#------------------------------------------------------------------------------
#$Date: 2017-07-25 12:01:30 +0300 (Tue, 25 Jul 2017) $
#$Revision: 199072 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/07/2020779.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2020779
loop_
_publ_author_name
'Fu, Wei-Wei'
'Li, Juan'
'Liu, Shu-Ting'
'Zhao, Dan'
'Zhou, Xue'
'Tong, Yang'
_publ_section_title
;
 A one-dimensional silver(I) coordination polymer based on
 5-methyl-1,3,4-thiadiazol-2-amine and pyridine-2,3-dicarboxylate
;
_journal_coeditor_code           LG3205
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              498
_journal_page_last               502
_journal_paper_doi               10.1107/S2053229617007653
_journal_volume                  73
_journal_year                    2017
_chemical_formula_iupac
'[Ag2 (C7 H3 N O4) (C3 H5 N3 S)3], H2 O, C2 H6 O'
_chemical_formula_moiety         'C16 H18 Ag2 N10 O4 S3, H2 O, C2 H6 O'
_chemical_formula_sum            'C18 H26 Ag2 N10 O6 S3'
_chemical_formula_weight         790.38
_chemical_name_systematic
'catena-Poly[[silver(I)-(μ₂-pyridine-2,3-dicarboxylato-κ²N:O³)-silver(I)-tris(μ₂-5-methyl-1,3,4-thiodiazol-2-amine-κ²N:N')] monohydrate ethanol monosolvate]'
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 98.2210(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.3665(4)
_cell_length_b                   23.1277(11)
_cell_length_c                   13.5984(7)
_cell_measurement_reflns_used    8981
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.6099
_cell_measurement_theta_min      2.8377
_cell_volume                     2604.2(2)
_computing_cell_refinement
;
SMART (Bruker, 2012)
;
_computing_data_collection
;
SMART (Bruker, 2012)
;
_computing_data_reduction
;
SAINT (Bruker, 2012)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg, 2008)
;
_computing_publication_material
;
publCIF (Westrip, 2010) and PLATON (Spek, 2009)
;
_computing_structure_refinement
;
SHELXL2014 (Sheldrick, 2015b) and OLEX2 (Dolomanov et al.,
2009)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a) and OLEX2 (Dolomanov et al.,
2009)
;
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_device_type  'Bruker SMART CCD area-detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0178
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            15594
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.612
_diffrn_reflns_theta_min         1.751
_exptl_absorpt_coefficient_mu    1.802
_exptl_absorpt_correction_T_max  0.7276
_exptl_absorpt_correction_T_min  0.7053
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(SADABS; Bruker, 2012)
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.016
_exptl_crystal_description       block
_exptl_crystal_F_000             1576
_exptl_crystal_size_max          0.220
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.180
_refine_diff_density_max         1.339
_refine_diff_density_min         -0.817
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.093
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     337
_refine_ls_number_reflns         5918
_refine_ls_number_restraints     7
_refine_ls_restrained_S_all      1.093
_refine_ls_R_factor_all          0.0304
_refine_ls_R_factor_gt           0.0269
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0262P)²+4.0926P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0627
_refine_ls_wR_factor_ref         0.0646
_reflns_number_gt                5458
_reflns_number_total             5918
