#------------------------------------------------------------------------------
#$Date: 2016-02-19 16:29:56 +0200 (Fri, 19 Feb 2016) $
#$Revision: 176759 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/58/2005895.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2005895
loop_
_publ_author_name
'Söhnel, T.'
'Reichelt, W.'
_publ_contact_author
;
W. Reichelt
Institut für Anorganische Chemie
TU Dresden
01062 Dresden
Mommsenstraße 6
Deutschland
;
_publ_section_title
;
 Os₃Sn₁₅O₁₄, ein ternäres Oxid mit osmiumgefüllten
 Sn₆-Oktaedern
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              9
_journal_page_last               11
_journal_paper_doi               10.1107/S0108270196009560
_journal_volume                  53
_journal_year                    1997
_chemical_formula_analytical     'Os Sn5 O4'
_chemical_formula_moiety         'Os3 Sn15 O14'
_chemical_formula_structural     'Os3 Sn15 O14'
_chemical_formula_sum            'O14 Os3 Sn15'
_chemical_formula_weight         2574.95
_chemical_name_systematic        Osmiumstannat
_space_group_IT_number           8
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2y'
_symmetry_space_group_name_H-M   'C 1 m 1'
_audit_creation_method           SHELXL
_cell_angle_alpha                90.00
_cell_angle_beta                 108.49(1)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.399(1)
_cell_length_b                   7.090(1)
_cell_length_c                   12.939(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      23.4
_cell_measurement_theta_min      7.9
_cell_volume                     1078.7(2)
_computing_cell_refinement       'CAD-4 Software'
_computing_data_collection       'CAD-4 Software (Enraf Nonius, 1994)'
_computing_data_reduction        'XCAD4PC (Enraf Nonius, 1994)'
_computing_molecular_graphics    'ATOMS (Dowty, 1994)'
_computing_structure_refinement  'SHELXL93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS86 (Sheldrick, 1985)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       CAD-4
_diffrn_measurement_method       ω-2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0355
_diffrn_reflns_av_sigmaI/netI    0.0410
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            7133
_diffrn_reflns_theta_max         39.97
_diffrn_reflns_theta_min         3.32
_diffrn_standards_decay_%        1.5
_diffrn_standards_interval_count 800
_diffrn_standards_interval_time  7200
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    34.653
_exptl_absorpt_correction_T_max  0.12
_exptl_absorpt_correction_T_min  0.04
_exptl_absorpt_correction_type   'empirical,\DF (XEMP; Siemens, 1989)'
_exptl_crystal_colour            Rot
_exptl_crystal_density_diffrn    7.927
_exptl_crystal_density_meas      ?
_exptl_crystal_description       Isometric
_exptl_crystal_F_000             2180
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_refine_diff_density_max         '6.161 (nahe Os3)'
_refine_diff_density_min         -6.305
_refine_ls_abs_structure_details 'Flack (1983)'
_refine_ls_abs_structure_Flack   0.034(8)
_refine_ls_extinction_coef       0.00036(5)
_refine_ls_extinction_method     'SHELXL93 (Sheldrick, 1993)'
_refine_ls_goodness_of_fit_all   1.049
_refine_ls_goodness_of_fit_obs   1.074
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     170
_refine_ls_number_reflns         3650
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.048
_refine_ls_restrained_S_obs      1.074
_refine_ls_R_factor_all          0.0410
_refine_ls_R_factor_obs          0.0344
_refine_ls_shift/esd_max         0.000
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²)+(0.0570P)²+10.7521P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0893
_refine_ls_wR_factor_obs         0.0871
_reflns_number_observed          3323
_reflns_number_total             3650
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            sk1025.cif
_cod_data_source_block           default
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'Yes' changed to 'yes' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (18
times).

'_geom_bond_publ_flag' value 'No' changed to 'no' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (62
times).

