#------------------------------------------------------------------------------
#$Date: 2019-12-25 21:57:46 +0200 (Wed, 25 Dec 2019) $
#$Revision: 245815 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/31/13/2311348.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2311348
loop_
_publ_author_name
'Rammohan, Alagappa'
'Kaduk, James A.'
_publ_section_title
;
 Crystal structure of dirubidium hydrogen citrate from laboratory X-ray
 powder diffraction data and DFT comparison.
;
_journal_coeditor_code           VN2120
_journal_issue                   'Pt 1'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first              92
_journal_page_last               95
_journal_paper_doi               10.1107/S2056989016020168
_journal_volume                  73
_journal_year                    2017
_chemical_formula_iupac          '2Rb +, H C6 H5 O7 2-'
_chemical_formula_moiety         '2(Rb +), H C6 H5 O7 2-'
_chemical_formula_structural     'Rb2 H C6 H5 O7'
_chemical_formula_sum            'C6 H6 O7 Rb2'
_chemical_formula_weight         361.04
_chemical_name_common            'dirubidium hydrogen citrate'
_chemical_name_systematic        'Dirubidium hydrogen citrate'
_space_group_IT_number           11
_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_audit_creation_method           'from EXP file using GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 93.9341(13)
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   5.97796(17)
_cell_length_b                   15.0960(4)
_cell_length_c                   5.32067(19)
_cell_measurement_temperature    300
_cell_volume                     479.02(3)
_computing_data_collection
;
DIFFRAC.Measurement (Bruker, 2009)
;
_computing_molecular_graphics
;
DIAMOND (Crystal Impact, 2015)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement  GSAS
_computing_structure_solution
;
Endeavour (Putz et al., 1999)
;
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type  'Bruker D2 Phaser'
_exptl_absorpt_correction_T_max  0.80324
_exptl_absorpt_correction_T_min  0.51355
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 3
 Surface roughness abs. correction (Suortti)
Terms =     0.34000        0.70000
Correction is not refined.
;
_exptl_crystal_density_diffrn    2.503
_pd_block_id                     2016-12-11T10:41|RAMM020C|James_A._Kaduk|D2
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  white
_pd_meas_2theta_range_inc        0.02021
_pd_meas_2theta_range_max        70.00603
_pd_meas_2theta_range_min        4.9978
_pd_meas_number_of_points        3217
_pd_meas_scan_method             step
_pd_phase_name                   'Rb2 H C6 H5 O7?'
_pd_prep_temperature             333
_pd_proc_2theta_range_inc        0.02021
_pd_proc_2theta_range_max        70.05003
_pd_proc_2theta_range_min        5.0418
_pd_proc_info_datetime           2016-12-11T10:41:50
_pd_proc_ls_background_function
;   GSAS Background function number 1 with  4 terms.
 Shifted Chebyshev function of 1st kind
      1:    3185.87     2:   -310.317     3:   -87.5319     4:    63.9418
;
_pd_proc_ls_peak_cutoff          0.01000
_pd_proc_ls_profile_function
;
CW Profile function number 4 with  21 terms
Pseudovoigt profile coefficients as parameterized in
P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl.
Cryst.,20,79-83.
Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
J. Appl. Cryst.,27,892-900.
Microstrain broadening by P.W. Stephens,  (1999). J. Appl.
Cryst.,32,281-289.
