#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/86/2208600.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2208600
loop_
_publ_author_name
'Bobev, Svilen'
'Bauer, Eric D.'
'Sarrao, John L.'
_publ_section_title
;
 Uranium and aluminium order--disorder in
 U~1{-~x}Pt₂Al~7{-~6x} [x = 0.33(1)]
;
_journal_coeditor_code           HB2014
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i77
_journal_page_last               i79
_journal_paper_doi               10.1107/S1600536806007288
_journal_volume                  62
_journal_year                    2006
_chemical_formula_iupac          'U0.67 Pt2 Al5'
_chemical_formula_moiety         'Al5 Pt2 U0.67'
_chemical_formula_sum            'Al5 Pt2 U0.67'
_chemical_formula_weight         684.56
_chemical_name_systematic
;
uranium diplatinum pentaaluminium
;
_space_group_IT_number           194
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            2
_cell_length_a                   4.2929(8)
_cell_length_b                   4.2929(8)
_cell_length_c                   16.276(6)
_cell_measurement_reflns_used    2248
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      28.06
_cell_measurement_theta_min      2.50
_cell_volume                     259.76(12)
_computing_cell_refinement       'SAINT (Bruker, 2002)'
_computing_data_collection       'SMART (Bruker, 2002)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'XP in SHELXTL'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXTL (Sheldrick, 2001)'
_computing_structure_solution    'SHELXTL (Sheldrick, 2001)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 8.3
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker SMART APEX'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0566
_diffrn_reflns_av_sigmaI/netI    0.0252
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            2248
_diffrn_reflns_theta_full        28.06
_diffrn_reflns_theta_max         28.06
_diffrn_reflns_theta_min         2.50
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    75.257
_exptl_absorpt_correction_T_max  0.105
_exptl_absorpt_correction_T_min  0.047
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2003)'
_exptl_crystal_colour            grey
_exptl_crystal_density_diffrn    8.752
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             565
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.035
_exptl_crystal_size_min          0.03
_refine_diff_density_max         1.000
_refine_diff_density_min         -1.497
_refine_ls_extinction_coef       0.0038(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL97