'_geom_angle_publ_flag' value 'No' changed to 'no' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (173 times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc w =
1/[\s^2^(Fo^2^)+(0.0570P)^2^+10.7521P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(Fo^2^)+(0.0570P)^2^+10.7521P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      'C m'
_cod_database_code               2005895
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_occupancy
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_type_symbol
Os1 1 0.69791(4) 0 0.69349(4) 0.01048(9) Uani d S Os
Os2 1 0.38401(4) 0.5000 0.23203(4) 0.01035(9) Uani d S Os
Os3 1 0.78859(6) 0.5000 0.96507(6) 0.01094(7) Uani d S Os
Sn1 1 0.90304(10) 0 0.82222(8) 0.0121(2) Uani d S Sn
Sn2 1 0.48695(9) 0 0.57930(9) 0.0131(2) Uani d S Sn
Sn3 1 0.74630(7) 0.74262(12) 0.57404(6) 0.01283(12) Uani d . Sn
Sn4 1 0.59471(9) 0.5000 0.34064(9) 0.0136(2) Uani d S Sn
Sn5 1 0.94262(10) 0.5000 0.87227(9) 0.0141(2) Uani d S Sn
Sn6 1 0.65008(9) 0.5000 0.07992(8) 0.0122(2) Uani d S Sn
Sn7 1 0.66889(7) 0.75983(12) 0.83755(6) 0.01333(12) Uani d . Sn
Sn8 1 0.17854(9) 0.5000 0.11128(8) 0.0125(2) Uani d S Sn
Sn9 1 0.40893(6) 0.26229(12) 0.08919(6) 0.01297(12) Uani d . Sn
Sn10 1 0.83543(7) 0.74056(13) 0.34646(6) 0.01425(13) Uani d . Sn
Sn11 1 0.51454(9) 0.5000 0.61927(8) 0.01295(14) Uani d S Sn
O1 1 0.9099(7) 0.2123(12) 0.5337(6) 0.0133(11) Uani d . O
O2 1 0.9594(12) 0 0.9908(10) 0.014(2) Uani d S O
O3 1 0.6236(10) 0.5000 0.5281(9) 0.015(2) Uani d S O
O4 1 1.1226(12) 0.5000 0.9430(9) 0.014(2) Uani d S O
O5 1 0.4239(11) 0 0.4106(9) 0.016(2) Uani d S O
O6 1 0.3477(10) 0 0.6335(10) 0.017(2) Uani d S O
O7 1 0.7005(6) 0.7223(13) 0.4059(6) 0.0147(12) Uani d . O
O8 1 0.5845(8) 0.7675(13) 0.1144(9) 0.0164(15) Uani d . O
O9 1 0.9893(8) 0.7530(13) 0.8159(7) 0.0158(15) Uani d . O
O10 1 0.7256(10) 0.5000 0.2507(9) 0.013(2) Uani d S O
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Sn1 Os1 Sn2 . . 175.04(4) no
Sn1 Os1 Sn3 . 1_545 91.03(3) no
Sn2 Os1 Sn3 . 1_545 92.48(3) no
Sn1 Os1 Sn3 . 2_565 91.03(3) no
Sn2 Os1 Sn3 . 2_565 92.48(3) no
Sn3 Os1 Sn3 1_545 2_565 89.94(4) no
Sn1 Os1 Sn7 . 2_565 82.53(3) no
Sn2 Os1 Sn7 . 2_565 93.70(3) no
Sn3 Os1 Sn7 1_545 2_565 172.29(3) no
Sn3 Os1 Sn7 2_565 2_565 94.39(3) no
Sn1 Os1 Sn7 . 1_545 82.53(3) no
Sn2 Os1 Sn7 . 1_545 93.70(3) no
Sn3 Os1 Sn7 1_545 1_545 94.39(3) no
