#------------------------------------------------------------------------------
#$Date: 2025-04-05 05:20:47 +0300 (Sat, 05 Apr 2025) $
#$Revision: 298793 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/57/37/1573786.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1573786
loop_
_publ_author_name
'Phang, Si Jia Isabel'
'Zhang, Zheng-Feng'
'Wu, Chi-Shiun'
'Wong, Zhen Xuan'
'Su, Ming-Der'
'So, Cheuk-Wai'
_publ_section_title
;
 A silicon analogue of a fused bicyclic borirene derivative.
;
_journal_issue                   10
_journal_name_full               'Chemical science'
_journal_page_first              4512
_journal_page_last               4518
_journal_paper_doi               10.1039/d4sc05867d
_journal_volume                  16
_journal_year                    2025
_chemical_formula_sum            'C61 H88 B2 Cl2.03 I1.97 N4 P2 Si2'
_chemical_formula_weight         1339.13
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_update_record
;
2023-05-29 deposited with the CCDC.	2025-01-26 downloaded from the CCDC.
;
_cell_angle_alpha                105.263(5)
_cell_angle_beta                 106.255(5)
_cell_angle_gamma                95.783(6)
_cell_formula_units_Z            1
_cell_length_a                   10.922(2)
_cell_length_b                   12.040(2)
_cell_length_c                   13.307(2)
_cell_measurement_reflns_used    3865
_cell_measurement_temperature    100.(2)
_cell_measurement_theta_max      24.7659
_cell_measurement_theta_min      3.2796
_cell_volume                     1591.7(5)
_computing_cell_refinement       'SAINT V8.40B (Bruker AXS LLC, 2019)'
_computing_data_collection       'APEX4 (Ver 2021.4-0, Bruker AXS Inc., 2021)'
_computing_data_reduction        'SAINT V8.40B (Bruker AXS LLC, 2019)'
_computing_molecular_graphics    'shelXle (C.B. Huebschle, rev 1242)'
_computing_publication_material  'APEX4 (Ver 2021.4-0, Bruker AXS Inc., 2021)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'XT, VERSION 2018/2'
_diffrn_ambient_temperature      100.(2)
_diffrn_detector_area_resol_mean 7.3910
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  'Multilayer Mirror'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1735
_diffrn_reflns_av_unetI/netI     0.1394
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            21946
_diffrn_reflns_theta_full        25.11
_diffrn_reflns_theta_max         25.11
_diffrn_reflns_theta_min         2.15
_diffrn_source                   'Incoatec microfocus source'
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_type              'Incoatec I\mS 3.0'
_diffrn_source_voltage           50
_exptl_absorpt_coefficient_mu    1.187
_exptl_absorpt_correction_T_max  0.99
_exptl_absorpt_correction_T_min  0.73
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
Krause, L., Herbst-Irmer, R., Sheldrick, G. M., Stalke, D. (2015).
"Comparison of silver and molybdenum microfocus X-ray sources for
single-crystal structure determination"
J. Appl. Cryst. 48, 3-10.
doi:10.1107/S1600576714022985
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.397
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             689
_exptl_crystal_size_max          0.120
_exptl_crystal_size_mid          0.020
_exptl_crystal_size_min          0.010
_refine_diff_density_max         0.797
_refine_diff_density_min         -0.735
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.019
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     365
_refine_ls_number_reflns         5646
_refine_ls_number_restraints     570
_refine_ls_restrained_S_all      0.976
_refine_ls_R_factor_all          0.1605
_refine_ls_R_factor_gt           0.0810
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0738P)²+7.5889P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1677
_refine_ls_wR_factor_ref         0.2110
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3140
_reflns_number_total             5646
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4sc05867d2.cif
_cod_data_source_block           scw2739m
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_diffrn_radiation_probe' value 'X-ray' was changed to
'x-ray' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 1573783--1573788.cif.
;
_cod_database_code               1573786
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
B B1 0.5389(11) 0.3866(9) 0.4522(8) 0.029(2) Uani d . . . 1.000000 . .
