#------------------------------------------------------------------------------
#$Date: 2017-03-22 08:54:23 +0200 (Wed, 22 Mar 2017) $
#$Revision: 194406 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/07/2020747.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2020747
loop_
_publ_author_name
'Pavlyuk, Volodymyr'
'Dmytriv, Grygoriy'
'Tarasiuk, Ivan'
'Ehrenberg, Helmut'
_publ_section_title
;
 Li₉Al₄Sn₅ as a new ordered superstructure of the Li₁₃Sn₅ type
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S205322961700420X
_journal_volume                  73
_journal_year                    2017
_chemical_formula_iupac          'Li9 Al4 Sn5'
_chemical_formula_moiety         'Al4 Li2 Sn5, 7(Li)'
_chemical_formula_sum            'Al4 Li9 Sn5'
_chemical_formula_weight         763.93
_chemical_name_systematic
;
Nonalithium tetraaluminium pentastannide
;
_space_group_crystal_system      trigonal
_space_group_IT_number           164
_space_group_name_Hall           '-P 3 2"'
_space_group_name_H-M_alt        'P -3 m 1'
_symmetry_space_group_name_Hall  '-P 3 2"'
_symmetry_space_group_name_H-M   'P -3 m 1'
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   4.7170(7)
_cell_length_b                   4.7170(7)
_cell_length_c                   17.077(3)
_cell_measurement_reflns_used    352
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.438
_cell_measurement_theta_min      2.385
_cell_volume                     329.06(9)
_computing_cell_refinement
;
CrysAlis CCD (Oxford Diffraction, 2008)
;
_computing_data_collection
;
CrysAlis CCD (Oxford Diffraction, 2008)
;
_computing_data_reduction
;
CrysAlis RED (Oxford Diffraction, 2008)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg, 2006)
;
_computing_publication_material
;
SHELXL2014 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL2014 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS2014 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur3 CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0737
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            3006
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.438
_diffrn_reflns_theta_min         2.385
_exptl_absorpt_coefficient_mu    9.569
_exptl_absorpt_correction_T_max  0.901
_exptl_absorpt_correction_T_min  0.520
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
(CrysAlis RED; Oxford Diffraction, 2008)
;
_exptl_crystal_colour            'metallic grey'
_exptl_crystal_density_diffrn    3.855
_exptl_crystal_density_meas      3.86(2)
_exptl_crystal_density_method    volumetric
_exptl_crystal_description       plate
_exptl_crystal_F_000             329
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.01
_refine_diff_density_max         1.268
_refine_diff_density_min         -1.241
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.103
_refine_ls_matrix_type           full
_refine_ls_number_parameters     24
_refine_ls_number_reflns         352
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.103
_refine_ls_R_factor_all          0.0243
