#------------------------------------------------------------------------------
#$Date: 2016-03-21 01:21:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178377 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/18/4001855.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4001855
loop_
_publ_author_name
'Zeilinger, Michael'
'Kurylyshyn, Iryna M.'
'Häussermann, Ulrich'
'Fässler, Thomas F.'
_publ_section_title
;
 Revision of the Li--Si Phase Diagram: Discovery and Single-Crystal X-ray
 Structure Determination of the High-Temperature Phase Li4.11Si
;
_journal_issue                   22
_journal_name_full               'Chemistry of Materials'
_journal_page_first              4623
_journal_paper_doi               10.1021/cm4029885
_journal_volume                  25
_journal_year                    2013
_chemical_formula_analytical     'Li4.105 Si'
_chemical_formula_moiety         'Li4.105 Si'
_chemical_formula_sum            'Li4.105 Si'
_chemical_formula_weight         56.59
_chemical_melting_point          '891 K, peritectic decomposition'
_chemical_name_common            'Lithium Silicide'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   4.5467(9)
_cell_length_b                   22.065(4)
_cell_length_c                   13.240(3)
_cell_measurement_reflns_used    2147
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      32.3
_cell_measurement_theta_min      3.6
_cell_volume                     1328.3(5)
_citation_year                   2013
_computing_cell_refinement
;X-Area (1.26) - Software for STOE IPDS 2, Stoe & Cie.,
 Darmstadt (Germany), 2004.
;
_computing_data_collection
;X-Area (1.26) - Software for STOE IPDS 2, Stoe & Cie.,
 Darmstadt (Germany), 2004.
;
_computing_data_reduction
;X-Red (1.26) - Data Reduction Program, Stoe & Cie.,
 Darmstadt (Germany), 2004.
;
_computing_molecular_graphics    'Diamond 3 (Crystal Impact 2011)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      298(2)
_diffrn_detector                 IPDS
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 0.955
_diffrn_measured_fraction_theta_max 0.955
_diffrn_measurement_device_type  'STOE IPDS 2T'
_diffrn_measurement_method       'phi- and omega-rotation'
_diffrn_radiation_monochromator  'MONTEL optic'
_diffrn_radiation_source         'rotating anode FR591'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0466
_diffrn_reflns_av_sigmaI/netI    0.0153
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            15579
_diffrn_reflns_theta_full        30.49
_diffrn_reflns_theta_max         30.49
_diffrn_reflns_theta_min         8.47
_exptl_absorpt_coefficient_mu    0.385
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   none
_exptl_crystal_colour            'metallic silver'
_exptl_crystal_density_diffrn    1.132
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             421
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.148
_refine_diff_density_min         -0.139
_refine_diff_density_rms         0.024
_refine_ls_extinction_coef       -
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.206
_refine_ls_matrix_type           full
_refine_ls_number_parameters     81
_refine_ls_number_reflns         1120
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.206
_refine_ls_R_factor_all          0.0213
_refine_ls_R_factor_gt           0.0188
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0071P)²+0.1167P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0311
_refine_ls_wR_factor_ref         0.0319
_reflns_number_gt                1049
_reflns_number_total             1120
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cm4029885_si_003.cif
_cod_data_source_block           Li4.11Si_298K
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               4001855
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Si1 Si 0.0000 0.256343(10) 0.2500 0.01302(6) Uani 1 4 d S .
Si2 Si 0.5000 0.454228(10) 0.2500 0.01238(6) Uani 1 4 d S .
Si3 Si 0.5000 0.105557(7) 0.067398(11) 0.01262(5) Uani 1 2 d S .
Li1 Li 0.5000 0.03229(8) 0.2500 0.0251(3) Uani 1 4 d S .
Li2 Li 0.5000 0.32954(7) 0.2500 0.0217(3) Uani 1 4 d S .
Li3 Li 0.0000 0.39256(9) 0.2500 0.0321(4) Uani 1 4 d S .
Li4A Li 0.5000 0.14727(19) 0.2500 0.064(3) Uani 0.582(10) 4 d SP 1
Li5A Li 0.0000 0.17362(16) 0.0858(6) 0.0255(9) Uani 0.91(3) 2 d SP 1
Li4B Li 0.2134(13) 0.13897(15) 0.2500 0.0429(19) Uani 0.418(10) 2 d SP 2
Li5B Li 0.0000 0.1622(16) 0.128(5) 0.022(9) Uani 0.09(3) 2 d SP 2
Li6 Li 0.0000 0.04662(5) 0.12234(9) 0.0225(2) Uani 1 2 d S .
Li7 Li 0.0000 0.31628(6) 0.07904(9) 0.0276(2) Uani 1 2 d S .
Li8 Li 0.0000 0.47120(7) 0.09090(11) 0.0355(3) Uani 1 2 d S .
Li9 Li 0.5000 0.23095(6) 0.13622(10) 0.0278(2) Uani 1 2 d S .
Li10 Li 0.5000 0.40482(6) 0.06375(8) 0.0254(2) Uani 1 2 d S .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Li7 Si1 Li7 119.41(7) 10_556 .
Li7 Si1 Li5B 82.5(16) 10_556 10_556
Li7 Si1 Li5B 158.1(16) . 10_556
Li7 Si1 Li5B 158.1(16) 10_556 .
Li7 Si1 Li5B 82.5(16) . .
Li5B Si1 Li5B 76(3) 10_556 .
Li7 Si1 Li4B 118.19(4) 10_556 3
Li7 Si1 Li4B 118.19(4) . 3
Li7 Si1 Li4B 118.19(4) 10_556 .
Li7 Si1 Li4B 118.19(4) . .
Li7 Si1 Li9 124.66(2) 10_556 1_455
Li7 Si1 Li9 68.55(3) . 1_455
Li5B Si1 Li9 99.9(9) 10_556 1_455
Li5B Si1 Li9 60.6(6) . 1_455
Li4B Si1 Li9 61.65(10) 3 1_455
Li4B Si1 Li9 95.62(11) . 1_455
Li7 Si1 Li9 68.55(3) 10_556 10_556
Li7 Si1 Li9 124.66(2) . 10_556
Li5B Si1 Li9 60.6(6) 10_556 10_556
Li5B Si1 Li9 99.9(9) . 10_556
Li4B Si1 Li9 95.62(11) 3 10_556
Li4B Si1 Li9 61.65(10) . 10_556
Li9 Si1 Li9 156.78(6) 1_455 10_556
Li7 Si1 Li9 68.55(3) 10_556 10_456
Li7 Si1 Li9 124.66(2) . 10_456
Li5B Si1 Li9 60.6(6) 10_556 10_456
Li5B Si1 Li9 99.9(9) . 10_456
Li4B Si1 Li9 61.65(10) 3 10_456
Li4B Si1 Li9 95.62(11) . 10_456
Li9 Si1 Li9 65.52(5) 1_455 10_456
Li9 Si1 Li9 109.48(4) 10_556 10_456
Li7 Si1 Li9 124.66(2) 10_556 .
Li7 Si1 Li9 68.55(3) . .
Li5B Si1 Li9 99.9(9) 10_556 .
Li5B Si1 Li9 60.6(6) . .
Li4B Si1 Li9 95.62(11) 3 .
Li4B Si1 Li9 61.64(10) . .
Li9 Si1 Li9 109.48(4) 1_455 .
Li9 Si1 Li9 65.52(5) 10_556 .
Li9 Si1 Li9 156.78(6) 10_456 .
Li7 Si1 Li2 73.01(2) 10_556 .
Li7 Si1 Li2 73.01(2) . .
Li5B Si1 Li2 117.2(7) 10_556 .
Li5B Si1 Li2 117.2(6) . .
Li4B Si1 Li2 145.93(13) 3 .
Li4B Si1 Li2 104.85(13) . .
Li9 Si1 Li2 141.46(3) 1_455 .
Li9 Si1 Li2 56.70(3) 10_556 .
Li9 Si1 Li2 141.46(3) 10_456 .
Li9 Si1 Li2 56.70(3) . .
Li7 Si1 Li2 73.01(2) 10_556 1_455
Li7 Si1 Li2 73.01(2) . 1_455
Li5B Si1 Li2 117.2(6) 10_556 1_455
Li5B Si1 Li2 117.2(6) . 1_455
Li4B Si1 Li2 104.86(13) 3 1_455
Li4B Si1 Li2 145.93(13) . 1_455
Li9 Si1 Li2 56.70(3) 1_455 1_455
Li9 Si1 Li2 141.46(3) 10_556 1_455
Li9 Si1 Li2 56.70(3) 10_456 1_455
Li9 Si1 Li2 141.46(3) . 1_455
Li2 Si1 Li2 109.21(6) . 1_455
Li6 Si2 Li6 79.32(6) 14_556 5
Li6 Si2 Li3 113.29(3) 14_556 1_655
Li6 Si2 Li3 113.29(3) 5 1_655
Li6 Si2 Li3 113.29(3) 14_556 .
