#------------------------------------------------------------------------------
#$Date: 2016-03-21 13:02:18 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178690 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/01/4080114.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4080114
loop_
_publ_author_name
'Nocton, Grégory'
'Booth, Corwin H.'
'Maron, Laurent'
'Andersen, Richard A.'
_publ_section_title
;
 Thermal Dihydrogen Elimination from Cp*2Yb(4,5-diazafluorene)
;
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1150
_journal_page_last               1158
_journal_paper_doi               10.1021/om300876b
_journal_volume                  32
_journal_year                    2013
_chemical_formula_sum            'C74 H84 N4 Yb2'
_chemical_formula_weight         1375.53
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 132.711(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.330(4)
_cell_length_b                   25.817(4)
_cell_length_c                   14.995(2)
_cell_measurement_reflns_used    9095
_cell_measurement_temperature    100(1)
_cell_measurement_theta_max      25.3897
_cell_measurement_theta_min      2.4303
_cell_volume                     6067.4(17)
_computing_cell_refinement       'Brucker APEX2 v.2009.1'
_computing_data_collection       'Brucker APEX2 v.2009.1'
_computing_data_reduction        'Brucker APEX2 v.2009.1'
_computing_publication_material  WINGX
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(1)
_diffrn_detector_area_resol_mean 8.366
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker APEX-II'
_diffrn_measurement_method       'φ or ω oscillation scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0640
_diffrn_reflns_av_sigmaI/netI    0.0380
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            45398
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.46
_diffrn_reflns_theta_min         1.52
_exptl_absorpt_coefficient_mu    3.101
_exptl_absorpt_correction_T_max  0.780
_exptl_absorpt_correction_T_min  0.718
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.506
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2456
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.274
_refine_diff_density_min         -0.753
_refine_diff_density_rms         0.117
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     361
_refine_ls_number_reflns         5598
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.061
_refine_ls_R_factor_all          0.0461
_refine_ls_R_factor_gt           0.0310
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0214P)²+40.7256P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0633
_refine_ls_wR_factor_ref         0.0695
_reflns_number_gt                4521
_reflns_number_total             5598
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om300876b_si_002.cif
_cod_data_source_block           4
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4080114
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C10 C 0.6889(3) 0.21482(19) 0.5205(4) 0.0236(11) Uani 1 1 d .
H10A H 0.6980 0.1932 0.4781 0.035 Uiso 1 1 calc R
H10B H 0.7429 0.2264 0.5953 0.035 Uiso 1 1 calc R
H10C H 0.6551 0.2443 0.4710 0.035 Uiso 1 1 calc R
C7 C 0.5160(3) 0.1708(2) 0.6334(4) 0.0258(11) Uani 1 1 d .
H7A H 0.5317 0.2030 0.6759 0.039 Uiso 1 1 calc R
H7B H 0.5263 0.1429 0.6843 0.039 Uiso 1 1 calc R
H7C H 0.4566 0.1716 0.5606 0.039 Uiso 1 1 calc R
C17 C 0.6168(3) 0.0731(2) 0.8383(5) 0.0313(13) Uani 1 1 d .
H17A H 0.5939 0.1029 0.8461 0.047 Uiso 1 1 calc R
H17B H 0.6256 0.0457 0.8892 0.047 Uiso 1 1 calc R
H17C H 0.5775 0.0617 0.7553 0.047 Uiso 1 1 calc R
C31 C 0.8486(3) 0.10312(18) 0.7221(4) 0.0169(10) Uani 1 1 d .
C6 C 0.6322(3) 0.25496(18) 0.6608(4) 0.0216(11) Uani 1 1 d .
H6A H 0.6083 0.2563 0.6966 0.032 Uiso 1 1 calc R
H6B H 0.6052 0.2805 0.5979 0.032 Uiso 1 1 calc R
H6C H 0.6923 0.2618 0.7219 0.032 Uiso 1 1 calc R
Yb1 Yb 0.723017(12) 0.127552(7) 0.741210(16) 0.01437(7) Uani 1 1 d .
C30 C 0.8694(3) 0.15383(17) 0.7672(4) 0.0148(10) Uani 1 1 d .
C4 C 0.6104(3) 0.13399(18) 0.5038(4) 0.0192(10) Uani 1 1 d .
C25 C 0.9652(3) 0.12902(18) 0.7488(4) 0.0155(9) Uani 1 1 d .
