#------------------------------------------------------------------------------
#$Date: 2024-07-05 18:01:51 +0300 (Fri, 05 Jul 2024) $
#$Revision: 292905 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/57/14/1571438.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1571438
loop_
_publ_author_name
'Li, Yijie'
'Tamizmani, Masilamani'
'Akram, Manjur O.'
'Martin, Caleb D.'
_publ_section_title
;
 Carborane-arene fused boracyclic analogues of polycyclic aromatic
 hydrocarbons accessed by intramolecular borylation.
;
_journal_issue                   20
_journal_name_full               'Chemical science'
_journal_page_first              7568
_journal_page_last               7575
_journal_paper_doi               10.1039/d4sc00990h
_journal_volume                  15
_journal_year                    2024
_chemical_formula_sum            'C22 H35 B21'
_chemical_formula_weight         526.51
_chemical_name_systematic        1
_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2024-02-09 deposited with the CCDC.	2024-04-16 downloaded from the CCDC.
;
_cell_angle_alpha                96.020(2)
_cell_angle_beta                 109.788(2)
_cell_angle_gamma                111.822(2)
_cell_formula_units_Z            2
_cell_length_a                   10.7014(7)
_cell_length_b                   11.5495(6)
_cell_length_c                   14.4626(9)
_cell_measurement_reflns_used    9011
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      30.59
_cell_measurement_theta_min      3.50
_cell_volume                     1505.99(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0415
_diffrn_reflns_av_unetI/netI     0.0196
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            96399
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.606
_diffrn_reflns_theta_min         2.253
_exptl_absorpt_coefficient_mu    0.055
_exptl_absorpt_correction_T_max  0.941
_exptl_absorpt_correction_T_min  0.931
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.161
_exptl_crystal_description       block
_exptl_crystal_F_000             544
_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: benzene'
_exptl_crystal_size_max          0.480
_exptl_crystal_size_mid          0.321
_exptl_crystal_size_min          0.282
_refine_diff_density_max         0.426
_refine_diff_density_min         -0.224
_refine_diff_density_rms         0.041
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     508
_refine_ls_number_reflns         9245
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.041
_refine_ls_R_factor_all          0.0490
_refine_ls_R_factor_gt           0.0431
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0658P)²+0.3879P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1180
_refine_ls_wR_factor_ref         0.1234
_reflns_Friedel_coverage         0.000
_reflns_number_gt                8186
_reflns_number_total             9245
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4sc00990h2.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_atom_sites_solution_primary' value 'DIRECT METHODS' was
changed to 'direct'.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 1571438--1571443.cif.
;
_cod_database_code               1571438
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.974
_shelx_estimated_absorpt_t_max   0.985
_shelxl_version_number           2013-3
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C7 C 0.81446(11) 0.13762(9) 0.46937(7) 0.02688(19) Uani 1 1 d . . . . .
C6 C 0.83151(11) 0.14109(9) 0.37832(7) 0.02476(18) Uani 1 1 d . . . . .
C3 C 0.80086(9) 0.22955(8) 0.32860(6) 0.02017(16) Uani 1 1 d . . . . .
C4 C 0.75245(9) 0.31539(8) 0.36622(6) 0.01945(15) Uani 1 1 d . . . . .
B1 B 0.72524(10) 0.40032(9) 0.29290(7) 0.01728(16) Uani 1 1 d . . . . .
C5 C 0.68683(9) 0.51842(8) 0.31155(6) 0.01757(15) Uani 1 1 d . . . . .
C10 C 0.51562(9) 0.50707(8) 0.25100(6) 0.01870(15) Uani 1 1 d . . . . .
C11 C 0.40144(9) 0.38232(8) 0.17231(7) 0.01941(15) Uani 1 1 d . . . . .
C12 C 0.35945(11) 0.26496(9) 0.19731(7) 0.02815(19) Uani 1 1 d . . . . .
H38 H 0.4006 0.2626 0.2661 0.034 Uiso 1 1 calc R U . . .
C13 C 0.25725(12) 0.15061(9) 0.12202(8) 0.0318(2) Uani 1 1 d . . . . .
C14 C 0.19546(10) 0.15289(9) 0.02192(8) 0.02634(18) Uani 1 1 d . . . . .
C16 C 0.33841(11) 0.38391(9) 0.07117(7) 0.02695(19) Uani 1 1 d . . . . .
H16 H 0.3657 0.4635 0.0530 0.032 Uiso 1 1 calc R U . . .
C15 C 0.23583(11) 0.26965(10) -0.00317(7) 0.0294(2) Uani 1 1 d . . . . .
H15 H 0.1930 0.2717 -0.0719 0.035 Uiso 1 1 calc R U . . .
C1 C 0.76204(9) 0.35857(8) 0.20060(6) 0.01731(15) Uani 1 1 d . . . . .
C2 C 0.81573(9) 0.24617(8) 0.23151(7) 0.01958(15) Uani 1 1 d . . . . .
C8 C 0.76920(11) 0.22145(9) 0.50980(7) 0.02553(18) Uani 1 1 d . . . . .
C9 C 0.73858(10) 0.31000(9) 0.45910(7) 0.02322(17) Uani 1 1 d . . . . .
C22 C 0.80349(12) -0.02304(10) 0.66735(8) 0.0293(2) Uani 1 1 d . . . . .
C21 C 0.90249(12) 0.08821(11) 0.74575(8) 0.0321(2) Uani 1 1 d . . . . .
H31 H 1.0054 0.1129 0.7693 0.038 Uiso 1 1 calc R U . . .
C20 C 0.85188(12) 0.16349(10) 0.78986(8) 0.0311(2) Uani 1 1 d . . . . .
C19 C 0.70217(12) 0.12733(10) 0.75581(8) 0.0314(2) Uani 1 1 d . . . . .
C18 C 0.60280(12) 0.01600(10) 0.67757(8) 0.0315(2) Uani 1 1 d . . . . .
C17 C 0.65355(12) -0.05838(10) 0.63276(8) 0.02831(19) Uani 1 1 d . . . . .
B17 B 0.81722(11) 0.67223(9) 0.33350(8) 0.02057(17) Uani 1 1 d . . . . .
B12 B 0.65491(11) 0.59974(9) 0.21862(7) 0.01928(17) Uani 1 1 d . . . . .
B19 B 0.71585(12) 0.76067(9) 0.28485(8) 0.02341(19) Uani 1 1 d . . . . .
B20 B 0.60747(12) 0.76034(10) 0.35548(9) 0.0261(2) Uani 1 1 d . . . . .
B21 B 0.64027(12) 0.67066(10) 0.44621(8) 0.02503(19) Uani 1 1 d . . . . .
B18 B 0.78776(12) 0.77243(10) 0.41802(8) 0.02409(19) Uani 1 1 d . . . . .
B16 B 0.77040(11) 0.61750(9) 0.43294(7) 0.02158(18) Uani 1 1 d . . . . .
B15 B 0.57953(11) 0.51015(10) 0.37875(7) 0.02144(18) Uani 1 1 d . . . . .
B14 B 0.47797(12) 0.59761(10) 0.33087(8) 0.02459(19) Uani 1 1 d . . . . .
B13 B 0.52525(11) 0.65374(10) 0.23214(8) 0.02313(19) Uani 1 1 d . . . . .
B2 B 0.64757(11) 0.19858(9) 0.13082(7) 0.02088(17) Uani 1 1 d . . . . .
B8 B 0.68500(12) 0.18179(10) 0.02227(8) 0.02488(19) Uani 1 1 d . . . . .
B7 B 0.77130(13) 0.13028(10) 0.12825(8) 0.0254(2) Uani 1 1 d . . . . .
B6 B 0.95559(12) 0.25149(11) 0.19867(9) 0.0265(2) Uani 1 1 d . . . . .
B10 B 0.98546(12) 0.37973(11) 0.13682(9) 0.0261(2) Uani 1 1 d . . . . .
B9 B 0.81804(12) 0.33535(10) 0.02759(8) 0.02432(19) Uani 1 1 d . . . . .
B11 B 0.87507(13) 0.21403(11) 0.06312(9) 0.0272(2) Uani 1 1 d . . . . .
B4 B 0.86161(11) 0.44782(10) 0.14065(8) 0.02179(18) Uani 1 1 d . . . . .
H4 H 0.8898 0.5525 0.1452 0.026 Uiso 1 1 calc R U . . .
B5 B 0.94907(11) 0.39747(10) 0.24579(8) 0.02250(18) Uani 1 1 d . . . . .
B3 B 0.67798(11) 0.32684(10) 0.07065(7) 0.02093(17) Uani 1 1 d . . . . .
H2 H 0.5879(16) -0.1339(14) 0.5787(11) 0.036(4) Uiso 1 1 d . . . . .
H1 H 0.9203(16) 0.2408(14) 0.8446(11) 0.037(4) Uiso 1 1 d . . . . .
H3 H 0.1244(17) 0.0751(14) -0.0290(11) 0.040(4) Uiso 1 1 d . . . . .
H5 H 0.7566(15) 0.2174(13) 0.5718(11) 0.034(3) Uiso 1 1 d . . . . .
H34 H 0.7062(14) 0.3681(12) 0.4887(10) 0.026(3) Uiso 1 1 d . . . . .
H6 H 0.8175(15) 0.3668(13) -0.0418(11) 0.034(3) Uiso 1 1 d . . . . .
H9 H 0.5792(16) 0.8404(14) 0.3682(11) 0.041(4) Uiso 1 1 d . . . . .
H10 H 0.9187(15) 0.6808(13) 0.3297(10) 0.031(3) Uiso 1 1 d . . . . .
H7 H 0.3630(16) 0.5577(14) 0.3225(11) 0.035(3) Uiso 1 1 d . . . . .
H8 H 0.4386(15) 0.6506(13) 0.1628(11) 0.034(3) Uiso 1 1 d . . . . .
H12 H 0.9126(16) 0.1650(14) 0.0165(11) 0.037(4) Uiso 1 1 d . . . . .
H11 H 1.0951(17) 0.4390(15) 0.1397(12) 0.044(4) Uiso 1 1 d . . . . .
H13 H 0.7409(15) 0.0318(13) 0.1361(11) 0.034(3) Uiso 1 1 d . . . . .
H14 H 0.7593(16) 0.8396(14) 0.2502(11) 0.038(4) Uiso 1 1 d . . . . .
H33 H 0.6357(16) 0.6906(14) 0.5211(11) 0.037(4) Uiso 1 1 d . . . . .
H32 H 0.8798(15) 0.8601(13) 0.4744(10) 0.034(3) Uiso 1 1 d . . . . .
H17 H 0.4982(17) -0.0099(14) 0.6531(11) 0.039(4) Uiso 1 1 d . . . . .
H19 H 0.8394(16) -0.0773(14) 0.6367(11) 0.040(4) Uiso 1 1 d . . . . .
H18 H 0.6651(17) 0.1773(15) 0.7891(12) 0.044(4) Uiso 1 1 d . . . . .
H20 H 0.2327(18) 0.0702(15) 0.1395(12) 0.046(4) Uiso 1 1 d . . . . .
H23 H 0.5514(15) 0.1484(13) 0.1438(10) 0.029(3) Uiso 1 1 d . . . . .
H25 H 1.0165(15) 0.4595(13) 0.3226(10) 0.031(3) Uiso 1 1 d . . . . .
H21 H 0.5863(15) 0.3523(13) 0.0383(10) 0.034(3) Uiso 1 1 d . . . . .
H24 H 1.0392(17) 0.2270(15) 0.2481(12) 0.044(4) Uiso 1 1 d . . . . .
H22 H 0.5973(15) 0.1125(13) -0.0488(11) 0.034(3) Uiso 1 1 d . . . . .
H28 H 0.5298(14) 0.4195(12) 0.3986(10) 0.028(3) Uiso 1 1 d . . . . .
H27 H 0.8638(16) 0.0814(14) 0.3489(11) 0.035(3) Uiso 1 1 d . . . . .
H26 H 0.8364(17) 0.0768(15) 0.5057(12) 0.045(4) Uiso 1 1 d . . . . .
H29 H 0.8463(16) 0.5930(14) 0.4903(11) 0.038(4) Uiso 1 1 d . . . . .
H30 H 0.6500(14) 0.5595(12) 0.1460(10) 0.025(3) Uiso 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C8 C7 C6 121.05(8) . . ?
C8 C7 H26 119.7(9) . . ?
C6 C7 H26 119.3(9) . . ?
