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#$Date: 2021-12-09 12:23:57 +0200 (Thu, 09 Dec 2021) $
#$Revision: 271307 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/56/1565632.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1565632
loop_
_publ_author_name
'Sánchez-Férez, Francisco'
'Pou, Roger'
'Bayés-García, Laura'
'Font-Bardia, Mercè'
'Pons, Josefina'
'Ayllón, José A.'
_publ_section_title
;
 Benzoate substituents effects on the structure of Zn(II) complexes and 1D
 4,4′-bipyridine derived coordination polymers
;
_journal_name_full               'Inorganica Chimica Acta'
_journal_page_first              119218
_journal_paper_doi               10.1016/j.ica.2019.119218
_journal_volume                  500
_journal_year                    2020
_chemical_formula_moiety         '2(C24 H18 N2 O8 Zn), 2(C10 H8 N2), C H4 O'
_chemical_formula_sum            'C69 H56 N8 O17 Zn2'
_chemical_formula_weight         1399.95
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                96.653(2)
_cell_angle_beta                 102.794(2)
_cell_angle_gamma                111.997(2)
_cell_formula_units_Z            1
_cell_length_a                   10.6316(6)
_cell_length_b                   11.6986(7)
_cell_length_c                   14.0895(8)
_cell_measurement_reflns_used    9879
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      30.05
_cell_measurement_theta_min      2.22
_cell_volume                     1545.70(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'D8 Venture'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0476
_diffrn_reflns_av_unetI/netI     0.0283
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            75712
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.097
_diffrn_reflns_theta_min         1.925
_diffrn_source                   microfocus
_exptl_absorpt_coefficient_mu    0.858
_exptl_absorpt_correction_T_max  0.7460
_exptl_absorpt_correction_T_min  0.6566
_exptl_absorpt_correction_type   multi-scan'
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.504
_exptl_crystal_description       prism
_exptl_crystal_F_000             722
_exptl_crystal_size_max          0.329
_exptl_crystal_size_mid          0.091
_exptl_crystal_size_min          0.075
_refine_diff_density_max         1.370
_refine_diff_density_min         -0.823
_refine_diff_density_rms         0.077
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     438
_refine_ls_number_reflns         9067
_refine_ls_number_restraints     7
_refine_ls_restrained_S_all      1.080
_refine_ls_R_factor_all          0.0458
_refine_ls_R_factor_gt           0.0371
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0663P)²+0.2950P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0990
_refine_ls_wR_factor_ref         0.1038
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                7698
_reflns_number_total             9067
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            cifcompound4.cif
_cod_data_source_block           mo_C20VB231_0m_aa
_cod_database_code               1565632
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn1 Zn 0.35454(2) 0.80584(2) 0.36937(2) 0.01328(6) Uani 1 1 d . . . . .
O1 O 0.46878(11) 0.75041(10) 0.46726(8) 0.0159(2) Uani 1 1 d . . . . .
O2 O 0.25112(11) 0.61897(10) 0.45953(8) 0.0172(2) Uani 1 1 d . . . . .
O3 O 0.76129(11) 0.66657(11) 0.77422(8) 0.0208(2) Uani 1 1 d . . . . .
H3A H 0.805150 0.737900 0.763497 0.031 Uiso 1 1 calc R U . . .
O4 O 0.31931(11) 0.30943(10) 0.65621(9) 0.0204(2) Uani 1 1 d . . . . .
H4A H 0.366189 0.275963 0.689393 0.024 Uiso 1 1 calc R U . . .
O5 O 0.49504(11) 0.96141(10) 0.34862(8) 0.0171(2) Uani 1 1 d . . . . .
O6 O 0.55518(12) 0.82782(10) 0.26313(8) 0.0183(2) Uani 1 1 d . . . . .
O7 O 0.89216(14) 1.39171(11) 0.39746(11) 0.0312(3) Uani 1 1 d . . . . .
H7A H 0.842889 1.392446 0.436428 0.047 Uiso 1 1 calc R U . . .
O8 O 1.03997(15) 1.11016(12) 0.23668(12) 0.0353(3) Uani 1 1 d . . . . .