C15 C 0.8310(3) 0.1238(2) 0.9778(4) 0.0327(13) Uani 1 1 d .
N2 N 0.8308(2) 0.18334(14) 0.7936(3) 0.0169(8) Uani 1 1 d .
C28 C 0.9313(3) 0.25011(18) 0.8543(4) 0.0185(10) Uani 1 1 d .
H28 H 0.9504 0.2836 0.8835 0.022 Uiso 1 1 calc R
C24 C 0.9084(3) 0.08786(17) 0.7114(4) 0.0166(10) Uani 1 1 d .
N1 N 0.7846(2) 0.07294(15) 0.6935(3) 0.0182(8) Uani 1 1 d .
C3 C 0.5647(3) 0.12019(19) 0.5381(4) 0.0201(10) Uani 1 1 d .
C18 C 0.7228(3) -0.00202(18) 0.8253(4) 0.0215(11) Uani 1 1 d .
H18A H 0.6642 -0.0065 0.7855 0.032 Uiso 1 1 calc R
H18B H 0.7575 -0.0268 0.8899 0.032 Uiso 1 1 calc R
H18C H 0.7287 -0.0072 0.7678 0.032 Uiso 1 1 calc R
C13 C 0.7511(3) 0.05163(18) 0.8763(4) 0.0172(10) Uani 1 1 d .
C27 C 0.9722(3) 0.21993(18) 0.8313(4) 0.0183(10) Uani 1 1 d .
H27 H 1.0198 0.2324 0.8471 0.022 Uiso 1 1 calc R
C19 C 0.9087(3) 0.0487(2) 0.9726(5) 0.0402(15) Uani 1 1 d .
H19A H 0.8934 0.0148 0.9368 0.060 Uiso 1 1 calc R
H19B H 0.9532 0.0457 1.0592 0.060 Uiso 1 1 calc R
H19C H 0.9284 0.0693 0.9425 0.060 Uiso 1 1 calc R
C21 C 0.7775(3) 0.02565(18) 0.6521(4) 0.0202(10) Uani 1 1 d .
H21 H 0.7354 0.0038 0.6336 0.024 Uiso 1 1 calc R
C23 C 0.8946(3) 0.03773(18) 0.6626(4) 0.0187(10) Uani 1 1 d .
H23 H 0.9285 0.0254 0.6490 0.022 Uiso 1 1 calc R
C11 C 0.7496(4) 0.1325(2) 0.9374(4) 0.0302(13) Uani 1 1 d .
C29 C 0.8612(3) 0.23090(17) 0.8342(4) 0.0182(10) Uani 1 1 d .
H29 H 0.8348 0.2524 0.8501 0.022 Uiso 1 1 calc R
C5 C 0.6431(3) 0.18462(18) 0.5469(4) 0.0187(10) Uani 1 1 d .
C22 C 0.8305(3) 0.00744(18) 0.6354(4) 0.0209(10) Uani 1 1 d .
H22 H 0.8223 -0.0258 0.6053 0.025 Uiso 1 1 calc R
C1 C 0.6178(3) 0.20222(17) 0.6079(4) 0.0161(10) Uani 1 1 d .
C8 C 0.5148(3) 0.0708(2) 0.5010(5) 0.0286(12) Uani 1 1 d .
H8A H 0.4896 0.0699 0.5350 0.043 Uiso 1 1 calc R
H8B H 0.5524 0.0417 0.5304 0.043 Uiso 1 1 calc R
H8C H 0.4708 0.0692 0.4141 0.043 Uiso 1 1 calc R
C26 C 0.9409(3) 0.16988(18) 0.7835(4) 0.0168(10) Uani 1 1 d .
C2 C 0.5682(3) 0.16267(18) 0.6011(4) 0.0177(10) Uani 1 1 d .
C9 C 0.6163(3) 0.1031(2) 0.4247(4) 0.0297(12) Uani 1 1 d .
H9A H 0.5897 0.0700 0.4075 0.045 Uiso 1 1 calc R
H9B H 0.6752 0.0982 0.4661 0.045 Uiso 1 1 calc R
H9C H 0.5878 0.1214 0.3501 0.045 Uiso 1 1 calc R
C14 C 0.8321(3) 0.0740(2) 0.9402(4) 0.0254(12) Uani 1 1 d .