C3 C6 C7 118.08(9) . . ?
C3 C6 H27 120.4(8) . . ?
C7 C6 H27 121.5(8) . . ?
C6 C3 C4 122.76(8) . . ?
C6 C3 C2 124.42(8) . . ?
C4 C3 C2 112.82(7) . . ?
C9 C4 C3 117.37(8) . . ?
C9 C4 B1 132.21(8) . . ?
C3 C4 B1 110.42(7) . . ?
C4 B1 C5 126.86(7) . . ?
C4 B1 C1 107.15(7) . . ?
C5 B1 C1 125.62(7) . . ?
B1 C5 C10 122.04(6) . . ?
B1 C5 B17 119.02(7) . . ?
C10 C5 B17 110.43(6) . . ?
B1 C5 B16 117.74(7) . . ?
C10 C5 B16 110.60(6) . . ?
B17 C5 B16 62.42(6) . . ?
B1 C5 B15 117.83(7) . . ?
C10 C5 B15 60.97(5) . . ?
B17 C5 B15 113.31(6) . . ?
B16 C5 B15 62.18(6) . . ?
B1 C5 B12 120.29(7) . . ?
C10 C5 B12 60.60(5) . . ?
B17 C5 B12 62.00(5) . . ?
B16 C5 B12 112.95(6) . . ?
B15 C5 B12 112.36(6) . . ?
C11 C10 C5 117.31(6) . . ?
C11 C10 B13 121.34(7) . . ?
C5 C10 B13 110.20(6) . . ?
C11 C10 B14 123.92(7) . . ?
C5 C10 B14 109.93(6) . . ?
B13 C10 B14 62.24(6) . . ?
C11 C10 B12 115.23(7) . . ?
C5 C10 B12 60.92(5) . . ?
B13 C10 B12 62.15(5) . . ?
B14 C10 B12 113.12(7) . . ?
C11 C10 B15 119.80(7) . . ?
C5 C10 B15 60.47(5) . . ?
B13 C10 B15 112.46(7) . . ?
B14 C10 B15 61.70(6) . . ?
B12 C10 B15 112.21(6) . . ?
C12 C11 C16 118.92(8) . . ?
C12 C11 C10 121.82(8) . . ?
C16 C11 C10 119.25(8) . . ?
C11 C12 C13 120.39(9) . . ?
C11 C12 H38 119.8 . . ?
C13 C12 H38 119.8 . . ?
C14 C13 C12 120.37(9) . . ?
C14 C13 H20 119.9(10) . . ?
C12 C13 H20 119.7(10) . . ?
C13 C14 C15 119.44(9) . . ?
C13 C14 H3 120.2(9) . . ?
C15 C14 H3 120.3(9) . . ?
C15 C16 C11 120.28(9) . . ?
C15 C16 H16 119.9 . . ?
C11 C16 H16 119.9 . . ?
C14 C15 C16 120.59(9) . . ?
C14 C15 H15 119.7 . . ?
C16 C15 H15 119.7 . . ?
B1 C1 C2 102.99(6) . . ?
B1 C1 B3 134.76(7) . . ?
C2 C1 B3 110.15(6) . . ?
B1 C1 B4 131.73(7) . . ?
C2 C1 B4 110.23(6) . . ?
B3 C1 B4 62.33(6) . . ?
B1 C1 B5 109.12(6) . . ?
C2 C1 B5 61.50(5) . . ?
B3 C1 B5 113.41(7) . . ?
B4 C1 B5 61.86(6) . . ?
B1 C1 B2 112.93(7) . . ?
C2 C1 B2 61.26(5) . . ?
B3 C1 B2 61.97(5) . . ?
B4 C1 B2 113.46(6) . . ?
B5 C1 B2 114.09(6) . . ?
C3 C2 C1 106.58(6) . . ?
C3 C2 B7 128.29(7) . . ?
C1 C2 B7 112.62(7) . . ?
C3 C2 B6 128.10(7) . . ?
C1 C2 B6 112.57(7) . . ?
B7 C2 B6 63.32(6) . . ?
C3 C2 B2 112.51(7) . . ?
C1 C2 B2 61.94(5) . . ?
B7 C2 B2 62.80(6) . . ?
B6 C2 B2 115.38(7) . . ?
C3 C2 B5 112.49(7) . . ?
C1 C2 B5 61.78(5) . . ?
B7 C2 B5 115.17(7) . . ?
B6 C2 B5 62.70(6) . . ?
B2 C2 B5 114.90(6) . . ?
C9 C8 C7 120.38(9) . . ?
C9 C8 H5 119.3(8) . . ?
C7 C8 H5 120.3(8) . . ?
C8 C9 C4 120.35(9) . . ?
C8 C9 H34 119.1(8) . . ?
C4 C9 H34 120.5(8) . . ?
C17 C22 C21 119.71(9) . . ?
C17 C22 H19 120.0(9) . . ?
C21 C22 H19 120.3(9) . . ?
C20 C21 C22 120.33(10) . . ?
C20 C21 H31 119.8 . . ?
C22 C21 H31 119.8 . . ?
C19 C20 C21 119.82(9) . . ?
C19 C20 H1 119.5(9) . . ?
C21 C20 H1 120.6(9) . . ?
C20 C19 C18 120.02(10) . . ?
C20 C19 H18 120.4(9) . . ?
C18 C19 H18 119.5(9) . . ?
C17 C18 C19 120.12(10) . . ?
C17 C18 H17 119.2(9) . . ?
C19 C18 H17 120.7(9) . . ?
C22 C17 C18 119.99(9) . . ?
C22 C17 H2 118.5(9) . . ?
C18 C17 H2 121.5(9) . . ?
C5 B17 B12 59.44(5) . . ?
C5 B17 B16 58.82(5) . . ?
B12 B17 B16 107.97(7) . . ?
C5 B17 B18 105.23(7) . . ?
B12 B17 B18 107.55(7) . . ?
B16 B17 B18 59.78(6) . . ?
C5 B17 B19 105.37(7) . . ?
B12 B17 B19 59.35(5) . . ?
B16 B17 B19 107.84(7) . . ?
B18 B17 B19 60.14(6) . . ?
C5 B17 H10 116.5(7) . . ?
B12 B17 H10 117.7(7) . . ?
B16 B17 H10 120.4(7) . . ?
B18 B17 H10 129.3(7) . . ?
B19 B17 H10 127.3(7) . . ?
C10 B12 C5 58.48(5) . . ?
C10 B12 B19 105.79(7) . . ?
C5 B12 B19 105.58(7) . . ?
C10 B12 B17 105.98(7) . . ?
C5 B12 B17 58.56(5) . . ?
B19 B12 B17 60.50(6) . . ?
C10 B12 B13 58.62(5) . . ?
C5 B12 B13 105.47(7) . . ?
B19 B12 B13 60.17(6) . . ?
B17 B12 B13 108.38(7) . . ?
C10 B12 H30 115.8(7) . . ?
C5 B12 H30 116.9(7) . . ?
B19 B12 H30 131.4(7) . . ?
B17 B12 H30 124.6(7) . . ?
B13 B12 H30 123.7(7) . . ?
B12 B19 B13 60.34(6) . . ?
B12 B19 B17 60.16(5) . . ?
B13 B19 B17 108.25(7) . . ?
B12 B19 B18 108.00(7) . . ?
B13 B19 B18 107.67(7) . . ?
B17 B19 B18 59.90(6) . . ?
B12 B19 B20 107.96(7) . . ?
B13 B19 B20 59.76(6) . . ?
B17 B19 B20 107.64(7) . . ?
B18 B19 B20 59.64(6) . . ?
B12 B19 H14 118.7(7) . . ?
B13 B19 H14 120.7(8) . . ?
B17 B19 H14 120.9(8) . . ?
B18 B19 H14 124.2(8) . . ?
B20 B19 H14 124.2(8) . . ?
B13 B20 B18 108.08(7) . . ?
B13 B20 B21 108.00(7) . . ?
B18 B20 B21 60.41(6) . . ?
B13 B20 B14 59.98(6) . . ?
B18 B20 B14 108.41(7) . . ?
B21 B20 B14 60.00(6) . . ?
B13 B20 B19 59.77(6) . . ?
B18 B20 B19 60.15(6) . . ?
B21 B20 B19 108.29(7) . . ?
B14 B20 B19 107.94(7) . . ?
B13 B20 H9 120.0(8) . . ?
B18 B20 H9 122.9(8) . . ?
B21 B20 H9 122.9(8) . . ?
B14 B20 H9 120.9(8) . . ?
B19 B20 H9 121.3(8) . . ?
B15 B21 B16 60.29(6) . . ?
B15 B21 B20 107.78(7) . . ?
B16 B21 B20 107.67(7) . . ?
B15 B21 B14 59.98(6) . . ?
B16 B21 B14 108.31(7) . . ?
B20 B21 B14 60.06(6) . . ?
B15 B21 B18 107.80(7) . . ?
B16 B21 B18 59.72(6) . . ?
B20 B21 B18 59.72(6) . . ?
B14 B21 B18 107.91(8) . . ?
B15 B21 H33 120.0(8) . . ?
B16 B21 H33 120.3(8) . . ?
B20 B21 H33 123.9(8) . . ?
B14 B21 H33 121.9(8) . . ?
B18 B21 H33 122.8(8) . . ?
B16 B18 B20 107.80(7) . . ?
B16 B18 B17 60.06(5) . . ?
B20 B18 B17 108.15(7) . . ?
B16 B18 B19 107.93(7) . . ?
B20 B18 B19 60.21(6) . . ?
B17 B18 B19 59.96(6) . . ?
B16 B18 B21 59.74(6) . . ?
B20 B18 B21 59.87(6) . . ?
B17 B18 B21 107.84(7) . . ?
B19 B18 B21 107.92(7) . . ?
B16 B18 H32 120.4(7) . . ?
B20 B18 H32 123.0(7) . . ?
B17 B18 H32 120.9(7) . . ?
B19 B18 H32 122.7(7) . . ?
B21 B18 H32 121.7(7) . . ?
C5 B16 B18 105.48(7) . . ?
C5 B16 B21 105.55(7) . . ?
B18 B16 B21 60.54(6) . . ?
C5 B16 B15 59.07(5) . . ?
B18 B16 B15 107.85(7) . . ?
B21 B16 B15 59.55(6) . . ?
C5 B16 B17 58.76(5) . . ?
B18 B16 B17 60.16(6) . . ?
B21 B16 B17 108.55(7) . . ?
B15 B16 B17 107.81(7) . . ?
C5 B16 H29 116.2(8) . . ?
B18 B16 H29 128.7(8) . . ?
B21 B16 H29 127.8(8) . . ?
B15 B16 H29 118.5(8) . . ?
B17 B16 H29 119.2(8) . . ?
C5 B15 C10 58.56(5) . . ?
C5 B15 B21 105.78(7) . . ?
C10 B15 B21 105.94(7) . . ?
C5 B15 B14 106.18(7) . . ?
C10 B15 B14 58.91(5) . . ?
B21 B15 B14 60.47(6) . . ?
C5 B15 B16 58.75(5) . . ?
C10 B15 B16 105.95(7) . . ?
B21 B15 B16 60.16(6) . . ?
B14 B15 B16 108.59(7) . . ?
C5 B15 H28 119.0(7) . . ?
C10 B15 H28 117.2(7) . . ?
B21 B15 H28 129.0(7) . . ?
B14 B15 H28 121.8(7) . . ?
B16 B15 H28 125.2(7) . . ?
C10 B14 B15 59.39(5) . . ?
C10 B14 B13 58.69(5) . . ?
B15 B14 B13 107.72(7) . . ?
C10 B14 B21 105.60(7) . . ?
B15 B14 B21 59.55(6) . . ?
B13 B14 B21 107.81(7) . . ?
C10 B14 B20 105.14(7) . . ?
B15 B14 B20 107.34(7) . . ?
B13 B14 B20 59.81(6) . . ?
B21 B14 B20 59.94(6) . . ?
C10 B14 H7 115.6(7) . . ?
B15 B14 H7 116.8(7) . . ?
B13 B14 H7 120.9(7) . . ?
B21 B14 H7 127.4(7) . . ?
B20 B14 H7 130.5(7) . . ?
C10 B13 B20 105.76(7) . . ?
C10 B13 B19 105.73(7) . . ?
B20 B13 B19 60.47(6) . . ?
C10 B13 B12 59.23(5) . . ?
B20 B13 B12 107.84(7) . . ?
B19 B13 B12 59.49(6) . . ?