#1(GU)   =  142.783 #2(GV)   =    0.000 #3(GW)   =    4.751
#4(GP)   =    0.000 #5(LX)   =    5.874 #6(ptec) =    -0.71
#7(trns) =     1.83 #8(shft) = -25.7226 #9(sfec) =     0.00
#10(S/L) =   0.0441 #11(H/L) =   0.0005 #12(eta) =   0.0000
#13(S400 ) =  3.9E-02 #14(S040 ) =  8.9E-05 #15(S004 ) =  3.1E-01
#16(S220 ) =  9.7E-03 #17(S202 ) = -6.4E-02 #18(S022 ) =  5.7E-04
#19(S301 ) = -8.2E-03 #20(S103 ) =  2.5E-02 #21(S121 ) = -8.8E-03
Peak tails are ignored  where the intensity is below 0.0100 times the peak
  Aniso. broadening axis   0.0   1.0   0.0
;
_pd_proc_ls_prof_R_factor        0.0212
_pd_proc_ls_prof_wR_expected     0.0154
_pd_proc_ls_prof_wR_factor       0.0277
_pd_proc_number_of_points        3217
_pd_spec_mounting                'Normal sample holder'
_pd_spec_mount_mode              reflection
_pd_spec_shape                   flat_sheet
_pd_spec_size_axial              24
_pd_spec_size_equat              24
_refine_diff_density_max         0.46
_refine_diff_density_min         -0.41
_refine_ls_goodness_of_fit_all   1.82
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     49
_refine_ls_number_restraints     15
_refine_ls_shift/su_max          0.08
_refine_ls_shift/su_mean         0.01
_refine_ls_weighting_scheme      sigma
_reflns_number_total             428
_cod_data_source_file            vn2120sup1.cif
_cod_data_source_block           RAMM020C_publ
_cod_original_cell_volume        479.02(4)
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               2311348
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y+1/2,-z
-1 -x,-y,-z
-2 +x,-y+1/2,+z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
C C1 0.2727(12) 0.4151(4) 0.5145(14) 0.0556(15) Uiso 1.0 4
C C2 0.3859(11) 0.33308(16) 0.4236(14) 0.026(4) Uiso 1.0 4
C C3 0.2821(12) 0.25 0.5368(15) 0.026(4) Uiso 1.0 2
C C6 0.0268(13) 0.25 0.463(2) 0.0556(15) Uiso 1.0 2
H H7 0.56395 0.33136 0.47541 0.018(5) Uiso 1.0 4
H H8 0.35795 0.33169 0.21841 0.018(5) Uiso 1.0 4
O O11 0.1036(11) 0.4467(5) 0.3841(15) 0.0556(15) Uiso 1.0 4
O O12 0.3502(12) 0.4512(5) 0.7178(14) 0.0556(15) Uiso 1.0 4
O O15 -0.0968(16) 0.25 0.650(2) 0.0556(15) Uiso 1.0 2
O O16 -0.0415(16) 0.25 0.232(2) 0.0556(15) Uiso 1.0 2
O O17 0.3416(14) 0.25 0.7999(15) 0.0556(15) Uiso 1.0 2
H H18 0.17127 0.25 0.87091 0.068(2) Uiso 1.0 2
Rb Rb19 -0.2264(3) 0.10523(10) -0.0313(3) 0.0590(9) Uiso 1.0 4
H H21 0.0 0.0 0.5 0.07 Uiso 1.0 2
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 12.0 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500 51.6512 0.21560
0.000 0.000 International_Tables_Vol_C
H 12.0 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081 57.7997 0.00304
