#------------------------------------------------------------------------------
#$Date: 2025-07-06 17:34:23 +0300 (Sun, 06 Jul 2025) $
#$Revision: 300640 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/57/41/1574176.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1574176
loop_
_publ_author_name
'Yuhara, Kazuhiro'
'Tanaka, Kazuo'
_publ_section_title
;
 Solid-state temperature-dependent luminescence of
 C,C′-diaryl-o-carboranes based on restriction of excited-state
 structural relaxation
;
_journal_issue                   15
_journal_name_full               'Chemical Science'
_journal_page_first              6495
_journal_page_last               6506
_journal_paper_doi               10.1039/D5SC00875A
_journal_volume                  16
_journal_year                    2025
_chemical_formula_moiety         'C26 H26 B10 S'
_chemical_formula_sum            'C26 H26 B10 S'
_chemical_formula_weight         478.63
_chemical_name_common            T-H
_chemical_name_systematic        T-H
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2024-12-20 deposited with the CCDC.	2025-03-05 downloaded from the CCDC.
;
_cell_angle_alpha                109.650(5)
_cell_angle_beta                 100.826(3)
_cell_angle_gamma                99.410(5)
_cell_formula_units_Z            2
_cell_length_a                   9.459(4)
_cell_length_b                   11.316(5)
_cell_length_c                   12.775(6)
_cell_measurement_reflns_used    3703
_cell_measurement_temperature    143(2)
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.1
_cell_volume                     1226.3(9)
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      143(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.977
_diffrn_measured_fraction_theta_max 0.953
_diffrn_measurement_device_type  'Rigaku Saturn724+ (4x4 bin mode)'
_diffrn_measurement_method       'profile data from ω-scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0486
_diffrn_reflns_av_unetI/netI     0.1152
_diffrn_reflns_Laue_measured_fraction_full 0.977
_diffrn_reflns_Laue_measured_fraction_max 0.953
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            10041
_diffrn_reflns_point_group_measured_fraction_full 0.977
_diffrn_reflns_point_group_measured_fraction_max 0.953
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.488
_diffrn_reflns_theta_min         3.057
_diffrn_source                   'Rotating Anode'
_exptl_absorpt_coefficient_mu    0.149
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.771
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'REQAB; Rigaku, 1998'
_exptl_crystal_colour            Orange
_exptl_crystal_density_diffrn    1.296
_exptl_crystal_description       Block
_exptl_crystal_F_000             496
_exptl_crystal_preparation       Luminescent
_exptl_crystal_size_max          0.170
_exptl_crystal_size_mid          0.170
_exptl_crystal_size_min          0.070
_refine_diff_density_max         0.263
_refine_diff_density_min         -0.275
_refine_diff_density_rms         0.051
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.872
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     334
_refine_ls_number_reflns         5379
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.872
_refine_ls_R_factor_all          0.0649
_refine_ls_R_factor_gt           0.0416
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0322P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0944
_refine_ls_wR_factor_ref         0.0990
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3074
_reflns_number_total             5379
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d5sc00875a2.cif
_cod_data_source_block           T-H
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 1574174--1574180.cif.
;
_cod_database_code               1574176
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.975
_shelx_estimated_absorpt_t_max   0.990
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
S1 S 0.29626(6) 0.29808(5) 0.43513(4) 0.03506(15) Uani 1 1 d . . . . .
C1 C 0.76667(18) 0.20716(16) 0.82559(15) 0.0177(4) Uani 1 1 d . . . . .
C2 C 0.63490(18) 0.26149(15) 0.90805(14) 0.0159(4) Uani 1 1 d . . . . .
C3 C 0.1412(2) 0.31518(18) 0.35297(17) 0.0324(5) Uani 1 1 d . . . . .
H3 H 0.125259 0.300074 0.274994 0.039 Uiso 1 1 calc R U . . .
C4 C 0.0460(2) 0.35307(19) 0.41536(17) 0.0337(5) Uani 1 1 d . . . . .
H4 H -0.043811 0.367892 0.385306 0.040 Uiso 1 1 calc R U . . .
C5 C 0.0967(2) 0.36825(19) 0.53243(17) 0.0295(5) Uani 1 1 d . . . . .
H5 H 0.043387 0.394000 0.586786 0.035 Uiso 1 1 calc R U . . .