Sn3 Os1 Sn7 2_565 1_545 172.29(3) no
Sn7 Os1 Sn7 2_565 1_545 80.62(4) no
Sn8 Os2 Sn4 . . 175.76(4) no
Sn8 Os2 Sn10 . 4_465 88.94(3) no
Sn4 Os2 Sn10 . 4_465 93.99(3) no
Sn8 Os2 Sn10 . 3_445 88.94(3) no
Sn4 Os2 Sn10 . 3_445 93.99(3) no
Sn10 Os2 Sn10 4_465 3_445 92.32(4) no
Sn8 Os2 Sn9 . . 83.35(3) no
Sn4 Os2 Sn9 . . 93.45(3) no
Sn10 Os2 Sn9 4_465 . 170.67(3) no
Sn10 Os2 Sn9 3_445 . 92.78(3) no
Sn8 Os2 Sn9 . 2_565 83.35(3) no
Sn4 Os2 Sn9 . 2_565 93.45(3) no
Sn10 Os2 Sn9 4_465 2_565 92.78(3) no
Sn10 Os2 Sn9 3_445 2_565 170.67(3) no
Sn9 Os2 Sn9 . 2_565 81.15(4) no
Sn5 Os3 Sn9 . 3_556 85.54(3) no
Sn5 Os3 Sn9 . 4_556 85.54(3) no
Sn9 Os3 Sn9 3_556 4_556 91.46(5) no
Sn5 Os3 Sn7 . 2_565 93.61(3) no
Sn9 Os3 Sn7 3_556 2_565 178.90(4) no
Sn9 Os3 Sn7 4_556 2_565 89.17(2) no
Sn5 Os3 Sn7 . . 93.61(3) no
Sn9 Os3 Sn7 3_556 . 89.17(2) no
Sn9 Os3 Sn7 4_556 . 178.90(4) no
Sn7 Os3 Sn7 2_565 . 90.19(5) no
Sn5 Os3 Sn6 . 1_556 173.65(4) no
Sn9 Os3 Sn6 3_556 1_556 90.04(3) no
Sn9 Os3 Sn6 4_556 1_556 90.04(3) no
Sn7 Os3 Sn6 2_565 1_556 90.87(3) no
Sn7 Os3 Sn6 . 1_556 90.87(3) no
O9 Sn1 O9 2_565 1_545 115.8(5) no
O9 Sn1 O2 2_565 . 92.1(3) no
O9 Sn1 O2 1_545 . 92.1(3) no
O9 Sn1 Os1 2_565 . 113.2(3) no
O9 Sn1 Os1 1_545 . 113.2(3) no
O2 Sn1 Os1 . . 128.3(4) no
O6 Sn2 O5 . . 106.3(5) no
O6 Sn2 O1 . 3_445 75.9(2) no
O5 Sn2 O1 . 3_445 74.7(2) no
O6 Sn2 O1 . 4_455 75.9(2) no
O5 Sn2 O1 . 4_455 74.7(2) no
O1 Sn2 O1 3_445 4_455 130.1(4) no
O6 Sn2 Os1 . . 128.0(3) no
O5 Sn2 Os1 . . 125.6(4) no
O1 Sn2 Os1 3_445 . 114.9(2) no
O1 Sn2 Os1 4_455 . 114.9(2) no
O7 Sn3 O6 . 3 104.9(4) no
O7 Sn3 O3 . . 74.5(4) no
O6 Sn3 O3 3 . 75.5(4) no
O7 Sn3 O1 . 2_565 74.7(3) no
O6 Sn3 O1 3 2_565 74.2(4) no
O3 Sn3 O1 . 2_565 128.7(3) no
O7 Sn3 Os1 . 1_565 129.7(3) no
O6 Sn3 Os1 3 1_565 125.4(3) no
O3 Sn3 Os1 . 1_565 115.6(3) no
O1 Sn3 Os1 2_565 1_565 115.6(2) no
O7 Sn4 O7 . 2_565 100.3(5) no
O7 Sn4 O10 . . 75.2(3) no
O7 Sn4 O10 2_565 . 75.2(3) no
O7 Sn4 O3 . . 72.9(3) no
O7 Sn4 O3 2_565 . 72.9(3) no
O10 Sn4 O3 . . 129.1(4) no
O7 Sn4 Os2 . . 129.6(2) no
O7 Sn4 Os2 2_565 . 129.6(2) no
O10 Sn4 Os2 . . 119.4(3) no
O3 Sn4 Os2 . . 111.5(3) no
O9 Sn5 O9 2_565 . 118.6(5) no
O9 Sn5 O4 2_565 . 77.4(3) no
O9 Sn5 O4 . . 77.4(3) no
O9 Sn5 Os3 2_565 . 119.7(3) no
O9 Sn5 Os3 . . 119.7(3) no
O4 Sn5 Os3 . . 129.5(3) no
O10 Sn6 O8 . . 81.7(3) no
O10 Sn6 O8 . 2_565 81.7(3) no