_refine_ls_R_factor_gt           0.0205
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0010P)²+0.0017P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0644
_refine_ls_wR_factor_ref         0.0663
_reflns_number_gt                324
_reflns_number_total             352
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            yo3033sup1.cif
_cod_data_source_block           I
_cod_original_cell_volume        329.06(12)
_cod_database_code               2020747
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z'
'x-y, -y, -z'
'-x, -x+y, -z'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z'
'-x+y, y, z'
'x, x-y, z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
Sn Sn1 0.6667 0.3333 0.38861(4) 0.0166(2) Uani d 1
Sn Sn2 0.6667 0.3333 0.22148(4) 0.0167(2) Uani d 1
Sn Sn3 0.0000 0.0000 0.0000 0.0109(3) Uani d 1
Al Al1 0.6667 0.3333 0.55327(17) 0.0129(6) Uani d 1
Al Al2 0.0000 0.0000 0.16567(18) 0.0238(8) Uani d 1
Li Li1 0.6667 0.3333 0.0701(11) 0.023(4) Uiso d 1
Li Li2 0.6667 0.3333 0.7209(9) 0.012(3) Uiso d 1
Li Li3 0.6667 0.3333 0.8807(16) 0.056(8) Uiso d 1
Li Li4 0.0000 0.0000 0.5000 0.020(6) Uiso d 1
Li Li5 0.0000 0.0000 0.3309(9) 0.012(3) Uiso d 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
Al1 Sn1 Sn2 . . 180.0
Al1 Sn1 Li5 . 1_655 109.9(3)
Sn2 Sn1 Li5 . 1_655 70.1(3)
Al1 Sn1 Li5 . 1_665 109.9(3)
Sn2 Sn1 Li5 . 1_665 70.1(3)
Li5 Sn1 Li5 1_655 1_665 109.0(3)
Al1 Sn1 Li5 . . 109.9(3)
Sn2 Sn1 Li5 . . 70.1(3)
Li5 Sn1 Li5 1_655 . 109.0(3)
Li5 Sn1 Li5 1_665 . 109.0(3)
Al1 Sn1 Al1 . 7_666 69.98(5)
Sn2 Sn1 Al1 . 7_666 110.02(5)
Li5 Sn1 Al1 1_655 7_666 179.9(3)
Li5 Sn1 Al1 1_665 7_666 71.02(16)
Li5 Sn1 Al1 . 7_666 71.02(16)
Al1 Sn1 Al1 . 7_766 69.98(5)
Sn2 Sn1 Al1 . 7_766 110.02(5)
Li5 Sn1 Al1 1_655 7_766 71.02(16)
Li5 Sn1 Al1 1_665 7_766 71.02(16)
Li5 Sn1 Al1 . 7_766 179.9(3)
Al1 Sn1 Al1 7_666 7_766 108.91(6)
Al1 Sn1 Al1 . 7_656 69.98(5)
Sn2 Sn1 Al1 . 7_656 110.02(5)
Li5 Sn1 Al1 1_655 7_656 71.02(16)
Li5 Sn1 Al1 1_665 7_656 179.9(3)
Li5 Sn1 Al1 . 7_656 71.02(16)
Al1 Sn1 Al1 7_666 7_656 108.91(6)
Al1 Sn1 Al1 7_766 7_656 108.91(6)
Al1 Sn1 Li2 . 7_666 124.5(2)
Sn2 Sn1 Li2 . 7_666 55.5(2)
Li5 Sn1 Li2 1_655 7_666 125.6(4)
Li5 Sn1 Li2 1_665 7_666 54.53(14)
Li5 Sn1 Li2 . 7_666 54.53(14)
Al1 Sn1 Li2 7_666 7_666 54.5(2)
Al1 Sn1 Li2 7_766 7_666 125.53(3)
Al1 Sn1 Li2 7_656 7_666 125.53(3)
Al1 Sn1 Li2 . 7_656 124.5(2)
Sn2 Sn1 Li2 . 7_656 55.5(2)
Li5 Sn1 Li2 1_655 7_656 54.53(14)
Li5 Sn1 Li2 1_665 7_656 125.6(4)
Li5 Sn1 Li2 . 7_656 54.53(14)
Al1 Sn1 Li2 7_666 7_656 125.53(3)
Al1 Sn1 Li2 7_766 7_656 125.53(3)
Al1 Sn1 Li2 7_656 7_656 54.5(2)
Li2 Sn1 Li2 7_666 7_656 91.1(3)
Al1 Sn1 Li2 . 7_766 124.5(2)
Sn2 Sn1 Li2 . 7_766 55.5(2)
Li5 Sn1 Li2 1_655 7_766 54.53(14)
Li5 Sn1 Li2 1_665 7_766 54.53(14)
Li5 Sn1 Li2 . 7_766 125.6(4)
Al1 Sn1 Li2 7_666 7_766 125.53(3)
Al1 Sn1 Li2 7_766 7_766 54.5(2)
Al1 Sn1 Li2 7_656 7_766 125.53(3)
Li2 Sn1 Li2 7_666 7_766 91.1(3)
Li2 Sn1 Li2 7_656 7_766 91.1(3)
Al1 Sn1 Li4 . 1_655 55.067(12)
Sn2 Sn1 Li4 . 1_655 124.933(12)
Li5 Sn1 Li4 1_655 1_655 54.8(3)
Li5 Sn1 Li4 1_665 1_655 125.47(15)