C6 C 0.23176(19) 0.34108(16) 0.55664(15) 0.0200(4) Uani 1 1 d . . . . .
C7 C 0.31596(18) 0.33492(16) 0.66356(15) 0.0184(4) Uani 1 1 d . . . . .
C8 C 0.27025(18) 0.22867(16) 0.69391(15) 0.0174(4) Uani 1 1 d . . . . .
C9 C 0.12738(18) 0.13978(16) 0.63490(15) 0.0209(4) Uani 1 1 d . . . . .
H9 H 0.066606 0.151742 0.574957 0.025 Uiso 1 1 calc R U . . .
C10 C 0.07957(19) 0.03977(16) 0.66434(15) 0.0224(4) Uani 1 1 d . . . . .
H10 H -0.014076 -0.015485 0.626210 0.027 Uiso 1 1 calc R U . . .
C11 C 0.17217(19) 0.01935(16) 0.75316(15) 0.0210(4) Uani 1 1 d . . . . .
H11 H 0.138044 -0.048741 0.774488 0.025 Uiso 1 1 calc R U . . .
C12 C 0.31117(18) 0.09759(15) 0.80866(15) 0.0186(4) Uani 1 1 d . . . . .
H12 H 0.371116 0.079096 0.864699 0.022 Uiso 1 1 calc R U . . .
C13 C 0.36756(17) 0.20727(16) 0.78324(14) 0.0162(4) Uani 1 1 d . . . . .
C14 C 0.50813(17) 0.29830(15) 0.84457(14) 0.0152(4) Uani 1 1 d . . . . .
C15 C 0.52868(18) 0.42153(16) 0.83540(14) 0.0165(4) Uani 1 1 d . . . . .
C16 C 0.63055(18) 0.53777(16) 0.92102(15) 0.0180(4) Uani 1 1 d . . . . .
H16 H 0.682228 0.535386 0.989520 0.022 Uiso 1 1 calc R U . . .
C17 C 0.65265(18) 0.65051(16) 0.90383(15) 0.0208(4) Uani 1 1 d . . . . .
H17 H 0.718780 0.723933 0.960954 0.025 Uiso 1 1 calc R U . . .
C18 C 0.57744(19) 0.65882(17) 0.80110(16) 0.0225(4) Uani 1 1 d . . . . .
H18 H 0.599519 0.735059 0.788183 0.027 Uiso 1 1 calc R U . . .
C19 C 0.47245(19) 0.55447(16) 0.72118(15) 0.0216(4) Uani 1 1 d . . . . .
H19 H 0.421568 0.560549 0.654169 0.026 Uiso 1 1 calc R U . . .
C20 C 0.43893(18) 0.43585(16) 0.73826(15) 0.0178(4) Uani 1 1 d . . . . .
C21 C 0.73754(17) 0.20464(16) 0.70503(15) 0.0184(4) Uani 1 1 d . . . . .
C22 C 0.75326(19) 0.31738(17) 0.68251(16) 0.0226(4) Uani 1 1 d . . . . .
H22 H 0.783288 0.397372 0.743434 0.027 Uiso 1 1 calc R U . . .
C23 C 0.7247(2) 0.31193(18) 0.57046(17) 0.0287(5) Uani 1 1 d . . . . .
H23 H 0.732929 0.388106 0.556722 0.034 Uiso 1 1 calc R U . . .
C24 C 0.6841(2) 0.19385(19) 0.47871(17) 0.0299(5) Uani 1 1 d . . . . .
H24 H 0.665882 0.190198 0.403430 0.036 Uiso 1 1 calc R U . . .
C25 C 0.6710(2) 0.08187(18) 0.50046(17) 0.0274(4) Uani 1 1 d . . . . .
H25 H 0.645519 0.002274 0.439292 0.033 Uiso 1 1 calc R U . . .
C26 C 0.69532(18) 0.08614(17) 0.61207(16) 0.0237(4) Uani 1 1 d . . . . .
H26 H 0.683408 0.009514 0.625140 0.028 Uiso 1 1 calc R U . . .
B1 B 0.8181(2) 0.35340(19) 0.93844(17) 0.0176(4) Uani 1 1 d . . . . .
H1A H 0.839897 0.444849 0.924714 0.021 Uiso 1 1 calc R U . . .
B2 B 0.7348(2) 0.33744(19) 1.04835(17) 0.0184(4) Uani 1 1 d . . . . .