0.000 0.000 International_Tables_Vol_C
O 14.0 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080
0.000 0.000 International_Tables_Vol_C
Rb 4.0 17.1784 1.78880 9.64350 17.3151 5.13990 0.27480 1.52920 164.934 3.48730
0.000 0.000 International_Tables_Vol_C
loop_
_diffrn_radiation_type
_diffrn_radiation_wavelength
K\a~1~ 1.540629
K\a~2~ 1.544451
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C2 C1 O11 1_555 1_555 119.2(4) n
C2 C1 O12 1_555 1_555 118.7(4) n
O11 C1 O12 1_555 1_555 122.1(4) n
C1 C2 C3 1_555 1_555 110.0(4) n
C1 C2 H7 1_555 1_555 113.2(4) n
C1 C2 H8 1_555 1_555 17.29(4) n
C3 C2 H7 1_555 1_555 107.3(5) n
C3 C2 H8 1_555 1_555 109.7(5) n
H7 C2 H8 1_555 1_555 109.5(5) n
C2 C3 C2 1_555 -2_565 109.1(4) n
C2 C3 C6 1_555 1_555 108.5(4) n
C2 C3 O17 1_555 1_555 107.8(4) n
C2 C3 C6 -2_565 1_555 108.5(4) n
C2 C3 O17 -2_565 1_555 107.8(4) n
C6 C3 O17 1_555 1_555 115.2(7) n
C3 C6 O15 1_555 1_555 114.4(9) n
C3 C6 O16 1_555 1_555 119.5(9) n
O15 C6 O16 1_555 1_555 126.1(9) n
C1 O11 Rb19 1_555 2_555 113.5(7) n
C1 O11 Rb19 1_555 -2_565 140.0(4) n
Rb19 O11 Rb19 2_555 -2_565 85.8(2) n
C1 O12 Rb19 1_555 2_556 136.0(4) n
C1 O12 Rb19 1_555 -2_666 121.4(4) n
Rb19 O12 Rb19 2_556 -2_666 102.3(2) n
C6 O15 Rb19 1_555 1_556 130.21(19) n
C6 O15 Rb19 1_555 -2_566 130.21(19) n
Rb19 O15 Rb19 1_556 -2_566 97.7(3) n
C6 O16 Rb19 1_555 1_555 125.3(2) n
C6 O16 Rb19 1_555 -2_565 125.3(2) n
Rb19 O16 Rb19 1_555 -2_565 103.5(4) n
C3 O17 H18 1_555 1_555 99.3(7) n
O11 Rb19 O11 2_545 -2_565 94.2(2) n
O11 Rb19 O12 2_545 2_546 79.54(16) n
O11 Rb19 O12 2_545 -2_464 74.7(2) n
O11 Rb19 O15 2_545 1_554 98.11(18) n
O11 Rb19 O16 2_545 1_555 142.5(2) n
O11 Rb19 O12 -2_565 2_546 63.59(19) n
O11 Rb19 O12 -2_565 -2_464 141.13(14) n
O11 Rb19 O15 -2_565 1_554 116.3(2) n
O11 Rb19 O16 -2_565 1_555 67.2(2) n
O12 Rb19 O12 2_546 -2_464 77.7(2) n
O12 Rb19 O15 2_546 1_554 177.6(2) n
O12 Rb19 O16 2_546 1_555 115.8(3) n
O12 Rb19 O15 -2_464 1_554 102.2(2) n
O12 Rb19 O16 -2_464 1_555 139.9(2) n
O15 Rb19 O16 1_554 1_555 65.8(2) n
O11 H21 O11 2_546 -2_565 180.0 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
C1 C2 1_555 1.5070(17) n
C1 O11 1_555 1.278(5) n
C1 O12 1_555 1.270(5) n
C2 C1 1_555 1.5070(17) n
C2 C3 1_555 1.5400(17) n
C2 H7 1_555 1.081(7) n
C2 H8 1_555 1.093(7) n
C3 C2 1_555 1.5400(17) n
C3 C2 -2_555 1.5400(17) n
C3 C6 1_555 1.5499(18) n
C3 O17 1_555 1.420(5) n
C6 C3 1_555 1.5499(18) n
C6 O15 1_555 1.281(5) n
C6 O16 1_555 1.267(5) n
H7 C2 1_555 1.081(7) n
H8 C2 1_555 1.093(8) n
O11 C1 1_555 1.278(5) n
O11 Rb19 2_555 3.159(7) n
O11 Rb19 -2_555 2.965(7) n
O11 H21 2_556 1.209(6) n
O12 C1 1_555 1.270(5) n
O12 Rb19 2_556 2.984(6) n