C10 B13 B14 59.08(5) . . ?
B20 B13 B14 60.21(6) . . ?
B19 B13 B14 108.69(7) . . ?
B12 B13 B14 108.18(7) . . ?
C10 B13 H8 116.1(7) . . ?
B20 B13 H8 128.7(7) . . ?
B19 B13 H8 127.5(7) . . ?
B12 B13 H8 118.2(7) . . ?
B14 B13 H8 119.3(7) . . ?
C2 B2 C1 56.80(5) . . ?
C2 B2 B8 104.22(7) . . ?
C1 B2 B8 105.19(7) . . ?
C2 B2 B3 103.78(7) . . ?
C1 B2 B3 58.37(5) . . ?
B8 B2 B3 60.66(6) . . ?
C2 B2 B7 57.73(5) . . ?
C1 B2 B7 104.37(7) . . ?
B8 B2 B7 60.69(6) . . ?
B3 B2 B7 108.59(7) . . ?
C2 B2 H23 116.7(7) . . ?
C1 B2 H23 118.1(7) . . ?
B8 B2 H23 131.6(7) . . ?
B3 B2 H23 126.4(7) . . ?
B7 B2 H23 122.1(7) . . ?
B2 B8 B3 60.29(6) . . ?
B2 B8 B7 60.42(6) . . ?
B3 B8 B7 108.09(7) . . ?
B2 B8 B9 108.26(7) . . ?
B3 B8 B9 59.87(6) . . ?
B7 B8 B9 107.46(8) . . ?
B2 B8 B11 108.19(7) . . ?
B3 B8 B11 107.68(7) . . ?
B7 B8 B11 59.56(6) . . ?
B9 B8 B11 59.73(6) . . ?
B2 B8 H22 119.1(7) . . ?
B3 B8 H22 120.6(7) . . ?
B7 B8 H22 121.7(7) . . ?
B9 B8 H22 123.3(7) . . ?
B11 B8 H22 124.0(7) . . ?
C2 B7 B11 104.15(7) . . ?
C2 B7 B6 58.45(6) . . ?
B11 B7 B6 60.09(6) . . ?
C2 B7 B2 59.47(5) . . ?
B11 B7 B2 107.52(7) . . ?
B6 B7 B2 108.65(7) . . ?
C2 B7 B8 104.16(7) . . ?
B11 B7 B8 60.26(6) . . ?
B6 B7 B8 108.32(7) . . ?
B2 B7 B8 58.89(6) . . ?
C2 B7 H13 116.9(7) . . ?
B11 B7 H13 130.3(7) . . ?
B6 B7 H13 120.1(7) . . ?
B2 B7 H13 116.8(7) . . ?
B8 B7 H13 127.7(7) . . ?
C2 B6 B11 103.78(7) . . ?
C2 B6 B7 58.23(6) . . ?
B11 B6 B7 59.82(6) . . ?
C2 B6 B5 59.57(5) . . ?
B11 B6 B5 107.30(7) . . ?
B7 B6 B5 108.43(7) . . ?
C2 B6 B10 104.19(7) . . ?
B11 B6 B10 60.39(6) . . ?
B7 B6 B10 108.25(8) . . ?
B5 B6 B10 58.77(6) . . ?
C2 B6 H24 118.4(8) . . ?
B11 B6 H24 128.9(8) . . ?
B7 B6 H24 120.2(8) . . ?
B5 B6 H24 118.0(8) . . ?
B10 B6 H24 127.0(8) . . ?
B5 B10 B4 60.14(6) . . ?
B5 B10 B9 107.96(7) . . ?
B4 B10 B9 59.69(6) . . ?
B5 B10 B6 60.42(6) . . ?
B4 B10 B6 107.91(7) . . ?
B9 B10 B6 107.31(8) . . ?
B5 B10 B11 107.89(7) . . ?
B4 B10 B11 107.25(7) . . ?
B9 B10 B11 59.57(6) . . ?
B6 B10 B11 59.49(6) . . ?
B5 B10 H11 120.3(8) . . ?
B4 B10 H11 121.6(8) . . ?
B9 B10 H11 123.0(8) . . ?
B6 B10 H11 121.6(8) . . ?
B11 B10 H11 123.1(8) . . ?
B4 B9 B11 108.31(7) . . ?
B4 B9 B3 59.80(6) . . ?
B11 B9 B3 108.10(7) . . ?
B4 B9 B8 108.01(7) . . ?
B11 B9 B8 60.16(6) . . ?
B3 B9 B8 59.96(6) . . ?
B4 B9 B10 60.11(6) . . ?
B11 B9 B10 60.48(6) . . ?
B3 B9 B10 108.17(7) . . ?
B8 B9 B10 108.65(7) . . ?
B4 B9 H6 120.6(7) . . ?
B11 B9 H6 123.1(7) . . ?
B3 B9 H6 120.3(7) . . ?
B8 B9 H6 121.8(7) . . ?
B10 B9 H6 122.0(7) . . ?
B7 B11 B6 60.10(6) . . ?
B7 B11 B9 108.26(7) . . ?
B6 B11 B9 108.12(7) . . ?
B7 B11 B8 60.19(6) . . ?
B6 B11 B8 108.28(7) . . ?
B9 B11 B8 60.10(6) . . ?
B7 B11 B10 108.26(7) . . ?
B6 B11 B10 60.12(6) . . ?
B9 B11 B10 59.95(6) . . ?
B8 B11 B10 108.19(7) . . ?
B7 B11 H12 121.4(8) . . ?
B6 B11 H12 121.6(8) . . ?
B9 B11 H12 121.7(8) . . ?
B8 B11 H12 121.4(7) . . ?
B10 B11 H12 121.8(7) . . ?
C1 B4 B5 59.65(5) . . ?
C1 B4 B3 58.80(5) . . ?
B5 B4 B3 108.71(7) . . ?
C1 B4 B9 104.93(7) . . ?
B5 B4 B9 107.51(7) . . ?
B3 B4 B9 60.20(6) . . ?
C1 B4 B10 105.06(7) . . ?
B5 B4 B10 59.07(6) . . ?
B3 B4 B10 108.56(7) . . ?
B9 B4 B10 60.20(6) . . ?
C1 B4 H4 124.3 . . ?
B5 B4 H4 121.5 . . ?
B3 B4 H4 121.0 . . ?
B9 B4 H4 122.5 . . ?
B10 B4 H4 122.4 . . ?
C2 B5 C1 56.72(5) . . ?
C2 B5 B10 104.37(7) . . ?
C1 B5 B10 105.49(7) . . ?
C2 B5 B4 103.77(7) . . ?
C1 B5 B4 58.48(5) . . ?
B10 B5 B4 60.79(6) . . ?
C2 B5 B6 57.73(6) . . ?
C1 B5 B6 104.43(7) . . ?
B10 B5 B6 60.82(6) . . ?
B4 B5 B6 108.73(7) . . ?
C2 B5 H25 117.1(7) . . ?
C1 B5 H25 115.9(7) . . ?
B10 B5 H25 132.5(7) . . ?
B4 B5 H25 124.3(7) . . ?
B6 B5 H25 124.4(7) . . ?
C1 B3 B4 58.87(5) . . ?
C1 B3 B2 59.66(5) . . ?
B4 B3 B2 108.74(7) . . ?
C1 B3 B9 104.83(7) . . ?
B4 B3 B9 60.00(6) . . ?
B2 B3 B9 107.51(7) . . ?
C1 B3 B8 104.93(7) . . ?
B4 B3 B8 108.32(7) . . ?
B2 B3 B8 59.05(6) . . ?
B9 B3 B8 60.16(6) . . ?
C1 B3 H21 118.4(7) . . ?
B4 B3 H21 121.3(7) . . ?
B2 B3 H21 117.2(7) . . ?
B9 B3 H21 128.8(7) . . ?
B8 B3 H21 125.6(7) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C7 C8 1.3913(14) . ?
C7 C6 1.3919(14) . ?
C7 H26 0.970(16) . ?
C6 C3 1.3828(12) . ?
C6 H27 0.996(14) . ?
C3 C4 1.4165(12) . ?
C3 C2 1.4896(12) . ?
C4 C9 1.4058(12) . ?
C4 B1 1.5468(12) . ?
B1 C5 1.5865(12) . ?
B1 C1 1.5910(12) . ?
C5 C10 1.6888(12) . ?
C5 B17 1.7154(12) . ?
C5 B16 1.7164(13) . ?
C5 B15 1.7222(13) . ?
C5 B12 1.7314(12) . ?
C10 C11 1.5066(11) . ?
C10 B13 1.7148(13) . ?
C10 B14 1.7219(13) . ?
C10 B12 1.7259(13) . ?
C10 B15 1.7306(13) . ?
C11 C12 1.3891(12) . ?
C11 C16 1.3935(12) . ?
C12 C13 1.3944(13) . ?
C12 H38 0.9500 . ?
C13 C14 1.3808(14) . ?
C13 H20 0.953(16) . ?
C14 C15 1.3829(14) . ?
C14 H3 0.950(15) . ?
C16 C15 1.3888(13) . ?
C16 H16 0.9500 . ?
C15 H15 0.9500 . ?
C1 C2 1.6485(11) . ?
C1 B3 1.7152(12) . ?
C1 B4 1.7165(13) . ?
C1 B5 1.7376(13) . ?
C1 B2 1.7385(13) . ?
C2 B7 1.6955(13) . ?
C2 B6 1.6995(13) . ?
C2 B2 1.7273(13) . ?
C2 B5 1.7330(13) . ?
C8 C9 1.3909(12) . ?
C8 H5 0.954(14) . ?
C9 H34 0.983(13) . ?
C22 C17 1.3850(15) . ?
C22 C21 1.3885(15) . ?
C22 H19 0.987(15) . ?
C21 C20 1.3870(16) . ?
C21 H31 0.9500 . ?
C20 C19 1.3816(16) . ?
C20 H1 0.966(15) . ?
C19 C18 1.3886(14) . ?
C19 H18 0.981(16) . ?
C18 C17 1.3861(14) . ?
C18 H17 0.964(15) . ?
C17 H2 0.946(14) . ?
B17 B12 1.7752(14) . ?
B17 B16 1.7782(14) . ?
B17 B18 1.7801(14) . ?
B17 B19 1.7812(14) . ?
B17 H10 1.074(13) . ?
B12 B19 1.7607(14) . ?
B12 B13 1.7760(14) . ?
B12 H30 1.079(13) . ?
B19 B13 1.7730(15) . ?
B19 B18 1.7844(15) . ?
B19 B20 1.7856(16) . ?
B19 H14 1.112(15) . ?
B20 B13 1.7729(15) . ?
B20 B18 1.7753(15) . ?
B20 B21 1.7780(16) . ?
B20 B14 1.7802(15) . ?
B20 H9 1.091(15) . ?
B21 B15 1.7625(14) . ?
B21 B16 1.7735(14) . ?
B21 B14 1.7790(15) . ?
B21 B18 1.7877(16) . ?
B21 H33 1.105(14) . ?
B18 B16 1.7732(14) . ?
B18 H32 1.096(14) . ?
B16 B15 1.7757(14) . ?
B16 H29 1.091(15) . ?
B15 B14 1.7704(15) . ?
B15 H28 1.102(13) . ?
B14 B13 1.7761(16) . ?
B14 H7 1.098(14) . ?
B13 H8 1.097(14) . ?
B2 B8 1.7558(14) . ?
B2 B3 1.7781(14) . ?
B2 B7 1.7835(14) . ?
B2 H23 1.068(13) . ?
B8 B3 1.7847(14) . ?
B8 B7 1.7882(16) . ?
B8 B9 1.7883(15) . ?
B8 B11 1.7894(16) . ?
B8 H22 1.093(14) . ?
B7 B11 1.7768(16) . ?
B7 B6 1.7818(16) . ?
B7 H13 1.091(14) . ?
B6 B11 1.7816(16) . ?
B6 B5 1.7862(15) . ?
B6 B10 1.7932(16) . ?
B6 H24 1.090(16) . ?
B10 B5 1.7562(15) . ?
B10 B4 1.7870(15) . ?
B10 B9 1.7887(16) . ?
B10 B11 1.7980(16) . ?
B10 H11 1.100(15) . ?
B9 B4 1.7794(14) . ?
B9 B11 1.7816(15) . ?
B9 B3 1.7830(14) . ?
B9 H6 1.101(14) . ?
B11 H12 1.099(14) . ?
B4 B5 1.7756(14) . ?