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            lg3205sup1.cif
_cod_data_source_block           I
_cod_database_code               2020779
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.694
_shelx_estimated_absorpt_t_max   0.739
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
Ag Ag1 0.31342(2) 0.12131(2) 0.21967(2) 0.01782(6) Uani d 1
Ag Ag2 0.26584(2) 0.26895(2) 0.20782(2) 0.01788(6) Uani d 1
S S1 -0.04351(9) 0.17446(3) -0.07942(5) 0.01951(14) Uani d 1
S S2 0.82115(8) 0.22203(3) 0.17491(6) 0.02212(15) Uani d 1
S S3 -0.01904(10) 0.18514(4) 0.46437(6) 0.02778(16) Uani d 1
N N1 0.5476(3) 0.17953(10) 0.19762(17) 0.0175(5) Uani d 1
N N2 0.5309(3) 0.23914(9) 0.20876(18) 0.0179(5) Uani d 1
N N3 0.6849(3) 0.32419(11) 0.2079(2) 0.0281(6) Uani d 1
H H3A 0.603(3) 0.3452(14) 0.216(3) 0.034 Uiso d 1
H H3B 0.781(3) 0.3381(15) 0.201(3) 0.034 Uiso d 1
N N4 0.1506(3) 0.22545(10) 0.33860(17) 0.0181(5) Uani d 1
N N5 0.1617(3) 0.16546(10) 0.33185(17) 0.0189(5) Uani d 1
N N6 0.0645(4) 0.08011(12) 0.3967(2) 0.0309(6) Uani d 1
H H6A 0.026(4) 0.0638(15) 0.449(2) 0.037 Uiso d 1
H H6B 0.096(4) 0.0587(14) 0.348(2) 0.037 Uiso d 1
N N7 0.1589(3) 0.21290(9) 0.06377(17) 0.0164(4) Uani d 1
N N8 0.1552(3) 0.15329(9) 0.07817(17) 0.0172(5) Uani d 1
N N9 0.0245(3) 0.07007(10) 0.00749(18) 0.0205(5) Uani d 1
H H9A 0.050(4) 0.0502(13) 0.0639(17) 0.025 Uiso d 1
H H9B -0.061(3) 0.0589(14) -0.033(2) 0.025 Uiso d 1
N N10 0.0586(3) 0.54262(9) 0.19787(17) 0.0156(4) Uani d 1
O O1 0.2551(2) 0.37189(8) 0.16865(16) 0.0248(4) Uani d 1
O O2 0.0125(3) 0.34120(8) 0.19185(18) 0.0310(5) Uani d 1
O O3 0.2492(3) 0.44391(9) 0.35920(16) 0.0290(5) Uani d 1
O O4 0.3729(2) 0.51789(9) 0.29542(17) 0.0285(5) Uani d 1
C C1 0.7371(4) 0.10357(14) 0.1620(3) 0.0308(7) Uani d 1
H H1A 0.6515 0.0774 0.1766 0.046 Uiso calc 1
H H1B 0.8377 0.0944 0.2055 0.046 Uiso calc 1
H H1C 0.7531 0.0990 0.0925 0.046 Uiso calc 1
C C2 0.6898(3) 0.16445(12) 0.1796(2) 0.0190(5) Uani d 1
C C3 0.6649(3) 0.26732(12) 0.1997(2) 0.0174(5) Uani d 1
C C4 0.0213(4) 0.30328(13) 0.4228(2) 0.0260(6) Uani d 1
H H4A 0.0814 0.3289 0.3838 0.039 Uiso calc 1
H H4B 0.0516 0.3117 0.4937 0.039 Uiso calc 1
H H4C -0.0948 0.3097 0.4040 0.039 Uiso calc 1
C C5 0.0604(3) 0.24235(13) 0.4031(2) 0.0211(6) Uani d 1
C C6 0.0783(3) 0.13841(13) 0.3920(2) 0.0210(6) Uani d 1
C C7 0.0401(4) 0.29227(12) -0.0412(2) 0.0236(6) Uani d 1
H H7A -0.0682 0.3046 -0.0307 0.035 Uiso calc 1
H H7B 0.0523 0.2974 -0.1113 0.035 Uiso calc 1
H H7C 0.1212 0.3156 0.0003 0.035 Uiso calc 1
C C8 0.0631(3) 0.23028(11) -0.01375(19) 0.0156(5) Uani d 1
C C9 0.0535(3) 0.12705(11) 0.01016(19) 0.0153(5) Uani d 1
C C10 0.1095(3) 0.38008(11) 0.1771(2) 0.0181(5) Uani d 1
C C11 0.0427(3) 0.44062(11) 0.16195(19) 0.0143(5) Uani d 1
C C12 -0.0946(3) 0.44998(12) 0.0934(2) 0.0184(5) Uani d 1
H H12 -0.1476 0.4184 0.0579 0.022 Uiso calc 1
C C13 -0.1540(3) 0.50573(12) 0.0768(2) 0.0196(5) Uani d 1
H H13 -0.2474 0.5131 0.0300 0.023 Uiso calc 1
C C14 -0.0728(3) 0.55029(12) 0.1306(2) 0.0186(5) Uani d 1
H H14 -0.1127 0.5885 0.1191 0.022 Uiso calc 1
C C15 0.1163(3) 0.48839(11) 0.21378(19) 0.0141(5) Uani d 1
C C16 0.2591(3) 0.48240(11) 0.2964(2) 0.0177(5) Uani d 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N8 Ag1 N10 . 2_545 146.03(8) y
N8 Ag1 N5 . . 95.96(8) y
N10 Ag1 N5 2_545 . 106.36(8) y
N8 Ag1 N1 . . 95.54(8) y
N10 Ag1 N1 2_545 . 99.78(8) y
N5 Ag1 N1 . . 111.02(8) y
N2 Ag2 N4 . . 111.20(8) y
N2 Ag2 N7 . . 95.04(8) y
N4 Ag2 N7 . . 103.79(8) y
N2 Ag2 O1 . . 107.25(7) y
N4 Ag2 O1 . . 124.98(7) y
N7 Ag2 O1 . . 110.46(7) y
C8 S1 C9 . . 87.42(12) ?
