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#$Date: 2016-02-19 16:29:56 +0200 (Fri, 19 Feb 2016) $
#$Revision: 176759 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/10/2001096.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2001096
loop_
_publ_author_name
'Kellö, E.'
'Vrábel, V.'
'Rattay, V.'
'Sivý, J.'
'Kožíšek, J.'
_publ_section_title
;
 Structure of tri-n-butyltin(IV) 1-uracilacetate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              51
_journal_page_last               53
_journal_paper_doi               10.1107/S0108270191008934
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C12 H27 Sn,C6 H5 N2 O4'
_chemical_formula_sum            'C18 H32 N2 O4 Sn'
_chemical_formula_weight         459.15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 117.04(7)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   18.402(17)
_cell_length_b                   16.861(19)
_cell_length_c                   16.328(16)
_cell_volume                     4512(8)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.15
_exptl_crystal_density_diffrn    1.35
_exptl_crystal_density_meas      1.31
_exptl_crystal_F_000             1888
_cod_data_source_file            mu0200.cif
_cod_data_source_block           mu0200a
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2001096
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Sn(1) .23758(4) .04461(4) .23116(4)
C(1) .3175(6) .0822(6) .1771(8)
C(2) .3508(6) .0226(7) .1380(7)
C(3) .4118(6) .0624(8) .1083(7)
C(4) .4543(8) -.0052(10) .0914(9)
C(5) .1480(6) .1262(6) .2323(7)
C(6) .1447(7) .2015(7) .1860(8)
C(7) .0845(7) .2651(8) .1884(8)
C(8) .1135(9) .3016(8) .2748(10)
C(9) .2742(6) -.0456(6) .3344(6)
C(10) .1992(11) -.0943(7) .3272(8)
C(11) .1943(12) -.1467(12) .3782(14)
C(12) .1217(10) -.1790(12) .3621(12)
C(13) .1193(4) -.0118(4) .0449(5)
C(14) .0754(4) -.0750(4) -.0261(5)
C(15) .0516(5) -.1882(5) .0526(6)
C(16) .0702(5) -.2590(5) .0929(6)
C(17) .1348(5) -.3044(4) .0920(5)
C(18) .1589(4) -.1910(4) .0100(5)
N(1) .0928(3) -.1561(3) .0112(4)
N(2) .1739(4) -.2678(4) .0479(4)
O(1) .1649(3) -.0359(3) .1254(3)
O(2) .1062(3) .0570(3) .0218(4)
O(3) .1972(3) -.1629(3) -.0256(4)
O(4) .1585(3) -.3694(4) .1264(4)
H(11) .2874000 .1283000 .1249000
H(12) .3717000 .1131000 .2350000
H(21) .3829000 -.0232000 .1915000
H(22) .3008000 -.0052000 .305000
H(31) .3805000 .0985000 .0466000
H(32) .4571000 .1002000 .1631000
H(41) .4999000 .0144000 .0688000
H(42) .4857000 -.0423000 .1511000
H(43) .4108000 -.0429000 .0352000
H(51) .0851000 .0997000 .1987000
H(52) .1594000 .1402000 .3044000
H(61) .2082000 .2265000 .2182000
H(62) .1307000 .1877000 .1134000
H(71) .0738000 .3135000 .1376000
H(72) .0246000 .2382000 .1707000
H(81) .0743000 .3446000 .2835000
H(82) .1259000 .2540000 .3303000
H(83) .1748000 .3294000 .2972000
H(91) .3195000 -.0873000 .3276000
H(92) .3078000 -.0197000 .4046000
H(101) .1563000 -.0478000 .3244000
H(102) .1747000 -.1217000 .2581000
H(111) .2279000 -.2058000 .3790000
H(112) .2304000 -.1308000 .4571000
H(121) .1074000 -.2093000 .4038000
H(122) .0834000 -.1857000 .2889000
H(141) .0096000 -.0632000 -.0587000
H(142) .0955000 -.0691000 -.0810000
H(151) .0012000 -.1545000 .0555000
H(161) .0350000 -.2832000 .1265000
H(20) .2337000 -.2660000 .0957000
