#------------------------------------------------------------------------------
#$Date: 2024-02-04 13:34:59 +0200 (Sun, 04 Feb 2024) $
#$Revision: 289431 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/57/05/1570538.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1570538
loop_
_publ_author_name
'Hasebe, Shodai'
'Hagiwara, Yuki'
'Ueno, Takashi'
'Asahi, Toru'
'Koshima, Hideko'
_publ_section_title
;
 Negative to positive axial thermal expansion switching of an organic
 crystal: contribution to multistep photoactuation.
;
_journal_issue                   3
_journal_name_full               'Chemical science'
_journal_page_first              1088
_journal_page_last               1097
_journal_paper_doi               10.1039/d3sc04796b
_journal_volume                  15
_journal_year                    2024
_chemical_formula_moiety         'C21 H26 N2 O3'
_chemical_formula_sum            'C21 H26 N2 O3'
_chemical_formula_weight         354.44
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_date             2022-06-06
_audit_creation_method
;
Olex2 1.5
(compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498)
;
_audit_update_record
;
2023-08-31 deposited with the CCDC.	2023-12-11 downloaded from the CCDC.
;
_cell_angle_alpha                101.178(7)
_cell_angle_beta                 92.181(6)
_cell_angle_gamma                101.469(7)
_cell_formula_units_Z            2
_cell_length_a                   6.0399(7)
_cell_length_b                   10.3202(11)
_cell_length_c                   16.7772(18)
_cell_measurement_reflns_used    7707
_cell_measurement_temperature    296.75
_cell_measurement_theta_max      68
_cell_measurement_theta_min      4
_cell_volume                     1002.25(19)
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2014/6 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/4 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296.75
_diffrn_detector_area_resol_mean 10
_diffrn_measured_fraction_theta_full 0.977
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  RAPID
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54187
_diffrn_reflns_av_R_equivalents  0.0660
_diffrn_reflns_av_unetI/netI     0.0665
_diffrn_reflns_Laue_measured_fraction_full 0.977
_diffrn_reflns_Laue_measured_fraction_max 0.974
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            11147
_diffrn_reflns_point_group_measured_fraction_full 0.977
_diffrn_reflns_point_group_measured_fraction_max 0.974
_diffrn_reflns_theta_full        67.687
_diffrn_reflns_theta_max         68.105
_diffrn_reflns_theta_min         4.467
_exptl_absorpt_coefficient_mu    0.631
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.6204
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ABSCOR(Rigaku,1995)
_exptl_crystal_colour            'clear yellowish yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   yellowish
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.174
_exptl_crystal_description       prism
_exptl_crystal_F_000             380
_exptl_crystal_size_max          1
_exptl_crystal_size_mid          0.6
_exptl_crystal_size_min          0.3
_refine_diff_density_max         0.139
_refine_diff_density_min         -0.233
_refine_diff_density_rms         0.050
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.149
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     273
_refine_ls_number_reflns         3581
_refine_ls_number_restraints     72
_refine_ls_restrained_S_all      1.152
_refine_ls_R_factor_all          0.1222
_refine_ls_R_factor_gt           0.0797
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0650P)²+0.2154P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1820
_refine_ls_wR_factor_ref         0.2019
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2031
_reflns_number_total             3581
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3sc04796b3.cif
_cod_data_source_block           23point6degC
_cod_depositor_comments
'Adding full bibliography for 1570536--1570543.cif.'