Li5 Sn1 Li4 . 1_655 125.47(15)
Al1 Sn1 Li4 7_666 1_655 125.04(6)
Al1 Sn1 Li4 7_766 1_655 54.47(3)
Al1 Sn1 Li4 7_656 1_655 54.47(3)
Li2 Sn1 Li4 7_666 1_655 179.5(2)
Li2 Sn1 Li4 7_656 1_655 89.21(16)
Li2 Sn1 Li4 7_766 1_655 89.21(16)
Li1 Sn2 Sn1 . . 180.0
Li1 Sn2 Al2 . . 70.71(6)
Sn1 Sn2 Al2 . . 109.29(6)
Li1 Sn2 Al2 . 1_655 70.71(6)
Sn1 Sn2 Al2 . 1_655 109.29(6)
Al2 Sn2 Al2 . 1_655 109.65(6)
Li1 Sn2 Al2 . 1_665 70.71(6)
Sn1 Sn2 Al2 . 1_665 109.29(6)
Al2 Sn2 Al2 . 1_665 109.65(6)
Al2 Sn2 Al2 1_655 1_665 109.65(6)
Li1 Sn2 Li2 . 7_666 109.9(3)
Sn1 Sn2 Li2 . 7_666 70.1(3)
Al2 Sn2 Li2 . 7_666 70.64(15)
Al2 Sn2 Li2 1_655 7_666 179.4(3)
Al2 Sn2 Li2 1_665 7_666 70.64(15)
Li1 Sn2 Li2 . 7_766 109.9(3)
Sn1 Sn2 Li2 . 7_766 70.1(3)
Al2 Sn2 Li2 . 7_766 179.4(3)
Al2 Sn2 Li2 1_655 7_766 70.64(15)
Al2 Sn2 Li2 1_665 7_766 70.64(15)
Li2 Sn2 Li2 7_666 7_766 109.1(3)
Li1 Sn2 Li2 . 7_656 109.9(3)
Sn1 Sn2 Li2 . 7_656 70.1(3)
Al2 Sn2 Li2 . 7_656 70.64(15)
Al2 Sn2 Li2 1_655 7_656 70.64(15)
Al2 Sn2 Li2 1_665 7_656 179.4(3)
Li2 Sn2 Li2 7_666 7_656 109.1(3)
Li2 Sn2 Li2 7_766 7_656 109.1(3)
Li1 Sn2 Li3 . 7_666 57.4(4)
Sn1 Sn2 Li3 . 7_666 122.6(4)
Al2 Sn2 Li3 . 7_666 54.86(3)
Al2 Sn2 Li3 1_655 7_666 128.1(4)
Al2 Sn2 Li3 1_665 7_666 54.86(3)
Li2 Sn2 Li3 7_666 7_666 52.5(5)
Li2 Sn2 Li3 7_766 7_666 125.40(13)
Li2 Sn2 Li3 7_656 7_666 125.40(13)
Li1 Sn2 Li3 . 7_656 57.4(4)
Sn1 Sn2 Li3 . 7_656 122.6(4)
Al2 Sn2 Li3 . 7_656 54.86(3)
Al2 Sn2 Li3 1_655 7_656 54.86(3)
Al2 Sn2 Li3 1_665 7_656 128.1(4)
Li2 Sn2 Li3 7_666 7_656 125.40(13)
Li2 Sn2 Li3 7_766 7_656 125.40(13)
Li2 Sn2 Li3 7_656 7_656 52.5(5)
Li3 Sn2 Li3 7_666 7_656 93.7(6)
Li1 Sn2 Li3 . 7_766 57.4(4)
Sn1 Sn2 Li3 . 7_766 122.6(4)
Al2 Sn2 Li3 . 7_766 128.1(4)
Al2 Sn2 Li3 1_655 7_766 54.86(3)
Al2 Sn2 Li3 1_665 7_766 54.86(3)
Li2 Sn2 Li3 7_666 7_766 125.40(13)
Li2 Sn2 Li3 7_766 7_766 52.5(5)
Li2 Sn2 Li3 7_656 7_766 125.40(13)
Li3 Sn2 Li3 7_666 7_766 93.7(6)
Li3 Sn2 Li3 7_656 7_766 93.7(6)
Li1 Sn2 Li5 . . 124.5(2)
Sn1 Sn2 Li5 . . 55.5(2)
Al2 Sn2 Li5 . . 53.7(2)
Al2 Sn2 Li5 1_655 . 125.17(3)
Al2 Sn2 Li5 1_665 . 125.17(3)
Li2 Sn2 Li5 7_666 . 54.55(14)
Li2 Sn2 Li5 7_766 . 125.7(4)
Li2 Sn2 Li5 7_656 . 54.55(14)
Li3 Sn2 Li5 7_666 . 87.6(3)
Li3 Sn2 Li5 7_656 . 87.6(3)
Li3 Sn2 Li5 7_766 . 178.2(5)
Al2 Sn3 Al2 7 . 180.0
Al2 Sn3 Li1 7 . 113.7(3)
Al2 Sn3 Li1 . . 66.3(3)
Al2 Sn3 Li1 7 7 66.3(3)
Al2 Sn3 Li1 . 7 113.7(3)
Li1 Sn3 Li1 . 7 180.0
Al2 Sn3 Li1 7 7_665 66.3(3)
Al2 Sn3 Li1 . 7_665 113.7(3)
Li1 Sn3 Li1 . 7_665 75.1(4)
Li1 Sn3 Li1 7 7_665 104.9(4)
Al2 Sn3 Li1 7 1_445 113.7(3)
Al2 Sn3 Li1 . 1_445 66.3(3)
Li1 Sn3 Li1 . 1_445 104.9(4)
Li1 Sn3 Li1 7 1_445 75.1(4)
Li1 Sn3 Li1 7_665 1_445 180.0(7)
Al2 Sn3 Li1 7 1_455 113.7(3)
Al2 Sn3 Li1 . 1_455 66.3(3)
Li1 Sn3 Li1 . 1_455 104.9(4)
Li1 Sn3 Li1 7 1_455 75.1(4)
Li1 Sn3 Li1 7_665 1_455 75.1(4)
Li1 Sn3 Li1 1_445 1_455 104.9(4)
Al2 Sn3 Li1 7 7_655 66.3(3)
Al2 Sn3 Li1 . 7_655 113.7(3)
Li1 Sn3 Li1 . 7_655 75.1(4)
Li1 Sn3 Li1 7 7_655 104.9(4)
Li1 Sn3 Li1 7_665 7_655 104.9(4)
Li1 Sn3 Li1 1_445 7_655 75.1(4)
Li1 Sn3 Li1 1_455 7_655 180.0(7)