O12 Rb19 -2_656 2.907(7) n
O15 C6 1_555 1.281(5) n
O15 Rb19 1_556 2.903(7) n
O15 Rb19 -2_556 2.903(7) n
O16 C6 1_555 1.267(5) n
O16 Rb19 1_555 2.784(7) n
O16 Rb19 -2_555 2.784(7) n
O17 C3 1_555 1.420(5) n
O17 H18 1_555 1.110(8) n
O17 Rb19 1_656 3.454(7) n
O17 Rb19 -2_656 3.455(7) n
H18 O17 1_555 1.110(8) n
Rb19 O11 2_545 3.159(7) n
Rb19 O11 -2_555 2.965(7) n
Rb19 O12 2_546 2.984(6) n
Rb19 O12 -2_454 2.907(7) n
Rb19 O15 1_554 2.903(7) n
Rb19 O16 1_555 2.784(7) n
Rb19 O17 1_454 3.454(7) n
H21 O11 2_546 1.209(6) n
H21 O11 -2_555 1.209(6) n
loop_
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
_pd_meas_counts_total
. . . 7127.0
. . . 6761.0
. . . 6710.0
. . . 6351.0
. . . 6376.0
. . . 6466.0
. . . 6046.0
. . . 6000.0
. . . 6043.0
. . . 5881.0
. . . 5869.0
. . . 5668.0
. . . 5542.0
. . . 5532.0
. . . 5537.0
. . . 5389.0
. . . 5281.0
. . . 5359.0
. . . 5221.0
. . . 5148.0
. . . 4966.0
. . . 4898.0
. . . 4891.0
. . . 4812.0
. . . 4839.0
. . . 4824.0
. . . 4860.0
. . . 4658.0
. . . 4532.0
. . . 4400.0
. . . 4348.0
. . . 4511.0
. . . 4296.0
. . . 4393.0
. . . 4203.0
. . . 4195.0
. . . 4255.0
. . . 4131.0
. . . 4062.0
. . . 4090.0
. . . 4091.0
. . . 4008.0
. . . 4043.0
. . . 3986.0
. . . 3910.0
. . . 3853.0
. . . 3734.0
. . . 3796.0
. . . 3793.0
. . . 3795.0
. . . 3678.0
. . . 3655.0
. . . 3611.0
. . . 3582.0
. . . 3623.0
. . . 3718.0
. . . 3618.0
. . . 3536.0
. . . 3641.0
. . . 3489.0
. . . 3524.0
. . . 3590.0
. . . 3395.0
. . . 3463.0
. . . 3437.0
. . . 3460.0
. . . 3524.0
. . . 3397.0
. . . 3375.0
. . . 3413.0
. . . 3350.0
. . . 3265.0
. . . 3320.0
. . . 3317.0
. . . 3279.0
. . . 3266.0
. . . 3226.0
. . . 3346.0
. . . 3156.0
. . . 3275.0
. . . 3061.0
. . . 3143.0
. . . 3090.0
. . . 3088.0
. . . 3199.0
. . . 3115.0
. . . 3168.0
. . . 3123.0
. . . 3078.0
. . . 2980.0
. . . 3127.0
. . . 3162.0
. . . 3113.0
. . . 2944.0
. . . 3056.0
. . . 3049.0
. . . 3044.0
. . . 2963.0
. . . 3052.0
. . . 2953.0
. . . 3126.0
. . . 3020.0
. . . 3086.0
. . . 3057.0
. . . 2987.0
. . . 3022.0
. . . 2948.0
. . . 3049.0
. . . 2904.0
. . . 2881.0
. . . 2879.0
. . . 2921.0
. . . 2914.0
. . . 2944.0
. . . 2953.0
. . . 2866.0
. . . 2934.0
. . . 2974.0
. . . 2974.0
. . . 2979.0
. . . 2974.0
. . . 2871.0
. . . 2869.0
. . . 2795.0
. . . 2899.0
. . . 2876.0
. . . 2909.0
. . . 2881.0
. . . 2881.0
. . . 2882.0
. . . 2846.0
. . . 2896.0
. . . 2895.0
. . . 2823.0
. . . 2834.0
. . . 2860.0
. . . 2908.0
. . . 2774.0
. . . 2920.0
. . . 2827.0
. . . 2944.0
. . . 2824.0
. . . 2852.0
. . . 2814.0
. . . 2919.0
. . . 2710.0
. . . 2805.0
. . . 2935.0
. . . 2828.0
. . . 2872.0
. . . 2891.0
. . . 2893.0
. . . 2854.0
. . . 2861.0
. . . 2806.0