_refine_ls_goodness_of_fit_ref   1.086
_refine_ls_matrix_type           full
_refine_ls_number_parameters     19
_refine_ls_number_reflns         154
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.086
_refine_ls_R_factor_all          0.0250
_refine_ls_R_factor_gt           0.0199
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0195P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0383
_refine_ls_wR_factor_ref         0.0392
_reflns_number_gt                135
_reflns_number_total             154
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            hb2014.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        259.77(12)
_cod_database_code               2208600
_cod_database_fobs_code          2208600
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z+1/2'
'y, -x+y, z+1/2'
'x-y, x, z+1/2'
'y, x, -z'
'x-y, -y, -z'
'-x, -x+y, -z'
'-y, -x, -z+1/2'
'-x+y, y, -z+1/2'
'x, x-y, -z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'x, y, -z-1/2'
'-y, x-y, -z-1/2'
'-x+y, -x, -z-1/2'
'-y, -x, z'
'-x+y, y, z'
'x, x-y, z'
'y, x, z-1/2'
'x-y, -y, z-1/2'
'-x, -x+y, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
U U 0.3333 0.6667 0.2500 0.0126(4) Uani d SP 0.670(4)
Pt Pt 0.3333 0.6667 0.60912(4) 0.0111(3) Uani d S 1
Al Al1 0.5350(14) 0.070(3) 0.2500 0.018(3) Uani d SP 0.349(14)
Al Al2 0.3333 0.6667 0.0457(3) 0.0117(10) Uani d S 1
Al Al3 0.0000 0.0000 0.1355(3) 0.0114(9) Uani d S 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
Al1 U Al1 2 1_565 120.001(2)
Al1 U Al1 2 3_665 119.9990(10)
Al1 U Al1 1_565 3_665 119.999(2)
Al1 U Al1 2 3_675 104.06(13)
Al1 U Al1 1_565 3_675 15.94(14)
Al1 U Al1 3_665 3_675 135.94(14)
Al1 U Al1 2 3_565 15.94(13)
Al1 U Al1 1_565 3_565 104.06(13)
Al1 U Al1 3_665 3_565 135.94(14)
Al1 U Al1 3_675 3_565 88.1(3)
Al1 U Al1 2 2_665 135.94(14)
Al1 U Al1 1_565 2_665 15.94(13)
Al1 U Al1 3_665 2_665 104.06(14)
Al1 U Al1 3_675 2_665 31.9(3)
Al1 U Al1 3_565 2_665 120.001(2)
Al1 U Al1 2 1_455 15.94(13)
Al1 U Al1 1_565 1_455 135.94(14)
Al1 U Al1 3_665 1_455 104.06(14)
Al1 U Al1 3_675 1_455 120.0010(10)
Al1 U Al1 3_565 1_455 31.9(3)
Al1 U Al1 2_665 1_455 151.9(3)
Al1 U Al1 2 . 104.06(14)
Al1 U Al1 1_565 . 135.94(14)
Al1 U Al1 3_665 . 15.94(14)
Al1 U Al1 3_675 . 151.9(3)
Al1 U Al1 3_565 . 120.000(3)
Al1 U Al1 2_665 . 120.000(3)
Al1 U Al1 1_455 . 88.1(3)
Al1 U Al1 2 2_655 135.94(14)
Al1 U Al1 1_565 2_655 104.06(14)
Al1 U Al1 3_665 2_655 15.94(14)
Al1 U Al1 3_675 2_655 120.000(4)
Al1 U Al1 3_565 2_655 151.9(3)
Al1 U Al1 2_665 2_655 88.1(3)
Al1 U Al1 1_455 2_655 120.000(2)
Al1 U Al1 . 2_655 31.9(3)