Al2 Sn3 Li3 7 7_666 126.8(4)
Al2 Sn3 Li3 . 7_666 53.2(4)
Li1 Sn3 Li3 . 7_666 52.58(17)
Li1 Sn3 Li3 7 7_666 127.42(17)
Li1 Sn3 Li3 7_665 7_666 60.5(5)
Li1 Sn3 Li3 1_445 7_666 119.5(5)
Li1 Sn3 Li3 1_455 7_666 52.58(17)
Li1 Sn3 Li3 7_655 7_666 127.42(17)
Al2 Sn3 Li3 7 1_444 53.2(4)
Al2 Sn3 Li3 . 1_444 126.8(4)
Li1 Sn3 Li3 . 1_444 127.42(17)
Li1 Sn3 Li3 7 1_444 52.58(17)
Li1 Sn3 Li3 7_665 1_444 119.5(5)
Li1 Sn3 Li3 1_445 1_444 60.5(5)
Li1 Sn3 Li3 1_455 1_444 127.42(17)
Li1 Sn3 Li3 7_655 1_444 52.58(17)
Li3 Sn3 Li3 7_666 1_444 180.0(7)
Al2 Sn3 Li3 7 7_556 126.8(4)
Al2 Sn3 Li3 . 7_556 53.2(4)
Li1 Sn3 Li3 . 7_556 119.5(5)
Li1 Sn3 Li3 7 7_556 60.5(5)
Li1 Sn3 Li3 7_665 7_556 127.42(17)
Li1 Sn3 Li3 1_445 7_556 52.58(17)
Li1 Sn3 Li3 1_455 7_556 52.58(17)
Li1 Sn3 Li3 7_655 7_556 127.42(17)
Li3 Sn3 Li3 7_666 7_556 87.8(5)
Li3 Sn3 Li3 1_444 7_556 92.2(5)
Al2 Sn3 Li3 7 1_554 53.2(4)
Al2 Sn3 Li3 . 1_554 126.8(4)
Li1 Sn3 Li3 . 1_554 60.5(5)
Li1 Sn3 Li3 7 1_554 119.5(5)
Li1 Sn3 Li3 7_665 1_554 52.58(17)
Li1 Sn3 Li3 1_445 1_554 127.42(17)
Li1 Sn3 Li3 1_455 1_554 127.42(17)
Li1 Sn3 Li3 7_655 1_554 52.58(17)
Li3 Sn3 Li3 7_666 1_554 92.2(5)
Li3 Sn3 Li3 1_444 1_554 87.8(5)
Li3 Sn3 Li3 7_556 1_554 180.0(7)
Sn1 Al1 Li2 . . 180.0
Sn1 Al1 Li4 . 1_655 71.53(5)
Li2 Al1 Li4 . 1_655 108.47(5)
Sn1 Al1 Li4 . . 71.53(5)
Li2 Al1 Li4 . . 108.47(5)
Li4 Al1 Li4 1_655 . 110.45(5)
Sn1 Al1 Li4 . 1_665 71.53(5)
Li2 Al1 Li4 . 1_665 108.47(5)
Li4 Al1 Li4 1_655 1_665 110.45(5)
Li4 Al1 Li4 . 1_665 110.45(5)
Sn1 Al1 Sn1 . 7_666 110.02(5)
Li2 Al1 Sn1 . 7_666 69.98(5)
Li4 Al1 Sn1 1_655 7_666 178.45(11)
Li4 Al1 Sn1 . 7_666 70.300(8)
Li4 Al1 Sn1 1_665 7_666 70.300(8)
Sn1 Al1 Sn1 . 7_766 110.02(5)
Li2 Al1 Sn1 . 7_766 69.98(5)
Li4 Al1 Sn1 1_655 7_766 70.300(7)
Li4 Al1 Sn1 . 7_766 178.45(11)
Li4 Al1 Sn1 1_665 7_766 70.301(7)
Sn1 Al1 Sn1 7_666 7_766 108.91(6)
Sn1 Al1 Sn1 . 7_656 110.02(5)
Li2 Al1 Sn1 . 7_656 69.98(5)
Li4 Al1 Sn1 1_655 7_656 70.300(7)
Li4 Al1 Sn1 . 7_656 70.301(7)
Li4 Al1 Sn1 1_665 7_656 178.45(11)
Sn1 Al1 Sn1 7_666 7_656 108.91(6)
Sn1 Al1 Sn1 7_766 7_656 108.91(6)
Li5 Al2 Sn3 . . 180.0
Li5 Al2 Li3 . 7_556 106.2(5)
Sn3 Al2 Li3 . 7_556 73.8(5)
Li5 Al2 Li3 . 7_666 106.2(5)
Sn3 Al2 Li3 . 7_666 73.8(5)
Li3 Al2 Li3 7_556 7_666 112.5(5)
Li5 Al2 Li3 . 7_656 106.2(5)
Sn3 Al2 Li3 . 7_656 73.8(5)
Li3 Al2 Li3 7_556 7_656 112.5(5)
Li3 Al2 Li3 7_666 7_656 112.5(5)
Li5 Al2 Sn2 . 1_445 70.71(6)
Sn3 Al2 Sn2 . 1_445 109.29(6)
Li3 Al2 Sn2 7_556 1_445 68.8(3)
Li3 Al2 Sn2 7_666 1_445 176.9(5)
Li3 Al2 Sn2 7_656 1_445 68.8(3)
Li5 Al2 Sn2 . . 70.71(6)
Sn3 Al2 Sn2 . . 109.29(6)
Li3 Al2 Sn2 7_556 . 176.9(5)
Li3 Al2 Sn2 7_666 . 68.8(3)
Li3 Al2 Sn2 7_656 . 68.8(3)
Sn2 Al2 Sn2 1_445 . 109.65(6)
Li5 Al2 Sn2 . 1_455 70.71(6)
Sn3 Al2 Sn2 . 1_455 109.29(6)
Li3 Al2 Sn2 7_556 1_455 68.8(3)
Li3 Al2 Sn2 7_666 1_455 68.8(3)
Li3 Al2 Sn2 7_656 1_455 176.9(5)
Sn2 Al2 Sn2 1_445 1_455 109.65(6)
Sn2 Al2 Sn2 . 1_455 109.65(6)
Li5 Al2 Li1 . 1_445 120.9(3)
Sn3 Al2 Li1 . 1_445 59.1(3)
Li3 Al2 Li1 7_556 1_445 56.3(2)
Li3 Al2 Li1 7_666 1_445 132.9(6)
Li3 Al2 Li1 7_656 1_445 56.3(2)