Li6 Si2 Li3 113.29(3) 5 .
Li3 Si2 Li3 118.19(7) 1_655 .
Li6 Si2 Li10 74.19(4) 14_556 10_556
Li6 Si2 Li10 153.51(4) 5 10_556
Li3 Si2 Li10 78.02(2) 1_655 10_556
Li3 Si2 Li10 78.02(2) . 10_556
Li6 Si2 Li10 153.51(4) 14_556 .
Li6 Si2 Li10 74.19(4) 5 .
Li3 Si2 Li10 78.02(2) 1_655 .
Li3 Si2 Li10 78.01(2) . .
Li10 Si2 Li10 132.30(6) 10_556 .
Li6 Si2 Li2 140.34(3) 14_556 .
Li6 Si2 Li2 140.34(3) 5 .
Li3 Si2 Li2 59.10(4) 1_655 .
Li3 Si2 Li2 59.10(4) . .
Li10 Si2 Li2 66.15(3) 10_556 .
Li10 Si2 Li2 66.15(3) . .
Li6 Si2 Li1 62.30(3) 14_556 5
Li6 Si2 Li1 62.30(3) 5 5
Li3 Si2 Li1 68.05(5) 1_655 5
Li3 Si2 Li1 173.75(5) . 5
Li10 Si2 Li1 104.13(2) 10_556 5
Li10 Si2 Li1 104.13(2) . 5
Li2 Si2 Li1 127.15(3) . 5
Li6 Si2 Li1 62.30(3) 14_556 5_455
Li6 Si2 Li1 62.30(3) 5 5_455
Li3 Si2 Li1 173.75(5) 1_655 5_455
Li3 Si2 Li1 68.05(5) . 5_455
Li10 Si2 Li1 104.13(2) 10_556 5_455
Li10 Si2 Li1 104.13(2) . 5_455
Li2 Si2 Li1 127.15(3) . 5_455
Li1 Si2 Li1 105.70(6) 5 5_455
Li6 Si2 Li8 109.78(3) 14_556 1_655
Li6 Si2 Li8 58.47(3) 5 1_655
Li3 Si2 Li8 55.72(4) 1_655 1_655
Li3 Si2 Li8 133.35(3) . 1_655
Li10 Si2 Li8 131.73(3) 10_556 1_655
Li10 Si2 Li8 55.34(3) . 1_655
Li2 Si2 Li8 96.89(3) . 1_655
Li1 Si2 Li8 49.24(3) 5 1_655
Li1 Si2 Li8 120.53(3) 5_455 1_655
Li6 Si2 Li8 58.47(3) 14_556 10_656
Li6 Si2 Li8 109.78(3) 5 10_656
Li3 Si2 Li8 55.72(4) 1_655 10_656
Li3 Si2 Li8 133.35(3) . 10_656
Li10 Si2 Li8 55.34(3) 10_556 10_656
Li10 Si2 Li8 131.73(3) . 10_656
Li2 Si2 Li8 96.89(3) . 10_656
Li1 Si2 Li8 49.24(3) 5 10_656
Li1 Si2 Li8 120.53(3) 5_455 10_656
Li8 Si2 Li8 84.88(4) 1_655 10_656
Li6 Si2 Li8 58.47(3) 14_556 10_556
Li6 Si2 Li8 109.78(3) 5 10_556
Li3 Si2 Li8 133.35(3) 1_655 10_556
Li3 Si2 Li8 55.72(4) . 10_556
Li10 Si2 Li8 55.34(3) 10_556 10_556
Li10 Si2 Li8 131.73(3) . 10_556
Li2 Si2 Li8 96.89(3) . 10_556
Li1 Si2 Li8 120.53(3) 5 10_556
Li1 Si2 Li8 49.24(3) 5_455 10_556
Li8 Si2 Li8 166.22(6) 1_655 10_556
Li8 Si2 Li8 93.47(4) 10_656 10_556
Li4A Si3 Li7 117.50(9) . 13
Li4A Si3 Li8 161.90(9) . 13
Li7 Si3 Li8 80.59(5) 13 13
Li4A Si3 Li5B 63.8(12) . .
Li7 Si3 Li5B 85.2(16) 13 .
Li8 Si3 Li5B 121.3(8) 13 .
Li4A Si3 Li5B 63.8(12) . 1_655
Li7 Si3 Li5B 85.2(16) 13 1_655
Li8 Si3 Li5B 121.3(8) 13 1_655
Li5B Si3 Li5B 113.6(6) . 1_655
Li4A Si3 Li6 85.42(5) . 1_655
Li7 Si3 Li6 121.19(2) 13 1_655
Li8 Si3 Li6 84.69(3) 13 1_655
Li5B Si3 Li6 147.2(15) . 1_655
Li5B Si3 Li6 56.0(8) 1_655 1_655
Li4A Si3 Li6 85.42(5) . .
Li7 Si3 Li6 121.19(2) 13 .
Li8 Si3 Li6 84.69(3) 13 .
Li5B Si3 Li6 56.0(8) . .
Li5B Si3 Li6 147.2(15) 1_655 .
Li6 Si3 Li6 113.51(4) 1_655 .
Li4A Si3 Li5A 73.83(15) . 1_655
Li7 Si3 Li5A 72.64(17) 13 1_655
Li8 Si3 Li5A 114.47(11) 13 1_655
Li5B Si3 Li5A 114.6(3) . 1_655
Li6 Si3 Li5A 62.85(10) 1_655 1_655
Li6 Si3 Li5A 159.05(16) . 1_655
Li4A Si3 Li5A 73.83(15) . .
Li7 Si3 Li5A 72.64(17) 13 .
Li8 Si3 Li5A 114.47(11) 13 .
Li5B Si3 Li5A 114.6(3) 1_655 .
Li6 Si3 Li5A 159.05(16) 1_655 .
Li6 Si3 Li5A 62.86(10) . .
Li5A Si3 Li5A 112.42(9) 1_655 .
Li7 Si3 Li4B 117.58(7) 13 .
Li8 Si3 Li4B 145.51(11) 13 .
Li5B Si3 Li4B 90.7(11) 1_655 .
Li6 Si3 Li4B 106.25(9) 1_655 .
Li6 Si3 Li4B 60.87(11) . .
Li5A Si3 Li4B 99.37(17) 1_655 .
Li5A Si3 Li4B 53.21(19) . .
Li7 Si3 Li4B 117.58(7) 13 3_655
Li8 Si3 Li4B 145.51(11) 13 3_655
Li5B Si3 Li4B 90.7(11) . 3_655
Li6 Si3 Li4B 60.88(11) 1_655 3_655
Li6 Si3 Li4B 106.24(9) . 3_655
Li5A Si3 Li4B 53.21(19) 1_655 3_655
Li5A Si3 Li4B 99.37(17) . 3_655
Li4B Si3 Li4B 54.5(2) . 3_655
Li4A Si3 Li10 126.43(3) . 13
Li7 Si3 Li10 66.48(3) 13 13
Li8 Si3 Li10 58.62(3) 13 13
Li5B Si3 Li10 63.5(10) . 13
Li5B Si3 Li10 151.6(15) 1_655 13
Li6 Si3 Li10 141.84(4) 1_655 13
Li6 Si3 Li10 57.40(3) . 13
Li5A Si3 Li10 139.11(17) 1_655 13
Li5A Si3 Li10 55.90(10) . 13
Li4B Si3 Li10 99.91(11) . 13
Li4B Si3 Li10 153.91(12) 3_655 13
Li8 Li1 Li8 114.77(11) 5_545 14_546
Li8 Li1 Li4A 122.61(6) 5_545 .
Li8 Li1 Li4A 122.61(6) 14_546 .
Li8 Li1 Li4B 118.14(6) 5_545 .
Li8 Li1 Li4B 118.14(6) 14_546 .
Li4A Li1 Li4B 28.97(13) . .