B4 B3 1.7759(14) . ?
B4 H4 1.1200 . ?
B5 H25 1.084(14) . ?
B3 H21 1.096(14) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C8 C7 C6 C3 -0.57(14) . . . . ?
C7 C6 C3 C4 -0.37(14) . . . . ?
C7 C6 C3 C2 179.13(8) . . . . ?
C6 C3 C4 C9 1.21(13) . . . . ?
C2 C3 C4 C9 -178.34(8) . . . . ?
C6 C3 C4 B1 -179.08(8) . . . . ?
C2 C3 C4 B1 1.37(10) . . . . ?
C9 C4 B1 C5 6.58(15) . . . . ?
C3 C4 B1 C5 -173.07(8) . . . . ?
C9 C4 B1 C1 179.81(9) . . . . ?
C3 C4 B1 C1 0.16(9) . . . . ?
C4 B1 C5 C10 -105.97(9) . . . . ?
C1 B1 C5 C10 82.00(10) . . . . ?
C4 B1 C5 B17 109.12(9) . . . . ?
C1 B1 C5 B17 -62.91(11) . . . . ?
C4 B1 C5 B16 36.97(12) . . . . ?
C1 B1 C5 B16 -135.06(8) . . . . ?
C4 B1 C5 B15 -34.45(12) . . . . ?
C1 B1 C5 B15 153.52(8) . . . . ?
C4 B1 C5 B12 -178.20(8) . . . . ?
C1 B1 C5 B12 9.76(12) . . . . ?
B1 C5 C10 C11 -4.11(11) . . . . ?
B17 C5 C10 C11 143.45(7) . . . . ?
B16 C5 C10 C11 -149.37(7) . . . . ?
B15 C5 C10 C11 -110.51(8) . . . . ?
B12 C5 C10 C11 105.18(8) . . . . ?
B1 C5 C10 B13 -148.56(7) . . . . ?
B17 C5 C10 B13 -1.00(9) . . . . ?
B16 C5 C10 B13 66.18(8) . . . . ?
B15 C5 C10 B13 105.03(7) . . . . ?
B12 C5 C10 B13 -39.28(6) . . . . ?
B1 C5 C10 B14 144.68(8) . . . . ?
B17 C5 C10 B14 -67.76(8) . . . . ?
B16 C5 C10 B14 -0.58(9) . . . . ?
B15 C5 C10 B14 38.28(7) . . . . ?
B12 C5 C10 B14 -106.03(7) . . . . ?
B1 C5 C10 B12 -109.28(8) . . . . ?
B17 C5 C10 B12 38.27(6) . . . . ?
B16 C5 C10 B12 105.45(7) . . . . ?
B15 C5 C10 B12 144.31(7) . . . . ?
B1 C5 C10 B15 106.41(8) . . . . ?
B17 C5 C10 B15 -106.04(7) . . . . ?
B16 C5 C10 B15 -38.86(6) . . . . ?
B12 C5 C10 B15 -144.31(7) . . . . ?
C5 C10 C11 C12 61.08(11) . . . . ?
B13 C10 C11 C12 -158.63(9) . . . . ?
B14 C10 C11 C12 -82.97(11) . . . . ?
B12 C10 C11 C12 129.89(9) . . . . ?
B15 C10 C11 C12 -8.83(12) . . . . ?
C5 C10 C11 C16 -117.44(9) . . . . ?
B13 C10 C11 C16 22.85(12) . . . . ?
B14 C10 C11 C16 98.51(10) . . . . ?
B12 C10 C11 C16 -48.63(11) . . . . ?
B15 C10 C11 C16 172.65(8) . . . . ?
C16 C11 C12 C13 0.79(15) . . . . ?
C10 C11 C12 C13 -177.74(9) . . . . ?
C11 C12 C13 C14 -0.67(17) . . . . ?
C12 C13 C14 C15 0.03(17) . . . . ?
C12 C11 C16 C15 -0.28(15) . . . . ?
C10 C11 C16 C15 178.29(9) . . . . ?
C13 C14 C15 C16 0.49(16) . . . . ?
C11 C16 C15 C14 -0.36(16) . . . . ?
C4 B1 C1 C2 -1.40(8) . . . . ?
C5 B1 C1 C2 171.94(7) . . . . ?
C4 B1 C1 B3 135.21(9) . . . . ?
C5 B1 C1 B3 -51.45(13) . . . . ?
C4 B1 C1 B4 -134.33(8) . . . . ?
C5 B1 C1 B4 39.01(13) . . . . ?
C4 B1 C1 B5 -65.40(8) . . . . ?
C5 B1 C1 B5 107.93(9) . . . . ?
C4 B1 C1 B2 62.61(8) . . . . ?
C5 B1 C1 B2 -124.05(8) . . . . ?
C6 C3 C2 C1 178.21(8) . . . . ?
C4 C3 C2 C1 -2.24(10) . . . . ?
C6 C3 C2 B7 39.93(14) . . . . ?
C4 C3 C2 B7 -140.52(9) . . . . ?
C6 C3 C2 B6 -43.86(14) . . . . ?
C4 C3 C2 B6 135.68(9) . . . . ?
C6 C3 C2 B2 112.28(9) . . . . ?
C4 C3 C2 B2 -68.17(9) . . . . ?
C6 C3 C2 B5 -116.04(9) . . . . ?
C4 C3 C2 B5 63.51(9) . . . . ?
B1 C1 C2 C3 2.15(8) . . . . ?
B3 C1 C2 C3 -146.54(7) . . . . ?
B4 C1 C2 C3 146.53(7) . . . . ?
B5 C1 C2 C3 107.05(7) . . . . ?
B2 C1 C2 C3 -107.10(7) . . . . ?
B1 C1 C2 B7 147.68(7) . . . . ?
B3 C1 C2 B7 -1.01(9) . . . . ?
B4 C1 C2 B7 -67.94(9) . . . . ?
B5 C1 C2 B7 -107.41(8) . . . . ?
B2 C1 C2 B7 38.43(7) . . . . ?
B1 C1 C2 B6 -143.03(7) . . . . ?
B3 C1 C2 B6 68.28(9) . . . . ?
B4 C1 C2 B6 1.35(9) . . . . ?
B5 C1 C2 B6 -38.12(7) . . . . ?
B2 C1 C2 B6 107.72(8) . . . . ?
B1 C1 C2 B2 109.24(7) . . . . ?
B3 C1 C2 B2 -39.44(6) . . . . ?
B4 C1 C2 B2 -106.37(7) . . . . ?
B5 C1 C2 B2 -145.85(7) . . . . ?
B1 C1 C2 B5 -104.91(7) . . . . ?
B3 C1 C2 B5 106.40(7) . . . . ?
B4 C1 C2 B5 39.48(7) . . . . ?
B2 C1 C2 B5 145.85(7) . . . . ?
C6 C7 C8 C9 0.63(15) . . . . ?
C7 C8 C9 C4 0.26(14) . . . . ?
C3 C4 C9 C8 -1.14(13) . . . . ?
B1 C4 C9 C8 179.23(9) . . . . ?
C17 C22 C21 C20 0.38(16) . . . . ?
C22 C21 C20 C19 0.22(16) . . . . ?
C21 C20 C19 C18 -0.08(16) . . . . ?
C20 C19 C18 C17 -0.65(17) . . . . ?
C21 C22 C17 C18 -1.11(16) . . . . ?
C19 C18 C17 C22 1.25(17) . . . . ?
B1 C5 B17 B12 110.99(8) . . . . ?
C10 C5 B17 B12 -37.67(6) . . . . ?
B16 C5 B17 B12 -140.91(7) . . . . ?
B15 C5 B17 B12 -103.89(7) . . . . ?
B1 C5 B17 B16 -108.10(8) . . . . ?
C10 C5 B17 B16 103.23(7) . . . . ?
B15 C5 B17 B16 37.02(7) . . . . ?
B12 C5 B17 B16 140.91(7) . . . . ?
B1 C5 B17 B18 -147.34(7) . . . . ?
C10 C5 B17 B18 63.99(8) . . . . ?
B16 C5 B17 B18 -39.24(6) . . . . ?
B15 C5 B17 B18 -2.22(9) . . . . ?
B12 C5 B17 B18 101.67(7) . . . . ?
B1 C5 B17 B19 150.07(7) . . . . ?
C10 C5 B17 B19 1.40(9) . . . . ?
B16 C5 B17 B19 -101.83(7) . . . . ?
B15 C5 B17 B19 -64.81(8) . . . . ?
B12 C5 B17 B19 39.07(6) . . . . ?
C11 C10 B12 C5 -108.56(7) . . . . ?
B13 C10 B12 C5 137.78(7) . . . . ?
B14 C10 B12 C5 100.76(7) . . . . ?
B15 C10 B12 C5 33.25(6) . . . . ?
C11 C10 B12 B19 152.58(7) . . . . ?
C5 C10 B12 B19 -98.86(7) . . . . ?
B13 C10 B12 B19 38.92(7) . . . . ?
B14 C10 B12 B19 1.90(9) . . . . ?
B15 C10 B12 B19 -65.61(8) . . . . ?
C11 C10 B12 B17 -144.25(7) . . . . ?
C5 C10 B12 B17 -35.69(6) . . . . ?
B13 C10 B12 B17 102.09(7) . . . . ?
B14 C10 B12 B17 65.07(8) . . . . ?
B15 C10 B12 B17 -2.44(8) . . . . ?
C11 C10 B12 B13 113.66(8) . . . . ?
C5 C10 B12 B13 -137.78(7) . . . . ?
B14 C10 B12 B13 -37.03(7) . . . . ?
B15 C10 B12 B13 -104.53(7) . . . . ?
B1 C5 B12 C10 112.09(8) . . . . ?
B17 C5 B12 C10 -138.90(7) . . . . ?
B16 C5 B12 C10 -101.53(7) . . . . ?
B15 C5 B12 C10 -33.47(6) . . . . ?
B1 C5 B12 B19 -148.68(7) . . . . ?
C10 C5 B12 B19 99.23(7) . . . . ?
B17 C5 B12 B19 -39.67(6) . . . . ?
B16 C5 B12 B19 -2.30(9) . . . . ?
B15 C5 B12 B19 65.76(8) . . . . ?
B1 C5 B12 B17 -109.01(8) . . . . ?
C10 C5 B12 B17 138.90(7) . . . . ?
B16 C5 B12 B17 37.37(7) . . . . ?
B15 C5 B12 B17 105.42(7) . . . . ?
B1 C5 B12 B13 148.62(7) . . . . ?
C10 C5 B12 B13 36.53(6) . . . . ?
B17 C5 B12 B13 -102.37(7) . . . . ?
B16 C5 B12 B13 -65.00(8) . . . . ?
B15 C5 B12 B13 3.05(9) . . . . ?
C5 B17 B12 C10 35.66(6) . . . . ?
B16 B17 B12 C10 1.11(8) . . . . ?
B18 B17 B12 C10 -61.99(8) . . . . ?
B19 B17 B12 C10 -99.39(7) . . . . ?
B16 B17 B12 C5 -34.55(6) . . . . ?
B18 B17 B12 C5 -97.65(7) . . . . ?
B19 B17 B12 C5 -135.05(7) . . . . ?
C5 B17 B12 B19 135.05(7) . . . . ?
B16 B17 B12 B19 100.50(7) . . . . ?
B18 B17 B12 B19 37.40(7) . . . . ?
C5 B17 B12 B13 97.26(7) . . . . ?
B16 B17 B12 B13 62.71(8) . . . . ?
B18 B17 B12 B13 -0.39(9) . . . . ?
B19 B17 B12 B13 -37.79(7) . . . . ?
C10 B12 B19 B13 -38.19(6) . . . . ?
C5 B12 B19 B13 -99.17(7) . . . . ?
B17 B12 B19 B13 -137.91(7) . . . . ?
C10 B12 B19 B17 99.72(7) . . . . ?
C5 B12 B19 B17 38.74(6) . . . . ?
B13 B12 B19 B17 137.91(7) . . . . ?
C10 B12 B19 B18 62.31(8) . . . . ?
C5 B12 B19 B18 1.34(9) . . . . ?
B17 B12 B19 B18 -37.40(7) . . . . ?
B13 B12 B19 B18 100.50(8) . . . . ?
C10 B12 B19 B20 -0.73(9) . . . . ?
C5 B12 B19 B20 -61.71(8) . . . . ?
B17 B12 B19 B20 -100.44(8) . . . . ?