C2 S2 C3 . . 87.59(13) ?
C6 S3 C5 . . 87.71(14) ?
C2 N1 N2 . . 113.3(2) ?
C2 N1 Ag1 . . 130.69(18) ?
N2 N1 Ag1 . . 115.99(16) ?
C3 N2 N1 . . 112.2(2) ?
C3 N2 Ag2 . . 132.68(18) ?
N1 N2 Ag2 . . 113.80(16) ?
C3 N3 H3A . . 118(2) ?
C3 N3 H3B . . 117(2) ?
H3A N3 H3B . . 124(3) ?
C5 N4 N5 . . 113.3(2) ?
C5 N4 Ag2 . . 136.0(2) ?
N5 N4 Ag2 . . 109.59(16) ?
C6 N5 N4 . . 112.8(2) ?
C6 N5 Ag1 . . 125.70(19) ?
N4 N5 Ag1 . . 121.47(16) ?
C6 N6 H6A . . 120(2) ?
C6 N6 H6B . . 119(2) ?
H6A N6 H6B . . 122(3) ?
C8 N7 N8 . . 113.5(2) ?
C8 N7 Ag2 . . 127.54(18) ?
N8 N7 Ag2 . . 115.52(15) ?
C9 N8 N7 . . 112.6(2) ?
C9 N8 Ag1 . . 132.80(18) ?
N7 N8 Ag1 . . 114.49(15) ?
C9 N9 H9A . . 118(2) ?
C9 N9 H9B . . 116(2) ?
H9A N9 H9B . . 117(3) ?
C14 N10 C15 . . 118.2(2) ?
C14 N10 Ag1 . 2 120.29(17) ?
C15 N10 Ag1 . 2 121.49(17) ?
C10 O1 Ag2 . . 97.66(16) ?
C2 C1 H1A . . 109.5 ?
C2 C1 H1B . . 109.5 ?
H1A C1 H1B . . 109.5 ?
C2 C1 H1C . . 109.5 ?
H1A C1 H1C . . 109.5 ?
H1B C1 H1C . . 109.5 ?
N1 C2 C1 . . 123.8(3) ?
N1 C2 S2 . . 113.8(2) ?
C1 C2 S2 . . 122.4(2) ?
N2 C3 N3 . . 125.4(3) ?
N2 C3 S2 . . 113.1(2) ?
N3 C3 S2 . . 121.5(2) ?
C5 C4 H4A . . 109.5 ?
C5 C4 H4B . . 109.5 ?
H4A C4 H4B . . 109.5 ?
C5 C4 H4C . . 109.5 ?
H4A C4 H4C . . 109.5 ?
H4B C4 H4C . . 109.5 ?
N4 C5 C4 . . 125.1(3) ?
N4 C5 S3 . . 113.1(2) ?
C4 C5 S3 . . 121.8(2) ?
N5 C6 N6 . . 124.2(3) ?
N5 C6 S3 . . 113.0(2) ?
N6 C6 S3 . . 122.7(2) ?
C8 C7 H7A . . 109.5 ?
C8 C7 H7B . . 109.5 ?
H7A C7 H7B . . 109.5 ?
C8 C7 H7C . . 109.5 ?