C12 C 0.7003(3) 0.08703(18) 0.8762(4) 0.0205(10) Uani 1 1 d .
C20 C 0.9073(4) 0.1592(3) 1.0590(5) 0.064(2) Uani 1 1 d .
H20A H 0.8904 0.1910 1.0710 0.096 Uiso 1 1 calc R
H20B H 0.9291 0.1666 1.0217 0.096 Uiso 1 1 calc R
H20C H 0.9507 0.1427 1.1359 0.096 Uiso 1 1 calc R
C16 C 0.7233(5) 0.1796(2) 0.9648(5) 0.0517(19) Uani 1 1 d .
H16A H 0.6650 0.1761 0.9269 0.078 Uiso 1 1 calc R
H16B H 0.7292 0.2100 0.9339 0.078 Uiso 1 1 calc R
H16C H 0.7591 0.1828 1.0510 0.078 Uiso 1 1 calc R
C1S C 0.7081(3) 0.1298(2) 1.2010(4) 0.0284(12) Uani 1 1 d .
H1S H 0.6536 0.1355 1.1260 0.034 Uiso 1 1 calc R
C2S C 0.7708(3) 0.11020(19) 1.2067(4) 0.0268(12) Uani 1 1 d .
H2S H 0.7586 0.1026 1.1357 0.032 Uiso 1 1 calc R
C6S C 0.7261(3) 0.14108(18) 1.3065(5) 0.0267(12) Uani 1 1 d .
H6S H 0.6837 0.1543 1.3025 0.032 Uiso 1 1 calc R
C3S C 0.8522(3) 0.10182(19) 1.3184(4) 0.0261(11) Uani 1 1 d .
H3S H 0.8946 0.0885 1.3227 0.031 Uiso 1 1 calc R
C4S C 0.8697(3) 0.11341(18) 1.4231(4) 0.0250(11) Uani 1 1 d .
H4S H 0.9244 0.1081 1.4982 0.030 Uiso 1 1 calc R
C5S C 0.8071(3) 0.13276(19) 1.4178(4) 0.0258(11) Uani 1 1 d .
H5S H 0.8193 0.1402 1.4889 0.031 Uiso 1 1 calc R
CT01 C 0.6008 0.1607 0.5596 0.010 Uiso 0.00 1 d P
CT02 C 0.7728 0.0938 0.9215 0.010 Uiso 0.00 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
N1 C31 C30 127.4(4) .
N1 C31 C24 125.5(4) .
C30 C31 C24 107.1(4) .
N1 C31 Yb1 51.0(2) .
C30 C31 Yb1 76.4(3) .
C24 C31 Yb1 176.4(3) .
CT02 Yb1 CT01 141.202(12) .
CT02 Yb1 N1 102.89(9) .
CT01 Yb1 N1 106.33(9) .
CT02 Yb1 N2 105.78(9) .
CT01 Yb1 N2 103.45(9) .
N1 Yb1 N2 81.21(13) .
CT02 Yb1 C13 27.65(10) .
CT01 Yb1 C13 133.17(10) .
N1 Yb1 C13 84.43(14) .
N2 Yb1 C13 123.33(13) .
CT02 Yb1 C1 131.16(10) .
CT01 Yb1 C1 27.78(10) .
N1 Yb1 C1 125.84(14) .
N2 Yb1 C1 86.60(13) .
C13 Yb1 C1 142.39(15) .
CT02 Yb1 C11 27.74(12) .
CT01 Yb1 C11 121.60(13) .
N1 Yb1 C11 129.68(15) .
N2 Yb1 C11 100.33(15) .
C13 Yb1 C11 52.49(15) .
C1 Yb1 C11 104.36(16) .
CT02 Yb1 C2 113.78(10) .
CT01 Yb1 C2 27.79(10) .
N1 Yb1 C2 129.17(13) .
N2 Yb1 C2 118.40(14) .
C13 Yb1 C2 113.04(14) .
C1 Yb1 C2 31.93(14) .
C11 Yb1 C2 94.61(16) .
CT02 Yb1 C12 27.67(11) .
CT01 Yb1 C12 114.29(11) .
N1 Yb1 C12 115.74(14) .
N2 Yb1 C12 130.01(14) .
C13 Yb1 C12 31.74(14) .
C1 Yb1 C12 112.36(15) .
C11 Yb1 C12 31.71(15) .
C2 Yb1 C12 87.96(15) .