B13 B12 B19 B20 37.46(7) . . . . ?
C5 B17 B19 B12 -39.12(6) . . . . ?
B16 B17 B19 B12 -100.72(7) . . . . ?
B18 B17 B19 B12 -138.11(7) . . . . ?
C5 B17 B19 B13 -1.29(9) . . . . ?
B12 B17 B19 B13 37.83(7) . . . . ?
B16 B17 B19 B13 -62.89(9) . . . . ?
B18 B17 B19 B13 -100.27(8) . . . . ?
C5 B17 B19 B18 98.99(7) . . . . ?
B12 B17 B19 B18 138.11(7) . . . . ?
B16 B17 B19 B18 37.39(7) . . . . ?
C5 B17 B19 B20 61.87(8) . . . . ?
B12 B17 B19 B20 100.99(8) . . . . ?
B16 B17 B19 B20 0.27(9) . . . . ?
B18 B17 B19 B20 -37.12(7) . . . . ?
B12 B19 B20 B13 -37.72(7) . . . . ?
B17 B19 B20 B13 -101.24(7) . . . . ?
B18 B19 B20 B13 -138.48(7) . . . . ?
B12 B19 B20 B18 100.76(7) . . . . ?
B13 B19 B20 B18 138.48(7) . . . . ?
B17 B19 B20 B18 37.23(7) . . . . ?
B12 B19 B20 B21 62.88(9) . . . . ?
B13 B19 B20 B21 100.60(8) . . . . ?
B17 B19 B20 B21 -0.64(9) . . . . ?
B18 B19 B20 B21 -37.87(7) . . . . ?
B12 B19 B20 B14 -0.60(10) . . . . ?
B13 B19 B20 B14 37.12(7) . . . . ?
B17 B19 B20 B14 -64.12(9) . . . . ?
B18 B19 B20 B14 -101.35(8) . . . . ?
B13 B20 B21 B15 0.37(10) . . . . ?
B18 B20 B21 B15 -100.62(8) . . . . ?
B14 B20 B21 B15 37.72(7) . . . . ?
B19 B20 B21 B15 -62.87(9) . . . . ?
B13 B20 B21 B16 64.01(9) . . . . ?
B18 B20 B21 B16 -36.99(7) . . . . ?
B14 B20 B21 B16 101.36(7) . . . . ?
B19 B20 B21 B16 0.77(9) . . . . ?
B13 B20 B21 B14 -37.35(7) . . . . ?
B18 B20 B21 B14 -138.35(7) . . . . ?
B19 B20 B21 B14 -100.59(8) . . . . ?
B13 B20 B21 B18 101.00(8) . . . . ?
B14 B20 B21 B18 138.35(7) . . . . ?
B19 B20 B21 B18 37.76(7) . . . . ?
B13 B20 B18 B16 -63.83(9) . . . . ?
B21 B20 B18 B16 37.03(7) . . . . ?
B14 B20 B18 B16 -0.31(10) . . . . ?
B19 B20 B18 B16 -100.88(7) . . . . ?
B13 B20 B18 B17 -0.34(10) . . . . ?
B21 B20 B18 B17 100.52(8) . . . . ?
B14 B20 B18 B17 63.18(9) . . . . ?
B19 B20 B18 B17 -37.39(7) . . . . ?
B13 B20 B18 B19 37.05(7) . . . . ?
B21 B20 B18 B19 137.91(7) . . . . ?
B14 B20 B18 B19 100.56(8) . . . . ?
B13 B20 B18 B21 -100.86(8) . . . . ?
B14 B20 B18 B21 -37.34(7) . . . . ?
B19 B20 B18 B21 -137.91(7) . . . . ?
C5 B17 B18 B16 38.78(6) . . . . ?
B12 B17 B18 B16 100.97(7) . . . . ?
B19 B17 B18 B16 138.02(7) . . . . ?
C5 B17 B18 B20 -61.74(9) . . . . ?
B12 B17 B18 B20 0.45(9) . . . . ?
B16 B17 B18 B20 -100.52(8) . . . . ?
B19 B17 B18 B20 37.50(7) . . . . ?
C5 B17 B18 B19 -99.24(7) . . . . ?
B12 B17 B18 B19 -37.05(6) . . . . ?
B16 B17 B18 B19 -138.02(7) . . . . ?
C5 B17 B18 B21 1.55(9) . . . . ?
B12 B17 B18 B21 63.74(9) . . . . ?
B16 B17 B18 B21 -37.23(7) . . . . ?
B19 B17 B18 B21 100.79(8) . . . . ?
B12 B19 B18 B16 -0.02(9) . . . . ?
B13 B19 B18 B16 63.72(9) . . . . ?
B17 B19 B18 B16 -37.53(7) . . . . ?
B20 B19 B18 B16 100.67(8) . . . . ?
B12 B19 B18 B20 -100.69(8) . . . . ?
B13 B19 B18 B20 -36.95(7) . . . . ?
B17 B19 B18 B20 -138.20(7) . . . . ?
B12 B19 B18 B17 37.52(7) . . . . ?
B13 B19 B18 B17 101.25(7) . . . . ?
B20 B19 B18 B17 138.20(7) . . . . ?
B12 B19 B18 B21 -63.14(9) . . . . ?
B13 B19 B18 B21 0.59(9) . . . . ?
B17 B19 B18 B21 -100.66(7) . . . . ?
B20 B19 B18 B21 37.54(7) . . . . ?
B15 B21 B18 B16 -37.80(7) . . . . ?
B20 B21 B18 B16 -138.41(7) . . . . ?
B14 B21 B18 B16 -101.16(7) . . . . ?
B15 B21 B18 B20 100.60(8) . . . . ?
B16 B21 B18 B20 138.41(7) . . . . ?
B14 B21 B18 B20 37.25(7) . . . . ?
B15 B21 B18 B17 -0.44(10) . . . . ?
B16 B21 B18 B17 37.37(7) . . . . ?
B20 B21 B18 B17 -101.04(8) . . . . ?
B14 B21 B18 B17 -63.79(9) . . . . ?
B15 B21 B18 B19 62.91(9) . . . . ?
B16 B21 B18 B19 100.71(7) . . . . ?
B20 B21 B18 B19 -37.69(7) . . . . ?
B14 B21 B18 B19 -0.45(9) . . . . ?
B1 C5 B16 B18 149.58(7) . . . . ?
C10 C5 B16 B18 -63.49(8) . . . . ?
B17 C5 B16 B18 39.48(6) . . . . ?
B15 C5 B16 B18 -101.82(7) . . . . ?
B12 C5 B16 B18 2.28(9) . . . . ?
B1 C5 B16 B21 -147.33(7) . . . . ?
C10 C5 B16 B21 -0.41(9) . . . . ?
B17 C5 B16 B21 102.56(7) . . . . ?
B15 C5 B16 B21 -38.74(7) . . . . ?
B12 C5 B16 B21 65.36(8) . . . . ?
B1 C5 B16 B15 -108.59(8) . . . . ?
C10 C5 B16 B15 38.33(6) . . . . ?
B17 C5 B16 B15 141.30(7) . . . . ?
B12 C5 B16 B15 104.10(7) . . . . ?
B1 C5 B16 B17 110.10(8) . . . . ?
C10 C5 B16 B17 -102.97(7) . . . . ?
B15 C5 B16 B17 -141.30(7) . . . . ?
B12 C5 B16 B17 -37.20(7) . . . . ?
B20 B18 B16 C5 62.29(9) . . . . ?
B17 B18 B16 C5 -38.81(6) . . . . ?
B19 B18 B16 C5 -1.32(9) . . . . ?
B21 B18 B16 C5 99.38(7) . . . . ?
B20 B18 B16 B21 -37.09(7) . . . . ?
B17 B18 B16 B21 -138.19(7) . . . . ?
B19 B18 B16 B21 -100.70(8) . . . . ?
B20 B18 B16 B15 0.40(9) . . . . ?
B17 B18 B16 B15 -100.70(7) . . . . ?
B19 B18 B16 B15 -63.21(9) . . . . ?
B21 B18 B16 B15 37.49(7) . . . . ?
B20 B18 B16 B17 101.10(8) . . . . ?
B19 B18 B16 B17 37.49(7) . . . . ?
B21 B18 B16 B17 138.19(7) . . . . ?
B15 B21 B16 C5 38.51(6) . . . . ?
B20 B21 B16 C5 -62.28(9) . . . . ?
B14 B21 B16 C5 1.21(9) . . . . ?
B18 B21 B16 C5 -99.27(7) . . . . ?
B15 B21 B16 B18 137.78(7) . . . . ?
B20 B21 B16 B18 36.99(7) . . . . ?
B14 B21 B16 B18 100.48(8) . . . . ?
B20 B21 B16 B15 -100.79(8) . . . . ?
B14 B21 B16 B15 -37.30(7) . . . . ?
B18 B21 B16 B15 -137.78(7) . . . . ?
B15 B21 B16 B17 100.19(7) . . . . ?
B20 B21 B16 B17 -0.60(9) . . . . ?
B14 B21 B16 B17 62.89(9) . . . . ?
B18 B21 B16 B17 -37.59(7) . . . . ?
B12 B17 B16 C5 34.81(6) . . . . ?
B18 B17 B16 C5 135.06(7) . . . . ?
B19 B17 B16 C5 97.51(7) . . . . ?
C5 B17 B16 B18 -135.06(7) . . . . ?
B12 B17 B16 B18 -100.25(7) . . . . ?
B19 B17 B16 B18 -37.55(7) . . . . ?
C5 B17 B16 B21 -97.30(7) . . . . ?
B12 B17 B16 B21 -62.49(8) . . . . ?
B18 B17 B16 B21 37.76(7) . . . . ?
B19 B17 B16 B21 0.21(9) . . . . ?
C5 B17 B16 B15 -34.28(6) . . . . ?
B12 B17 B16 B15 0.53(9) . . . . ?
B18 B17 B16 B15 100.78(7) . . . . ?
B19 B17 B16 B15 63.23(8) . . . . ?
B1 C5 B15 C10 -113.15(8) . . . . ?
B17 C5 B15 C10 101.28(7) . . . . ?
B16 C5 B15 C10 138.39(7) . . . . ?
B12 C5 B15 C10 33.34(6) . . . . ?
B1 C5 B15 B21 147.53(7) . . . . ?
C10 C5 B15 B21 -99.31(7) . . . . ?
B17 C5 B15 B21 1.97(9) . . . . ?
B16 C5 B15 B21 39.08(7) . . . . ?
B12 C5 B15 B21 -65.98(8) . . . . ?
B1 C5 B15 B14 -149.29(7) . . . . ?
C10 C5 B15 B14 -36.14(6) . . . . ?
B17 C5 B15 B14 65.14(8) . . . . ?
B16 C5 B15 B14 102.25(7) . . . . ?
B12 C5 B15 B14 -2.80(9) . . . . ?
B1 C5 B15 B16 108.45(8) . . . . ?
C10 C5 B15 B16 -138.39(7) . . . . ?
B17 C5 B15 B16 -37.11(7) . . . . ?
B12 C5 B15 B16 -105.06(7) . . . . ?
C11 C10 B15 C5 106.45(8) . . . . ?
B13 C10 B15 C5 -101.26(7) . . . . ?
B14 C10 B15 C5 -138.59(7) . . . . ?
B12 C10 B15 C5 -33.42(6) . . . . ?
C11 C10 B15 B21 -154.53(7) . . . . ?
C5 C10 B15 B21 99.02(7) . . . . ?
B13 C10 B15 B21 -2.23(9) . . . . ?
B14 C10 B15 B21 -39.57(7) . . . . ?
B12 C10 B15 B21 65.61(8) . . . . ?
C11 C10 B15 B14 -114.96(8) . . . . ?
C5 C10 B15 B14 138.59(7) . . . . ?
B13 C10 B15 B14 37.33(7) . . . . ?
B12 C10 B15 B14 105.17(7) . . . . ?
C11 C10 B15 B16 142.63(7) . . . . ?
C5 C10 B15 B16 36.19(6) . . . . ?
B13 C10 B15 B16 -65.07(8) . . . . ?
B14 C10 B15 B16 -102.41(7) . . . . ?
B12 C10 B15 B16 2.77(9) . . . . ?
B16 B21 B15 C5 -38.41(6) . . . . ?
B20 B21 B15 C5 62.19(9) . . . . ?
B14 B21 B15 C5 99.95(7) . . . . ?
B18 B21 B15 C5 -0.86(9) . . . . ?