_cod_database_code               1570538
_shelxl_version_number           2014/6
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   1
_shelx_estimated_absorpt_t_min   0.624
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups, All O(H) groups
2. Uiso/Uaniso restraints and constraints
C00I \\sim C00O \\sim C00P \\sim C00Q: within 2A with sigma of 0.04 and sigma
for terminal atoms of 0.08 within 2A
C00I \\sim C1 \\sim C00R \\sim C2: within 2A with sigma of 0.04 and sigma for
terminal atoms of 0.08 within 2A
3. Rigid body (RIGU) restrains
 C00I, C00P, C00O, C00Q
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C00I, C1, C00R, C2
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
4. Others
 Sof(C1)=Sof(H1A)=Sof(H1B)=Sof(H1C)=Sof(C2)=Sof(H2A)=Sof(H2B)=Sof(H2C)=
 Sof(C00R)=Sof(H00Y)=Sof(H)=Sof(HA)=1-FVAR(1)
 Sof(C00O)=Sof(H00P)=Sof(H00Q)=Sof(H00R)=Sof(C00P)=Sof(H00S)=Sof(H00T)=
 Sof(H00U)=Sof(C00Q)=Sof(H00V)=Sof(H00W)=Sof(H00X)=FVAR(1)
5.a Aromatic/amide H refined with riding coordinates:
 C009(H009), C00C(H00C), C00D(H00D), C00E(H00E), C00G(H00G), C00J(H00J),
 C00K(H00K)
5.b Idealised Me refined as rotating group:
 C00L(H00A,H00B,H00F), C00M(H00H,H00I,H00L), C00N(H00M,H00N,H00O), C00O(H00P,
 H00Q,H00R), C00P(H00S,H00T,H00U), C00Q(H00V,H00W,H00X), C1(H1A,H1B,H1C),
 C2(H2A,H2B,H2C), C00R(H00Y,H,HA)
5.c Idealised tetrahedral OH refined as rotating group:
 O001(H001)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O001 O 0.3523(4) 0.3982(2) 0.31641(13) 0.0769(7) Uani 1 1 d . . . . .
H001 H 0.2759 0.4422 0.3456 0.115 Uiso 1 1 calc R U . . .
N002 N 0.1896(4) 0.6061(2) 0.38120(15) 0.0684(7) Uani 1 1 d . . . . .
N003 N 0.1544(6) 0.9867(3) 0.60122(18) 0.0857(9) Uani 1 1 d . . . . .
O004 O 0.3558(5) 1.0291(3) 0.59768(17) 0.1192(10) Uani 1 1 d . . . . .
O005 O 0.0385(5) 1.0447(3) 0.64778(17) 0.1182(10) Uani 1 1 d . . . . .
C006 C 0.4615(5) 0.4743(3) 0.26664(17) 0.0609(8) Uani 1 1 d . . . . .
C007 C 0.4433(5) 0.6096(3) 0.27441(16) 0.0605(8) Uani 1 1 d . . . . .
C008 C 0.6911(5) 0.6367(3) 0.16613(17) 0.0616(8) Uani 1 1 d . . . . .
C009 C 0.3062(5) 0.6704(3) 0.33352(17) 0.0665(8) Uani 1 1 d . . . . .
H009 H 0.3026 0.7610 0.3371 0.080 Uiso 1 1 calc R U . . .
C00A C 0.5959(5) 0.4175(3) 0.20939(17) 0.0612(8) Uani 1 1 d . . . . .
C00B C 0.0698(5) 0.6757(3) 0.44009(17) 0.0632(8) Uani 1 1 d . . . . .
C00C C 0.5597(5) 0.6876(3) 0.22409(17) 0.0640(8) Uani 1 1 d . . . . .
H00C H 0.5479 0.7774 0.2300 0.077 Uiso 1 1 calc R U . . .
C00D C 0.1699(5) 0.7985(3) 0.48959(18) 0.0663(8) Uani 1 1 d . . . . .
H00D H 0.3186 0.8399 0.4843 0.080 Uiso 1 1 calc R U . . .
C00E C 0.7044(5) 0.5012(3) 0.16097(17) 0.0636(8) Uani 1 1 d . . . . .
H00E H 0.7928 0.4646 0.1221 0.076 Uiso 1 1 calc R U . . .
C00F C 0.0434(6) 0.8580(3) 0.54702(18) 0.0665(8) Uani 1 1 d . . . . .
C00G C -0.1515(6) 0.6163(3) 0.45000(19) 0.0727(9) Uani 1 1 d . . . . .
H00G H -0.2183 0.5328 0.4176 0.087 Uiso 1 1 calc R U . . .
C00H C 0.6216(5) 0.2703(3) 0.20028(19) 0.0685(8) Uani 1 1 d . . . . .
C00I C 0.8177(6) 0.7192(3) 0.10974(18) 0.0683(8) Uani 1 1 d . U . . .
C00J C -0.1763(6) 0.8023(4) 0.55682(19) 0.0749(9) Uani 1 1 d . . . . .
