) . 2_655
N3 C3 C4 110.0(9) . .
N4 C4 C3 110.8(9) . .
C1 C2 N2 110.3(9) . .
C2 C1 N1 111.7(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
I3 Ag3 2.747(4) .
I3 Ag3' 2.774(2) 32_554
I3 Ag3 2.884(4) 32_554
I3 Ag1 2.8710(15) .
I3 Ag3' 2.895(2) .
I2 Ag3' 2.808(2) .
I2 Ag1 2.8343(14) 2_655
I2 Ag3 2.830(4) 33_544
I2 Ag2 2.9246(9) .
I2 Ag1 2.9481(14) .
I1 Ag1 2.7693(13) .
I1 Ag1 2.7695(13) 12_554
Ag1 I2 2.8343(14) 3_665
Ag1 Ag3 2.944(4) 32_554
Ag1 Ag3' 2.967(2) .
Ag1 Ag2 3.0908(14) .
Ag2 N1 2.395(14) .
Ag2 I2 2.9246(9) 2_655
Ag2 I2 2.9246(9) 3_665
Ag2 Ag1 3.0908(14) 2_655
Ag2 Ag1 3.0908(14) 3_665
I4 Ag3 2.900(4) 32_554
I4 Ag3 2.900(4) 31_654
I4 Ag3 2.900(4) .
I4 Ag3 2.900(4) 2_655
I4 Ag3 2.900(4) 3_665
I4 Ag3 2.900(4) 33_544
I4 Ag3' 2.899(3) 2_655
I4 Ag3' 2.899(3) .
I4 Ag3' 2.899(3) 3_665
I4 Ag3' 2.899(3) 31_654
I4 Ag3' 2.899(3) 32_554
I4 Ag3' 2.899(3) 33_544
Ag3' Ag3 1.953(5) .
Ag3' Ag3 2.046(5) 33_544
Ag3' I3 2.774(2) 33_544
Ag3' Ag3' 3.301(3) 32_554
Ag3' Ag3' 3.301(3) 33_544
Ag3 Ag3' 2.045(5) 32_554
Ag3 I2 2.830(4) 32_554
Ag3 I3 2.884(4) 33_544
Ag3 Ag1 2.944(4) 33_544
Ag3 Ag3 3.271(5) 32_554
Ag3 Ag3 3.271(5) 33_544
N4 C4 1.486(11) 3_665
N4 C4 1.486(11) 2_655
N4 C4 1.486(11) .
N1 C1 1.491(13) 3_665
N1 C1 1.491(13) .
N1 C1 1.491(13) 2_655
N3 C3 1.492(12) 3_665
N3 C3 1.492(12) 2_655
N3 C3 1.492(12) .
N2 C2 1.511(11) 3_665
N2 C2 1.511(11) .
N2 C2 1.511(11) 2_655
C3 C4 1.519(14) .
C2 C1 1.484(16) .