Sn2 Al2 Li1 1_445 1_445 50.2(3)
Sn2 Al2 Li1 . 1_445 125.07(3)
Sn2 Al2 Li1 1_455 1_445 125.07(3)
Li5 Al2 Li1 . 1_455 120.9(3)
Sn3 Al2 Li1 . 1_455 59.1(3)
Li3 Al2 Li1 7_556 1_455 56.3(2)
Li3 Al2 Li1 7_666 1_455 56.3(2)
Li3 Al2 Li1 7_656 1_455 132.9(6)
Sn2 Al2 Li1 1_445 1_455 125.07(3)
Sn2 Al2 Li1 . 1_455 125.07(3)
Sn2 Al2 Li1 1_455 1_455 50.2(3)
Li1 Al2 Li1 1_445 1_455 96.0(4)
Li5 Al2 Li1 . . 120.9(3)
Sn3 Al2 Li1 . . 59.1(3)
Li3 Al2 Li1 7_556 . 132.9(6)
Li3 Al2 Li1 7_666 . 56.3(2)
Li3 Al2 Li1 7_656 . 56.3(2)
Sn2 Al2 Li1 1_445 . 125.07(3)
Sn2 Al2 Li1 . . 50.2(3)
Sn2 Al2 Li1 1_455 . 125.07(3)
Li1 Al2 Li1 1_445 . 96.0(4)
Li1 Al2 Li1 1_455 . 96.0(4)
Sn2 Li1 Li3 . 7_666 72.9(6)
Sn2 Li1 Li3 . 7_766 72.9(6)
Li3 Li1 Li3 7_666 7_766 111.7(5)
Sn2 Li1 Li3 . 7_656 72.9(6)
Li3 Li1 Li3 7_666 7_656 111.7(5)
Li3 Li1 Li3 7_766 7_656 111.7(5)
Sn2 Li1 Sn3 . 1_655 113.7(3)
Li3 Li1 Sn3 7_666 1_655 173.4(8)
Li3 Li1 Sn3 7_766 1_655 71.4(3)
Li3 Li1 Sn3 7_656 1_655 71.4(3)
Sn2 Li1 Sn3 . . 113.7(3)
Li3 Li1 Sn3 7_666 . 71.4(3)
Li3 Li1 Sn3 7_766 . 173.4(8)
Li3 Li1 Sn3 7_656 . 71.4(3)
Sn3 Li1 Sn3 1_655 . 104.9(4)
Sn2 Li1 Sn3 . 1_665 113.7(3)
Li3 Li1 Sn3 7_666 1_665 71.4(3)
Li3 Li1 Sn3 7_766 1_665 71.4(3)
Li3 Li1 Sn3 7_656 1_665 173.4(8)
Sn3 Li1 Sn3 1_655 1_665 104.9(4)
Sn3 Li1 Sn3 . 1_665 104.9(4)
Sn2 Li1 Al2 . 1_655 59.1(3)
Li3 Li1 Al2 7_666 1_655 131.9(8)
Li3 Li1 Al2 7_766 1_655 55.8(3)
Li3 Li1 Al2 7_656 1_655 55.8(3)
Sn3 Li1 Al2 1_655 1_655 54.66(6)
Sn3 Li1 Al2 . 1_655 126.83(8)
Sn3 Li1 Al2 1_665 1_655 126.83(8)
Sn2 Li1 Al2 . 1_665 59.1(3)
Li3 Li1 Al2 7_666 1_665 55.8(3)
Li3 Li1 Al2 7_766 1_665 55.8(3)
Li3 Li1 Al2 7_656 1_665 131.9(8)
Sn3 Li1 Al2 1_655 1_665 126.83(8)
Sn3 Li1 Al2 . 1_665 126.83(8)
Sn3 Li1 Al2 1_665 1_665 54.66(6)
Al2 Li1 Al2 1_655 1_665 96.0(4)
Sn2 Li1 Al2 . . 59.1(3)
Li3 Li1 Al2 7_666 . 55.8(3)
Li3 Li1 Al2 7_766 . 131.9(8)
Li3 Li1 Al2 7_656 . 55.8(3)
Sn3 Li1 Al2 1_655 . 126.83(8)
Sn3 Li1 Al2 . . 54.66(6)
Sn3 Li1 Al2 1_665 . 126.83(8)
Al2 Li1 Al2 1_655 . 96.0(4)
Al2 Li1 Al2 1_665 . 96.0(4)
Sn2 Li1 Li3 . 1_554 180.0
Li3 Li1 Li3 7_666 1_554 107.1(6)
Li3 Li1 Li3 7_766 1_554 107.1(6)
Li3 Li1 Li3 7_656 1_554 107.1(6)
Sn3 Li1 Li3 1_655 1_554 66.3(3)
Sn3 Li1 Li3 . 1_554 66.3(3)
Sn3 Li1 Li3 1_665 1_554 66.3(3)
Al2 Li1 Li3 1_655 1_554 120.9(3)
Al2 Li1 Li3 1_665 1_554 120.9(3)
Al2 Li1 Li3 . 1_554 120.9(3)
Li3 Li2 Li5 . 7_656 108.0(4)
Li3 Li2 Li5 . 7_556 108.0(4)
Li5 Li2 Li5 7_656 7_556 110.9(4)
Li3 Li2 Li5 . 7_666 108.0(4)
Li5 Li2 Li5 7_656 7_666 110.9(4)
Li5 Li2 Li5 7_556 7_666 110.9(4)
Li3 Li2 Al1 . . 180.0
Li5 Li2 Al1 7_656 . 72.0(4)
Li5 Li2 Al1 7_556 . 72.0(4)
Li5 Li2 Al1 7_666 . 72.0(4)
Li3 Li2 Sn2 . 7_666 70.1(3)
Li5 Li2 Sn2 7_656 7_666 178.1(7)
Li5 Li2 Sn2 7_556 7_666 69.98(15)
Li5 Li2 Sn2 7_666 7_666 69.98(15)
Al1 Li2 Sn2 . 7_666 109.9(3)
Li3 Li2 Sn2 . 7_766 70.1(3)
Li5 Li2 Sn2 7_656 7_766 69.98(15)
Li5 Li2 Sn2 7_556 7_766 178.1(7)
Li5 Li2 Sn2 7_666 7_766 69.98(15)
Al1 Li2 Sn2 . 7_766 109.9(3)
Sn2 Li2 Sn2 7_666 7_766 109.1(3)
Li3 Li2 Sn2 . 7_656 70.1(3)
Li5 Li2 Sn2 7_656 7_656 69.98(15)
Li5 Li2 Sn2 7_556 7_656 69.98(15)