Al1 U Al3 2 . 66.44(2)
Al1 U Al3 1_565 . 143.06(7)
Al1 U Al3 3_665 . 66.45(2)
Al1 U Al3 3_675 . 140.22(8)
Al1 U Al3 3_565 . 78.80(11)
Al1 U Al3 2_665 . 140.22(8)
Al1 U Al3 1_455 . 54.95(10)
Al1 U Al3 . . 54.95(10)
Al1 U Al3 2_655 . 78.80(11)
Al1 U Al3 2 1_565 66.45(2)
Al1 U Al3 1_565 1_565 66.45(2)
Al1 U Al3 3_665 1_565 143.06(7)
Al1 U Al3 3_675 1_565 54.95(10)
Al1 U Al3 3_565 1_565 54.95(10)
Al1 U Al3 2_665 1_565 78.80(11)
Al1 U Al3 1_455 1_565 78.80(11)
Al1 U Al3 . 1_565 140.22(8)
Al1 U Al3 2_655 1_565 140.22(8)
Al3 U Al3 . 1_565 87.60(11)
Al1 U Al3 2 1_665 143.06(7)
Al1 U Al3 1_565 1_665 66.45(2)
Al1 U Al3 3_665 1_665 66.45(2)
Al1 U Al3 3_675 1_665 78.80(11)
Al1 U Al3 3_565 1_665 140.22(8)
Al1 U Al3 2_665 1_665 54.95(10)
Al1 U Al3 1_455 1_665 140.22(8)
Al1 U Al3 . 1_665 78.80(11)
Al1 U Al3 2_655 1_665 54.95(10)
Al3 U Al3 . 1_665 87.60(11)
Al3 U Al3 1_565 1_665 87.60(11)
Al1 Pt Al1 15_556 13_666 39.8(4)
Al1 Pt Al1 15_556 14_566 39.8(4)
Al1 Pt Al1 13_666 14_566 39.8(4)
Al1 Pt Al3 15_556 4_565 103.3(2)
Al1 Pt Al3 13_666 4_565 69.49(14)
Al1 Pt Al3 14_566 4_565 69.49(13)
Al1 Pt Al3 15_556 4_665 69.49(13)
Al1 Pt Al3 13_666 4_665 69.49(13)
Al1 Pt Al3 14_566 4_665 103.3(3)
Al3 Pt Al3 4_565 4_665 117.15(6)
Al1 Pt Al3 15_556 4 69.49(13)
Al1 Pt Al3 13_666 4 103.3(3)
Al1 Pt Al3 14_566 4 69.49(13)
Al3 Pt Al3 4_565 4 117.15(6)
Al3 Pt Al3 4_665 4 117.15(6)
Al1 Pt Al2 15_556 16_556 156.9(2)
Al1 Pt Al2 13_666 16_556 156.9(2)
Al1 Pt Al2 14_566 16_556 156.9(2)
Al3 Pt Al2 4_565 16_556 99.83(11)
Al3 Pt Al2 4_665 16_556 99.83(11)
Al3 Pt Al2 4 16_556 99.83(11)
Al1 Pt Al2 15_556 4_665 89.5(2)
Al1 Pt Al2 13_666 4_665 122.32(11)
Al1 Pt Al2 14_566 4_665 122.32(11)
Al3 Pt Al2 4_565 4_665 167.23(15)
Al3 Pt Al2 4_665 4_665 67.09(7)
Al3 Pt Al2 4 4_665 67.09(7)
Al2 Pt Al2 16_556 4_665 67.40(10)
Al1 Pt Al2 15_556 4_565 122.32(11)
Al1 Pt Al2 13_666 4_565 122.32(11)
Al1 Pt Al2 14_566 4_565 89.5(2)
Al3 Pt Al2 4_565 4_565 67.09(7)
Al3 Pt Al2 4_665 4_565 167.23(15)
Al3 Pt Al2 4 4_565 67.09(7)
Al2 Pt Al2 16_556 4_565 67.40(10)
Al2 Pt Al2 4_665 4_565 106.17(11)
Al1 Pt Al2 15_556 4_675 122.32(11)
Al1 Pt Al2 13_666 4_675 89.5(2)
Al1 Pt Al2 14_566 4_675 122.32(11)
Al3 Pt Al2 4_565 4_675 67.09(7)
Al3 Pt Al2 4_665 4_675 67.09(7)
Al3 Pt Al2 4 4_675 167.23(15)
Al2 Pt Al2 16_556 4_675 67.40(10)
Al2 Pt Al2 4_665 4_675 106.17(11)
Al2 Pt Al2 4_565 4_675 106.17(11)
Al1 Pt U 15_556 13_666 24.1(2)
Al1 Pt U 13_666 13_666 61.28(15)
Al1 Pt U 14_566 13_666 61.28(15)
Al3 Pt U 4_565 13_666 127.40(11)
Al3 Pt U 4_665 13_666 61.48(8)
Al3 Pt U 4 13_666 61.48(8)
Al2 Pt U 16_556 13_666 132.773(14)