Li8 Li1 Li4B 118.14(6) 5_545 3_655
Li8 Li1 Li4B 118.14(6) 14_546 3_655
Li4A Li1 Li4B 28.97(13) . 3_655
Li4B Li1 Li4B 57.9(3) . 3_655
Li8 Li1 Li6 124.01(4) 5_545 10_656
Li8 Li1 Li6 63.92(3) 14_546 10_656
Li4A Li1 Li6 83.63(4) . 10_656
Li4B Li1 Li6 106.81(11) . 10_656
Li4B Li1 Li6 61.10(10) 3_655 10_656
Li8 Li1 Li6 124.01(4) 5_545 10_556
Li8 Li1 Li6 63.92(3) 14_546 10_556
Li4A Li1 Li6 83.63(4) . 10_556
Li4B Li1 Li6 61.10(10) . 10_556
Li4B Li1 Li6 106.81(11) 3_655 10_556
Li6 Li1 Li6 105.79(4) 10_656 10_556
Li8 Li1 Li6 63.92(3) 5_545 .
Li8 Li1 Li6 124.01(4) 14_546 .
Li4A Li1 Li6 83.63(4) . .
Li4B Li1 Li6 61.10(10) . .
Li4B Li1 Li6 106.81(11) 3_655 .
Li6 Li1 Li6 167.26(9) 10_656 .
Li6 Li1 Li6 72.74(4) 10_556 .
Li8 Li1 Li6 63.92(3) 5_545 1_655
Li8 Li1 Li6 124.01(4) 14_546 1_655
Li4A Li1 Li6 83.63(4) . 1_655
Li4B Li1 Li6 106.81(12) . 1_655
Li4B Li1 Li6 61.10(10) 3_655 1_655
Li6 Li1 Li6 72.74(4) 10_656 1_655
Li6 Li1 Li6 167.26(9) 10_556 1_655
Li6 Li1 Li6 105.79(4) . 1_655
Li8 Li1 Si2 71.00(4) 5_545 5_445
Li8 Li1 Si2 71.00(4) 14_546 5_445
Li4A Li1 Si2 127.15(3) . 5_445
Li4B Li1 Si2 98.18(13) . 5_445
Li4B Li1 Si2 156.12(14) 3_655 5_445
Li6 Li1 Si2 134.64(5) 10_656 5_445
Li6 Li1 Si2 55.34(2) 10_556 5_445
Li6 Li1 Si2 55.34(2) . 5_445
Li6 Li1 Si2 134.64(5) 1_655 5_445
Li8 Li1 Si2 71.00(4) 5_545 5_545
Li8 Li1 Si2 71.00(4) 14_546 5_545
Li4A Li1 Si2 127.15(3) . 5_545
Li4B Li1 Si2 156.12(14) . 5_545
Li4B Li1 Si2 98.18(13) 3_655 5_545
Li6 Li1 Si2 55.34(2) 10_656 5_545
Li6 Li1 Si2 134.64(5) 10_556 5_545
Li6 Li1 Si2 134.64(5) . 5_545
Li6 Li1 Si2 55.34(2) 1_655 5_545
Si2 Li1 Si2 105.70(6) 5_445 5_545
Li8 Li1 Si3 66.39(4) 5_545 .
Li8 Li1 Si3 178.84(8) 14_546 .
Li4A Li1 Si3 56.23(3) . .
Li4B Li1 Si3 60.90(5) . .
Li4B Li1 Si3 60.90(5) 3_655 .
Li6 Li1 Si3 115.55(5) 10_656 .
Li6 Li1 Si3 115.55(5) 10_556 .
Li6 Li1 Si3 56.32(2) . .
Li6 Li1 Si3 56.32(2) 1_655 .
Si2 Li1 Si3 109.614(7) 5_445 .
Si2 Li1 Si3 109.614(7) 5_545 .
Li9 Li2 Li9 69.41(7) 10_556 .
Li9 Li2 Li3 115.40(3) 10_556 .
Li9 Li2 Li3 115.40(3) . .
Li9 Li2 Li3 115.40(3) 10_556 1_655
Li9 Li2 Li3 115.40(3) . 1_655
Li3 Li2 Li3 117.09(9) . 1_655
Li9 Li2 Si2 145.30(4) 10_556 .
Li9 Li2 Si2 145.30(4) . .
Li3 Li2 Si2 58.55(5) . .
Li3 Li2 Si2 58.55(5) 1_655 .
Li9 Li2 Si1 61.57(3) 10_556 .
Li9 Li2 Si1 61.57(3) . .
Li3 Li2 Si1 66.85(4) . .
Li3 Li2 Si1 176.06(7) 1_655 .
Si2 Li2 Si1 125.39(3) . .
Li9 Li2 Si1 61.57(3) 10_556 1_655
Li9 Li2 Si1 61.57(3) . 1_655
Li3 Li2 Si1 176.06(7) . 1_655
Li3 Li2 Si1 66.85(4) 1_655 1_655
Si2 Li2 Si1 125.39(3) . 1_655
Si1 Li2 Si1 109.22(6) . 1_655
Li9 Li2 Li10 158.67(6) 10_556 .
Li9 Li2 Li10 89.26(4) . .
Li3 Li2 Li10 73.05(3) . .
Li3 Li2 Li10 73.05(3) 1_655 .
Si2 Li2 Li10 56.04(4) . .
Si1 Li2 Li10 108.879(14) . .
Si1 Li2 Li10 108.879(14) 1_655 .
Li9 Li2 Li10 89.26(4) 10_556 10_556
Li9 Li2 Li10 158.67(6) . 10_556
Li3 Li2 Li10 73.05(3) . 10_556
Li3 Li2 Li10 73.05(3) 1_655 10_556
Si2 Li2 Li10 56.03(4) . 10_556
Si1 Li2 Li10 108.879(14) . 10_556
Si1 Li2 Li10 108.879(14) 1_655 10_556
Li10 Li2 Li10 112.07(7) . 10_556
Li9 Li2 Li7 108.99(5) 10_556 1_655
Li9 Li2 Li7 61.66(3) . 1_655
Li3 Li2 Li7 130.50(4) . 1_655
Li3 Li2 Li7 56.32(3) 1_655 1_655
Si2 Li2 Li7 95.21(4) . 1_655
Si1 Li2 Li7 121.51(4) . 1_655
Si1 Li2 Li7 51.11(2) 1_655 1_655
Li10 Li2 Li7 57.86(3) . 1_655
Li10 Li2 Li7 129.31(4) 10_556 1_655
Li9 Li2 Li7 61.66(3) 10_556 10_656
Li9 Li2 Li7 108.99(5) . 10_656
Li3 Li2 Li7 130.50(4) . 10_656
Li3 Li2 Li7 56.32(3) 1_655 10_656
Si2 Li2 Li7 95.21(4) . 10_656
Si1 Li2 Li7 121.51(4) . 10_656
Si1 Li2 Li7 51.11(2) 1_655 10_656
Li10 Li2 Li7 129.31(4) . 10_656
Li10 Li2 Li7 57.86(3) 10_556 10_656
Li7 Li2 Li7 89.28(3) 1_655 10_656
Li9 Li2 Li7 61.66(3) 10_556 10_556
Li9 Li2 Li7 108.99(5) . 10_556
Li3 Li2 Li7 56.32(3) . 10_556
Li3 Li2 Li7 130.50(4) 1_655 10_556
Si2 Li2 Li7 95.21(4) . 10_556
Si1 Li2 Li7 51.11(2) . 10_556
Si1 Li2 Li7 121.51(4) 1_655 10_556
Li10 Li2 Li7 129.31(4) . 10_556
Li10 Li2 Li7 57.86(3) 10_556 10_556
Li7 Li2 Li7 169.58(8) 1_655 10_556
Li7 Li2 Li7 89.77(4) 10_656 10_556
Si2 Li3 Si2 118.19(7) 1_455 .
Si2 Li3 Li2 62.35(3) 1_455 1_455
Si2 Li3 Li2 179.45(8) . 1_455
Si2 Li3 Li2 179.45(8) 1_455 .
Si2 Li3 Li2 62.36(3) . .
Li2 Li3 Li2 117.10(9) 1_455 .
Si2 Li3 Li8 70.94(4) 1_455 10_556
Si2 Li3 Li8 70.94(4) . 10_556
Li2 Li3 Li8 109.37(2) 1_455 10_556
Li2 Li3 Li8 109.37(2) . 10_556
Si2 Li3 Li8 70.94(4) 1_455 .
Si2 Li3 Li8 70.94(4) . .
Li2 Li3 Li8 109.37(2) 1_455 .
Li2 Li3 Li8 109.37(2) . .