H7A C7 H7C . . 109.5 ?
H7B C7 H7C . . 109.5 ?
N7 C8 C7 . . 123.2(2) ?
N7 C8 S1 . . 113.6(2) ?
C7 C8 S1 . . 123.2(2) ?
N8 C9 N9 . . 124.8(2) ?
N8 C9 S1 . . 112.97(19) ?
N9 C9 S1 . . 122.2(2) ?
O2 C10 O1 . . 124.7(2) ?
O2 C10 C11 . . 117.0(2) ?
O1 C10 C11 . . 118.2(2) ?
C12 C11 C15 . . 118.4(2) ?
C12 C11 C10 . . 119.4(2) ?
C15 C11 C10 . . 122.3(2) ?
C11 C12 C13 . . 119.8(2) ?
C11 C12 H12 . . 120.1 ?
C13 C12 H12 . . 120.1 ?
C14 C13 C12 . . 117.9(2) ?
C14 C13 H13 . . 121.0 ?
C12 C13 H13 . . 121.0 ?
N10 C14 C13 . . 123.8(2) ?
N10 C14 H14 . . 118.1 ?
C13 C14 H14 . . 118.1 ?
N10 C15 C11 . . 122.0(2) ?
N10 C15 C16 . . 115.3(2) ?
C11 C15 C16 . . 122.6(2) ?
O3 C16 O4 . . 126.7(2) ?
O3 C16 C15 . . 116.7(2) ?
O4 C16 C15 . . 116.6(2) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ag1 N8 . 2.296(2) y
Ag1 N10 2_545 2.318(2) y
Ag1 N5 . 2.352(2) y
Ag1 N1 . 2.431(2) y
Ag2 N2 . 2.320(2) y
Ag2 N4 . 2.365(2) y
Ag2 N7 . 2.412(2) y
Ag2 O1 . 2.4386(19) y
S1 C8 . 1.741(3) ?
S1 C9 . 1.750(3) ?
S2 C2 . 1.733(3) ?
S2 C3 . 1.745(3) ?
S3 C6 . 1.740(3) ?
S3 C5 . 1.745(3) ?
N1 C2 . 1.296(3) ?
N1 N2 . 1.396(3) ?
N2 C3 . 1.318(3) ?
N3 C3 . 1.328(4) ?
N3 H3A . 0.864(18) ?
N3 H3B . 0.884(18) ?
N4 C5 . 1.297(4) ?
N4 N5 . 1.395(3) ?
N5 C6 . 1.308(4) ?
N6 C6 . 1.355(4) ?
N6 H6A . 0.901(18) ?
N6 H6B . 0.894(18) ?
N7 C8 . 1.294(3) ?
N7 N8 . 1.393(3) ?
N8 C9 . 1.312(3) ?
N9 C9 . 1.340(3) ?
N9 H9A . 0.894(18) ?
N9 H9B . 0.874(18) ?
N10 C14 . 1.338(3) ?
N10 C15 . 1.350(3) ?
N10 Ag1 2 2.318(2) ?
O1 C10 . 1.255(3) ?
O2 C10 . 1.246(3) ?
O3 C16 . 1.244(3) ?
O4 C16 . 1.259(3) ?
C1 C2 . 1.491(4) ?
C1 H1A . 0.9800 ?
C1 H1B . 0.9800 ?
C1 H1C . 0.9800 ?
C4 C5 . 1.480(4) ?
C4 H4A . 0.9800 ?
C4 H4B . 0.9800 ?
C4 H4C . 0.9800 ?
C7 C8 . 1.487(4) ?
C7 H7A . 0.9800 ?
C7 H7B . 0.9800 ?
C7 H7C . 0.9800 ?
C10 C11 . 1.511(3) ?
C11 C12 . 1.389(4) ?
C11 C15 . 1.404(3) ?
C12 C13 . 1.389(4) ?
C12 H12 . 0.9500 ?
C13 C14 . 1.384(4) ?
C13 H13 . 0.9500 ?
C14 H14 . 0.9500 ?