Cl Cl1 0.816(2) 0.625(2) 0.6426(18) 0.044(5) Uani d U P . 0.493(5) A 1
I I1 0.8426(5) 0.6127(5) 0.6613(4) 0.0350(10) Uani d U P . 0.507(5) A 2
Cl Cl2 0.593(2) 0.2638(17) 0.5021(17) 0.032(3) Uani d U P . 0.522(5) B 1
I I2 0.6137(6) 0.2438(5) 0.5191(5) 0.0336(10) Uani d U P . 0.478(5) B 2
C C1 0.6898(8) 0.6481(7) 0.3588(7) 0.0265(17) Uani d U . . 1.000000 . .
C C2 0.7763(5) 0.7541(4) 0.4477(4) 0.0315(19) Uani d U . G 1.000000 . .
C C3 0.7273(4) 0.8395(5) 0.5096(5) 0.048(2) Uani d U . G 1.000000 . .
H H3 0.636382 0.831528 0.496856 0.058000 Uiso calc U . R 1.000000 . .
C C4 0.8114(6) 0.9366(5) 0.5902(5) 0.052(3) Uani d U . G 1.000000 . .
H H4 0.777992 0.994984 0.632447 0.062000 Uiso calc U . R 1.000000 . .
C C5 0.9445(6) 0.9483(5) 0.6088(4) 0.048(2) Uani d U . G 1.000000 . .
H H5 1.002007 1.014703 0.663881 0.058000 Uiso calc U . R 1.000000 . .
C C6 0.9935(4) 0.8630(5) 0.5470(5) 0.042(2) Uani d U . G 1.000000 . .
H H6 1.084414 0.870966 0.559724 0.050000 Uiso calc U . R 1.000000 . .
C C7 0.9094(5) 0.7659(5) 0.4664(5) 0.037(2) Uani d U . G 1.000000 . .
H H7 0.942806 0.707508 0.424131 0.045000 Uiso calc U . R 1.000000 . .
C C8 0.7074(5) 0.7298(4) 0.2196(4) 0.0278(17) Uani d U . G 1.000000 . .
C C9 0.6249(5) 0.8094(5) 0.2075(5) 0.0326(18) Uani d U . G 1.000000 . .
C C10 0.6498(5) 0.8948(4) 0.1593(5) 0.035(2) Uani d U . G 1.000000 . .
H H10 0.593406 0.949210 0.151031 0.042000 Uiso calc U . R 1.000000 . .
C C11 0.7574(6) 0.9006(4) 0.1232(5) 0.036(2) Uani d U . G 1.000000 . .
H H11 0.774410 0.958967 0.090226 0.043000 Uiso calc U . R 1.000000 . .
C C12 0.8399(5) 0.8210(5) 0.1353(5) 0.0339(19) Uani d U . G 1.000000 . .
H H12 0.913399 0.824941 0.110579 0.041000 Uiso calc U . R 1.000000 . .
C C13 0.8150(5) 0.7356(4) 0.1835(5) 0.0315(18) Uani d U . G 1.000000 . .
C C14 0.9084(9) 0.6508(9) 0.1933(8) 0.040(2) Uani d U . . 1.000000 . .
H H14 0.891094 0.609781 0.245637 0.048000 Uiso calc U . R 1.000000 . .
C C15 0.8824(10) 0.5561(10) 0.0823(8) 0.047(3) Uani d U . . 1.000000 . .
H H15A 0.936598 0.497341 0.092752 0.070000 Uiso calc U . R 1.000000 . .
H H15B 0.903333 0.592497 0.029948 0.070000 Uiso calc U . R 1.000000 . .
H H15C 0.790601 0.518169 0.053681 0.070000 Uiso calc U . R 1.000000 . .
C C16 1.0528(10) 0.7079(11) 0.2385(10) 0.058(3) Uani d U . . 1.000000 . .
H H16A 1.105532 0.648041 0.248591 0.086000 Uiso calc U . R 1.000000 . .
H H16B 1.070148 0.767988 0.309330 0.086000 Uiso calc U . R 1.000000 . .
H H16C 1.075032 0.744205 0.186516 0.086000 Uiso calc U . R 1.000000 . .
C C17 0.5006(9) 0.8054(8) 0.2406(8) 0.039(2) Uani d U . . 1.000000 . .
H H17 0.505376 0.752445 0.287662 0.047000 Uiso calc U . R 1.000000 . .
C C18 0.4872(12) 0.9245(9) 0.3072(10) 0.060(3) Uani d U . . 1.000000 . .
H H18A 0.412590 0.915181 0.333487 0.089000 Uiso calc U . R 1.000000 . .