H2A H 0.705419 0.419141 1.108602 0.022 Uiso 1 1 calc R U . . .
B3 B 0.6250(2) 0.17603(18) 0.99585(17) 0.0179(4) Uani 1 1 d . . . . .
H3A H 0.523783 0.150637 1.022274 0.022 Uiso 1 1 calc R U . . .
B4 B 0.6419(2) 0.09887(18) 0.85222(18) 0.0177(4) Uani 1 1 d . . . . .
H4A H 0.549870 0.025630 0.782904 0.021 Uiso 1 1 calc R U . . .
B5 B 0.8290(2) 0.0895(2) 0.86151(19) 0.0209(5) Uani 1 1 d . . . . .
H5A H 0.858501 0.008539 0.800519 0.025 Uiso 1 1 calc R U . . .
B6 B 0.9404(2) 0.25018(19) 0.91581(18) 0.0209(5) Uani 1 1 d . . . . .
H6A H 1.042845 0.274930 0.890648 0.025 Uiso 1 1 calc R U . . .
B7 B 0.9227(2) 0.33041(19) 1.05643(18) 0.0207(5) Uani 1 1 d . . . . .
H7A H 1.014188 0.407697 1.122746 0.025 Uiso 1 1 calc R U . . .
B8 B 0.7431(2) 0.0691(2) 0.96774(18) 0.0213(5) Uani 1 1 d . . . . .
H8A H 0.716691 -0.025505 0.975313 0.026 Uiso 1 1 calc R U . . .
B9 B 0.9302(2) 0.16477(19) 1.00921(18) 0.0218(5) Uani 1 1 d . . . . .
H9A H 1.025702 0.133441 1.044983 0.026 Uiso 1 1 calc R U . . .
B10 B 0.8037(2) 0.21836(19) 1.09055(19) 0.0214(5) Uani 1 1 d . . . . .
H10A H 0.818610 0.221525 1.179024 0.026 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 S1 C6 92.46(10) . . ?
C21 C1 B5 122.64(14) . . ?
C21 C1 B6 123.45(14) . . ?
B5 C1 B6 62.71(11) . . ?
C21 C1 B1 118.83(14) . . ?
B5 C1 B1 112.64(14) . . ?
B6 C1 B1 62.33(11) . . ?
C21 C1 B4 117.11(14) . . ?
B5 C1 B4 62.40(11) . . ?
B6 C1 B4 113.03(14) . . ?
B1 C1 B4 109.88(14) . . ?
C21 C1 C2 117.09(13) . . ?
B5 C1 C2 109.38(13) . . ?
B6 C1 C2 109.96(13) . . ?
B1 C1 C2 59.76(10) . . ?
B4 C1 C2 59.06(10) . . ?
C14 C2 B2 128.10(15) . . ?
C14 C2 B3 127.07(14) . . ?
B2 C2 B3 62.62(11) . . ?
C14 C2 B4 116.51(14) . . ?
B2 C2 B4 111.65(13) . . ?
B3 C2 B4 62.44(11) . . ?
C14 C2 B1 118.89(14) . . ?
B2 C2 B1 61.62(11) . . ?
B3 C2 B1 110.62(13) . . ?
B4 C2 B1 105.90(13) . . ?
C14 C2 C1 114.95(14) . . ?
B2 C2 C1 106.32(13) . . ?
B3 C2 C1 106.81(12) . . ?
B4 C2 C1 57.42(10) . . ?
B1 C2 C1 56.72(9) . . ?
C4 C3 S1 111.44(16) . . ?
C3 C4 C5 112.98(18) . . ?
C6 C5 C4 113.01(18) . . ?
C5 C6 C7 129.79(17) . . ?
C5 C6 S1 110.11(14) . . ?
C7 C6 S1 119.92(13) . . ?
C20 C7 C8 119.13(16) . . ?
C20 C7 C6 121.02(16) . . ?
C8 C7 C6 119.81(15) . . ?
C7 C8 C9 120.45(16) . . ?
C7 C8 C13 120.09(15) . . ?
C9 C8 C13 119.45(16) . . ?
C10 C9 C8 121.58(17) . . ?
C9 C10 C11 119.55(16) . . ?
C12 C11 C10 121.22(17) . . ?
C11 C12 C13 122.02(17) . . ?