O8 Sn6 O8 . 2_565 122.4(4) no
O10 Sn6 O2 . 3_454 125.1(4) no
O8 Sn6 O2 . 3_454 73.0(3) no
O8 Sn6 O2 2_565 3_454 73.0(3) no
O10 Sn6 Os3 . 1_554 116.4(3) no
O8 Sn6 Os3 . 1_554 118.4(2) no
O8 Sn6 Os3 2_565 1_554 118.4(2) no
O2 Sn6 Os3 3_454 1_554 118.5(3) no
O9 Sn7 O4 4_465 3_455 71.1(4) no
O9 Sn7 Os3 4_465 . 114.3(3) no
O4 Sn7 Os3 3_455 . 109.8(3) no
O9 Sn7 Os1 4_465 1_565 107.6(3) no
O4 Sn7 Os1 3_455 1_565 93.2(2) no
Os3 Sn7 Os1 . 1_565 136.78(4) no
O8 Sn8 O8 3_445 4_465 108.9(5) no
O8 Sn8 O4 3_445 1_454 91.0(4) no
O8 Sn8 O4 4_465 1_454 91.0(4) no
O8 Sn8 Os2 3_445 . 117.4(3) no
O8 Sn8 Os2 4_465 . 117.4(3) no
O4 Sn8 Os2 1_454 . 125.9(4) no
O8 Sn9 O2 2_565 3_454 73.2(4) no
O8 Sn9 Os2 2_565 . 107.8(3) no
O2 Sn9 Os2 3_454 . 91.9(2) no
O8 Sn9 Os3 2_565 3_444 112.7(3) no
O2 Sn9 Os3 3_454 3_444 112.6(3) no
Os2 Sn9 Os3 . 3_444 137.04(4) no
O5 Sn10 O7 3 . 100.9(4) no
O5 Sn10 O10 3 . 75.5(3) no
O7 Sn10 O10 . . 74.9(4) no
O5 Sn10 O1 3 2_565 73.4(3) no
O7 Sn10 O1 . 2_565 73.8(3) no
O10 Sn10 O1 . 2_565 130.0(3) no
O5 Sn10 Os2 3 3 129.7(3) no
O7 Sn10 Os2 . 3 129.3(3) no
O10 Sn10 Os2 . 3 115.7(2) no
O1 Sn10 Os2 2_565 3 114.3(2) no
O3 Sn11 O1 3_445 2_455 96.2(3) no
O3 Sn11 O1 3_445 1_455 96.2(3) no
O1 Sn11 O1 2_455 1_455 93.6(4) no
Sn11 O1 Sn2 1_655 3 112.2(3) no
Sn11 O1 Sn3 1_655 2_565 115.7(3) no
Sn2 O1 Sn3 3 2_565 98.5(3) no
Sn11 O1 Sn10 1_655 2_565 129.6(4) no
Sn2 O1 Sn10 3 2_565 97.9(3) no
Sn3 O1 Sn10 2_565 2_565 97.5(3) no
Sn1 O2 Sn6 . 3_546 118.9(6) no
Sn1 O2 Sn9 . 4_556 121.3(4) no
Sn6 O2 Sn9 3_546 4_556 98.0(4) no
Sn1 O2 Sn9 . 3_546 121.3(4) no
Sn6 O2 Sn9 3_546 3_546 98.0(4) no
Sn9 O2 Sn9 4_556 3_546 93.4(5) no
Sn11 O3 Sn3 3 . 111.2(4) no
Sn11 O3 Sn3 3 2_565 111.2(4) no
Sn3 O3 Sn3 . 2_565 99.9(5) no
Sn11 O3 Sn4 3 . 133.1(6) no
Sn3 O3 Sn4 . . 98.2(3) no
Sn3 O3 Sn4 2_565 . 98.2(3) no
Sn8 O4 Sn5 1_656 . 114.2(5) no
Sn8 O4 Sn7 1_656 3_545 123.1(4) no
Sn5 O4 Sn7 . 3_545 99.5(4) no
Sn8 O4 Sn7 1_656 4_565 123.1(4) no
Sn5 O4 Sn7 . 4_565 99.5(4) no
Sn7 O4 Sn7 3_545 4_565 92.1(3) no
Sn10 O5 Sn10 4_455 3_445 112.2(6) no
Sn10 O5 Sn2 4_455 . 113.6(3) no
Sn10 O5 Sn2 3_445 . 113.6(3) no
Sn2 O6 Sn3 . 4_455 109.9(4) no
Sn2 O6 Sn3 . 3_445 109.9(4) no
Sn3 O6 Sn3 4_455 3_445 108.0(5) no
Sn4 O7 Sn10 . . 112.6(4) no
Sn4 O7 Sn3 . . 114.3(4) no
Sn10 O7 Sn3 . . 113.8(4) no
Sn8 O8 Sn9 3 2_565 130.6(5) no
Sn8 O8 Sn6 3 . 116.9(4) no
Sn9 O8 Sn6 2_565 . 108.5(4) no