Li8 Li3 Li8 101.05(9) 10_556 .
Si2 Li3 Li7 107.845(14) 1_455 10_556
Si2 Li3 Li7 107.846(14) . 10_556
Li2 Li3 Li7 71.86(4) 1_455 10_556
Li2 Li3 Li7 71.86(4) . 10_556
Li8 Li3 Li7 76.11(4) 10_556 10_556
Li8 Li3 Li7 177.16(7) . 10_556
Si2 Li3 Li7 107.846(14) 1_455 .
Si2 Li3 Li7 107.846(14) . .
Li2 Li3 Li7 71.86(4) 1_455 .
Li2 Li3 Li7 71.86(4) . .
Li8 Li3 Li7 177.16(7) 10_556 .
Li8 Li3 Li7 76.11(4) . .
Li7 Li3 Li7 106.73(8) 10_556 .
Si2 Li3 Si1 120.90(4) 1_455 .
Si2 Li3 Si1 120.90(4) . .
Li2 Li3 Si1 58.55(5) 1_455 .
Li2 Li3 Si1 58.55(5) . .
Li8 Li3 Si1 129.48(4) 10_556 .
Li8 Li3 Si1 129.48(4) . .
Li7 Li3 Si1 53.37(4) 10_556 .
Li7 Li3 Si1 53.37(4) . .
Si2 Li3 Li1 59.10(4) 1_455 5_455
Si2 Li3 Li1 59.10(4) . 5_455
Li2 Li3 Li1 121.45(5) 1_455 5_455
Li2 Li3 Li1 121.45(5) . 5_455
Li8 Li3 Li1 50.52(4) 10_556 5_455
Li8 Li3 Li1 50.52(4) . 5_455
Li7 Li3 Li1 126.63(4) 10_556 5_455
Li7 Li3 Li1 126.63(4) . 5_455
Si1 Li3 Li1 180.0 . 5_455
Si2 Li3 Li10 122.57(4) 1_455 .
Si2 Li3 Li10 51.61(2) . .
Li2 Li3 Li10 128.19(4) 1_455 .
Li2 Li3 Li10 57.70(2) . .
Li8 Li3 Li10 120.97(5) 10_556 .
Li8 Li3 Li10 51.92(3) . .
Li7 Li3 Li10 129.50(4) 10_556 .
Li7 Li3 Li10 57.31(3) . .
Si1 Li3 Li10 94.61(4) . .
Li1 Li3 Li10 85.39(4) 5_455 .
Si2 Li3 Li10 51.61(2) 1_455 1_455
Si2 Li3 Li10 122.57(4) . 1_455
Li2 Li3 Li10 57.70(2) 1_455 1_455
Li2 Li3 Li10 128.19(4) . 1_455
Li8 Li3 Li10 120.97(5) 10_556 1_455
Li8 Li3 Li10 51.92(3) . 1_455
Li7 Li3 Li10 129.50(4) 10_556 1_455
Li7 Li3 Li10 57.31(3) . 1_455
Si1 Li3 Li10 94.61(4) . 1_455
Li1 Li3 Li10 85.39(4) 5_455 1_455
Li10 Li3 Li10 85.00(3) . 1_455
Li9 Li4A Li9 78.43(14) . 10_556
Li9 Li4A Li1 140.79(7) . .
Li9 Li4A Li1 140.79(7) 10_556 .
Li9 Li4A Si3 71.63(4) . .
Li9 Li4A Si3 150.06(15) 10_556 .
Li1 Li4A Si3 69.16(9) . .
Li9 Li4A Si3 150.06(15) . 10_556
Li9 Li4A Si3 71.63(4) 10_556 10_556
Li1 Li4A Si3 69.16(9) . 10_556
Si3 Li4A Si3 138.31(17) . 10_556
Li9 Li4A Li5A 55.22(9) . 1_655
Li9 Li4A Li5A 106.79(11) 10_556 1_655
Li1 Li4A Li5A 100.47(9) . 1_655
Si3 Li4A Li5A 55.21(7) . 1_655
Si3 Li4A Li5A 134.41(11) 10_556 1_655
Li9 Li4A Li5A 106.79(11) . 10_656
Li9 Li4A Li5A 55.22(9) 10_556 10_656
Li1 Li4A Li5A 100.47(9) . 10_656
Si3 Li4A Li5A 134.41(11) . 10_656
Si3 Li4A Li5A 55.21(7) 10_556 10_656
Li5A Li4A Li5A 85.64(19) 1_655 10_656
Li9 Li4A Li5A 55.22(9) . .
Li9 Li4A Li5A 106.79(11) 10_556 .
Li1 Li4A Li5A 100.47(9) . .
Si3 Li4A Li5A 55.21(7) . .
Si3 Li4A Li5A 134.41(11) 10_556 .
Li5A Li4A Li5A 90.6(2) 1_655 .
Li5A Li4A Li5A 159.06(17) 10_656 .
Li9 Li4A Li5A 106.79(11) . 10_556
Li9 Li4A Li5A 55.22(9) 10_556 10_556
Li1 Li4A Li5A 100.47(9) . 10_556
Si3 Li4A Li5A 134.41(11) . 10_556
Si3 Li4A Li5A 55.21(7) 10_556 10_556
Li5A Li4A Li5A 159.06(17) 1_655 10_556
Li5A Li4A Li5A 90.6(2) 10_656 10_556
Li5A Li4A Li5A 85.64(19) . 10_556
Li10 Li5A Li9 119.81(13) 13 .
Li10 Li5A Li9 119.81(13) 13 1_455
Li9 Li5A Li9 115.64(8) . 1_455
Li10 Li5A Si3 64.64(5) 13 .
Li9 Li5A Si3 64.99(3) . .
Li9 Li5A Si3 169.8(4) 1_455 .
Li10 Li5A Si3 64.64(5) 13 1_455
Li9 Li5A Si3 169.8(4) . 1_455
Li9 Li5A Si3 64.99(4) 1_455 1_455
Si3 Li5A Si3 112.42(9) . 1_455
Li10 Li5A Si1 178.9(3) 13 .
Li9 Li5A Si1 60.45(7) . .
Li9 Li5A Si1 60.45(7) 1_455 .
Si3 Li5A Si1 114.91(16) . .
Si3 Li5A Si1 114.91(16) 1_455 .
Li10 Li5A Li6 58.64(5) 13 .
Li9 Li5A Li6 114.95(16) . .
Li9 Li5A Li6 114.95(16) 1_455 .
Si3 Li5A Li6 58.28(7) . .
Si3 Li5A Li6 58.28(7) 1_455 .
Si1 Li5A Li6 120.2(3) . .
Li10 Li5A Li7 129.5(3) 13 .
Li9 Li5A Li7 62.37(6) . .
Li9 Li5A Li7 62.37(6) 1_455 .
Si3 Li5A Li7 123.11(9) . .
Si3 Li5A Li7 123.11(9) 1_455 .
Si1 Li5A Li7 51.61(4) . .
Li6 Li5A Li7 171.8(3) . .
Li10 Li5A Li7 61.73(12) 13 13_455
Li9 Li5A Li7 138.4(3) . 13_455
Li9 Li5A Li7 61.93(9) 1_455 13_455
Si3 Li5A Li7 125.12(19) . 13_455
Si3 Li5A Li7 51.63(7) 1_455 13_455
Si1 Li5A Li7 118.93(7) . 13_455
Li6 Li5A Li7 100.78(6) . 13_455
Li7 Li5A Li7 84.83(15) . 13_455
Li10 Li5A Li7 61.73(12) 13 13
Li9 Li5A Li7 61.93(9) . 13
Li9 Li5A Li7 138.4(3) 1_455 13
Si3 Li5A Li7 51.63(7) . 13
Si3 Li5A Li7 125.12(19) 1_455 13
Si1 Li5A Li7 118.93(7) . 13
Li6 Li5A Li7 100.78(6) . 13
Li7 Li5A Li7 84.83(15) . 13
Li7 Li5A Li7 92.0(2) 13_455 13
Li10 Li5A Li4A 113.09(10) 13 1_455
Li9 Li5A Li4A 121.2(2) . 1_455
Li9 Li5A Li4A 46.77(10) 1_455 1_455
Si3 Li5A Li4A 123.5(3) . 1_455
Si3 Li5A Li4A 50.96(9) 1_455 1_455
Si1 Li5A Li4A 66.19(14) . 1_455
Li6 Li5A Li4A 72.86(16) . 1_455
Li7 Li5A Li4A 101.59(10) . 1_455
Li7 Li5A Li4A 88.34(2) 13_455 1_455
Li7 Li5A Li4A 173.58(13) 13 1_455
Li10 Li5A Li4A 113.09(10) 13 .