B16 B21 B15 C10 -99.53(7) . . . . ?
B20 B21 B15 C10 1.07(9) . . . . ?
B14 B21 B15 C10 38.82(7) . . . . ?
B18 B21 B15 C10 -61.98(9) . . . . ?
B16 B21 B15 B14 -138.36(8) . . . . ?
B20 B21 B15 B14 -37.76(7) . . . . ?
B18 B21 B15 B14 -100.81(8) . . . . ?
B20 B21 B15 B16 100.60(8) . . . . ?
B14 B21 B15 B16 138.36(8) . . . . ?
B18 B21 B15 B16 37.55(7) . . . . ?
B18 B16 B15 C5 97.70(7) . . . . ?
B21 B16 B15 C5 135.62(7) . . . . ?
B17 B16 B15 C5 34.16(6) . . . . ?
C5 B16 B15 C10 -36.10(6) . . . . ?
B18 B16 B15 C10 61.60(8) . . . . ?
B21 B16 B15 C10 99.52(7) . . . . ?
B17 B16 B15 C10 -1.95(8) . . . . ?
C5 B16 B15 B21 -135.62(7) . . . . ?
B18 B16 B15 B21 -37.93(7) . . . . ?
B17 B16 B15 B21 -101.47(8) . . . . ?
C5 B16 B15 B14 -98.04(7) . . . . ?
B18 B16 B15 B14 -0.34(9) . . . . ?
B21 B16 B15 B14 37.59(7) . . . . ?
B17 B16 B15 B14 -63.88(8) . . . . ?
C11 C10 B14 B15 108.55(9) . . . . ?
C5 C10 B14 B15 -37.74(6) . . . . ?
B13 C10 B14 B15 -140.70(7) . . . . ?
B12 C10 B14 B15 -103.71(7) . . . . ?
C11 C10 B14 B13 -110.75(9) . . . . ?
C5 C10 B14 B13 102.96(7) . . . . ?
B12 C10 B14 B13 36.99(7) . . . . ?
B15 C10 B14 B13 140.70(7) . . . . ?
C11 C10 B14 B21 147.60(8) . . . . ?
C5 C10 B14 B21 1.31(9) . . . . ?
B13 C10 B14 B21 -101.65(8) . . . . ?
B12 C10 B14 B21 -64.66(9) . . . . ?
B15 C10 B14 B21 39.05(7) . . . . ?
C11 C10 B14 B20 -149.99(8) . . . . ?
C5 C10 B14 B20 63.72(8) . . . . ?
B13 C10 B14 B20 -39.24(7) . . . . ?
B12 C10 B14 B20 -2.25(9) . . . . ?
B15 C10 B14 B20 101.46(8) . . . . ?
C5 B15 B14 C10 35.99(6) . . . . ?
B21 B15 B14 C10 135.26(7) . . . . ?
B16 B15 B14 C10 97.80(7) . . . . ?
C5 B15 B14 B13 1.37(9) . . . . ?
C10 B15 B14 B13 -34.62(6) . . . . ?
B21 B15 B14 B13 100.64(8) . . . . ?
B16 B15 B14 B13 63.19(9) . . . . ?
C5 B15 B14 B21 -99.27(7) . . . . ?
C10 B15 B14 B21 -135.26(7) . . . . ?
B16 B15 B14 B21 -37.45(7) . . . . ?
C5 B15 B14 B20 -61.67(9) . . . . ?
C10 B15 B14 B20 -97.66(8) . . . . ?
B21 B15 B14 B20 37.60(7) . . . . ?
B16 B15 B14 B20 0.15(9) . . . . ?
B15 B21 B14 C10 -38.98(6) . . . . ?
B16 B21 B14 C10 -1.54(10) . . . . ?
B20 B21 B14 C10 98.73(8) . . . . ?
B18 B21 B14 C10 61.64(9) . . . . ?
B16 B21 B14 B15 37.44(7) . . . . ?
B20 B21 B14 B15 137.71(7) . . . . ?
B18 B21 B14 B15 100.62(7) . . . . ?
B15 B21 B14 B13 -100.48(7) . . . . ?
B16 B21 B14 B13 -63.05(9) . . . . ?
B20 B21 B14 B13 37.23(7) . . . . ?
B18 B21 B14 B13 0.13(9) . . . . ?
B15 B21 B14 B20 -137.71(7) . . . . ?
B16 B21 B14 B20 -100.28(8) . . . . ?
B18 B21 B14 B20 -37.09(7) . . . . ?
B13 B20 B14 C10 38.70(6) . . . . ?
B18 B20 B14 C10 -61.99(9) . . . . ?
B21 B20 B14 C10 -99.51(7) . . . . ?
B19 B20 B14 C10 1.67(10) . . . . ?
B13 B20 B14 B15 100.79(8) . . . . ?
B18 B20 B14 B15 0.10(10) . . . . ?
B21 B20 B14 B15 -37.42(7) . . . . ?
B19 B20 B14 B15 63.76(9) . . . . ?
B18 B20 B14 B13 -100.69(8) . . . . ?
B21 B20 B14 B13 -138.21(7) . . . . ?
B19 B20 B14 B13 -37.03(7) . . . . ?
B13 B20 B14 B21 138.21(7) . . . . ?
B18 B20 B14 B21 37.52(7) . . . . ?
B19 B20 B14 B21 101.18(8) . . . . ?
C11 C10 B13 B20 154.27(8) . . . . ?
C5 C10 B13 B20 -62.95(8) . . . . ?
B14 C10 B13 B20 39.57(7) . . . . ?
B12 C10 B13 B20 -101.68(7) . . . . ?
B15 C10 B13 B20 2.45(9) . . . . ?
C11 C10 B13 B19 -142.63(8) . . . . ?
C5 C10 B13 B19 0.15(9) . . . . ?
B14 C10 B13 B19 102.67(8) . . . . ?
B12 C10 B13 B19 -38.59(7) . . . . ?
B15 C10 B13 B19 65.55(9) . . . . ?
C11 C10 B13 B12 -104.05(8) . . . . ?
C5 C10 B13 B12 38.74(6) . . . . ?
B14 C10 B13 B12 141.25(7) . . . . ?
B15 C10 B13 B12 104.14(7) . . . . ?
C11 C10 B13 B14 114.70(9) . . . . ?
C5 C10 B13 B14 -102.52(7) . . . . ?
B12 C10 B13 B14 -141.25(7) . . . . ?
B15 C10 B13 B14 -37.12(7) . . . . ?
B18 B20 B13 C10 62.22(9) . . . . ?
B21 B20 B13 C10 -1.67(9) . . . . ?
B14 B20 B13 C10 -39.03(6) . . . . ?
B19 B20 B13 C10 99.43(7) . . . . ?
B18 B20 B13 B19 -37.22(7) . . . . ?
B21 B20 B13 B19 -101.11(8) . . . . ?
B14 B20 B13 B19 -138.46(7) . . . . ?
B18 B20 B13 B12 0.09(10) . . . . ?
B21 B20 B13 B12 -63.80(9) . . . . ?
B14 B20 B13 B12 -101.15(7) . . . . ?
B19 B20 B13 B12 37.31(7) . . . . ?
B18 B20 B13 B14 101.24(8) . . . . ?
B21 B20 B13 B14 37.36(7) . . . . ?
B19 B20 B13 B14 138.46(7) . . . . ?
B12 B19 B13 C10 38.47(6) . . . . ?
B17 B19 B13 C10 0.72(9) . . . . ?
B18 B19 B13 C10 -62.59(8) . . . . ?
B20 B19 B13 C10 -99.49(8) . . . . ?
B12 B19 B13 B20 137.95(7) . . . . ?
B17 B19 B13 B20 100.20(8) . . . . ?
B18 B19 B13 B20 36.90(7) . . . . ?
B17 B19 B13 B12 -37.75(7) . . . . ?
B18 B19 B13 B12 -101.06(7) . . . . ?
B20 B19 B13 B12 -137.95(7) . . . . ?
B12 B19 B13 B14 100.54(7) . . . . ?
B17 B19 B13 B14 62.79(9) . . . . ?
B18 B19 B13 B14 -0.51(9) . . . . ?
B20 B19 B13 B14 -37.41(7) . . . . ?
C5 B12 B13 C10 -36.47(6) . . . . ?
B19 B12 B13 C10 -135.82(7) . . . . ?
B17 B12 B13 C10 -97.89(7) . . . . ?
C10 B12 B13 B20 98.08(8) . . . . ?
C5 B12 B13 B20 61.61(8) . . . . ?
B19 B12 B13 B20 -37.75(7) . . . . ?
B17 B12 B13 B20 0.19(9) . . . . ?
C10 B12 B13 B19 135.82(7) . . . . ?
C5 B12 B13 B19 99.36(7) . . . . ?
B17 B12 B13 B19 37.94(7) . . . . ?
C10 B12 B13 B14 34.41(6) . . . . ?
C5 B12 B13 B14 -2.05(9) . . . . ?
B19 B12 B13 B14 -101.41(8) . . . . ?
B17 B12 B13 B14 -63.48(8) . . . . ?
B15 B14 B13 C10 34.91(6) . . . . ?
B21 B14 B13 C10 97.77(7) . . . . ?
B20 B14 B13 C10 135.05(7) . . . . ?
C10 B14 B13 B20 -135.05(7) . . . . ?
B15 B14 B13 B20 -100.14(8) . . . . ?
B21 B14 B13 B20 -37.29(7) . . . . ?
C10 B14 B13 B19 -97.53(7) . . . . ?
B15 B14 B13 B19 -62.62(9) . . . . ?
B21 B14 B13 B19 0.24(9) . . . . ?
B20 B14 B13 B19 37.52(7) . . . . ?
C10 B14 B13 B12 -34.47(6) . . . . ?
B15 B14 B13 B12 0.44(9) . . . . ?
B21 B14 B13 B12 63.29(9) . . . . ?
B20 B14 B13 B12 100.58(8) . . . . ?
C3 C2 B2 C1 97.41(7) . . . . ?
B7 C2 B2 C1 -139.82(7) . . . . ?
B6 C2 B2 C1 -103.21(8) . . . . ?
B5 C2 B2 C1 -33.05(7) . . . . ?
C3 C2 B2 B8 -163.54(7) . . . . ?
C1 C2 B2 B8 99.05(7) . . . . ?
B7 C2 B2 B8 -40.77(7) . . . . ?
B6 C2 B2 B8 -4.16(9) . . . . ?
B5 C2 B2 B8 66.00(8) . . . . ?
C3 C2 B2 B3 133.74(7) . . . . ?
C1 C2 B2 B3 36.33(6) . . . . ?
B7 C2 B2 B3 -103.50(7) . . . . ?
B6 C2 B2 B3 -66.88(8) . . . . ?
B5 C2 B2 B3 3.28(9) . . . . ?
C3 C2 B2 B7 -122.76(8) . . . . ?
C1 C2 B2 B7 139.82(7) . . . . ?
B6 C2 B2 B7 36.61(7) . . . . ?
B5 C2 B2 B7 106.77(8) . . . . ?
B1 C1 B2 C2 -92.65(7) . . . . ?
B3 C1 B2 C2 137.49(7) . . . . ?
B4 C1 B2 C2 101.06(7) . . . . ?
B5 C1 B2 C2 32.72(7) . . . . ?
B1 C1 B2 B8 170.08(7) . . . . ?
C2 C1 B2 B8 -97.26(7) . . . . ?
B3 C1 B2 B8 40.23(7) . . . . ?
B4 C1 B2 B8 3.80(9) . . . . ?
B5 C1 B2 B8 -64.55(8) . . . . ?
B1 C1 B2 B3 129.86(8) . . . . ?
C2 C1 B2 B3 -137.49(7) . . . . ?
B4 C1 B2 B3 -36.43(7) . . . . ?
B5 C1 B2 B3 -104.78(7) . . . . ?
B1 C1 B2 B7 -126.92(7) . . . . ?
C2 C1 B2 B7 -34.27(6) . . . . ?
B3 C1 B2 B7 103.22(7) . . . . ?
B4 C1 B2 B7 66.79(8) . . . . ?
B5 C1 B2 B7 -1.56(9) . . . . ?
C2 B2 B8 B3 -98.01(7) . . . . ?
C1 B2 B8 B3 -39.11(6) . . . . ?
B7 B2 B8 B3 -137.30(7) . . . . ?
C2 B2 B8 B7 39.29(6) . . . . ?
C1 B2 B8 B7 98.20(7) . . . . ?