C15 C16 . 1.525(3) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
N3 H3B O2 1_655 0.88(3) 1.96(3) 2.808(4) 161(3)
N6 H6B O4 2_545 0.90(3) 2.22(3) 3.092(4) 166(3)
N9 H9A O4 2_545 0.89(3) 2.07(2) 2.953(3) 170(3)
N9 H9B O3 4_565 0.88(3) 2.00(3) 2.854(3) 164(3)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion
C2 N1 N2 C3 . -0.8(3)
Ag1 N1 N2 C3 . 177.41(18)
C2 N1 N2 Ag2 . 167.85(19)
Ag1 N1 N2 Ag2 . -14.0(2)
C5 N4 N5 C6 . 0.2(3)
Ag2 N4 N5 C6 . -169.88(18)
C5 N4 N5 Ag1 . 179.07(18)
Ag2 N4 N5 Ag1 . 9.0(2)
C8 N7 N8 C9 . -0.6(3)
Ag2 N7 N8 C9 . 160.06(18)
C8 N7 N8 Ag1 . -176.86(18)
Ag2 N7 N8 Ag1 . -16.2(2)
N2 N1 C2 C1 . -178.3(3)
Ag1 N1 C2 C1 . 3.9(4)
N2 N1 C2 S2 . 0.3(3)
Ag1 N1 C2 S2 . -177.51(13)
C3 S2 C2 N1 . 0.1(2)
C3 S2 C2 C1 . 178.7(3)
N1 N2 C3 N3 . -179.2(3)
Ag2 N2 C3 N3 . 15.1(4)
N1 N2 C3 S2 . 0.9(3)
Ag2 N2 C3 S2 . -164.92(14)
C2 S2 C3 N2 . -0.6(2)
C2 S2 C3 N3 . 179.4(3)
N5 N4 C5 C4 . -177.3(3)
Ag2 N4 C5 C4 . -10.8(4)
N5 N4 C5 S3 . 0.8(3)
Ag2 N4 C5 S3 . 167.31(15)
C6 S3 C5 N4 . -1.2(2)
C6 S3 C5 C4 . 176.9(2)
N4 N5 C6 N6 . 177.4(3)
Ag1 N5 C6 N6 . -1.4(4)
N4 N5 C6 S3 . -1.1(3)
Ag1 N5 C6 S3 . -179.95(12)
C5 S3 C6 N5 . 1.3(2)
C5 S3 C6 N6 . -177.2(3)
N8 N7 C8 C7 . 176.7(2)
Ag2 N7 C8 C7 . 18.9(4)
N8 N7 C8 S1 . -0.4(3)
Ag2 N7 C8 S1 . -158.19(13)
C9 S1 C8 N7 . 0.9(2)
C9 S1 C8 C7 . -176.2(3)
N7 N8 C9 N9 . -178.8(3)
Ag1 N8 C9 N9 . -3.4(4)
N7 N8 C9 S1 . 1.2(3)
Ag1 N8 C9 S1 . 176.65(14)
C8 S1 C9 N8 . -1.2(2)
C8 S1 C9 N9 . 178.8(2)
Ag2 O1 C10 O2 . -5.8(3)
Ag2 O1 C10 C11 . 178.3(2)
O2 C10 C11 C12 . -50.2(4)
O1 C10 C11 C12 . 125.9(3)
O2 C10 C11 C15 . 130.9(3)
O1 C10 C11 C15 . -52.9(4)
C15 C11 C12 C13 . 0.8(4)
C10 C11 C12 C13 . -178.1(2)
C11 C12 C13 C14 . -0.3(4)
C15 N10 C14 C13 . 0.5(4)
Ag1 N10 C14 C13 2 178.6(2)
C12 C13 C14 N10 . -0.4(4)
C14 N10 C15 C11 . 0.1(4)
Ag1 N10 C15 C11 2 -177.95(18)
C14 N10 C15 C16 . -176.0(2)
Ag1 N10 C15 C16 2 6.0(3)
C12 C11 C15 N10 . -0.8(4)
C10 C11 C15 N10 . 178.1(2)
C12 C11 C15 C16 . 175.0(2)
C10 C11 C15 C16 . -6.1(4)
N10 C15 C16 O3 . 130.6(3)
C11 C15 C16 O3 . -45.5(4)
N10 C15 C16 O4 . -47.6(3)
C11 C15 C16 O4 . 136.3(3)

_cod_database_fobs_code 2020779