Li9 Li5A Li4A 46.77(10) . .
Li9 Li5A Li4A 121.2(2) 1_455 .
Si3 Li5A Li4A 50.96(9) . .
Si3 Li5A Li4A 123.5(3) 1_455 .
Si1 Li5A Li4A 66.19(14) . .
Li6 Li5A Li4A 72.86(16) . .
Li7 Li5A Li4A 101.59(10) . .
Li7 Li5A Li4A 173.58(13) 13_455 .
Li7 Li5A Li4A 88.34(2) 13 .
Li4A Li5A Li4A 90.6(2) 1_455 .
Li4B Li4B Li5B 60.2(11) 3 .
Li4B Li4B Li5B 60.2(11) 3 10_556
Li5B Li4B Li5B 111.5(16) . 10_556
Li4B Li4B Li4B 179.998(1) 3 3_655
Li5B Li4B Li4B 119.8(11) . 3_655
Li5B Li4B Li4B 119.8(11) 10_556 3_655
Li4B Li4B Li1 118.97(13) 3 .
Li5B Li4B Li1 118.1(4) . .
Li5B Li4B Li1 118.1(4) 10_556 .
Li4B Li4B Li1 61.03(13) 3_655 .
Li4B Li4B Si1 69.46(13) 3 .
Li5B Li4B Si1 65.1(5) . .
Li5B Li4B Si1 65.1(5) 10_556 .
Li4B Li4B Si1 110.54(13) 3_655 .
Li1 Li4B Si1 171.6(3) . .
Li4B Li4B Li6 69.87(11) 3 10_556
Li5B Li4B Li6 120.9(11) . 10_556
Li5B Li4B Li6 61.5(7) 10_556 10_556
Li4B Li4B Li6 110.13(11) 3_655 10_556
Li1 Li4B Li6 62.25(7) . 10_556
Si1 Li4B Li6 123.78(16) . 10_556
Li4B Li4B Li6 69.87(11) 3 .
Li5B Li4B Li6 61.5(7) . .
Li5B Li4B Li6 120.9(11) 10_556 .
Li4B Li4B Li6 110.13(11) 3_655 .
Li1 Li4B Li6 62.25(7) . .
Si1 Li4B Li6 123.78(16) . .
Li6 Li4B Li6 73.66(12) 10_556 .
Li4B Li4B Li9 117.27(10) 3 .
Li5B Li4B Li9 66.6(11) . .
Li5B Li4B Li9 118.6(8) 10_556 .
Li4B Li4B Li9 62.73(10) 3_655 .
Li1 Li4B Li9 113.73(18) . .
Si1 Li4B Li9 59.50(7) . .
Li6 Li4B Li9 172.3(2) 10_556 .
Li6 Li4B Li9 110.85(4) . .
Li4B Li4B Li9 117.27(10) 3 10_556
Li5B Li4B Li9 118.6(8) . 10_556
Li5B Li4B Li9 66.6(11) 10_556 10_556
Li4B Li4B Li9 62.73(10) 3_655 10_556
Li1 Li4B Li9 113.73(18) . 10_556
Si1 Li4B Li9 59.50(7) . 10_556
Li6 Li4B Li9 110.85(4) 10_556 10_556
Li6 Li4B Li9 172.3(2) . 10_556
Li9 Li4B Li9 63.98(12) . 10_556
Li4B Li4B Si3 117.27(11) 3 .
Li5B Li4B Si3 66.0(8) . .
Li5B Li4B Si3 177.4(10) 10_556 .
Li4B Li4B Si3 62.73(11) 3_655 .
Li1 Li4B Si3 63.34(7) . .
Si1 Li4B Si3 113.80(8) . .
Li6 Li4B Si3 118.68(11) 10_556 .
Li6 Li4B Si3 57.36(4) . .
Li9 Li4B Si3 61.62(8) . .
Li9 Li4B Si3 115.2(2) 10_556 .
Li4B Li4B Si3 117.27(11) 3 10_556
Li5B Li4B Si3 177.4(10) . 10_556
Li5B Li4B Si3 66.0(8) 10_556 10_556
Li4B Li4B Si3 62.73(11) 3_655 10_556
Li1 Li4B Si3 63.34(7) . 10_556
Si1 Li4B Si3 113.80(8) . 10_556
Li6 Li4B Si3 57.36(4) 10_556 10_556
Li6 Li4B Si3 118.68(11) . 10_556
Li9 Li4B Si3 115.2(2) . 10_556
Li9 Li4B Si3 61.62(8) 10_556 10_556
Si3 Li4B Si3 116.46(17) . 10_556
Li4B Li5B Li4B 60(2) . 3
Li4B Li5B Li6 76.3(18) . .
Li4B Li5B Li6 76.3(18) 3 .
Li4B Li5B Si1 72.6(13) . .
Li4B Li5B Si1 72.6(13) 3 .
Li6 Li5B Si1 144(3) . .
Li4B Li5B Si3 73.0(8) . .
Li4B Li5B Si3 123(3) 3 .
Li6 Li5B Si3 62.0(4) . .
Si1 Li5B Si3 123.0(5) . .
Li4B Li5B Si3 123(3) . 1_455
Li4B Li5B Si3 73.0(8) 3 1_455
Li6 Li5B Si3 62.0(4) . 1_455
Si1 Li5B Si3 123.0(5) . 1_455
Si3 Li5B Si3 113.6(6) . 1_455
Li4B Li5B Li9 72.6(5) . .
Li4B Li5B Li9 122(2) 3 .
Li6 Li5B Li9 123.8(7) . .
Si1 Li5B Li9 62.5(3) . .
Si3 Li5B Li9 64.6(3) . .
Si3 Li5B Li9 164(3) 1_455 .
Li4B Li5B Li9 122(2) . 1_455
Li4B Li5B Li9 72.6(5) 3 1_455
Li6 Li5B Li9 123.8(7) . 1_455
Si1 Li5B Li9 62.5(3) . 1_455
Si3 Li5B Li9 164(3) . 1_455
Si3 Li5B Li9 64.6(3) 1_455 1_455
Li9 Li5B Li9 112.4(11) . 1_455
Li4B Li5B Li10 125.6(10) . 13
Li4B Li5B Li10 125.6(10) 3 13
Li6 Li5B Li10 58.1(4) . 13
Si1 Li5B Li10 158(3) . 13
Si3 Li5B Li10 60.8(6) . 13
Si3 Li5B Li10 60.8(6) 1_455 13
Li9 Li5B Li10 108.2(16) . 13
Li9 Li5B Li10 108.2(16) 1_455 13
Li4B Li5B Li5B 34.2(8) . 10_556
Li4B Li5B Li5B 34.2(8) 3 10_556
Li6 Li5B Li5B 91.8(15) . 10_556
Si1 Li5B Li5B 52.2(16) . 10_556
Si3 Li5B Li5B 107.3(15) . 10_556
Si3 Li5B Li5B 107.3(15) 1_455 10_556
Li9 Li5B Li5B 87.8(14) . 10_556
Li9 Li5B Li5B 87.8(14) 1_455 10_556
Li10 Li5B Li5B 149.8(12) 13 10_556
Li4B Li5B Li7 114.4(6) . .
Li4B Li5B Li7 114.4(6) 3 .
Li6 Li5B Li7 167(3) . .
Si1 Li5B Li7 48.6(7) . .
Si3 Li5B Li7 113.3(15) . .
Si3 Li5B Li7 113.3(15) 1_455 .
Li9 Li5B Li7 57.5(8) . .
Li9 Li5B Li7 57.5(8) 1_455 .
Li10 Li5B Li7 109(2) 13 .
Li5B Li5B Li7 100.9(10) 10_556 .
Li5B Li6 Si2 138.6(15) . 5_445
Li5B Li6 Li10 68.3(15) . 13
Si2 Li6 Li10 153.17(6) 5_445 13
Li5B Li6 Si3 62.0(5) . 1_455
Si2 Li6 Si3 122.62(2) 5_445 1_455
Li10 Li6 Si3 64.14(3) 13 1_455
Li5B Li6 Si3 62.0(5) . .
Si2 Li6 Si3 122.62(2) 5_445 .
Li10 Li6 Si3 64.14(3) 13 .
Si3 Li6 Si3 113.51(4) 1_455 .