Al2 Pt U 4_665 13_666 65.37(10)
Al2 Pt U 4_565 13_666 126.86(6)
Al2 Pt U 4_675 13_666 126.86(6)
Al1 Pt U 15_556 13_676 61.28(15)
Al1 Pt U 13_666 13_676 24.1(2)
Al1 Pt U 14_566 13_676 61.28(16)
Al3 Pt U 4_565 13_676 61.48(8)
Al3 Pt U 4_665 13_676 61.48(8)
Al3 Pt U 4 13_676 127.40(11)
Al2 Pt U 16_556 13_676 132.774(14)
Al2 Pt U 4_665 13_676 126.86(6)
Al2 Pt U 4_565 13_676 126.85(6)
Al2 Pt U 4_675 13_676 65.37(10)
U Pt U 13_666 13_676 78.94(2)
U Al1 Al1 1_545 3_665 150.0
U Al1 Al1 1_545 2_655 149.9990(10)
Al1 Al1 Al1 3_665 2_655 60.0000(10)
U Al1 Pt 1_545 13_666 113.1(2)
Al1 Al1 Pt 3_665 13_666 70.12(19)
Al1 Al1 Pt 2_655 13_666 70.12(18)
U Al1 Pt 1_545 4_664 113.1(2)
Al1 Al1 Pt 3_665 4_664 70.13(19)
Al1 Al1 Pt 2_655 4_664 70.13(18)
Pt Al1 Pt 13_666 4_664 133.8(4)
U Al1 Al1 1_545 2_545 30.0000(10)
Al1 Al1 Al1 3_665 2_545 120.001(2)
Al1 Al1 Al1 2_655 2_545 179.9990(10)
Pt Al1 Al1 13_666 2_545 109.88(19)
Pt Al1 Al1 4_664 2_545 109.88(19)
U Al1 Al1 1_545 3_655 30.0
Al1 Al1 Al1 3_665 3_655 179.9990(10)
Al1 Al1 Al1 2_655 3_655 120.0
Pt Al1 Al1 13_666 3_655 109.88(19)
Pt Al1 Al1 4_664 3_655 109.88(19)
Al1 Al1 Al1 2_545 3_655 60.0
U Al1 Al3 1_545 . 84.8(2)
Al1 Al1 Al3 3_665 . 72.73(19)
Al1 Al1 Al3 2_655 . 117.07(19)
Pt Al1 Al3 13_666 . 129.52(15)
Pt Al1 Al3 4_664 . 55.62(7)
Al1 Al1 Al3 2_545 . 62.9(2)
Al1 Al1 Al3 3_655 . 107.27(19)
U Al1 Al3 1_545 1_655 84.8(2)
Al1 Al1 Al3 3_665 1_655 117.1(2)
Al1 Al1 Al3 2_655 1_655 72.73(19)
Pt Al1 Al3 13_666 1_655 129.52(15)
Pt Al1 Al3 4_664 1_655 55.62(7)
Al1 Al1 Al3 2_545 1_655 107.27(19)
Al1 Al1 Al3 3_655 1_655 62.9(2)
Al3 Al1 Al3 . 1_655 97.52(15)
U Al1 Al3 1_545 16_656 84.8(2)
Al1 Al1 Al3 3_665 16_656 117.1(2)
Al1 Al1 Al3 2_655 16_656 72.73(19)
Pt Al1 Al3 13_666 16_656 55.62(7)
Pt Al1 Al3 4_664 16_656 129.52(15)
Al1 Al1 Al3 2_545 16_656 107.27(19)
Al1 Al1 Al3 3_655 16_656 62.93(19)
Al3 Al1 Al3 . 16_656 169.5(4)
Al3 Al1 Al3 1_655 16_656 81.52(15)
U Al1 Al3 1_545 16_556 84.8(2)
Al1 Al1 Al3 3_665 16_556 72.73(19)
Al1 Al1 Al3 2_655 16_556 117.1(2)
Pt Al1 Al3 13_666 16_556 55.62(7)
Pt Al1 Al3 4_664 16_556 129.52(15)
Al1 Al1 Al3 2_545 16_556 62.9(2)
Al1 Al1 Al3 3_655 16_556 107.27(19)
Al3 Al1 Al3 . 16_556 81.52(15)
Al3 Al1 Al3 1_655 16_556 169.5(4)
Al3 Al1 Al3 16_656 16_556 97.52(15)
U Al1 U 1_545 1_655 135.94(13)
Al1 Al1 U 3_665 1_655 74.06(13)
Al1 Al1 U 2_655 1_655 14.06(13)
Pt Al1 U 13_666 1_655 73.61(19)
Pt Al1 U 4_664 1_655 73.62(19)
Al1 Al1 U 2_545 1_655 165.94(13)
Al1 Al1 U 3_655 1_655 105.94(13)
Al3 Al1 U . 1_655 126.1(3)
Al3 Al1 U 1_655 1_655 62.79(9)
Al3 Al1 U 16_656 1_655 62.78(9)