Li5 Li2 Sn2 7_666 7_656 178.1(7)
Al1 Li2 Sn2 . 7_656 109.9(3)
Sn2 Li2 Sn2 7_666 7_656 109.1(3)
Sn2 Li2 Sn2 7_766 7_656 109.1(3)
Li3 Li2 Sn1 . 7_666 124.5(2)
Li5 Li2 Sn1 7_656 7_666 127.5(6)
Li5 Li2 Sn1 7_556 7_666 55.5(2)
Li5 Li2 Sn1 7_666 7_666 55.5(2)
Al1 Li2 Sn1 . 7_666 55.5(2)
Sn2 Li2 Sn1 7_666 7_666 54.34(7)
Sn2 Li2 Sn1 7_766 7_666 125.45(14)
Sn2 Li2 Sn1 7_656 7_666 125.45(14)
Li3 Li2 Sn1 . 7_656 124.5(2)
Li5 Li2 Sn1 7_656 7_656 55.5(2)
Li5 Li2 Sn1 7_556 7_656 55.5(2)
Li5 Li2 Sn1 7_666 7_656 127.5(6)
Al1 Li2 Sn1 . 7_656 55.5(2)
Sn2 Li2 Sn1 7_666 7_656 125.45(14)
Sn2 Li2 Sn1 7_766 7_656 125.45(14)
Sn2 Li2 Sn1 7_656 7_656 54.34(7)
Sn1 Li2 Sn1 7_666 7_656 91.1(3)
Li3 Li2 Sn1 . 7_766 124.5(2)
Li5 Li2 Sn1 7_656 7_766 55.5(2)
Li5 Li2 Sn1 7_556 7_766 127.5(6)
Li5 Li2 Sn1 7_666 7_766 55.5(2)
Al1 Li2 Sn1 . 7_766 55.5(2)
Sn2 Li2 Sn1 7_666 7_766 125.45(14)
Sn2 Li2 Sn1 7_766 7_766 54.34(7)
Sn2 Li2 Sn1 7_656 7_766 125.45(14)
Sn1 Li2 Sn1 7_666 7_766 91.1(3)
Sn1 Li2 Sn1 7_656 7_766 91.1(3)
Li2 Li3 Al2 . 7_656 73.8(5)
Li2 Li3 Al2 . 7_556 73.8(5)
Al2 Li3 Al2 7_656 7_556 112.5(5)
Li2 Li3 Al2 . 7_666 73.8(5)
Al2 Li3 Al2 7_656 7_666 112.5(5)
Al2 Li3 Al2 7_556 7_666 112.5(5)
Li2 Li3 Li1 . 7_666 107.1(6)
Al2 Li3 Li1 7_656 7_666 179.0(11)
Al2 Li3 Li1 7_556 7_666 67.88(16)
Al2 Li3 Li1 7_666 7_666 67.88(16)
Li2 Li3 Li1 . 7_766 107.1(6)
Al2 Li3 Li1 7_656 7_766 67.88(16)
Al2 Li3 Li1 7_556 7_766 179.0(11)
Al2 Li3 Li1 7_666 7_766 67.88(16)
Li1 Li3 Li1 7_666 7_766 111.7(5)
Li2 Li3 Li1 . 7_656 107.1(6)
Al2 Li3 Li1 7_656 7_656 67.88(16)
Al2 Li3 Li1 7_556 7_656 67.88(16)
Al2 Li3 Li1 7_666 7_656 179.0(11)
Li1 Li3 Li1 7_666 7_656 111.7(5)
Li1 Li3 Li1 7_766 7_656 111.7(5)
Li2 Li3 Sn2 . 7_666 57.4(4)
Al2 Li3 Sn2 7_656 7_666 131.2(9)
Al2 Li3 Sn2 7_556 7_666 56.3(2)
Al2 Li3 Sn2 7_666 7_666 56.3(2)
Li1 Li3 Sn2 7_666 7_666 49.8(4)
Li1 Li3 Sn2 7_766 7_666 124.1(3)
Li1 Li3 Sn2 7_656 7_666 124.1(3)
Li2 Li3 Sn2 . 7_656 57.4(4)
Al2 Li3 Sn2 7_656 7_656 56.3(2)
Al2 Li3 Sn2 7_556 7_656 56.3(2)
Al2 Li3 Sn2 7_666 7_656 131.2(9)
Li1 Li3 Sn2 7_666 7_656 124.1(3)
Li1 Li3 Sn2 7_766 7_656 124.1(3)
Li1 Li3 Sn2 7_656 7_656 49.8(4)
Sn2 Li3 Sn2 7_666 7_656 93.7(6)
Li2 Li3 Sn2 . 7_766 57.4(4)
Al2 Li3 Sn2 7_656 7_766 56.3(2)
Al2 Li3 Sn2 7_556 7_766 131.2(9)
Al2 Li3 Sn2 7_666 7_766 56.3(2)
Li1 Li3 Sn2 7_666 7_766 124.1(3)
Li1 Li3 Sn2 7_766 7_766 49.8(4)
Li1 Li3 Sn2 7_656 7_766 124.1(3)
Sn2 Li3 Sn2 7_666 7_766 93.7(6)
Sn2 Li3 Sn2 7_656 7_766 93.7(6)
Li2 Li3 Li1 . 1_556 180.0
Al2 Li3 Li1 7_656 1_556 106.2(5)
Al2 Li3 Li1 7_556 1_556 106.2(5)
Al2 Li3 Li1 7_666 1_556 106.2(5)
Li1 Li3 Li1 7_666 1_556 72.9(6)
Li1 Li3 Li1 7_766 1_556 72.9(6)
Li1 Li3 Li1 7_656 1_556 72.9(6)
Sn2 Li3 Li1 7_666 1_556 122.6(4)
Sn2 Li3 Li1 7_656 1_556 122.6(4)
Sn2 Li3 Li1 7_766 1_556 122.6(4)
Li2 Li3 Sn3 . 1_656 126.8(4)
Al2 Li3 Sn3 7_656 1_656 53.01(17)
Al2 Li3 Sn3 7_556 1_656 123.5(3)
Al2 Li3 Sn3 7_666 1_656 123.5(3)
Li1 Li3 Sn3 7_666 1_656 126.0(9)
Li1 Li3 Sn3 7_766 1_656 56.0(3)
Li1 Li3 Sn3 7_656 1_656 56.0(3)
Sn2 Li3 Sn3 7_666 1_656 175.8(8)
Sn2 Li3 Sn3 7_656 1_656 89.20(4)