Li5B Li6 Li4B 42.2(13) . .
Si2 Li6 Li4B 100.00(6) 5_445 .
Li10 Li6 Li4B 105.16(7) 13 .
Si3 Li6 Li4B 95.88(10) 1_455 .
Si3 Li6 Li4B 61.76(10) . .
Li5B Li6 Li4B 42.2(13) . 3
Si2 Li6 Li4B 100.01(6) 5_445 3
Li10 Li6 Li4B 105.16(7) 13 3
Si3 Li6 Li4B 61.76(10) 1_455 3
Si3 Li6 Li4B 95.88(10) . 3
Li4B Li6 Li4B 40.3(2) . 3
Li5B Li6 Li5A 11.6(14) . .
Si2 Li6 Li5A 150.14(15) 5_445 .
Li10 Li6 Li5A 56.70(15) 13 .
Si3 Li6 Li5A 58.87(4) 1_455 .
Si3 Li6 Li5A 58.87(4) . .
Li4B Li6 Li5A 52.40(14) . .
Li4B Li6 Li5A 52.40(14) 3 .
Li5B Li6 Li8 126.1(2) . 5_445
Si2 Li6 Li8 69.11(4) 5_445 5_445
Li10 Li6 Li8 95.68(5) 13 5_445
Si3 Li6 Li8 64.71(3) 1_455 5_445
Si3 Li6 Li8 155.24(6) . 5_445
Li4B Li6 Li8 141.68(11) . 5_445
Li4B Li6 Li8 103.61(11) 3 5_445
Li5A Li6 Li8 123.43(6) . 5_445
Li5B Li6 Li8 126.1(2) . 5_545
Si2 Li6 Li8 69.11(4) 5_445 5_545
Li10 Li6 Li8 95.68(5) 13 5_545
Si3 Li6 Li8 155.24(6) 1_455 5_545
Si3 Li6 Li8 64.71(3) . 5_545
Li4B Li6 Li8 103.61(11) . 5_545
Li4B Li6 Li8 141.68(11) 3 5_545
Li5A Li6 Li8 123.43(6) . 5_545
Li8 Li6 Li8 105.92(6) 5_445 5_545
Li5B Li6 Li1 95.3(9) . .
Si2 Li6 Li1 62.36(4) 5_445 .
Li10 Li6 Li1 126.02(3) 13 .
Si3 Li6 Li1 151.50(6) 1_455 .
Si3 Li6 Li1 62.92(3) . .
Li4B Li6 Li1 56.65(10) . .
Li4B Li6 Li1 89.95(11) 3 .
Li5A Li6 Li1 102.14(10) . .
Li8 Li6 Li1 131.18(6) 5_445 .
Li8 Li6 Li1 52.06(4) 5_545 .
Li5B Li6 Li1 95.3(9) . 1_455
Si2 Li6 Li1 62.36(4) 5_445 1_455
Li10 Li6 Li1 126.02(3) 13 1_455
Si3 Li6 Li1 62.92(3) 1_455 1_455
Si3 Li6 Li1 151.50(6) . 1_455
Li4B Li6 Li1 89.95(11) . 1_455
Li4B Li6 Li1 56.65(10) 3 1_455
Li5A Li6 Li1 102.14(10) . 1_455
Li8 Li6 Li1 52.07(4) 5_445 1_455
Li8 Li6 Li1 131.18(6) 5_545 1_455
Li1 Li6 Li1 105.79(4) . 1_455
Si3 Li7 Si1 168.64(6) 13 .
Si3 Li7 Li3 101.71(6) 13 .
Si1 Li7 Li3 66.93(4) . .
Si3 Li7 Li10 61.15(3) 13 .
Si1 Li7 Li10 112.72(4) . .
Li3 Li7 Li10 70.49(4) . .
Si3 Li7 Li10 61.15(3) 13 1_455
Si1 Li7 Li10 112.72(4) . 1_455
Li3 Li7 Li10 70.49(4) . 1_455
Li10 Li7 Li10 98.35(6) . 1_455
Si3 Li7 Li9 61.74(4) 13 13
Si1 Li7 Li9 129.62(6) . 13
Li3 Li7 Li9 163.45(6) . 13
Li10 Li7 Li9 99.21(4) . 13
Li10 Li7 Li9 99.21(4) 1_455 13
Si3 Li7 Li9 126.60(3) 13 1_455
Si1 Li7 Li9 58.25(3) . 1_455
Li3 Li7 Li9 99.75(4) . 1_455
Li10 Li7 Li9 169.43(6) . 1_455
Li10 Li7 Li9 81.61(3) 1_455 1_455
Li9 Li7 Li9 91.21(5) 13 1_455
Si3 Li7 Li9 126.60(3) 13 .
Si1 Li7 Li9 58.25(3) . .
Li3 Li7 Li9 99.75(4) . .
Li10 Li7 Li9 81.61(3) . .
Li10 Li7 Li9 169.43(6) 1_455 .
Li9 Li7 Li9 91.21(4) 13 .
Li9 Li7 Li9 96.49(5) 1_455 .
Si3 Li7 Li5A 133.28(15) 13 .
Si1 Li7 Li5A 58.08(14) . .
Li3 Li7 Li5A 125.01(15) . .
Li10 Li7 Li5A 130.69(3) . .
Li10 Li7 Li5A 130.69(3) 1_455 .
Li9 Li7 Li5A 71.54(15) 13 .
Li9 Li7 Li5A 51.34(5) 1_455 .
Li9 Li7 Li5A 51.34(5) . .
Si3 Li7 Li5A 55.73(11) 13 13_455
Si1 Li7 Li5A 129.20(12) . 13_455
Li3 Li7 Li5A 120.81(6) . 13_455
Li10 Li7 Li5A 116.88(12) . 13_455
Li10 Li7 Li5A 50.44(4) 1_455 13_455
Li9 Li7 Li5A 51.35(7) 13 13_455
Li9 Li7 Li5A 71.24(11) 1_455 13_455
Li9 Li7 Li5A 138.77(6) . 13_455
Li5A Li7 Li5A 95.17(15) . 13_455
Si3 Li7 Li5A 55.73(11) 13 13
Si1 Li7 Li5A 129.20(12) . 13
Li3 Li7 Li5A 120.81(6) . 13
Li10 Li7 Li5A 50.44(4) . 13
Li10 Li7 Li5A 116.88(12) 1_455 13
Li9 Li7 Li5A 51.35(7) 13 13
Li9 Li7 Li5A 138.77(6) 1_455 13
Li9 Li7 Li5A 71.24(11) . 13
Li5A Li7 Li5A 95.17(15) . 13
Li5A Li7 Li5A 92.0(2) 13_455 13
Si3 Li7 Li2 117.69(4) 13 .
Si1 Li7 Li2 55.88(3) . .
Li3 Li7 Li2 51.83(3) . .
Li10 Li7 Li2 56.93(3) . .
Li10 Li7 Li2 121.48(6) 1_455 .
Li9 Li7 Li2 133.72(3) 13 .
Li9 Li7 Li2 114.08(5) 1_455 .
Li9 Li7 Li2 49.84(4) . .
Li5A Li7 Li2 94.06(11) . .
Li5A Li7 Li2 170.68(8) 13_455 .
Li5A Li7 Li2 88.35(10) 13 .
Li1 Li8 Si3 173.67(9) 5_455 13
Li1 Li8 Li8 119.55(10) 5_455 9_565
Si3 Li8 Li8 66.78(5) 13 9_565
Li1 Li8 Li10 113.60(5) 5_455 1_455
Si3 Li8 Li10 63.90(3) 13 1_455
Li8 Li8 Li10 97.71(5) 9_565 1_455
Li1 Li8 Li10 113.60(5) 5_455 .
Si3 Li8 Li10 63.90(3) 13 .
Li8 Li8 Li10 97.71(5) 9_565 .
Li10 Li8 Li10 112.88(7) 1_455 .
Li1 Li8 Li3 72.09(6) 5_455 .
Si3 Li8 Li3 101.58(6) 13 .
Li8 Li8 Li3 168.36(9) 9_565 .
Li10 Li8 Li3 76.14(5) 1_455 .
Li10 Li8 Li3 76.14(5) . .