Al3 Al1 U 16_556 1_655 126.1(3)
Pt Al2 Pt 16_556 4_664 112.60(10)
Pt Al2 Pt 16_556 4_674 112.60(10)
Pt Al2 Pt 4_664 4_674 106.17(11)
Pt Al2 Pt 16_556 4_564 112.60(10)
Pt Al2 Pt 4_664 4_564 106.17(11)
Pt Al2 Pt 4_674 4_564 106.17(11)
Pt Al2 Al3 16_556 1_565 120.52(12)
Pt Al2 Al3 4_664 1_565 126.9(2)
Pt Al2 Al3 4_674 1_565 53.64(5)
Pt Al2 Al3 4_564 1_565 53.64(5)
Pt Al2 Al3 16_556 1_665 120.52(12)
Pt Al2 Al3 4_664 1_665 53.64(5)
Pt Al2 Al3 4_674 1_665 53.65(5)
Pt Al2 Al3 4_564 1_665 126.9(2)
Al3 Al2 Al3 1_565 1_665 96.50(16)
Pt Al2 Al3 16_556 . 120.52(12)
Pt Al2 Al3 4_664 . 53.64(5)
Pt Al2 Al3 4_674 . 126.9(2)
Pt Al2 Al3 4_564 . 53.65(5)
Al3 Al2 Al3 1_565 . 96.50(16)
Al3 Al2 Al3 1_665 . 96.50(16)
Pt Al2 Al2 16_556 13_665 59.01(17)
Pt Al2 Al2 4_664 13_665 53.59(7)
Pt Al2 Al2 4_674 13_665 126.41(2)
Pt Al2 Al2 4_564 13_665 126.41(2)
Al3 Al2 Al2 1_565 13_665 179.5(3)
Al3 Al2 Al2 1_665 13_665 83.81(8)
Al3 Al2 Al2 . 13_665 83.81(8)
Pt Al2 Al2 16_556 13_565 59.01(17)
Pt Al2 Al2 4_664 13_565 126.41(2)
Pt Al2 Al2 4_674 13_565 126.41(2)
Pt Al2 Al2 4_564 13_565 53.59(7)
Al3 Al2 Al2 1_565 13_565 83.81(8)
Al3 Al2 Al2 1_665 13_565 179.5(3)
Al3 Al2 Al2 . 13_565 83.81(8)
Al2 Al2 Al2 13_665 13_565 95.9(2)
Pt Al2 Al2 16_556 13_675 59.01(17)
Pt Al2 Al2 4_664 13_675 126.41(2)
Pt Al2 Al2 4_674 13_675 53.59(7)
Pt Al2 Al2 4_564 13_675 126.41(2)
Al3 Al2 Al2 1_565 13_675 83.81(8)
Al3 Al2 Al2 1_665 13_675 83.81(8)
Al3 Al2 Al2 . 13_675 179.5(3)
Al2 Al2 Al2 13_665 13_675 95.9(2)
Al2 Al2 Al2 13_565 13_675 95.9(2)
Pt Al2 U 16_556 . 180.0
Pt Al2 U 4_664 . 67.40(10)
Pt Al2 U 4_674 . 67.40(10)
Pt Al2 U 4_564 . 67.40(10)
Al3 Al2 U 1_565 . 59.48(12)
Al3 Al2 U 1_665 . 59.48(12)
Al3 Al2 U . . 59.48(12)
Al2 Al2 U 13_665 . 120.99(17)
Al2 Al2 U 13_565 . 120.99(17)
Al2 Al2 U 13_675 . 120.99(17)
Pt Al3 Pt 4_554 4_664 117.15(6)
Pt Al3 Pt 4_554 4_564 117.15(6)
Pt Al3 Pt 4_664 4_564 117.15(6)
Pt Al3 Al1 4_554 2 135.1(2)
Pt Al3 Al1 4_664 2 101.6(2)
Pt Al3 Al1 4_564 2 54.89(12)
Pt Al3 Al1 4_554 1_455 101.6(2)
Pt Al3 Al1 4_664 1_455 135.1(2)
Pt Al3 Al1 4_564 1_455 54.89(12)
Al1 Al3 Al1 2 1_455 34.5(4)
Pt Al3 Al1 4_554 . 101.6(2)
Pt Al3 Al1 4_664 . 54.89(12)
Pt Al3 Al1 4_564 . 135.1(2)
Al1 Al3 Al1 2 . 81.99(12)
Al1 Al3 Al1 1_455 . 97.52(15)
Pt Al3 Al1 4_554 3_665 135.1(2)
Pt Al3 Al1 4_664 3_665 54.89(12)
Pt Al3 Al1 4_564 3_665 101.6(2)
Al1 Al3 Al1 2 3_665 54.1(4)
Al1 Al3 Al1 1_455 3_665 81.99(12)
Al1 Al3 Al1 . 3_665 34.5(4)
Pt Al3 Al1 4_554 3 54.89(12)
Pt Al3 Al1 4_664 3 135.1(2)
Pt Al3 Al1 4_564 3 101.6(2)
Al1 Al3 Al1 2 3 81.99(12)
Al1 Al3 Al1 1_455 3 54.1(4)
Al1 Al3 Al1 . 3 81.99(12)