C12 C13 C14 124.42(16) . . ?
C12 C13 C8 116.10(15) . . ?
C14 C13 C8 119.39(15) . . ?
C15 C14 C13 117.43(15) . . ?
C15 C14 C2 120.77(14) . . ?
C13 C14 C2 121.59(15) . . ?
C14 C15 C20 119.53(15) . . ?
C14 C15 C16 124.17(16) . . ?
C20 C15 C16 116.23(15) . . ?
C17 C16 C15 121.40(17) . . ?
C16 C17 C18 121.40(16) . . ?
C19 C18 C17 119.45(17) . . ?
C18 C19 C20 121.18(17) . . ?
C7 C20 C19 120.62(16) . . ?
C7 C20 C15 119.92(16) . . ?
C19 C20 C15 119.42(15) . . ?
C22 C21 C26 118.37(17) . . ?
C22 C21 C1 122.10(15) . . ?
C26 C21 C1 119.53(16) . . ?
C23 C22 C21 120.76(17) . . ?
C22 C23 C24 120.44(18) . . ?
C25 C24 C23 119.08(19) . . ?
C24 C25 C26 120.92(18) . . ?
C25 C26 C21 120.39(18) . . ?
C1 B1 B7 106.54(14) . . ?
C1 B1 C2 63.51(10) . . ?
B7 B1 C2 106.40(14) . . ?
C1 B1 B6 58.77(11) . . ?
B7 B1 B6 60.29(12) . . ?
C2 B1 B6 110.13(14) . . ?
C1 B1 B2 108.42(14) . . ?
B7 B1 B2 60.26(11) . . ?
C2 B1 B2 57.48(10) . . ?
B6 B1 B2 109.24(15) . . ?
C2 B2 B3 58.97(10) . . ?
C2 B2 B7 108.47(15) . . ?
B3 B2 B7 107.74(14) . . ?
C2 B2 B1 60.90(11) . . ?
B3 B2 B1 107.23(14) . . ?
B7 B2 B1 59.42(11) . . ?
C2 B2 B10 106.88(14) . . ?
B3 B2 B10 59.59(11) . . ?
B7 B2 B10 59.85(11) . . ?
B1 B2 B10 106.66(15) . . ?
C2 B3 B10 107.02(14) . . ?
C2 B3 B8 107.59(14) . . ?
B10 B3 B8 60.75(11) . . ?
C2 B3 B2 58.40(10) . . ?
B10 B3 B2 60.34(11) . . ?
B8 B3 B2 108.44(14) . . ?
C2 B3 B4 59.82(11) . . ?
B10 B3 B4 107.22(14) . . ?
B8 B3 B4 59.26(11) . . ?
B2 B3 B4 106.30(14) . . ?
C1 B4 C2 63.53(10) . . ?
C1 B4 B8 105.73(13) . . ?
C2 B4 B8 106.21(14) . . ?
C1 B4 B5 58.22(10) . . ?
C2 B4 B5 109.62(13) . . ?
B8 B4 B5 59.87(11) . . ?
C1 B4 B3 107.91(13) . . ?
C2 B4 B3 57.73(10) . . ?
B8 B4 B3 59.63(11) . . ?
B5 B4 B3 108.06(14) . . ?
C1 B5 B8 106.60(14) . . ?
C1 B5 B6 58.80(11) . . ?
B8 B5 B6 108.45(15) . . ?
C1 B5 B4 59.38(10) . . ?
B8 B5 B4 59.81(11) . . ?
B6 B5 B4 107.47(14) . . ?
C1 B5 B9 106.17(14) . . ?
B8 B5 B9 60.75(12) . . ?
B6 B5 B9 59.94(11) . . ?
B4 B5 B9 108.09(15) . . ?
C1 B6 B1 58.90(10) . . ?
C1 B6 B7 106.17(14) . . ?
B1 B6 B7 59.70(11) . . ?
C1 B6 B5 58.49(10) . . ?
B1 B6 B5 106.53(14) . . ?
B7 B6 B5 107.96(14) . . ?
C1 B6 B9 106.18(14) . . ?
B1 B6 B9 107.54(15) . . ?
B7 B6 B9 60.32(12) . . ?
B5 B6 B9 60.25(12) . . ?
B1 B7 B6 60.01(11) . . ?
B1 B7 B10 107.63(14) . . ?