Li1 Li8 Li6 64.02(4) 5_455 5
Si3 Li8 Li6 118.75(4) 13 5
Li8 Li8 Li6 81.74(6) 9_565 5
Li10 Li8 Li6 176.51(6) 1_455 5
Li10 Li8 Li6 70.60(3) . 5
Li3 Li8 Li6 104.99(5) . 5
Li1 Li8 Li6 64.02(4) 5_455 5_455
Si3 Li8 Li6 118.75(4) 13 5_455
Li8 Li8 Li6 81.74(6) 9_565 5_455
Li10 Li8 Li6 70.60(3) 1_455 5_455
Li10 Li8 Li6 176.52(6) . 5_455
Li3 Li8 Li6 104.99(5) . 5_455
Li6 Li8 Li6 105.92(6) 5 5_455
Li1 Li8 Si3 63.38(5) 5_455 5_455
Si3 Li8 Si3 122.95(6) 13 5_455
Li8 Li8 Si3 56.17(6) 9_565 5_455
Li10 Li8 Si3 121.34(4) 1_455 5_455
Li10 Li8 Si3 121.34(4) . 5_455
Li3 Li8 Si3 135.47(6) . 5_455
Li6 Li8 Si3 55.53(3) 5 5_455
Li6 Li8 Si3 55.53(3) 5_455 5_455
Li1 Li8 Si2 59.75(3) 5_455 .
Si3 Li8 Si2 116.71(4) 13 .
Li8 Li8 Si2 130.75(3) 9_565 .
Li10 Li8 Si2 129.15(6) 1_455 .
Li10 Li8 Si2 54.39(3) . .
Li3 Li8 Si2 53.34(3) . .
Li6 Li8 Si2 52.42(3) 5 .
Li6 Li8 Si2 123.55(5) 5_455 .
Si3 Li8 Si2 100.94(3) 5_455 .
Li1 Li8 Si2 59.75(3) 5_455 1_455
Si3 Li8 Si2 116.71(4) 13 1_455
Li8 Li8 Si2 130.75(3) 9_565 1_455
Li10 Li8 Si2 54.39(3) 1_455 1_455
Li10 Li8 Si2 129.15(6) . 1_455
Li3 Li8 Si2 53.34(3) . 1_455
Li6 Li8 Si2 123.55(5) 5 1_455
Li6 Li8 Si2 52.42(3) 5_455 1_455
Si3 Li8 Si2 100.94(3) 5_455 1_455
Si2 Li8 Si2 93.47(4) . 1_455
Li1 Li8 Li7 125.24(7) 5_455 .
Si3 Li8 Li7 48.43(3) 13 .
Li8 Li8 Li7 115.21(7) 9_565 .
Li10 Li8 Li7 57.16(4) 1_455 .
Li10 Li8 Li7 57.16(4) . .
Li3 Li8 Li7 53.15(5) . .
Li6 Li8 Li7 126.19(3) 5 .
Li6 Li8 Li7 126.19(3) 5_455 .
Si3 Li8 Li7 171.38(6) 5_455 .
Si2 Li8 Li7 84.90(4) . .
Si2 Li8 Li7 84.90(4) 1_455 .
Li4A Li9 Li2 106.08(8) . .
Li4A Li9 Li5A 78.01(17) . .
Li2 Li9 Li5A 121.92(6) . .
Li4A Li9 Li5A 78.01(17) . 1_655
Li2 Li9 Li5A 121.92(6) . 1_655
Li5A Li9 Li5A 115.64(8) . 1_655
Li4A Li9 Li5B 66.1(14) . 1_655
Li2 Li9 Li5B 118.6(5) . 1_655
Li5A Li9 Li5B 115.6(3) . 1_655
Li5A Li9 Li5B 13.0(14) 1_655 1_655
Li4A Li9 Li5B 66.1(14) . .
Li2 Li9 Li5B 118.6(5) . .
Li5A Li9 Li5B 13.0(14) . .
Li5A Li9 Li5B 115.6(3) 1_655 .
Li5B Li9 Li5B 112.4(11) 1_655 .
Li4A Li9 Si1 79.27(5) . .
Li2 Li9 Si1 61.74(3) . .
Li5A Li9 Si1 62.50(10) . .
Li5A Li9 Si1 156.99(18) 1_655 .
Li5B Li9 Si1 144.2(15) 1_655 .
Li5B Li9 Si1 56.9(6) . .
Li4A Li9 Si1 79.27(5) . 1_655
Li2 Li9 Si1 61.74(3) . 1_655
Li5A Li9 Si1 156.99(18) . 1_655
Li5A Li9 Si1 62.50(10) 1_655 1_655
Li5B Li9 Si1 56.9(6) 1_655 1_655
Li5B Li9 Si1 144.2(15) . 1_655
Si1 Li9 Si1 109.47(4) . 1_655
Li4A Li9 Li4B 27.39(10) . 3_655
Li2 Li9 Li4B 106.57(6) . 3_655
Li5A Li9 Li4B 100.57(17) . 3_655
Li5A Li9 Li4B 53.7(2) 1_655 3_655
Li5B Li9 Li4B 40.8(15) 1_655 3_655
Li5B Li9 Li4B 90.3(13) . 3_655
Si1 Li9 Li4B 103.36(10) . 3_655
Si1 Li9 Li4B 58.86(8) 1_655 3_655
Li4A Li9 Li4B 27.39(10) . .
Li2 Li9 Li4B 106.57(6) . .
Li5A Li9 Li4B 53.7(2) . .
Li5A Li9 Li4B 100.57(17) 1_655 .
Li5B Li9 Li4B 90.3(13) 1_655 .
Li5B Li9 Li4B 40.8(15) . .
Si1 Li9 Li4B 58.86(8) . .
Si1 Li9 Li4B 103.36(10) 1_655 .
Li4B Li9 Li4B 54.5(2) 3_655 .
Li4A Li9 Si3 57.44(7) . .
Li2 Li9 Si3 163.53(6) . .
Li5A Li9 Si3 58.32(4) . .
Li5A Li9 Si3 58.32(4) 1_655 .
Li5B Li9 Si3 57.4(3) 1_655 .
Li5B Li9 Si3 57.4(3) . .
Si1 Li9 Si3 111.13(3) . .
Si1 Li9 Si3 111.13(3) 1_655 .
Li4B Li9 Si3 59.19(6) 3_655 .
Li4B Li9 Si3 59.19(6) . .
Li4A Li9 Li9 50.79(7) . 10_556
Li2 Li9 Li9 55.30(4) . 10_556
Li5A Li9 Li9 104.40(17) . 10_556
Li5A Li9 Li9 104.40(17) 1_655 10_556
Li5B Li9 Li9 92.2(14) 1_655 10_556
Li5B Li9 Li9 92.2(14) . 10_556
Si1 Li9 Li9 57.24(2) . 10_556
Si1 Li9 Li9 57.24(2) 1_655 10_556
Li4B Li9 Li9 58.01(6) 3_655 10_556
Li4B Li9 Li9 58.01(6) . 10_556
Si3 Li9 Li9 108.23(3) . 10_556
Li5A Li10 Li6 64.66(17) 13 13
Li5A Li10 Si2 162.69(17) 13 .
Li6 Li10 Si2 132.65(6) 13 .
Li5A Li10 Li8 116.91(7) 13 .
Li6 Li10 Li8 84.65(5) 13 .
Si2 Li10 Li8 70.27(4) . .
Li5A Li10 Li8 116.91(7) 13 1_655
Li6 Li10 Li8 84.65(5) 13 1_655
Si2 Li10 Li8 70.27(4) . 1_655
Li8 Li10 Li8 112.88(7) . 1_655
Li5A Li10 Si3 59.46(7) 13 13
Li6 Li10 Si3 58.46(2) 13 13
Si2 Li10 Si3 125.85(2) . 13
Li8 Li10 Si3 57.48(3) . 13
Li8 Li10 Si3 141.51(6) 1_655 13
Li5A Li10 Si3 59.46(7) 13 13_655
Li6 Li10 Si3 58.46(2) 13 13_655
Si2 Li10 Si3 125.85(2) . 13_655
Li8 Li10 Si3 141.51(6) . 13_655
Li8 Li10 Si3 57.48(3) 1_655 13_655
Si3 Li10 Si3 104.78(4) 13 13_655
Li5A Li10 Li5B 11.0(11) 13 13
Li6 Li10 Li5B 53.7(12) 13 13
Si2 Li10 Li5B 173.7(12) . 13
Li8 Li10 Li5B 112.6(5) . 13
Li8 Li10 Li5B 112.6(5) 1_655 13
Si3 Li10 Li5B 55.7(4) 13 13
Si3 Li10 Li5B 55.7(4) 13_655 13
Li5A Li10 Li2 104.88(17) 13 .