. . . 2780.0
. . . 2873.0
. . . 2852.0
. . . 2827.0
. . . 2974.0
. . . 2852.0
. . . 2840.0
. . . 2841.0
. . . 2832.0
. . . 2876.0
. . . 2891.0
. . . 2932.0
. . . 2946.0
. . . 2848.0
. . . 2794.0
. . . 2921.0
. . . 2844.0
. . . 2665.0
. . . 2830.0
. . . 2849.0
. . . 2818.0
. . . 2836.0
. . . 2928.0
. . . 2831.0
. . . 2841.0
. . . 2811.0
. . . 2803.0
. . . 2845.0
. . . 2830.0
. . . 2869.0
. . . 2924.0
. . . 2918.0
. . . 2784.0
. . . 2780.0
. . . 2813.0
. . . 2807.0
. . . 2892.0
. . . 2934.0
. . . 2828.0
. . . 2865.0
. . . 2860.0
. . . 2795.0
. . . 2955.0
. . . 2880.0
. . . 2870.0
. . . 2782.0
. . . 2825.0
. . . 2820.0
. . . 2791.0
. . . 2797.0
. . . 2910.0
. . . 2871.0
. . . 2769.0
. . . 2843.0
. . . 2883.0
. . . 2895.0
. . . 2890.0
. . . 2879.0
. . . 2798.0
. . . 2886.0
. . . 2926.0
. . . 2890.0
. . . 2923.0
. . . 3032.0
. . . 2839.0
. . . 2887.0
. . . 2841.0
. . . 2780.0
. . . 2872.0
. . . 2903.0
. . . 2872.0
. . . 2829.0
. . . 2784.0
. . . 2775.0
. . . 3017.0
. . . 2826.0
. . . 2976.0
. . . 2874.0
. . . 2908.0
. . . 2862.0
. . . 2860.0
. . . 2841.0
. . . 2812.0
. . . 2946.0
. . . 2990.0
. . . 2954.0
. . . 2885.0
. . . 2792.0
. . . 2871.0
. . . 2937.0
. . . 2902.0
. . . 2804.0
. . . 2922.0
. . . 2906.0
. . . 2916.0
. . . 2819.0
. . . 2904.0
. . . 2885.0
. . . 2841.0
. . . 2831.0
. . . 3005.0
. . . 2907.0
. . . 2952.0
. . . 2871.0
. . . 2877.0
. . . 2857.0
. . . 2902.0
. . . 2973.0
. . . 2908.0
. . . 2917.0
. . . 3018.0
. . . 2964.0
. . . 2867.0
. . . 2941.0
. . . 2833.0
. . . 2901.0
. . . 2886.0
. . . 2969.0
. . . 2917.0
. . . 2874.0
. . . 2962.0
. . . 2934.0
. . . 2934.0
. . . 2909.0
. . . 3006.0
. . . 2860.0
. . . 2897.0
. . . 2918.0
. . . 2852.0
. . . 2998.0
. . . 3012.0
. . . 2925.0
. . . 2967.0
. . . 2971.0
. . . 2934.0
. . . 2910.0
. . . 2884.0
. . . 2885.0
. . . 2887.0
. . . 2964.0
. . . 2956.0
. . . 2913.0
. . . 2865.0
. . . 2911.0
. . . 2956.0
. . . 2882.0
. . . 2953.0
. . . 2898.0
. . . 2881.0
. . . 3004.0
. . . 2884.0
. . . 3078.0
. . . 2946.0
. . . 2985.0
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0.0003416 2860.85400 3017.30957 2927.0
0.0003306 2860.73511 3030.36621 3025.0
0.0003309 2860.61670 3047.52979 3022.0
0.0003292 2860.49902 3067.64551 3038.0
0.0003243 2860.38184 3085.59741 3084.0
0.0003191 2860.26514 3107.91162 3134.0
0.0003189 2860.14917 3128.16504 3136.0
0.0003132 2860.03369 3145.19580 3193.0
0.0002958 2859.91870 3158.74048 3381.0
0.0002970 2859.80444 3166.26074 3367.0
0.0003042 2859.69067 3169.45972 3287.0
0.0002955 2859.57739 3168.63477 3384.0
0.0003116 2859.46484 3165.65161 3209.0
0.0003036 2859.35254 3156.02856 3294.0
0.0003119 2859.24121 3146.35376 3206.0