H00J H -0.2577 0.8458 0.5956 0.090 Uiso 1 1 calc R U . . .
C00K C -0.2734(6) 0.6793(4) 0.5072(2) 0.0798(10) Uani 1 1 d . . . . .
H00K H -0.4226 0.6388 0.5124 0.096 Uiso 1 1 calc R U . . .
C00L C 0.3899(6) 0.1734(3) 0.1786(2) 0.0909(11) Uani 1 1 d . . . . .
H00A H 0.2919 0.1925 0.2211 0.136 Uiso 1 1 calc R U . . .
H00B H 0.4087 0.0820 0.1730 0.136 Uiso 1 1 calc R U . . .
H00F H 0.3242 0.1852 0.1282 0.136 Uiso 1 1 calc R U . . .
C00M C 0.7291(6) 0.2497(3) 0.2801(2) 0.0903(11) Uani 1 1 d . . . . .
H00H H 0.8745 0.3098 0.2934 0.135 Uiso 1 1 calc R U . . .
H00I H 0.7472 0.1580 0.2736 0.135 Uiso 1 1 calc R U . . .
H00L H 0.6326 0.2682 0.3232 0.135 Uiso 1 1 calc R U . . .
C00N C 0.7764(6) 0.2334(3) 0.1333(2) 0.0974(12) Uani 1 1 d . . . . .
H00M H 0.7104 0.2408 0.0818 0.146 Uiso 1 1 calc R U . . .
H00N H 0.7942 0.1423 0.1307 0.146 Uiso 1 1 calc R U . . .
H00O H 0.9219 0.2938 0.1453 0.146 Uiso 1 1 calc R U . . .
C00O C 0.7693(11) 0.8597(5) 0.1209(4) 0.110(2) Uani 0.793(6) 1 d . U P A 1
H00P H 0.6100 0.8534 0.1096 0.165 Uiso 0.793(6) 1 calc R U P A 1
H00Q H 0.8526 0.9077 0.0841 0.165 Uiso 0.793(6) 1 calc R U P A 1
H00R H 0.8146 0.9073 0.1760 0.165 Uiso 0.793(6) 1 calc R U P A 1
C00P C 0.7458(10) 0.6479(5) 0.0209(3) 0.1009(19) Uani 0.793(6) 1 d . U P A 1
H00S H 0.7749 0.5583 0.0120 0.151 Uiso 0.793(6) 1 calc R U P A 1
H00T H 0.8306 0.6979 -0.0147 0.151 Uiso 0.793(6) 1 calc R U P A 1
H00U H 0.5870 0.6430 0.0097 0.151 Uiso 0.793(6) 1 calc R U P A 1
C00Q C 1.0708(8) 0.7312(6) 0.1258(4) 0.114(2) Uani 0.793(6) 1 d . U P A 1
H00V H 1.1172 0.7762 0.1813 0.171 Uiso 0.793(6) 1 calc R U P A 1
H00W H 1.1508 0.7824 0.0898 0.171 Uiso 0.793(6) 1 calc R U P A 1
H00X H 1.1043 0.6427 0.1165 0.171 Uiso 0.793(6) 1 calc R U P A 1
C1 C 0.645(3) 0.776(2) 0.0617(12) 0.093(5) Uani 0.207(6) 1 d . U P A 2
H1A H 0.5369 0.7027 0.0288 0.139 Uiso 0.207(6) 1 calc R U P A 2
H1B H 0.7250 0.8308 0.0273 0.139 Uiso 0.207(6) 1 calc R U P A 2
H1C H 0.5678 0.8304 0.0995 0.139 Uiso 0.207(6) 1 calc R U P A 2
C2 C 0.988(3) 0.8513(18) 0.1659(10) 0.089(5) Uani 0.207(6) 1 d . U P A 2
H2A H 0.9000 0.9079 0.1971 0.133 Uiso 0.207(6) 1 calc R U P A 2
H2B H 1.0773 0.9012 0.1314 0.133 Uiso 0.207(6) 1 calc R U P A 2
H2C H 1.0857 0.8224 0.2021 0.133 Uiso 0.207(6) 1 calc R U P A 2
C00R C 0.964(4) 0.646(2) 0.0533(14) 0.108(6) Uani 0.207(6) 1 d . U P A 2
H00Y H 1.0781 0.6213 0.0850 0.162 Uiso 0.207(6) 1 calc R U P A 2
H H 1.0344 0.7043 0.0192 0.162 Uiso 0.207(6) 1 calc R U P A 2
HA H 0.8707 0.5662 0.0199 0.162 Uiso 0.207(6) 1 calc R U P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C006 O001 H001 109.5 . . ?