Al1 Al3 Al1 3_665 3 97.52(15)
Pt Al3 Al1 4_554 2_545 54.89(12)
Pt Al3 Al1 4_664 2_545 101.6(2)
Pt Al3 Al1 4_564 2_545 135.1(2)
Al1 Al3 Al1 2 2_545 97.52(15)
Al1 Al3 Al1 1_455 2_545 81.99(12)
Al1 Al3 Al1 . 2_545 54.1(4)
Al1 Al3 Al1 3_665 2_545 81.99(12)
Al1 Al3 Al1 3 2_545 34.5(4)
Pt Al3 Al2 4_554 1_445 59.26(5)
Pt Al3 Al2 4_664 1_445 139.7(2)
Pt Al3 Al2 4_564 1_445 59.26(5)
Al1 Al3 Al2 2 1_445 104.6(2)
Al1 Al3 Al2 1_455 1_445 79.04(12)
Al1 Al3 Al2 . 1_445 158.7(2)
Al1 Al3 Al2 3_665 1_445 158.7(2)
Al1 Al3 Al2 3 1_445 79.04(12)
Al1 Al3 Al2 2_545 1_445 104.6(2)
Pt Al3 Al2 4_554 . 139.7(2)
Pt Al3 Al2 4_664 . 59.26(5)
Pt Al3 Al2 4_564 . 59.26(5)
Al1 Al3 Al2 2 . 79.04(13)
Al1 Al3 Al2 1_455 . 104.6(2)
Al1 Al3 Al2 . . 104.6(2)
Al1 Al3 Al2 3_665 . 79.04(12)
Al1 Al3 Al2 3 . 158.7(2)
Al1 Al3 Al2 2_545 . 158.7(2)
Al2 Al3 Al2 1_445 . 96.50(16)
Pt Al3 Al2 4_554 1_545 59.26(5)
Pt Al3 Al2 4_664 1_545 59.26(5)
Pt Al3 Al2 4_564 1_545 139.7(2)
Al1 Al3 Al2 2 1_545 158.7(2)
Al1 Al3 Al2 1_455 1_545 158.7(2)
Al1 Al3 Al2 . 1_545 79.04(12)
Al1 Al3 Al2 3_665 1_545 104.6(2)
Al1 Al3 Al2 3 1_545 104.6(2)
Al1 Al3 Al2 2_545 1_545 79.04(12)
Al2 Al3 Al2 1_445 1_545 96.50(16)
Al2 Al3 Al2 . 1_545 96.50(16)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
U Al1 2 1.500(10) ?
U Al1 1_565 1.500(10) ?
U Al1 3_665 1.500(10) ?
U Al1 3_675 3.087(8) ?
U Al1 3_565 3.087(8) ?
U Al1 2_665 3.087(8) ?
U Al1 1_455 3.087(8) ?
U Al1 . 3.087(7) y
U Al1 2_655 3.087(7) ?
U Al3 . 3.101(3) y
U Al3 1_565 3.101(3) ?
U Al3 1_665 3.101(3) ?
Pt Al1 15_556 2.493(4) y
Pt Al1 13_666 2.493(4) ?
Pt Al1 14_566 2.493(4) ?
Pt Al3 4_565 2.5154(9) y
Pt Al3 4_665 2.5154(10) ?
Pt Al3 4 2.5154(10) ?
Pt Al2 16_556 2.521(5) y
Pt Al2 4_665 2.685(2) y
Pt Al2 4_565 2.685(2) ?
Pt Al2 4_675 2.685(2) ?
Pt U 13_666 3.3765(8) y
Pt U 13_676 3.3765(8) ?
Al1 U 1_545 1.500(10) ?
Al1 Al1 3_665 1.695(18) ?
Al1 Al1 2_655 1.695(18) ?
Al1 Pt 13_666 2.493(4) ?
Al1 Pt 4_664 2.493(4) ?
Al1 Al1 2_545 2.598(18) y
Al1 Al1 3_655 2.598(18) ?
Al1 Al3 . 2.855(3) y
Al1 Al3 1_655 2.855(3) ?
Al1 Al3 16_656 2.855(3) ?
Al1 Al3 16_556 2.855(3) ?
Al1 U 1_655 3.087(7) ?
Al2 Pt 16_556 2.521(5) ?
Al2 Pt 4_664 2.685(2) ?
Al2 Pt 4_674 2.685(2) ?
Al2 Pt 4_564 2.685(2) ?
Al2 Al3 1_565 2.877(4) ?
Al2 Al3 1_665 2.877(4) ?
Al2 Al3 . 2.877(4) ?
Al2 Al2 13_665 2.891(5) y
Al2 Al2 13_565 2.891(5) ?
Al2 Al2 13_675 2.891(5) ?
Al3 Pt 4_554 2.5154(10) ?
Al3 Pt 4_664 2.5154(10) ?
Al3 Pt 4_564 2.5154(9) ?
Al3 Al1 2 2.855(3) ?
Al3 Al1 1_455 2.855(3) ?
Al3 Al1 3_665 2.855(3) ?
Al3 Al1 3 2.855(3) ?
Al3 Al1 2_545 2.855(3) ?
Al3 Al2 1_445 2.877(4) ?
Al3 Al2 1_545 2.877(4) ?