Sn2 Li3 Sn3 7_766 1_656 89.20(4)
Li1 Li3 Sn3 1_556 1_656 53.2(4)
Al1 Li4 Al1 . 7_556 180.0
Al1 Li4 Al1 . 7_666 69.55(5)
Al1 Li4 Al1 7_556 7_666 110.45(5)
Al1 Li4 Al1 . 1_445 110.45(5)
Al1 Li4 Al1 7_556 1_445 69.55(5)
Al1 Li4 Al1 7_666 1_445 180.0
Al1 Li4 Al1 . 7_656 69.55(5)
Al1 Li4 Al1 7_556 7_656 110.45(5)
Al1 Li4 Al1 7_666 7_656 110.45(5)
Al1 Li4 Al1 1_445 7_656 69.55(5)
Al1 Li4 Al1 . 1_455 110.45(5)
Al1 Li4 Al1 7_556 1_455 69.55(5)
Al1 Li4 Al1 7_666 1_455 69.55(5)
Al1 Li4 Al1 1_445 1_455 110.45(5)
Al1 Li4 Al1 7_656 1_455 180.00(11)
Al1 Li4 Li5 . 7_556 71.53(5)
Al1 Li4 Li5 7_556 7_556 108.47(5)
Al1 Li4 Li5 7_666 7_556 108.47(5)
Al1 Li4 Li5 1_445 7_556 71.53(5)
Al1 Li4 Li5 7_656 7_556 108.47(5)
Al1 Li4 Li5 1_455 7_556 71.53(5)
Al1 Li4 Li5 . . 108.47(5)
Al1 Li4 Li5 7_556 . 71.53(5)
Al1 Li4 Li5 7_666 . 71.53(5)
Al1 Li4 Li5 1_445 . 108.47(5)
Al1 Li4 Li5 7_656 . 71.53(5)
Al1 Li4 Li5 1_455 . 108.47(5)
Li5 Li4 Li5 7_556 . 180.0
Al1 Li4 Sn1 . 7_666 55.23(3)
Al1 Li4 Sn1 7_556 7_666 124.77(3)
Al1 Li4 Sn1 7_666 7_666 53.41(6)
Al1 Li4 Sn1 1_445 7_666 126.59(6)
Al1 Li4 Sn1 7_656 7_666 124.77(3)
Al1 Li4 Sn1 1_455 7_666 55.23(3)
Li5 Li4 Sn1 7_556 7_666 55.066(12)
Li5 Li4 Sn1 . 7_666 124.934(12)
Al1 Li4 Sn1 . 1_445 124.77(3)
Al1 Li4 Sn1 7_556 1_445 55.23(3)
Al1 Li4 Sn1 7_666 1_445 126.59(6)
Al1 Li4 Sn1 1_445 1_445 53.41(6)
Al1 Li4 Sn1 7_656 1_445 55.23(3)
Al1 Li4 Sn1 1_455 1_445 124.77(3)
Li5 Li4 Sn1 7_556 1_445 124.934(12)
Li5 Li4 Sn1 . 1_445 55.066(12)
Sn1 Li4 Sn1 7_666 1_445 180.0
Al1 Li4 Sn1 . 7_556 126.60(6)
Al1 Li4 Sn1 7_556 7_556 53.41(6)
Al1 Li4 Sn1 7_666 7_556 124.77(3)
Al1 Li4 Sn1 1_445 7_556 55.23(3)
Al1 Li4 Sn1 7_656 7_556 124.77(3)
Al1 Li4 Sn1 1_455 7_556 55.23(3)
Li5 Li4 Sn1 7_556 7_556 55.066(11)
Li5 Li4 Sn1 . 7_556 124.934(12)
Sn1 Li4 Sn1 7_666 7_556 90.467(16)
Sn1 Li4 Sn1 1_445 7_556 89.533(16)
Al1 Li4 Sn1 . . 53.40(6)
Al1 Li4 Sn1 7_556 . 126.59(6)
Al1 Li4 Sn1 7_666 . 55.23(3)
Al1 Li4 Sn1 1_445 . 124.77(3)
Al1 Li4 Sn1 7_656 . 55.23(3)
Al1 Li4 Sn1 1_455 . 124.77(3)
Li5 Li4 Sn1 7_556 . 124.933(12)
Li5 Li4 Sn1 . . 55.067(12)
Sn1 Li4 Sn1 7_666 . 89.533(16)
Sn1 Li4 Sn1 1_445 . 90.467(16)
Sn1 Li4 Sn1 7_556 . 180.0
Al2 Li5 Li2 . 7_556 72.0(4)
Al2 Li5 Li2 . 7_666 72.0(4)
Li2 Li5 Li2 7_556 7_666 110.9(4)
Al2 Li5 Li2 . 7_656 72.0(4)
Li2 Li5 Li2 7_556 7_656 110.9(4)
Li2 Li5 Li2 7_666 7_656 110.9(4)
Al2 Li5 Li4 . . 180.0
Li2 Li5 Li4 7_556 . 108.0(4)
Li2 Li5 Li4 7_666 . 108.0(4)
Li2 Li5 Li4 7_656 . 108.0(4)
Al2 Li5 Sn1 . 1_445 109.9(3)
Li2 Li5 Sn1 7_556 1_445 70.00(15)
Li2 Li5 Sn1 7_666 1_445 178.1(7)
Li2 Li5 Sn1 7_656 1_445 70.00(15)
Li4 Li5 Sn1 . 1_445 70.1(3)
Al2 Li5 Sn1 . . 109.9(3)
Li2 Li5 Sn1 7_556 . 178.1(7)
Li2 Li5 Sn1 7_666 . 70.00(15)
Li2 Li5 Sn1 7_656 . 70.00(15)
Li4 Li5 Sn1 . . 70.1(3)
Sn1 Li5 Sn1 1_445 . 109.0(3)
Al2 Li5 Sn1 . 1_455 109.9(3)
Li2 Li5 Sn1 7_556 1_455 70.00(15)
Li2 Li5 Sn1 7_666 1_455 70.00(15)
Li2 Li5 Sn1 7_656 1_455 178.1(7)
Li4 Li5 Sn1 . 1_455 70.1(3)
Sn1 Li5 Sn1 1_445 1_455 109.0(3)
Sn1 Li5 Sn1 . 1_455 109.0(3)
Al2 Li5 Sn2 . . 55.5(2)
Li2 Li5 Sn2 7_556 . 127.6(6)
Li2 Li5 Sn2 7_666 . 55.5(2)