H H18B 0.473954 0.976242 0.260860 0.089000 Uiso calc U . R 1.000000 . .
H H18C 0.566307 0.958744 0.370191 0.089000 Uiso calc U . R 1.000000 . .
C C19 0.3826(10) 0.7505(10) 0.1374(9) 0.049(3) Uani d U . . 1.000000 . .
H H19A 0.303998 0.742090 0.158603 0.074000 Uiso calc U . R 1.000000 . .
H H19B 0.393665 0.673149 0.097606 0.074000 Uiso calc U . R 1.000000 . .
H H19C 0.374593 0.801036 0.089867 0.074000 Uiso calc U . R 1.000000 . .
C C20 0.4478(10) 0.3828(9) 0.1975(7) 0.039(2) Uani d U . . 1.000000 . .
C C21 0.3730(10) 0.4833(8) 0.2158(7) 0.039(2) Uani d U . . 1.000000 . .
H H21A 0.287938 0.461804 0.158602 0.058000 Uiso calc U . R 1.000000 . .
H H21B 0.422068 0.554185 0.212271 0.058000 Uiso calc U . R 1.000000 . .
H H21C 0.361005 0.498264 0.288123 0.058000 Uiso calc U . R 1.000000 . .
C C22 0.4816(11) 0.3732(9) 0.0911(7) 0.049(3) Uani d U . . 1.000000 . .
H H22A 0.401629 0.360541 0.029794 0.073000 Uiso calc U . R 1.000000 . .
H H22B 0.526286 0.307150 0.076017 0.073000 Uiso calc U . R 1.000000 . .
H H22C 0.538349 0.445864 0.099770 0.073000 Uiso calc U . R 1.000000 . .
C C23 0.3632(10) 0.2642(8) 0.1819(7) 0.042(3) Uani d U . . 1.000000 . .
H H23A 0.281883 0.250739 0.121750 0.063000 Uiso calc U . R 1.000000 . .
H H23B 0.343825 0.266315 0.249904 0.063000 Uiso calc U . R 1.000000 . .
H H23C 0.410414 0.200583 0.164199 0.063000 Uiso calc U . R 1.000000 . .
C C24 0.7251(10) 0.3429(8) 0.3015(8) 0.040(2) Uani d U . . 1.000000 . .
C C25 0.8368(11) 0.3798(10) 0.4110(9) 0.052(3) Uani d U . . 1.000000 . .
H H25A 0.908491 0.339840 0.401398 0.079000 Uiso calc U . R 1.000000 . .
H H25B 0.806029 0.358387 0.467070 0.079000 Uiso calc U . R 1.000000 . .
H H25C 0.867207 0.464841 0.434425 0.079000 Uiso calc U . R 1.000000 . .
C C26 0.6837(12) 0.2071(8) 0.2621(9) 0.052(3) Uani d U . . 1.000000 . .
H H26A 0.760911 0.171276 0.265571 0.078000 Uiso calc U . R 1.000000 . .
H H26B 0.624959 0.181288 0.186144 0.078000 Uiso calc U . R 1.000000 . .
H H26C 0.639183 0.183040 0.309589 0.078000 Uiso calc U . R 1.000000 . .
C C27 0.7770(12) 0.3781(9) 0.2171(9) 0.052(3) Uani d U . . 1.000000 . .
H H27A 0.867527 0.368159 0.230624 0.078000 Uiso calc U . R 1.000000 . .
H H27B 0.772131 0.460365 0.223226 0.078000 Uiso calc U . R 1.000000 . .
H H27C 0.724621 0.328487 0.143033 0.078000 Uiso calc U . R 1.000000 . .