C009 N002 C00B 119.5(3) . . ?
O004 N003 O005 123.5(3) . . ?
O004 N003 C00F 118.7(3) . . ?
O005 N003 C00F 117.8(3) . . ?
O001 C006 C007 119.9(3) . . ?
O001 C006 C00A 119.3(3) . . ?
C00A C006 C007 120.8(3) . . ?
C006 C007 C009 121.7(3) . . ?
C00C C007 C006 119.4(3) . . ?
C00C C007 C009 118.9(3) . . ?
C00C C008 C00E 116.0(3) . . ?
C00C C008 C00I 123.4(3) . . ?
C00E C008 C00I 120.6(3) . . ?
N002 C009 C007 123.4(3) . . ?
N002 C009 H009 118.3 . . ?
C007 C009 H009 118.3 . . ?
C006 C00A C00H 122.0(3) . . ?
C00E C00A C006 116.3(3) . . ?
C00E C00A C00H 121.7(3) . . ?
C00D C00B N002 121.8(3) . . ?
C00D C00B C00G 119.4(3) . . ?
C00G C00B N002 118.7(3) . . ?
C007 C00C H00C 118.8 . . ?
C008 C00C C007 122.3(3) . . ?
C008 C00C H00C 118.8 . . ?
C00B C00D H00D 120.9 . . ?
C00F C00D C00B 118.2(3) . . ?
C00F C00D H00D 120.9 . . ?
C008 C00E H00E 117.5 . . ?
C00A C00E C008 125.1(3) . . ?
C00A C00E H00E 117.5 . . ?
C00D C00F N003 117.7(3) . . ?
C00J C00F N003 119.0(3) . . ?
C00J C00F C00D 123.3(3) . . ?
C00B C00G H00G 119.6 . . ?
C00K C00G C00B 120.8(3) . . ?
C00K C00G H00G 119.6 . . ?
C00A C00H C00M 110.0(3) . . ?
C00L C00H C00A 110.4(3) . . ?
C00L C00H C00M 109.5(3) . . ?
C00N C00H C00A 111.5(2) . . ?
C00N C00H C00L 108.1(3) . . ?
C00N C00H C00M 107.2(3) . . ?
C008 C00I C00P 109.4(3) . . ?
C008 C00I C1 109.2(7) . . ?
C008 C00I C2 108.2(6) . . ?
C00O C00I C008 112.5(3) . . ?
C00O C00I C00P 107.7(4) . . ?
C00O C00I C00Q 108.8(4) . . ?
C00Q C00I C008 109.4(3) . . ?
C00Q C00I C00P 109.0(4) . . ?
C1 C00I C2 105.7(11) . . ?
C00R C00I C008 114.9(7) . . ?
C00R C00I C1 111.8(12) . . ?
C00R C00I C2 106.6(12) . . ?
C00F C00J H00J 121.1 . . ?
C00F C00J C00K 117.7(3) . . ?
C00K C00J H00J 121.1 . . ?
C00G C00K C00J 120.6(3) . . ?
C00G C00K H00K 119.7 . . ?
C00J C00K H00K 119.7 . . ?
C00H C00L H00A 109.5 . . ?
C00H C00L H00B 109.5 . . ?
C00H C00L H00F 109.5 . . ?
H00A C00L H00B 109.5 . . ?
H00A C00L H00F 109.5 . . ?
H00B C00L H00F 109.5 . . ?
C00H C00M H00H 109.5 . . ?
C00H C00M H00I 109.5 . . ?
C00H C00M H00L 109.5 . . ?
H00H C00M H00I 109.5 . . ?
H00H C00M H00L 109.5 . . ?
H00I C00M H00L 109.5 . . ?
C00H C00N H00M 109.5 . . ?
C00H C00N H00N 109.5 . . ?
C00H C00N H00O 109.5 . . ?
H00M C00N H00N 109.5 . . ?