H8A H 1.008282 1.036706 0.201770 0.042 Uiso 1 1 calc R U . . .
N1 N 0.22246(12) 0.87501(11) 0.41480(9) 0.0146(2) Uani 1 1 d . . . . .
N2 N 0.22447(13) 0.68834(12) 0.23705(9) 0.0172(2) Uani 1 1 d . . . . .
C1 C 0.38284(15) 0.65958(13) 0.49413(10) 0.0139(3) Uani 1 1 d . . . . .
C2 C 0.44310(15) 0.60148(13) 0.57178(10) 0.0136(3) Uani 1 1 d . . . . .
C3 C 0.58218(15) 0.66565(13) 0.63388(11) 0.0148(3) Uani 1 1 d . . . . .
H3 H 0.641856 0.746141 0.626682 0.018 Uiso 1 1 calc R U . . .
C4 C 0.63104(15) 0.60887(14) 0.70639(11) 0.0152(3) Uani 1 1 d . . . . .
C5 C 0.54549(16) 0.48808(14) 0.71415(11) 0.0161(3) Uani 1 1 d . . . . .
H5 H 0.580895 0.448880 0.762404 0.019 Uiso 1 1 calc R U . . .
C6 C 0.40802(15) 0.42554(13) 0.65069(11) 0.0153(3) Uani 1 1 d . . . . .
C7 C 0.35530(15) 0.48270(13) 0.58022(11) 0.0150(3) Uani 1 1 d . . . . .
H7 H 0.260528 0.441093 0.538412 0.018 Uiso 1 1 calc R U . . .
C8 C 0.57852(15) 0.93696(14) 0.30484(10) 0.0146(3) Uani 1 1 d . . . . .
C9 C 0.71088(16) 1.04676(14) 0.30683(11) 0.0163(3) Uani 1 1 d . . . . .
C10 C 0.73401(16) 1.16917(14) 0.35003(11) 0.0178(3) Uani 1 1 d . . . . .
H10 H 0.664710 1.183966 0.375689 0.021 Uiso 1 1 calc R U . . .
C11 C 0.86070(17) 1.26962(15) 0.35495(12) 0.0213(3) Uani 1 1 d . . . . .
C12 C 0.96077(18) 1.24810(16) 0.31552(13) 0.0246(3) Uani 1 1 d . . . . .
H12 H 1.046024 1.316898 0.318138 0.030 Uiso 1 1 calc R U . . .
C13 C 0.93578(18) 1.12551(15) 0.27217(13) 0.0227(3) Uani 1 1 d . . . . .
C14 C 0.81080(17) 1.02343(15) 0.26729(12) 0.0201(3) Uani 1 1 d . . . . .
H14 H 0.793939 0.939861 0.237741 0.024 Uiso 1 1 calc R U . . .
C15 C 0.26200(15) 1.00021(14) 0.43995(11) 0.0155(3) Uani 1 1 d . . . . .
H15 H 0.350926 1.055163 0.434374 0.019 Uiso 1 1 calc R U . . .
C16 C 0.17842(16) 1.05259(14) 0.47370(11) 0.0167(3) Uani 1 1 d . . . . .
H16 H 0.210860 1.141797 0.491531 0.020 Uiso 1 1 calc R U . . .
C17 C 0.04623(15) 0.97404(13) 0.48152(10) 0.0144(3) Uani 1 1 d . . . . .
C18 C 0.00573(16) 0.84386(15) 0.45302(13) 0.0219(3) Uani 1 1 d . . . . .
H18 H -0.083790 0.786322 0.455729 0.026 Uiso 1 1 calc R U . . .
C19 C 0.09529(16) 0.79881(14) 0.42103(13) 0.0216(3) Uani 1 1 d . . . . .
H19 H 0.065685 0.709989 0.402595 0.026 Uiso 1 1 calc R U . . .
C20 C 0.22023(19) 0.73789(16) 0.15563(12) 0.0284(4) Uani 1 1 d . . . . .
H20 H 0.278782 0.824542 0.162478 0.034 Uiso 1 1 calc R U . . .
C21 C 0.13333(19) 0.66672(17) 0.06219(13) 0.0291(4) Uani 1 1 d . . . . .