C C28 -0.075(2) 0.161(2) 0.0443(17) 0.049(5) Uani d U P D 0.500000 C -1
H H28A -0.141023 0.158452 -0.023933 0.073000 Uiso calc U P R 0.500000 C -1
H H28B -0.007754 0.231183 0.067790 0.073000 Uiso calc U P R 0.500000 C -1
H H28C -0.115564 0.162935 0.101625 0.073000 Uiso calc U P R 0.500000 C -1
C C29 -0.0161(14) 0.0563(11) 0.0254(11) 0.044(4) Uani d U P G 0.500000 C -1
C C30 0.0880(13) 0.0446(11) 0.1079(9) 0.044(4) Uani d U P DG 0.500000 C -1
H H30 0.119169 0.103140 0.177567 0.052000 Uiso calc U P R 0.500000 C -1
C C31 0.1466(12) -0.0527(12) 0.0885(10) 0.041(4) Uani d U P G 0.500000 C -1
H H31 0.217742 -0.060644 0.144872 0.049000 Uiso calc U P R 0.500000 C -1
C C32 0.1010(15) -0.1383(11) -0.0134(12) 0.046(5) Uani d U P G 0.500000 C -1
H H32 0.141016 -0.204816 -0.026667 0.056000 Uiso calc U P R 0.500000 C -1
C C33 -0.0031(15) -0.1267(11) -0.0959(10) 0.049(4) Uani d U P G 0.500000 C -1
H H33 -0.034282 -0.185205 -0.165512 0.058000 Uiso calc U P R 0.500000 C -1
C C34 -0.0617(13) -0.0294(13) -0.0765(10) 0.043(4) Uani d U P DG 0.500000 C -1
H H34 -0.132856 -0.021421 -0.132819 0.052000 Uiso calc U P R 0.500000 C -1
N N1 0.6412(7) 0.5574(6) 0.3949(6) 0.0287(17) Uani d U . . 1.000000 . .
N N2 0.6698(7) 0.6343(6) 0.2564(5) 0.0271(16) Uani d U . . 1.000000 . .
P P1 0.5868(2) 0.4108(2) 0.32566(18) 0.0303(7) Uani d . . . 1.000000 . .
Si Si1 0.6236(2) 0.5583(2) 0.52597(19) 0.0267(6) Uani d . . . 1.000000 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Cl2 B1 P1 . . 117.7(9) ?
Cl2 B1 Si1 . 2_666 119.6(9) ?
P1 B1 Si1 . 2_666 116.9(5) ?
Cl2 B1 Si1 . . 124.9(9) ?
P1 B1 Si1 . . 83.8(4) ?
Si1 B1 Si1 2_666 . 84.4(4) ?
P1 B1 I2 . . 117.8(5) ?
Si1 B1 I2 2_666 . 120.8(5) ?
Si1 B1 I2 . . 122.0(5) ?
N2 C1 N1 . . 121.0(7) ?
N2 C1 C2 . . 122.9(7) ?
N1 C1 C2 . . 115.8(7) ?
C3 C2 C7 . . 120.000000 ?
C3 C2 C1 . . 122.3(5) ?
C7 C2 C1 . . 117.7(5) ?
C2 C3 C4 . . 120.000000 ?
C3 C4 C5 . . 120.000000 ?
C6 C5 C4 . . 120.000000 ?
C5 C6 C7 . . 120.000000 ?
C6 C7 C2 . . 120.000000 ?
C9 C8 C13 . . 120.000000 ?
C9 C8 N2 . . 118.3(5) ?
C13 C8 N2 . . 121.2(5) ?
C8 C9 C10 . . 120.000000 ?
C8 C9 C17 . . 123.1(5) ?
C10 C9 C17 . . 116.8(5) ?
C9 C10 C11 . . 120.000000 ?
C12 C11 C10 . . 120.000000 ?
C11 C12 C13 . . 120.000000 ?
C12 C13 C8 . . 120.000000 ?
C12 C13 C14 . . 117.3(5) ?
C8 C13 C14 . . 122.7(5) ?
C13 C14 C16 . . 115.0(8) ?
C13 C14 C15 . . 111.1(8) ?
C16 C14 C15 . . 109.0(8) ?
C18 C17 C19 . . 111.8(9) ?
C18 C17 C9 . . 113.0(8) ?
C19 C17 C9 . . 109.3(7) ?
C21 C20 C22 . . 108.0(8) ?
C21 C20 C23 . . 111.1(8) ?
C22 C20 C23 . . 107.7(7) ?
C21 C20 P1 . . 107.4(6) ?
C22 C20 P1 . . 116.7(7) ?
C23 C20 P1 . . 106.1(7) ?
C27 C24 C25 . . 107.7(9) ?
C27 C24 C26 . . 108.0(8) ?
C25 C24 C26 . . 108.8(9) ?
C27 C24 P1 . . 114.5(7) ?
C25 C24 P1 . . 108.2(7) ?
C26 C24 P1 . . 109.5(7) ?
C30 C29 C34 . . 120.000000 ?
C30 C29 C28 . . 120.1(7) ?