H00M C00N H00O 109.5 . . ?
H00N C00N H00O 109.5 . . ?
C00I C00O H00P 109.5 . . ?
C00I C00O H00Q 109.5 . . ?
C00I C00O H00R 109.5 . . ?
H00P C00O H00Q 109.5 . . ?
H00P C00O H00R 109.5 . . ?
H00Q C00O H00R 109.5 . . ?
C00I C00P H00S 109.5 . . ?
C00I C00P H00T 109.5 . . ?
C00I C00P H00U 109.5 . . ?
H00S C00P H00T 109.5 . . ?
H00S C00P H00U 109.5 . . ?
H00T C00P H00U 109.5 . . ?
C00I C00Q H00V 109.5 . . ?
C00I C00Q H00W 109.5 . . ?
C00I C00Q H00X 109.5 . . ?
H00V C00Q H00W 109.5 . . ?
H00V C00Q H00X 109.5 . . ?
H00W C00Q H00X 109.5 . . ?
C00I C1 H1A 109.5 . . ?
C00I C1 H1B 109.5 . . ?
C00I C1 H1C 109.5 . . ?
H1A C1 H1B 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
C00I C2 H2A 109.5 . . ?
C00I C2 H2B 109.5 . . ?
C00I C2 H2C 109.5 . . ?
H2A C2 H2B 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C00I C00R H00Y 109.5 . . ?
C00I C00R H 109.5 . . ?
C00I C00R HA 109.5 . . ?
H00Y C00R H 109.5 . . ?
H00Y C00R HA 109.5 . . ?
H C00R HA 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O001 H001 0.8200 . ?
O001 C006 1.357(3) . ?
N002 C009 1.280(3) . ?
N002 C00B 1.415(3) . ?
N003 O004 1.216(4) . ?
N003 O005 1.218(3) . ?
N003 C00F 1.474(4) . ?
C006 C007 1.403(4) . ?
C006 C00A 1.398(4) . ?
C007 C009 1.446(4) . ?
C007 C00C 1.393(4) . ?
C008 C00C 1.370(4) . ?
C008 C00E 1.404(4) . ?
C008 C00I 1.521(4) . ?
C009 H009 0.9300 . ?
C00A C00E 1.386(3) . ?
C00A C00H 1.536(4) . ?
C00B C00D 1.382(4) . ?
C00B C00G 1.386(4) . ?
C00C H00C 0.9300 . ?
C00D H00D 0.9300 . ?
C00D C00F 1.379(4) . ?
C00E H00E 0.9300 . ?
C00F C00J 1.367(4) . ?
C00G H00G 0.9300 . ?
C00G C00K 1.374(4) . ?
C00H C00L 1.535(4) . ?
C00H C00M 1.536(4) . ?
C00H C00N 1.529(4) . ?
C00I C00O 1.513(5) . ?
C00I C00P 1.534(5) . ?
C00I C00Q 1.518(5) . ?
C00I C1 1.564(18) . ?
C00I C2 1.634(17) . ?
C00I C00R 1.515(18) . ?
C00J H00J 0.9300 . ?
C00J C00K 1.380(4) . ?
C00K H00K 0.9300 . ?
C00L H00A 0.9600 . ?
C00L H00B 0.9600 . ?
C00L H00F 0.9600 . ?
C00M H00H 0.9600 . ?
C00M H00I 0.9600 . ?
C00M H00L 0.9600 . ?
C00N H00M 0.9600 . ?
C00N H00N 0.9600 . ?
C00N H00O 0.9600 . ?
C00O H00P 0.9600 . ?
C00O H00Q 0.9600 . ?
C00O H00R 0.9600 . ?
C00P H00S 0.9600 . ?
C00P H00T 0.9600 . ?
C00P H00U 0.9600 . ?
C00Q H00V 0.9600 . ?
C00Q H00W 0.9600 . ?
C00Q H00X 0.9600 . ?
C1 H1A 0.9600 . ?
C1 H1B 0.9600 . ?
C1 H1C 0.9600 . ?
C2 H2A 0.9600 . ?
C2 H2B 0.9600 . ?
C2 H2C 0.9600 . ?
C00R H00Y 0.9600 . ?
C00R H 0.9600 . ?
C00R HA 0.9600 . ?