B3 B2 B8 B7 137.30(7) . . . . ?
C2 B2 B8 B9 -60.85(9) . . . . ?
C1 B2 B8 B9 -1.94(9) . . . . ?
B3 B2 B8 B9 37.17(7) . . . . ?
B7 B2 B8 B9 -100.14(8) . . . . ?
C2 B2 B8 B11 2.39(9) . . . . ?
C1 B2 B8 B11 61.30(9) . . . . ?
B3 B2 B8 B11 100.40(8) . . . . ?
B7 B2 B8 B11 -36.90(7) . . . . ?
C3 C2 B7 B11 -159.57(8) . . . . ?
C1 C2 B7 B11 64.14(9) . . . . ?
B6 C2 B7 B11 -40.68(7) . . . . ?
B2 C2 B7 B11 102.22(8) . . . . ?
B5 C2 B7 B11 -4.13(10) . . . . ?
C3 C2 B7 B6 -118.89(10) . . . . ?
C1 C2 B7 B6 104.83(8) . . . . ?
B2 C2 B7 B6 142.91(7) . . . . ?
B5 C2 B7 B6 36.55(7) . . . . ?
C3 C2 B7 B2 98.21(9) . . . . ?
C1 C2 B7 B2 -38.08(7) . . . . ?
B6 C2 B7 B2 -142.91(7) . . . . ?
B5 C2 B7 B2 -106.35(7) . . . . ?
C3 C2 B7 B8 138.08(8) . . . . ?
C1 C2 B7 B8 1.79(9) . . . . ?
B6 C2 B7 B8 -103.03(8) . . . . ?
B2 C2 B7 B8 39.87(7) . . . . ?
B5 C2 B7 B8 -66.48(9) . . . . ?
C1 B2 B7 C2 33.87(6) . . . . ?
B8 B2 B7 C2 133.45(7) . . . . ?
B3 B2 B7 C2 94.86(7) . . . . ?
C2 B2 B7 B11 -96.40(8) . . . . ?
C1 B2 B7 B11 -62.53(9) . . . . ?
B8 B2 B7 B11 37.04(7) . . . . ?
B3 B2 B7 B11 -1.54(10) . . . . ?
C2 B2 B7 B6 -32.85(7) . . . . ?
C1 B2 B7 B6 1.02(9) . . . . ?
B8 B2 B7 B6 100.59(8) . . . . ?
B3 B2 B7 B6 62.01(9) . . . . ?
C2 B2 B7 B8 -133.45(7) . . . . ?
C1 B2 B7 B8 -99.58(7) . . . . ?
B3 B2 B7 B8 -38.59(7) . . . . ?
B2 B8 B7 C2 -40.17(6) . . . . ?
B3 B8 B7 C2 -1.88(9) . . . . ?
B9 B8 B7 C2 61.32(9) . . . . ?
B11 B8 B7 C2 98.41(8) . . . . ?
B2 B8 B7 B11 -138.57(7) . . . . ?
B3 B8 B7 B11 -100.29(8) . . . . ?
B9 B8 B7 B11 -37.09(7) . . . . ?
B2 B8 B7 B6 -101.16(8) . . . . ?
B3 B8 B7 B6 -62.88(9) . . . . ?
B9 B8 B7 B6 0.32(9) . . . . ?
B11 B8 B7 B6 37.41(7) . . . . ?
B3 B8 B7 B2 38.28(7) . . . . ?
B9 B8 B7 B2 101.49(7) . . . . ?
B11 B8 B7 B2 138.57(7) . . . . ?
C3 C2 B6 B11 159.63(8) . . . . ?
C1 C2 B6 B11 -64.44(9) . . . . ?
B7 C2 B6 B11 40.47(7) . . . . ?
B2 C2 B6 B11 4.05(10) . . . . ?
B5 C2 B6 B11 -102.19(8) . . . . ?
C3 C2 B6 B7 119.16(10) . . . . ?
C1 C2 B6 B7 -104.91(8) . . . . ?
B2 C2 B6 B7 -36.42(7) . . . . ?
B5 C2 B6 B7 -142.66(7) . . . . ?
C3 C2 B6 B5 -98.19(9) . . . . ?
C1 C2 B6 B5 37.75(7) . . . . ?
B7 C2 B6 B5 142.66(7) . . . . ?
B2 C2 B6 B5 106.24(7) . . . . ?
C3 C2 B6 B10 -137.93(9) . . . . ?
C1 C2 B6 B10 -2.00(10) . . . . ?
B7 C2 B6 B10 102.91(8) . . . . ?
B2 C2 B6 B10 66.49(9) . . . . ?
B5 C2 B6 B10 -39.75(7) . . . . ?
B11 B7 B6 C2 133.18(7) . . . . ?
B2 B7 B6 C2 33.25(7) . . . . ?
B8 B7 B6 C2 95.69(7) . . . . ?
C2 B7 B6 B11 -133.18(7) . . . . ?
B2 B7 B6 B11 -99.93(8) . . . . ?
B8 B7 B6 B11 -37.49(7) . . . . ?
C2 B7 B6 B5 -33.45(7) . . . . ?
B11 B7 B6 B5 99.72(8) . . . . ?
B2 B7 B6 B5 -0.20(10) . . . . ?
B8 B7 B6 B5 62.24(9) . . . . ?
C2 B7 B6 B10 -95.71(7) . . . . ?
B11 B7 B6 B10 37.47(7) . . . . ?
B2 B7 B6 B10 -62.46(9) . . . . ?
B8 B7 B6 B10 -0.01(9) . . . . ?
C2 B6 B10 B5 40.15(7) . . . . ?
B11 B6 B10 B5 138.13(8) . . . . ?
B7 B6 B10 B5 100.91(8) . . . . ?
C2 B6 B10 B4 1.88(10) . . . . ?
B11 B6 B10 B4 99.86(8) . . . . ?
B7 B6 B10 B4 62.65(9) . . . . ?
B5 B6 B10 B4 -38.26(7) . . . . ?
C2 B6 B10 B9 -61.06(9) . . . . ?
B11 B6 B10 B9 36.92(7) . . . . ?
B7 B6 B10 B9 -0.30(10) . . . . ?
B5 B6 B10 B9 -101.21(8) . . . . ?
C2 B6 B10 B11 -97.98(8) . . . . ?
B7 B6 B10 B11 -37.22(7) . . . . ?
B5 B6 B10 B11 -138.13(8) . . . . ?
B2 B8 B9 B4 -0.37(10) . . . . ?
B3 B8 B9 B4 36.98(7) . . . . ?
B7 B8 B9 B4 -64.20(9) . . . . ?
B11 B8 B9 B4 -101.20(8) . . . . ?
B2 B8 B9 B11 100.83(8) . . . . ?
B3 B8 B9 B11 138.18(7) . . . . ?
B7 B8 B9 B11 37.01(7) . . . . ?
B2 B8 B9 B3 -37.35(7) . . . . ?
B7 B8 B9 B3 -101.17(7) . . . . ?
B11 B8 B9 B3 -138.18(7) . . . . ?
B2 B8 B9 B10 63.31(9) . . . . ?
B3 B8 B9 B10 100.66(8) . . . . ?
B7 B8 B9 B10 -0.51(9) . . . . ?
B11 B8 B9 B10 -37.52(7) . . . . ?
B5 B10 B9 B4 37.28(7) . . . . ?
B6 B10 B9 B4 101.01(8) . . . . ?
B11 B10 B9 B4 137.89(7) . . . . ?
B5 B10 B9 B11 -100.61(8) . . . . ?
B4 B10 B9 B11 -137.89(7) . . . . ?
B6 B10 B9 B11 -36.88(7) . . . . ?
B5 B10 B9 B3 0.33(10) . . . . ?
B4 B10 B9 B3 -36.95(7) . . . . ?
B6 B10 B9 B3 64.06(9) . . . . ?
B11 B10 B9 B3 100.95(8) . . . . ?
B5 B10 B9 B8 -63.23(9) . . . . ?
B4 B10 B9 B8 -100.51(8) . . . . ?
B6 B10 B9 B8 0.50(9) . . . . ?
B11 B10 B9 B8 37.38(7) . . . . ?
C2 B7 B11 B6 39.86(7) . . . . ?
B2 B7 B11 B6 101.84(8) . . . . ?
B8 B7 B11 B6 138.29(7) . . . . ?
C2 B7 B11 B9 -60.98(9) . . . . ?
B6 B7 B11 B9 -100.84(8) . . . . ?
B2 B7 B11 B9 1.00(10) . . . . ?
B8 B7 B11 B9 37.44(7) . . . . ?
C2 B7 B11 B8 -98.43(7) . . . . ?
B6 B7 B11 B8 -138.29(7) . . . . ?
B2 B7 B11 B8 -36.44(7) . . . . ?
C2 B7 B11 B10 2.51(10) . . . . ?
B6 B7 B11 B10 -37.35(7) . . . . ?
B2 B7 B11 B10 64.49(9) . . . . ?
B8 B7 B11 B10 100.94(8) . . . . ?
C2 B6 B11 B7 -39.67(6) . . . . ?
B5 B6 B11 B7 -101.64(8) . . . . ?
B10 B6 B11 B7 -138.36(7) . . . . ?
C2 B6 B11 B9 61.40(9) . . . . ?
B7 B6 B11 B9 101.07(8) . . . . ?
B5 B6 B11 B9 -0.57(10) . . . . ?
B10 B6 B11 B9 -37.28(7) . . . . ?
C2 B6 B11 B8 -2.23(10) . . . . ?
B7 B6 B11 B8 37.44(7) . . . . ?
B5 B6 B11 B8 -64.20(9) . . . . ?
B10 B6 B11 B8 -100.91(8) . . . . ?
C2 B6 B11 B10 98.69(7) . . . . ?
B7 B6 B11 B10 138.36(7) . . . . ?
B5 B6 B11 B10 36.71(7) . . . . ?
B4 B9 B11 B7 63.22(10) . . . . ?
B3 B9 B11 B7 -0.09(10) . . . . ?
B8 B9 B11 B7 -37.48(7) . . . . ?
B10 B9 B11 B7 100.97(8) . . . . ?
B4 B9 B11 B6 -0.40(10) . . . . ?
B3 B9 B11 B6 -63.70(9) . . . . ?
B8 B9 B11 B6 -101.10(8) . . . . ?
B10 B9 B11 B6 37.36(7) . . . . ?
B4 B9 B11 B8 100.70(8) . . . . ?
B3 B9 B11 B8 37.39(7) . . . . ?
B10 B9 B11 B8 138.46(7) . . . . ?
B4 B9 B11 B10 -37.76(7) . . . . ?
B3 B9 B11 B10 -101.06(8) . . . . ?
B8 B9 B11 B10 -138.46(7) . . . . ?
B2 B8 B11 B7 37.28(7) . . . . ?
B3 B8 B11 B7 100.99(8) . . . . ?
B9 B8 B11 B7 138.24(7) . . . . ?
B2 B8 B11 B6 -0.13(10) . . . . ?
B3 B8 B11 B6 63.58(9) . . . . ?
B7 B8 B11 B6 -37.40(7) . . . . ?
B9 B8 B11 B6 100.83(8) . . . . ?
B2 B8 B11 B9 -100.96(8) . . . . ?
B3 B8 B11 B9 -37.25(7) . . . . ?
B7 B8 B11 B9 -138.24(7) . . . . ?
B2 B8 B11 B10 -63.79(9) . . . . ?
B3 B8 B11 B10 -0.07(10) . . . . ?
B7 B8 B11 B10 -101.06(8) . . . . ?
B9 B8 B11 B10 37.18(7) . . . . ?
B5 B10 B11 B7 -0.24(10) . . . . ?
B4 B10 B11 B7 -63.66(9) . . . . ?
B9 B10 B11 B7 -100.97(8) . . . . ?
B6 B10 B11 B7 37.34(7) . . . . ?
B5 B10 B11 B6 -37.59(7) . . . . ?
B4 B10 B11 B6 -101.00(8) . . . . ?
B9 B10 B11 B6 -138.31(7) . . . . ?
B5 B10 B11 B9 100.72(8) . . . . ?
B4 B10 B11 B9 37.31(7) . . . . ?
B6 B10 B11 B9 138.31(7) . . . . ?
B5 B10 B11 B8 63.48(9) . . . . ?
B4 B10 B11 B8 0.07(10) . . . . ?
B9 B10 B11 B8 -37.24(7) . . . . ?