Li2 Li5 Sn2 7_656 . 55.5(2)
Li4 Li5 Sn2 . . 124.5(2)
Sn1 Li5 Sn2 1_445 . 125.47(14)
Sn1 Li5 Sn2 . . 54.35(7)
Sn1 Li5 Sn2 1_455 . 125.47(14)
Al2 Li5 Sn2 . 1_445 55.5(2)
Li2 Li5 Sn2 7_556 1_445 55.5(2)
Li2 Li5 Sn2 7_666 1_445 127.6(6)
Li2 Li5 Sn2 7_656 1_445 55.5(2)
Li4 Li5 Sn2 . 1_445 124.5(2)
Sn1 Li5 Sn2 1_445 1_445 54.35(7)
Sn1 Li5 Sn2 . 1_445 125.47(14)
Sn1 Li5 Sn2 1_455 1_445 125.46(14)
Sn2 Li5 Sn2 . 1_445 91.1(3)
Al2 Li5 Sn2 . 1_455 55.5(2)
Li2 Li5 Sn2 7_556 1_455 55.5(2)
Li2 Li5 Sn2 7_666 1_455 55.5(2)
Li2 Li5 Sn2 7_656 1_455 127.6(6)
Li4 Li5 Sn2 . 1_455 124.5(2)
Sn1 Li5 Sn2 1_445 1_455 125.47(14)
Sn1 Li5 Sn2 . 1_455 125.47(14)
Sn1 Li5 Sn2 1_455 1_455 54.35(7)
Sn2 Li5 Sn2 . 1_455 91.1(3)
Sn2 Li5 Sn2 1_445 1_455 91.1(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Sn1 Al1 . 2.812(3)
Sn1 Sn2 . 2.8541(12)
Sn1 Li5 1_655 2.896(5)
Sn1 Li5 1_665 2.896(5)
Sn1 Li5 . 2.896(5)
Sn1 Al1 7_666 2.8985(11)
Sn1 Al1 7_766 2.8986(11)
Sn1 Al1 7_656 2.8986(11)
Sn1 Li2 7_666 3.303(9)
Sn1 Li2 7_656 3.304(9)
Sn1 Li2 7_766 3.304(9)
Sn1 Li4 1_655 3.3219(5)
Sn2 Li1 . 2.585(19)
Sn2 Al2 . 2.8853(11)
Sn2 Al2 1_655 2.8853(11)
Sn2 Al2 1_665 2.8853(11)
Sn2 Li2 7_666 2.896(5)
Sn2 Li2 7_766 2.896(5)
Sn2 Li2 7_656 2.896(5)
Sn2 Li3 7_666 3.234(15)
Sn2 Li3 7_656 3.234(15)
Sn2 Li3 7_766 3.234(15)
Sn2 Li5 . 3.303(9)
Sn3 Al2 7 2.829(3)
Sn3 Al2 . 2.829(3)
Sn3 Li1 . 2.975(8)
Sn3 Li1 7 2.975(8)
Sn3 Li1 7_665 2.975(8)
Sn3 Li1 1_445 2.975(8)
Sn3 Li1 1_455 2.975(8)
Sn3 Li1 7_655 2.975(8)
Sn3 Li3 7_666 3.401(16)
Sn3 Li3 1_444 3.401(16)
Sn3 Li3 7_556 3.401(16)
Sn3 Li3 1_554 3.401(16)
Al1 Li2 . 2.862(16)
Al1 Li4 1_655 2.8713(10)
Al1 Li4 . 2.8713(10)
Al1 Li4 1_665 2.8713(10)
Al1 Sn1 7_666 2.8986(11)
Al1 Sn1 7_766 2.8986(11)
Al1 Sn1 7_656 2.8986(11)
Al2 Li5 . 2.822(16)
Al2 Li3 7_556 2.836(8)
Al2 Li3 7_666 2.836(8)
Al2 Li3 7_656 2.836(8)
Al2 Sn2 1_445 2.8853(11)
Al2 Sn2 1_455 2.8853(11)
Al2 Li1 1_445 3.175(10)
Al2 Li1 1_455 3.175(10)
Al2 Li1 . 3.175(10)
Li1 Li3 7_666 2.850(9)
Li1 Li3 7_766 2.850(9)
Li1 Li3 7_656 2.850(9)
Li1 Sn3 1_655 2.975(8)
Li1 Sn3 1_665 2.975(8)
Li1 Al2 1_655 3.175(10)
Li1 Al2 1_665 3.175(10)
Li1 Li3 1_554 3.24(4)
Li2 Li3 . 2.73(3)
Li2 Li5 7_656 2.863(7)
Li2 Li5 7_556 2.863(7)
Li2 Li5 7_666 2.863(7)
Li2 Sn2 7_666 2.896(5)
Li2 Sn2 7_766 2.896(5)
Li2 Sn2 7_656 2.896(5)
Li2 Sn1 7_666 3.304(9)
Li2 Sn1 7_656 3.304(9)
Li2 Sn1 7_766 3.304(9)
Li3 Al2 7_656 2.836(8)
Li3 Al2 7_556 2.836(8)
Li3 Al2 7_666 2.836(8)
Li3 Li1 7_666 2.850(9)
Li3 Li1 7_766 2.850(9)
Li3 Li1 7_656 2.850(9)
Li3 Sn2 7_666 3.234(15)
Li3 Sn2 7_656 3.234(15)
Li3 Sn2 7_766 3.234(15)
Li3 Li1 1_556 3.24(4)
Li3 Sn3 1_656 3.402(16)
Li4 Al1 7_556 2.8713(10)
Li4 Al1 7_666 2.8713(10)
Li4 Al1 1_445 2.8713(10)
Li4 Al1 7_656 2.8713(10)
Li4 Al1 1_455 2.8713(10)
Li4 Li5 7_556 2.888(16)
Li4 Li5 . 2.888(16)
Li4 Sn1 7_666 3.3219(5)
Li4 Sn1 1_445 3.3219(5)
Li4 Sn1 7_556 3.3219(5)
Li5 Li2 7_556 2.863(7)
Li5 Li2 7_666 2.863(7)
Li5 Li2 7_656 2.863(7)
Li5 Sn1 1_445 2.896(5)
Li5 Sn1 1_455 2.896(5)
Li5 Sn2 1_445 3.303(9)
Li5 Sn2 1_455 3.303(9)

_cod_database_fobs_code 2020747