H21 H 0.132425 0.704946 0.006267 0.035 Uiso 1 1 calc R U . . .
C22 C 0.04719(16) 0.53933(14) 0.04971(11) 0.0176(3) Uani 1 1 d . . . . .
C23 C 0.05215(19) 0.49039(15) 0.13505(13) 0.0261(4) Uani 1 1 d . . . . .
H23 H -0.005407 0.404144 0.130663 0.031 Uiso 1 1 calc R U . . .
C24 C 0.14086(18) 0.56722(15) 0.22639(12) 0.0232(3) Uani 1 1 d . . . . .
H24 H 0.142110 0.532017 0.283877 0.028 Uiso 1 1 calc R U . . .
N3 N 0.7875(3) 0.6347(3) 0.08669(17) 0.0652(7) Uani 1 1 d . U . . .
N4 N 0.3368(4) 0.0029(3) 0.06935(19) 0.0804(9) Uani 1 1 d . . . . .
C25 C 0.8051(4) 0.6032(5) 0.1690(3) 0.0825(12) Uani 1 1 d . U . . .
H25 H 0.869461 0.660538 0.229097 0.099 Uiso 1 1 calc R U . . .
C26 C 0.7131(4) 0.4635(4) 0.1646(2) 0.0734(11) Uani 1 1 d . . . . .
H26 H 0.719813 0.429335 0.222520 0.088 Uiso 1 1 calc R U . . .
C27 C 0.6238(3) 0.3924(3) 0.07630(17) 0.0540(6) Uani 1 1 d D U . . .
C28 C 0.6122(3) 0.4328(3) -0.00935(18) 0.0557(7) Uani 1 1 d . . . . .
H28 H 0.549566 0.379055 -0.071323 0.067 Uiso 1 1 calc R U . . .
C29 C 0.7049(3) 0.5680(3) 0.0002(2) 0.0610(7) Uani 1 1 d . U . . .
H29 H 0.703181 0.604510 -0.056641 0.073 Uiso 1 1 calc R U . . .
C30 C 0.5255(3) 0.2534(3) 0.07157(17) 0.0558(6) Uani 1 1 d D U . . .
C31 C 0.4650(4) 0.1649(3) -0.0158(2) 0.0696(9) Uani 1 1 d . . . . .
H31 H 0.481511 0.185905 -0.076440 0.083 Uiso 1 1 calc R U . . .
C32 C 0.3778(5) 0.0421(4) -0.0131(2) 0.0882(12) Uani 1 1 d . . . . .
H32 H 0.343162 -0.020561 -0.073077 0.106 Uiso 1 1 calc R U . . .
C33 C 0.4031(4) 0.0995(3) 0.1521(2) 0.0681(8) Uani 1 1 d . U . . .
H33 H 0.383156 0.080477 0.212344 0.082 Uiso 1 1 calc R U . . .
C34 C 0.4969(4) 0.2231(3) 0.15795(19) 0.0598(7) Uani 1 1 d . U . . .
H34 H 0.539271 0.283923 0.219361 0.072 Uiso 1 1 calc R U . . .
O1W O 0.9619(4) 0.8855(3) 0.12176(19) 0.0408(6) Uani 0.5 1 d D . P A -1
H1WO H 0.897344 0.814015 0.115845 0.049 Uiso 0.5 1 calc R U P A -1
C1W C 0.9738(6) 0.9058(4) 0.0226(3) 0.0408(6) Uani 0.5 1 d D . P A -1
H1WA H 0.901079 0.833007 -0.028603 0.061 Uiso 0.5 1 calc R U P A -1
H1WB H 1.067791 0.915598 0.018052 0.061 Uiso 0.5 1 calc R U P A -1
H1WC H 0.960392 0.982337 0.012134 0.061 Uiso 0.5 1 calc R U P A -1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Zn1 O5 103.78(4) . .
O1 Zn1 N2 121.25(5) . .
O5 Zn1 N2 110.99(5) . .
O1 Zn1 N1 118.00(5) . .
O5 Zn1 N1 100.25(5) . .
N2 Zn1 N1 100.78(5) . .
C1 O1 Zn1 107.15(9) . .