C34 C29 C28 . . 119.8(7) ?
C29 C30 C31 . . 120.000000 ?
C32 C31 C30 . . 120.000000 ?
C33 C32 C31 . . 120.000000 ?
C32 C33 C34 . . 120.000000 ?
C33 C34 C29 . . 120.000000 ?
C1 N1 P1 . . 129.4(6) ?
C1 N1 Si1 . . 131.4(6) ?
P1 N1 Si1 . . 99.2(3) ?
C1 N2 C8 . . 120.7(6) ?
N1 P1 C24 . . 109.3(4) ?
N1 P1 C20 . . 112.6(4) ?
C24 P1 C20 . . 113.1(5) ?
N1 P1 B1 . . 90.3(4) ?
C24 P1 B1 . . 114.3(5) ?
C20 P1 B1 . . 115.0(4) ?
N1 P1 Si1 . . 41.6(2) ?
C24 P1 Si1 . . 117.6(3) ?
C20 P1 Si1 . . 128.6(3) ?
B1 P1 Si1 . . 48.9(3) ?
N1 Si1 B1 . 2_666 113.3(4) ?
N1 Si1 B1 . . 86.2(4) ?
B1 Si1 B1 2_666 . 95.6(4) ?
N1 Si1 Cl1 . . 105.1(7) ?
B1 Si1 Cl1 2_666 . 124.6(7) ?
B1 Si1 Cl1 . . 126.0(7) ?
N1 Si1 I1 . . 107.4(3) ?
B1 Si1 I1 2_666 . 127.0(3) ?
B1 Si1 I1 . . 120.0(4) ?
N1 Si1 P1 . . 39.2(2) ?
B1 Si1 P1 2_666 . 114.1(3) ?
B1 Si1 P1 . . 47.2(3) ?
Cl1 Si1 P1 . . 120.9(7) ?
I1 Si1 P1 . . 118.89(17) ?
N1 Si1 Si1 . 2_666 104.1(3) ?
B1 Si1 Si1 2_666 2_666 47.9(3) ?
B1 Si1 Si1 . 2_666 47.7(3) ?
Cl1 Si1 Si1 . 2_666 149.4(7) ?
I1 Si1 Si1 . 2_666 145.1(2) ?
P1 Si1 Si1 . 2_666 78.29(11) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
B1 Cl2 . 1.856(17) ?
B1 P1 . 1.979(10) ?
B1 Si1 2_666 2.025(11) ?
B1 Si1 . 2.033(10) ?
B1 I2 . 2.258(11) ?
Cl1 Si1 . 2.16(2) ?
I1 Si1 . 2.458(6) ?
C1 N2 . 1.281(10) ?
C1 N1 . 1.416(10) ?
C1 C2 . 1.503(9) ?
C2 C3 . 1.390000 ?
C2 C7 . 1.390000 ?
C3 C4 . 1.390000 ?
C4 C5 . 1.390000 ?
C5 C6 . 1.390000 ?
C6 C7 . 1.390000 ?
C8 C9 . 1.390000 ?
C8 C13 . 1.390000 ?
C8 N2 . 1.430(7) ?
C9 C10 . 1.390000 ?
C9 C17 . 1.539(10) ?
C10 C11 . 1.390000 ?
C11 C12 . 1.390000 ?
C12 C13 . 1.390000 ?
C13 C14 . 1.518(11) ?
C14 C16 . 1.535(13) ?
C14 C15 . 1.541(13) ?
C17 C18 . 1.520(14) ?
C17 C19 . 1.531(14) ?
C20 C21 . 1.533(14) ?
C20 C22 . 1.538(12) ?
C20 C23 . 1.552(12) ?
C20 P1 . 1.863(10) ?
C24 C27 . 1.524(13) ?
C24 C25 . 1.537(14) ?
C24 C26 . 1.556(13) ?
C24 P1 . 1.854(10) ?
C28 C29 . 1.47(2) ?
C29 C30 . 1.390000 ?
C29 C34 . 1.390000 ?
C30 C31 . 1.390000 ?
C31 C32 . 1.390000 ?
C32 C33 . 1.390000 ?
C33 C34 . 1.390000 ?
N1 P1 . 1.716(7) ?
N1 Si1 . 1.804(7) ?
P1 Si1 . 2.680(3) ?
Si1 Si1 2_666 2.725(5) ?