Sn1 O9 Sn5 1_565 . 120.7(5) no
Sn1 O9 Sn7 1_565 4_565 123.8(5) no
Sn5 O9 Sn7 . 4_565 107.9(4) no
Sn6 O10 Sn4 . . 112.6(5) no
Sn6 O10 Sn10 . . 123.9(3) no
Sn4 O10 Sn10 . . 97.0(3) no
Sn6 O10 Sn10 . 2_565 123.9(3) no
Sn4 O10 Sn10 . 2_565 97.0(3) no
Sn10 O10 Sn10 . 2_565 96.5(4) no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Os1 Sn1 . 2.5604(13) yes
Os1 Sn2 . 2.5639(13) yes
Os1 Sn3 1_545 2.5820(9) yes
Os1 Sn3 2_565 2.5820(9) yes
Os1 Sn7 2_565 2.6323(9) yes
Os1 Sn7 1_545 2.6323(9) yes
Os2 Sn8 . 2.5311(13) yes
Os2 Sn4 . 2.5439(13) yes
Os2 Sn10 4_465 2.5503(9) yes
Os2 Sn10 3_445 2.5503(9) yes
Os2 Sn9 . 2.5911(9) yes
Os2 Sn9 2_565 2.5911(9) yes
Os3 Sn5 . 2.5580(13) yes
Os3 Sn9 3_556 2.5969(10) yes
Os3 Sn9 4_556 2.5969(10) yes
Os3 Sn7 2_565 2.6010(10) yes
Os3 Sn7 . 2.6010(10) yes
Os3 Sn6 1_556 2.6031(12) yes
Sn1 O9 2_565 2.067(10) no
Sn1 O9 1_545 2.067(10) no
Sn1 O2 . 2.068(13) no
Sn2 O6 . 2.058(12) no
Sn2 O5 . 2.072(11) no
Sn2 O1 3_445 2.250(8) no
Sn2 O1 4_455 2.250(8) no
Sn3 O7 . 2.072(8) no
Sn3 O6 3 2.126(7) no
Sn3 O3 . 2.248(8) no
Sn3 O1 2_565 2.272(8) no
Sn3 Os1 1_565 2.5820(9) no
Sn4 O7 . 2.053(8) no
Sn4 O7 2_565 2.053(8) no
Sn4 O10 . 2.277(11) no
Sn4 O3 . 2.337(11) no
Sn5 O9 2_565 2.086(9) no
Sn5 O9 . 2.086(9) no
Sn5 O4 . 2.126(14) no
Sn6 O10 . 2.108(11) no
Sn6 O8 . 2.165(9) no
Sn6 O8 2_565 2.165(9) no
Sn6 O2 3_454 2.278(14) no
Sn6 Os3 1_554 2.6031(12) no
Sn7 O9 4_465 2.157(10) no
Sn7 O4 3_455 2.364(7) no
Sn7 Os1 1_565 2.6323(9) no
Sn8 O8 3_445 2.026(9) no
Sn8 O8 4_465 2.026(9) no
Sn8 O4 1_454 2.065(12) no
Sn9 O8 2_565 2.108(9) no
Sn9 O2 3_454 2.315(10) no
Sn9 Os3 3_444 2.5969(10) no
Sn10 O5 3 2.055(7) no
Sn10 O7 . 2.056(8) no
Sn10 O10 . 2.287(7) no
Sn10 O1 2_565 2.327(7) no
Sn10 Os2 3 2.5503(9) no
Sn11 O3 3_445 2.057(11) no
Sn11 O1 2_455 2.065(8) no
Sn11 O1 1_455 2.065(8) no
O1 Sn11 1_655 2.065(8) no
O1 Sn2 3 2.250(8) no
O1 Sn3 2_565 2.272(8) no
O1 Sn10 2_565 2.327(7) no
O2 Sn6 3_546 2.278(14) no
O2 Sn9 4_556 2.315(10) no
O2 Sn9 3_546 2.315(10) no
O3 Sn11 3 2.057(11) no
O3 Sn3 2_565 2.248(8) no
O4 Sn8 1_656 2.065(12) no
O4 Sn7 3_545 2.364(7) no
O4 Sn7 4_565 2.364(7) no
O5 Sn10 4_455 2.055(7) no
O5 Sn10 3_445 2.055(7) no
O6 Sn3 4_455 2.126(7) no
O6 Sn3 3_445 2.126(7) no
O8 Sn8 3 2.026(9) no
O8 Sn9 2_565 2.108(9) no
O9 Sn1 1_565 2.067(10) no
O9 Sn7 4_565 2.157(10) no
O10 Sn10 2_565 2.287(7) no