B6 B10 B11 B8 101.07(8) . . . . ?
B1 C1 B4 B5 91.19(9) . . . . ?
C2 C1 B4 B5 -39.32(7) . . . . ?
B3 C1 B4 B5 -142.11(7) . . . . ?
B2 C1 B4 B5 -105.82(7) . . . . ?
B1 C1 B4 B3 -126.70(9) . . . . ?
C2 C1 B4 B3 102.79(7) . . . . ?
B5 C1 B4 B3 142.11(7) . . . . ?
B2 C1 B4 B3 36.29(7) . . . . ?
B1 C1 B4 B9 -166.99(8) . . . . ?
C2 C1 B4 B9 62.50(8) . . . . ?
B3 C1 B4 B9 -40.29(6) . . . . ?
B5 C1 B4 B9 101.82(7) . . . . ?
B2 C1 B4 B9 -4.00(9) . . . . ?
B1 C1 B4 B10 130.45(9) . . . . ?
C2 C1 B4 B10 -0.06(9) . . . . ?
B3 C1 B4 B10 -102.85(7) . . . . ?
B5 C1 B4 B10 39.26(7) . . . . ?
B2 C1 B4 B10 -66.56(8) . . . . ?
B11 B9 B4 C1 -61.12(9) . . . . ?
B3 B9 B4 C1 39.60(6) . . . . ?
B8 B9 B4 C1 2.55(9) . . . . ?
B10 B9 B4 C1 -99.04(7) . . . . ?
B11 B9 B4 B5 1.22(10) . . . . ?
B3 B9 B4 B5 101.94(7) . . . . ?
B8 B9 B4 B5 64.89(9) . . . . ?
B10 B9 B4 B5 -36.70(7) . . . . ?
B11 B9 B4 B3 -100.72(8) . . . . ?
B8 B9 B4 B3 -37.05(7) . . . . ?
B10 B9 B4 B3 -138.64(7) . . . . ?
B11 B9 B4 B10 37.92(7) . . . . ?
B3 B9 B4 B10 138.64(7) . . . . ?
B8 B9 B4 B10 101.59(8) . . . . ?
B5 B10 B4 C1 -39.54(6) . . . . ?
B9 B10 B4 C1 98.82(7) . . . . ?
B6 B10 B4 C1 -1.15(9) . . . . ?
B11 B10 B4 C1 61.56(9) . . . . ?
B9 B10 B4 B5 138.36(7) . . . . ?
B6 B10 B4 B5 38.39(7) . . . . ?
B11 B10 B4 B5 101.11(8) . . . . ?
B5 B10 B4 B3 -101.15(7) . . . . ?
B9 B10 B4 B3 37.22(7) . . . . ?
B6 B10 B4 B3 -62.76(9) . . . . ?
B11 B10 B4 B3 -0.04(9) . . . . ?
B5 B10 B4 B9 -138.36(7) . . . . ?
B6 B10 B4 B9 -99.97(8) . . . . ?
B11 B10 B4 B9 -37.26(7) . . . . ?
C3 C2 B5 C1 -97.37(7) . . . . ?
B7 C2 B5 C1 103.31(8) . . . . ?
B6 C2 B5 C1 140.09(7) . . . . ?
B2 C2 B5 C1 33.11(6) . . . . ?
C3 C2 B5 B10 163.33(7) . . . . ?
C1 C2 B5 B10 -99.30(7) . . . . ?
B7 C2 B5 B10 4.01(9) . . . . ?
B6 C2 B5 B10 40.79(7) . . . . ?
B2 C2 B5 B10 -66.20(9) . . . . ?
C3 C2 B5 B4 -133.79(7) . . . . ?
C1 C2 B5 B4 -36.43(6) . . . . ?
B7 C2 B5 B4 66.88(9) . . . . ?
B6 C2 B5 B4 103.67(8) . . . . ?
B2 C2 B5 B4 -3.32(9) . . . . ?
C3 C2 B5 B6 122.54(8) . . . . ?
C1 C2 B5 B6 -140.09(7) . . . . ?
B7 C2 B5 B6 -36.79(7) . . . . ?
B2 C2 B5 B6 -106.99(8) . . . . ?
B1 C1 B5 C2 94.73(7) . . . . ?
B3 C1 B5 C2 -101.08(7) . . . . ?
B4 C1 B5 C2 -137.43(7) . . . . ?
B2 C1 B5 C2 -32.63(7) . . . . ?
B1 C1 B5 B10 -168.03(7) . . . . ?
C2 C1 B5 B10 97.24(7) . . . . ?
B3 C1 B5 B10 -3.83(9) . . . . ?
B4 C1 B5 B10 -40.18(7) . . . . ?
B2 C1 B5 B10 64.62(9) . . . . ?
B1 C1 B5 B4 -127.84(7) . . . . ?
C2 C1 B5 B4 137.43(7) . . . . ?
B3 C1 B5 B4 36.35(7) . . . . ?
B2 C1 B5 B4 104.80(7) . . . . ?
B1 C1 B5 B6 128.79(7) . . . . ?
C2 C1 B5 B6 34.06(6) . . . . ?
B3 C1 B5 B6 -67.01(8) . . . . ?
B4 C1 B5 B6 -103.37(7) . . . . ?
B2 C1 B5 B6 1.43(9) . . . . ?
B4 B10 B5 C2 97.94(7) . . . . ?
B9 B10 B5 C2 60.86(9) . . . . ?
B6 B10 B5 C2 -39.25(6) . . . . ?
B11 B10 B5 C2 -2.08(9) . . . . ?
B4 B10 B5 C1 39.07(6) . . . . ?
B9 B10 B5 C1 1.99(9) . . . . ?
B6 B10 B5 C1 -98.13(7) . . . . ?
B11 B10 B5 C1 -60.96(9) . . . . ?
B9 B10 B5 B4 -37.08(7) . . . . ?
B6 B10 B5 B4 -137.20(8) . . . . ?
B11 B10 B5 B4 -100.02(8) . . . . ?
B4 B10 B5 B6 137.20(8) . . . . ?
B9 B10 B5 B6 100.12(8) . . . . ?
B11 B10 B5 B6 37.18(7) . . . . ?
C1 B4 B5 C2 35.61(6) . . . . ?
B3 B4 B5 C2 1.92(9) . . . . ?
B9 B4 B5 C2 -61.76(8) . . . . ?
B10 B4 B5 C2 -98.96(7) . . . . ?
B3 B4 B5 C1 -33.69(6) . . . . ?
B9 B4 B5 C1 -97.37(7) . . . . ?
B10 B4 B5 C1 -134.57(7) . . . . ?
C1 B4 B5 B10 134.57(7) . . . . ?
B3 B4 B5 B10 100.88(8) . . . . ?
B9 B4 B5 B10 37.20(7) . . . . ?
C1 B4 B5 B6 95.78(7) . . . . ?
B3 B4 B5 B6 62.10(9) . . . . ?
B9 B4 B5 B6 -1.58(9) . . . . ?
B10 B4 B5 B6 -38.78(7) . . . . ?
B11 B6 B5 C2 96.10(8) . . . . ?
B7 B6 B5 C2 32.93(7) . . . . ?
B10 B6 B5 C2 133.54(7) . . . . ?
C2 B6 B5 C1 -33.63(6) . . . . ?
B11 B6 B5 C1 62.48(9) . . . . ?
B7 B6 B5 C1 -0.70(9) . . . . ?
B10 B6 B5 C1 99.91(7) . . . . ?
C2 B6 B5 B10 -133.54(7) . . . . ?
B11 B6 B5 B10 -37.43(7) . . . . ?
B7 B6 B5 B10 -100.61(8) . . . . ?
C2 B6 B5 B4 -94.76(7) . . . . ?
B11 B6 B5 B4 1.34(10) . . . . ?
B7 B6 B5 B4 -61.84(9) . . . . ?
B10 B6 B5 B4 38.77(7) . . . . ?
B1 C1 B3 B4 122.58(10) . . . . ?
C2 C1 B3 B4 -102.91(7) . . . . ?
B5 C1 B3 B4 -36.17(7) . . . . ?
B2 C1 B3 B4 -142.04(7) . . . . ?
B1 C1 B3 B2 -95.38(10) . . . . ?
C2 C1 B3 B2 39.13(6) . . . . ?
B4 C1 B3 B2 142.04(7) . . . . ?
B5 C1 B3 B2 105.87(7) . . . . ?
B1 C1 B3 B9 162.75(8) . . . . ?
C2 C1 B3 B9 -62.74(8) . . . . ?
B4 C1 B3 B9 40.17(6) . . . . ?
B5 C1 B3 B9 4.00(9) . . . . ?
B2 C1 B3 B9 -101.87(7) . . . . ?
B1 C1 B3 B8 -134.77(9) . . . . ?
C2 C1 B3 B8 -0.26(9) . . . . ?
B4 C1 B3 B8 102.65(7) . . . . ?
B5 C1 B3 B8 66.48(8) . . . . ?
B2 C1 B3 B8 -39.39(6) . . . . ?
B5 B4 B3 C1 34.03(6) . . . . ?
B9 B4 B3 C1 133.94(7) . . . . ?
B10 B4 B3 C1 96.72(7) . . . . ?
C1 B4 B3 B2 -34.10(6) . . . . ?
B5 B4 B3 B2 -0.07(9) . . . . ?
B9 B4 B3 B2 99.84(7) . . . . ?
B10 B4 B3 B2 62.62(8) . . . . ?
C1 B4 B3 B9 -133.94(7) . . . . ?
B5 B4 B3 B9 -99.91(8) . . . . ?
B10 B4 B3 B9 -37.22(7) . . . . ?
C1 B4 B3 B8 -96.73(7) . . . . ?
B5 B4 B3 B8 -62.70(9) . . . . ?
B9 B4 B3 B8 37.21(7) . . . . ?
B10 B4 B3 B8 -0.01(9) . . . . ?
C2 B2 B3 C1 -35.60(6) . . . . ?
B8 B2 B3 C1 -134.36(7) . . . . ?
B7 B2 B3 C1 -95.76(7) . . . . ?
C2 B2 B3 B4 -1.82(8) . . . . ?
C1 B2 B3 B4 33.78(6) . . . . ?
B8 B2 B3 B4 -100.58(8) . . . . ?
B7 B2 B3 B4 -61.98(9) . . . . ?
C2 B2 B3 B9 61.65(8) . . . . ?
C1 B2 B3 B9 97.25(7) . . . . ?
B8 B2 B3 B9 -37.11(7) . . . . ?
B7 B2 B3 B9 1.49(9) . . . . ?
C2 B2 B3 B8 98.76(7) . . . . ?
C1 B2 B3 B8 134.36(7) . . . . ?
B7 B2 B3 B8 38.60(7) . . . . ?
B4 B9 B3 C1 -39.61(6) . . . . ?
B11 B9 B3 C1 61.47(9) . . . . ?
B8 B9 B3 C1 98.95(7) . . . . ?
B10 B9 B3 C1 -2.53(9) . . . . ?
B11 B9 B3 B4 101.08(8) . . . . ?
B8 B9 B3 B4 138.56(7) . . . . ?
B10 B9 B3 B4 37.08(7) . . . . ?
B4 B9 B3 B2 -101.94(7) . . . . ?
B11 B9 B3 B2 -0.86(9) . . . . ?
B8 B9 B3 B2 36.62(7) . . . . ?
B10 B9 B3 B2 -64.86(9) . . . . ?
B4 B9 B3 B8 -138.56(7) . . . . ?
B11 B9 B3 B8 -37.48(7) . . . . ?
B10 B9 B3 B8 -101.48(8) . . . . ?
B2 B8 B3 C1 39.69(6) . . . . ?
B7 B8 B3 C1 1.34(9) . . . . ?
B9 B8 B3 C1 -98.76(7) . . . . ?
B11 B8 B3 C1 -61.57(9) . . . . ?
B2 B8 B3 B4 101.31(7) . . . . ?
B7 B8 B3 B4 62.96(9) . . . . ?
B9 B8 B3 B4 -37.14(7) . . . . ?
B11 B8 B3 B4 0.05(9) . . . . ?
B7 B8 B3 B2 -38.34(7) . . . . ?
B9 B8 B3 B2 -138.45(7) . . . . ?
B11 B8 B3 B2 -101.26(8) . . . . ?
B2 B8 B3 B9 138.45(7) . . . . ?
B7 B8 B3 B9 100.10(8) . . . . ?
B11 B8 B3 B9 37.19(7) . . . . ?