C4 O3 H3A 109.5 . .
C6 O4 H4A 109.5 . .
C8 O5 Zn1 111.36(9) . .
C11 O7 H7A 109.5 . .
C13 O8 H8A 109.5 . .
C19 N1 C15 117.88(13) . .
C19 N1 Zn1 122.02(10) . .
C15 N1 Zn1 120.10(10) . .
C24 N2 C20 118.24(14) . .
C24 N2 Zn1 124.35(11) . .
C20 N2 Zn1 117.39(10) . .
O2 C1 O1 122.54(13) . .
O2 C1 C2 119.25(12) . .
O1 C1 C2 118.20(12) . .
C7 C2 C3 121.44(13) . .
C7 C2 C1 117.59(13) . .
C3 C2 C1 120.97(12) . .
C4 C3 C2 118.48(13) . .
C4 C3 H3 120.8 . .
C2 C3 H3 120.8 . .
O3 C4 C3 123.01(13) . .
O3 C4 C5 116.19(13) . .
C3 C4 C5 120.79(13) . .
C6 C5 C4 119.59(13) . .
C6 C5 H5 120.2 . .
C4 C5 H5 120.2 . .
O4 C6 C7 117.33(13) . .
O4 C6 C5 122.16(13) . .
C7 C6 C5 120.48(13) . .
C2 C7 C6 119.14(13) . .
C2 C7 H7 120.4 . .
C6 C7 H7 120.4 . .
O6 C8 O5 123.17(13) . .
O6 C8 C9 119.99(13) . .
O5 C8 C9 116.82(13) . .
C10 C9 C14 121.29(14) . .
C10 C9 C8 119.86(13) . .
C14 C9 C8 118.83(13) . .
C9 C10 C11 118.98(14) . .
C9 C10 H10 120.5 . .
C11 C10 H10 120.5 . .
O7 C11 C12 117.08(14) . .
O7 C11 C10 122.50(14) . .
C12 C11 C10 120.42(15) . .
C11 C12 C13 119.89(15) . .
C11 C12 H12 120.1 . .
C13 C12 H12 120.1 . .
O8 C13 C12 117.09(14) . .
O8 C13 C14 122.10(15) . .
C12 C13 C14 120.79(15) . .
C13 C14 C9 118.61(14) . .
C13 C14 H14 120.7 . .
C9 C14 H14 120.7 . .
N1 C15 C16 122.66(13) . .
N1 C15 H15 118.7 . .
C16 C15 H15 118.7 . .
C15 C16 C17 119.96(13) . .
C15 C16 H16 120.0 . .
C17 C16 H16 120.0 . .
C16 C17 C18 116.49(13) . .
C16 C17 C17 121.83(16) . 2_576
C18 C17 C17 121.69(16) . 2_576
C19 C18 C17 120.20(14) . .
C19 C18 H18 119.9 . .
C17 C18 H18 119.9 . .
N1 C19 C18 122.80(14) . .
N1 C19 H19 118.6 . .
C18 C19 H19 118.6 . .
N2 C20 C21 122.06(15) . .
N2 C20 H20 119.0 . .
C21 C20 H20 119.0 . .
C20 C21 C22 120.28(15) . .
C20 C21 H21 119.9 . .
C22 C21 H21 119.9 . .
C23 C22 C21 116.69(14) . .
C23 C22 C22 121.86(17) . 2_565
C21 C22 C22 121.44(18) . 2_565
C24 C23 C22 120.00(15) . .
C24 C23 H23 120.0 . .
C22 C23 H23 120.0 . .
N2 C24 C23 122.71(15) . .
N2 C24 H24 118.6 . .
C23 C24 H24 118.6 . .
C25 N3 C29 129.6(4) . .
C33 N4 C32 110.8(3) . .
N3 C25 C26 114.3(4) . .
N3 C25 H25 122.8 . .
C26 C25 H25 122.8 . .
C27 C26 C25 117.6(3) . .
C27 C26 H26 121.2 . .
C25 C26 H26 121.2 . .
C26 C27 C28 124.6(3) . .
C26 C27 C30 118.2(3) . .
C28 C27 C30 117.2(3) . .
C27 C28 C29 114.9(3) . .