B6 B7 B10 108.10(14) . . ?
B1 B7 B2 60.32(11) . . ?
B6 B7 B2 109.06(14) . . ?
B10 B7 B2 60.19(11) . . ?
B1 B7 B9 107.47(14) . . ?
B6 B7 B9 59.93(12) . . ?
B10 B7 B9 59.90(11) . . ?
B2 B7 B9 108.51(13) . . ?
B4 B8 B5 60.32(12) . . ?
B4 B8 B3 61.11(11) . . ?
B5 B8 B3 109.60(15) . . ?
B4 B8 B10 107.72(14) . . ?
B5 B8 B10 107.74(15) . . ?
B3 B8 B10 59.53(11) . . ?
B4 B8 B9 107.95(14) . . ?
B5 B8 B9 60.06(11) . . ?
B3 B8 B9 108.03(14) . . ?
B10 B8 B9 59.44(11) . . ?
B6 B9 B10 107.92(14) . . ?
B6 B9 B5 59.80(11) . . ?
B10 B9 B5 107.63(14) . . ?
B6 B9 B7 59.75(12) . . ?
B10 B9 B7 59.84(11) . . ?
B5 B9 B7 107.16(14) . . ?
B6 B9 B8 107.10(14) . . ?
B10 B9 B8 60.17(11) . . ?
B5 B9 B8 59.19(11) . . ?
B7 B9 B8 107.21(14) . . ?
B3 B10 B7 108.21(15) . . ?
B3 B10 B9 108.94(15) . . ?
B7 B10 B9 60.26(11) . . ?
B3 B10 B2 60.07(11) . . ?
B7 B10 B2 59.96(11) . . ?
B9 B10 B2 108.61(15) . . ?
B3 B10 B8 59.72(11) . . ?
B7 B10 B8 107.71(16) . . ?
B9 B10 B8 60.39(11) . . ?
B2 B10 B8 107.42(15) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S1 C3 1.715(2) . ?
S1 C6 1.7215(19) . ?
C1 C21 1.502(2) . ?
C1 B5 1.702(3) . ?
C1 B6 1.707(2) . ?
C1 B1 1.710(3) . ?
C1 B4 1.723(3) . ?
C1 C2 1.830(2) . ?
C2 C14 1.515(2) . ?
C2 B2 1.705(3) . ?
C2 B3 1.715(3) . ?
C2 B4 1.754(3) . ?
C2 B1 1.767(2) . ?
C3 C4 1.340(3) . ?
C4 C5 1.424(3) . ?
C5 C6 1.366(2) . ?
C6 C7 1.476(2) . ?
C7 C20 1.408(2) . ?
C7 C8 1.410(2) . ?
C8 C9 1.438(2) . ?
C8 C13 1.440(2) . ?
C9 C10 1.345(2) . ?
C10 C11 1.406(2) . ?
C11 C12 1.365(2) . ?
C12 C13 1.432(2) . ?
C13 C14 1.436(2) . ?
C14 C15 1.423(2) . ?
C15 C20 1.439(2) . ?
C15 C16 1.441(2) . ?
C16 C17 1.356(2) . ?
C17 C18 1.411(2) . ?
C18 C19 1.359(2) . ?
C19 C20 1.426(2) . ?
C21 C22 1.391(2) . ?
C21 C26 1.394(2) . ?
C22 C23 1.384(2) . ?
C23 C24 1.384(3) . ?
C24 C25 1.377(3) . ?
C25 C26 1.384(2) . ?
B1 B7 1.763(3) . ?
B1 B6 1.768(3) . ?
B1 B2 1.779(3) . ?
B2 B3 1.777(3) . ?
B2 B7 1.778(3) . ?
B2 B10 1.782(3) . ?
B3 B10 1.769(3) . ?
B3 B8 1.772(3) . ?
B3 B4 1.798(3) . ?
B4 B8 1.765(3) . ?
B4 B5 1.774(3) . ?
B5 B8 1.766(3) . ?
B5 B6 1.774(3) . ?
B5 B9 1.782(3) . ?
B6 B7 1.773(3) . ?
B6 B9 1.776(3) . ?
B7 B10 1.776(3) . ?
B7 B9 1.783(3) . ?
B8 B10 1.790(3) . ?
B8 B9 1.794(3) . ?
B9 B10 1.777(3) . ?