Li6 Li10 Li2 169.54(7) 13 .
Si2 Li10 Li2 57.81(4) . .
Li8 Li10 Li2 100.99(5) . .
Li8 Li10 Li2 100.99(5) 1_655 .
Si3 Li10 Li2 117.21(3) 13 .
Si3 Li10 Li2 117.21(3) 13_655 .
Li5B Li10 Li2 115.9(12) 13 .
Li5A Li10 Li7 67.84(10) 13 1_655
Li6 Li10 Li7 108.73(4) 13 1_655
Si2 Li10 Li7 101.61(4) . 1_655
Li8 Li10 Li7 166.12(6) . 1_655
Li8 Li10 Li7 73.12(4) 1_655 1_655
Si3 Li10 Li7 126.04(5) 13 1_655
Si3 Li10 Li7 52.37(2) 13_655 1_655
Li5B Li10 Li7 74.4(8) 13 1_655
Li2 Li10 Li7 65.22(4) . 1_655
Li5A Li10 Li7 67.84(10) 13 .
Li6 Li10 Li7 108.73(4) 13 .
Si2 Li10 Li7 101.61(4) . .
Li8 Li10 Li7 73.12(4) . .
Li8 Li10 Li7 166.12(6) 1_655 .
Si3 Li10 Li7 52.37(2) 13 .
Si3 Li10 Li7 126.04(5) 13_655 .
Li5B Li10 Li7 74.4(8) 13 .
Li2 Li10 Li7 65.22(4) . .
Li7 Li10 Li7 98.35(6) 1_655 .
Li5A Li10 Li6 145.08(17) 13 5
Li6 Li10 Li6 80.42(6) 13 5
Si2 Li10 Li6 52.23(3) . 5
Li8 Li10 Li6 56.44(3) . 5
Li8 Li10 Li6 56.44(3) 1_655 5
Si3 Li10 Li6 102.89(4) 13 5
Si3 Li10 Li6 102.89(4) 13_655 5
Li5B Li10 Li6 134.1(12) 13 5
Li2 Li10 Li6 110.04(5) . 5
Li7 Li10 Li6 127.95(3) 1_655 5
Li7 Li10 Li6 127.95(3) . 5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Si1 Li7 2.6216(12) 10_556
Si1 Li7 2.6216(12) .
Si1 Li5B 2.63(2) 10_556
Si1 Li5B 2.63(2) .
Si1 Li4B 2.766(3) 3
Si1 Li4B 2.766(3) .
Si1 Li9 2.7842(8) 1_455
Si1 Li9 2.7842(8) 10_556
Si1 Li9 2.7842(8) 10_456
Si1 Li9 2.7842(8) .
Si1 Li2 2.7887(10) .
Si1 Li2 2.7887(10) 1_455
Si2 Li6 2.6482(12) 14_556
Si2 Li6 2.6483(12) 5
Si2 Li3 2.6495(11) 1_655
Si2 Li3 2.6495(11) .
Si2 Li10 2.6962(12) 10_556
Si2 Li10 2.6963(12) .
Si2 Li2 2.7513(17) .
Si2 Li1 2.8522(12) 5
Si2 Li1 2.8522(12) 5_455
Si2 Li8 3.1219(12) 1_655
Si2 Li8 3.1219(12) 10_656
Si2 Li8 3.1219(12) 10_556
Si3 Li4A 2.5870(15) .
Si3 Li7 2.5950(12) 13
Si3 Li8 2.6947(14) 13
Si3 Li5B 2.716(9) .
Si3 Li5B 2.716(9) 1_655
Si3 Li6 2.7181(7) 1_655
Si3 Li6 2.7182(7) .
Si3 Li5A 2.7354(14) 1_655
Si3 Li5A 2.7354(14) .
Si3 Li4B 2.844(3) .
Si3 Li4B 2.844(3) 3_655
Si3 Li10 2.8698(8) 13
Li1 Li8 2.5010(17) 5_545
Li1 Li8 2.5010(17) 14_546
Li1 Li4A 2.537(5) .
Li1 Li4B 2.691(4) .
Li1 Li4B 2.691(4) 3_655
Li1 Li6 2.8504(9) 10_656
Li1 Li6 2.8504(9) 10_556
Li1 Li6 2.8505(9) .
Li1 Li6 2.8505(9) 1_655
Li1 Si2 2.8522(12) 5_445
Li1 Si2 2.8522(12) 5_545
Li2 Li9 2.6462(19) 10_556
Li2 Li9 2.6462(19) .
Li2 Li3 2.6649(14) .
Li2 Li3 2.6649(14) 1_655
Li2 Si1 2.7887(10) 1_655
Li2 Li10 2.9733(16) .
Li2 Li10 2.9734(16) 10_556
Li2 Li7 3.2214(10) 1_655
Li2 Li7 3.2214(10) 10_656
Li2 Li7 3.2214(10) 10_556
Li3 Si2 2.6495(11) 1_455
Li3 Li2 2.6649(14) 1_455
Li3 Li8 2.729(2) 10_556
Li3 Li8 2.729(2) .
Li3 Li7 2.8207(19) 10_556
Li3 Li7 2.8208(19) .
Li3 Li1 3.083(3) 5_455
Li3 Li10 3.3649(10) .
Li3 Li10 3.3649(10) 1_455
Li4A Li9 2.383(4) .
Li4A Li9 2.383(4) 10_556
Li4A Si3 2.5871(15) 10_556
Li4A Li5A 3.199(6) 1_655
Li4A Li5A 3.199(6) 10_656
Li4A Li5A 3.199(6) .
Li4A Li5A 3.199(6) 10_556
Li5A Li10 2.630(4) 13
Li5A Li9 2.6859(13) .
Li5A Li9 2.6860(13) 1_455
Li5A Si3 2.7354(14) 1_455
Li5A Li6 2.844(5) .
Li5A Li7 3.149(4) .
Li5A Li7 3.159(6) 13_455
Li5A Li7 3.159(6) 13
Li5A Li4A 3.199(6) 1_455
Li4B Li4B 1.941(12) 3
Li4B Li5B 1.95(6) .
Li4B Li5B 1.95(6) 10_556
Li4B Li4B 2.606(12) 3_655
Li4B Li6 2.820(4) 10_556
Li4B Li6 2.820(4) .
Li4B Li9 2.844(4) .
Li4B Li9 2.844(4) 10_556
Li4B Si3 2.844(3) 10_556
Li5B Li4B 1.95(6) 3
Li5B Li6 2.55(3) .
Li5B Si3 2.716(9) 1_455
Li5B Li9 2.735(18) .
Li5B Li9 2.735(18) 1_455
Li5B Li10 2.94(4) 13
Li5B Li5B 3.22(14) 10_556
Li5B Li7 3.46(5) .
Li6 Si2 2.6483(12) 5_445
Li6 Li10 2.6868(17) 13
Li6 Si3 2.7182(7) 1_455
Li6 Li4B 2.820(4) 3
Li6 Li8 2.8480(12) 5_445
Li6 Li8 2.8480(12) 5_545
Li6 Li1 2.8505(9) 1_455
Li7 Si3 2.5950(12) 13
Li7 Li10 3.0043(14) .
Li7 Li10 3.0044(14) 1_455
Li7 Li9 3.0346(18) 13
Li7 Li9 3.0474(13) 1_455
Li7 Li9 3.0474(13) .
Li7 Li5A 3.159(6) 13_455
Li7 Li5A 3.159(6) 13
Li8 Li1 2.5010(17) 5_455
Li8 Si3 2.6946(14) 13
Li8 Li8 2.722(3) 9_565
Li8 Li10 2.7280(11) 1_455
Li8 Li10 2.7281(11) .
Li8 Li6 2.8480(12) 5
Li8 Li6 2.8480(12) 5_455
Li8 Si3 2.9810(17) 5_455
Li8 Si2 3.1219(11) 1_455
Li9 Li5A 2.6859(13) 1_655
Li9 Li5B 2.735(18) 1_655
Li9 Si1 2.7842(8) 1_655
Li9 Li4B 2.844(4) 3_655
Li9 Li9 3.013(3) 10_556
Li10 Li5A 2.630(4) 13
Li10 Li6 2.6868(17) 13
Li10 Li8 2.7281(11) 1_655
Li10 Si3 2.8698(8) 13
Li10 Si3 2.8698(8) 13_655
Li10 Li5B 2.94(4) 13
Li10 Li7 3.0043(14) 1_655
Li10 Li6 3.2236(18) 5