C27 C28 H28 122.5 . .
C29 C28 H28 122.5 . .
N3 C29 C28 118.9(3) . .
N3 C29 H29 120.5 . .
C28 C29 H29 120.5 . .
C31 C30 C34 120.7(3) . .
C31 C30 C27 121.5(2) . .
C34 C30 C27 117.8(3) . .
C30 C31 C32 117.6(3) . .
C30 C31 H31 121.2 . .
C32 C31 H31 121.2 . .
N4 C32 C31 126.1(3) . .
N4 C32 H32 116.9 . .
C31 C32 H32 116.9 . .
N4 C33 C34 127.2(3) . .
N4 C33 H33 116.4 . .
C34 C33 H33 116.4 . .
C30 C34 C33 117.5(3) . .
C30 C34 H34 121.3 . .
C33 C34 H34 121.3 . .
C1W O1W H1WO 109.5 . .
O1W C1W H1WA 109.5 . .
O1W C1W H1WB 109.5 . .
H1WA C1W H1WB 109.5 . .
O1W C1W H1WC 109.5 . .
H1WA C1W H1WC 109.5 . .
H1WB C1W H1WC 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Zn1 O1 1.9630(11) .
Zn1 O5 1.9771(11) .
Zn1 N2 2.0292(13) .
Zn1 N1 2.0410(12) .
O1 C1 1.2753(17) .
O2 C1 1.2530(18) .
O3 C4 1.3604(18) .
O3 H3A 0.8400 .
O4 C6 1.3556(17) .
O4 H4A 0.8400 .
O5 C8 1.2813(18) .
O6 C8 1.2494(18) .
O7 C11 1.3659(19) .
O7 H7A 0.8400 .
O8 C13 1.372(2) .
O8 H8A 0.8400 .
N1 C19 1.3409(19) .
N1 C15 1.3416(19) .
N2 C24 1.330(2) .
N2 C20 1.343(2) .
C1 C2 1.502(2) .
C2 C7 1.390(2) .
C2 C3 1.400(2) .
C3 C4 1.391(2) .
C3 H3 0.9500 .
C4 C5 1.398(2) .
C5 C6 1.393(2) .
C5 H5 0.9500 .
C6 C7 1.391(2) .
C7 H7 0.9500 .
C8 C9 1.500(2) .
C9 C10 1.396(2) .
C9 C14 1.399(2) .
C10 C11 1.398(2) .
C10 H10 0.9500 .
C11 C12 1.391(2) .
C12 C13 1.393(2) .
C12 H12 0.9500 .
C13 C14 1.396(2) .
C14 H14 0.9500 .
C15 C16 1.385(2) .
C15 H15 0.9500 .
C16 C17 1.399(2) .
C16 H16 0.9500 .
C17 C18 1.399(2) .
C17 C17 1.486(3) 2_576
C18 C19 1.378(2) .
C18 H18 0.9500 .
C19 H19 0.9500 .
C20 C21 1.382(2) .
C20 H20 0.9500 .
C21 C22 1.391(2) .
C21 H21 0.9500 .
C22 C23 1.389(2) .
C22 C22 1.484(3) 2_565
C23 C24 1.383(2) .
C23 H23 0.9500 .
C24 H24 0.9500 .
N3 C25 1.253(4) .
N3 C29 1.287(4) .
N4 C33 1.367(4) .
N4 C32 1.396(4) .
C25 C26 1.544(6) .
C25 H25 0.9500 .
C26 C27 1.337(4) .
C26 H26 0.9500 .
C27 C28 1.343(3) .
C27 C30 1.553(4) .
C28 C29 1.489(5) .
C28 H28 0.9500 .
C29 H29 0.9500 .
C30 C31 1.363(4) .
C30 C34 1.372(3) .
C31 C32 1.399(5) .
C31 H31 0.9500 .
C32 H32 0.9500 .
C33 C34 1.395(5) .
C33 H33 0.9500 .
C34 H34 0.9500 .
O1W C1W 1.469(4) .
O1W H1WO 0.8400 .
C1W H1WA 0.9800 .
C1W H1WB 0.9800 .
C1W H1WC 0.9800 .