0.0003155 2859.13013 3135.41113 3170.0
0.0003136 2859.01978 3123.83398 3189.0
0.0003171 2858.90991 3110.52905 3154.0
0.0003128 2858.80078 3099.36670 3197.0
0.0003121 2858.69214 3089.20703 3204.0
0.0003200 2858.58398 3081.11426 3125.0
0.0003132 2858.47656 3075.73486 3193.0
0.0003200 2858.36963 3074.50024 3125.0
0.0003144 2858.26318 3076.42358 3181.0
0.0003280 2858.15723 3082.96533 3049.0
0.0003233 2858.05200 3094.32715 3093.0
0.0003189 2857.94751 3109.46753 3136.0
0.0003269 2857.84351 3129.15869 3059.0
0.0003247 2857.73999 3151.42505 3080.0
0.0003203 2857.63696 3174.55859 3122.0
0.0003195 2857.53467 3196.76440 3130.0
0.0002966 2857.43286 3216.43555 3371.0
0.0002965 2857.33154 3232.44653 3373.0
0.0003014 2857.23120 3244.29395 3318.0
0.0002972 2857.13110 3252.14160 3365.0
0.0003029 2857.03149 3256.78076 3301.0
0.0003137 2856.93262 3259.52832 3188.0
0.0003039 2856.83447 3261.80420 3291.0
0.0003115 2856.73682 3264.91626 3210.0
0.0003054 2856.63965 3269.67603 3274.0
0.0003121 2856.54321 3276.30615 3204.0
0.0003030 2856.44727 3284.49219 3300.0
0.0003035 2856.35181 3292.21338 3295.0
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0.0003077 2856.06934 3311.10889 3250.0
0.0003004 2855.97632 3308.78174 3329.0
0.0003041 2855.88379 3301.59106 3288.0
0.0003019 2855.79199 3288.29663 3312.0
0.0003025 2855.70068 3269.60107 3306.0
0.0003070 2855.61011 3247.01636 3257.0
0.0003199 2855.52002 3221.68726 3126.0
0.0003180 2855.43042 3196.56543 3145.0
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0.0003341 2855.25342 3151.21826 2993.0
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0.0003213 2854.99194 3086.98633 3112.0
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0.0003323 2854.73608 3025.29590 3009.0
0.0003385 2854.65186 3004.86157 2954.0
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0.0003408 2854.40308 2952.88525 2934.0
0.000353 2854.32129 2937.74878 2833.0
0.0003429 2854.23999 2925.67236 2916.0
0.000357 2854.15967 2915.74072 2798.0
0.000359 2854.07959 2907.99365 2789.0
0.0003455 2854.00024 2901.34595 2894.0
0.0003418 2853.92163 2897.80542 2926.0
0.0003454 2853.84351 2896.12207 2895.0
0.000357 2853.76587 2896.26563 2798.0
0.000355 2853.68896 2898.29517 2815.0
0.000357 2853.61255 2902.79980 2803.0
0.000355 2853.53687 2908.80249 2818.0
0.0003455 2853.46167 2917.84302 2894.0
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0.000351 2853.02368 3041.68530 2850.0
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0.0003344 2852.88257 3106.97021 2990.0
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0.0002958 2852.02466 3385.42505 3381.0
0.0002940 2851.96313 3373.72998 3401.0
. . . 3363.0