CT02 Yb1 C3 123.08(10) .
CT01 Yb1 C3 27.65(11) .
N1 Yb1 C3 98.61(14) .
N2 Yb1 C3 129.40(14) .
C13 Yb1 C3 106.82(15) .
C1 Yb1 C3 52.51(14) .
C11 Yb1 C3 116.30(17) .
C2 Yb1 C3 31.63(14) .
C12 Yb1 C3 95.91(15) .
CT02 Yb1 C14 27.54(12) .
CT01 Yb1 C14 164.67(11) .
N1 Yb1 C14 77.37(15) .
N2 Yb1 C14 91.79(14) .
C13 Yb1 C14 31.55(15) .
C1 Yb1 C14 155.98(16) .
C11 Yb1 C14 52.36(17) .
C2 Yb1 C14 140.26(15) .
C12 Yb1 C14 52.30(15) .
C3 Yb1 C14 137.97(15) .
CT02 Yb1 C15 27.30(11) .
CT01 Yb1 C15 150.19(14) .
N1 Yb1 C15 103.40(16) .
N2 Yb1 C15 78.86(14) .
C13 Yb1 C15 52.00(15) .
C1 Yb1 C15 125.60(17) .
C11 Yb1 C15 31.59(17) .
C2 Yb1 C15 125.37(17) .
C12 Yb1 C15 52.10(16) .
C3 Yb1 C15 146.81(16) .
C14 Yb1 C15 31.33(17) .
CT02 Yb1 C5 162.76(11) .
CT01 Yb1 C5 27.54(10) .
N1 Yb1 C5 94.34(14) .
N2 Yb1 C5 77.15(13) .
C13 Yb1 C5 158.76(14) .
C1 Yb1 C5 31.62(14) .
C11 Yb1 C5 135.43(16) .
C2 Yb1 C5 52.44(14) .
C12 Yb1 C5 140.36(15) .
C3 Yb1 C5 52.30(14) .
C14 Yb1 C5 167.19(15) .
C15 Yb1 C5 147.46(16) .
CT02 Yb1 C4 152.44(11) .
CT01 Yb1 C4 27.33(10) .
N1 Yb1 C4 79.09(13) .
N2 Yb1 C4 101.69(14) .
C13 Yb1 C4 128.69(14) .
C1 Yb1 C4 52.15(14) .
C11 Yb1 C4 146.20(17) .
C2 Yb1 C4 52.21(14) .
C12 Yb1 C4 126.87(15) .
C3 Yb1 C4 31.58(14) .
C14 Yb1 C4 150.66(16) .
C15 Yb1 C4 177.50(17) .
C5 Yb1 C4 31.36(14) .
N2 C30 C31 127.4(4) .
N2 C30 C26 124.9(4) .
C31 C30 C26 107.7(4) .
N2 C30 Yb1 51.2(2) .
C31 C30 Yb1 76.2(3) .
C26 C30 Yb1 176.1(3) .
CT01 C4 C5 54.2(3) .
CT01 C4 C3 54.0(3) .
C5 C4 C3 108.2(4) .
CT01 C4 C9 175.2(4) .
C5 C4 C9 124.8(4) .
C3 C4 C9 126.7(4) .
CT01 C4 Yb1 61.56(17) .
C5 C4 Yb1 74.0(2) .
C3 C4 Yb1 73.4(2) .
C9 C4 Yb1 123.2(3) .
C24 C25 C26 106.2(4) .
C24 C25 C25 126.4(3) 2_756
C26 C25 C25 127.4(3) 2_756
CT02 C15 C14 54.4(3) .
CT02 C15 C11 54.2(3) .
C14 C15 C11 108.6(4) .
CT02 C15 C20 174.8(5) .
C14 C15 C20 125.1(6) .
C11 C15 C20 126.0(6) .
CT02 C15 Yb1 61.89(19) .
C14 C15 Yb1 74.3(3) .
C11 C15 Yb1 73.6(3) .
C20 C15 Yb1 123.3(3) .
C29 N2 C30 116.5(4) .
C29 N2 Yb1 141.5(3) .
C30 N2 Yb1 102.0(3) .
C27 C28 C29 120.7(4) .
C25 C24 C23 135.8(4) .
C25 C24 C31 109.5(4) .
C23 C24 C31 114.6(4) .
C21 N1 C31 116.3(4) .
C21 N1 Yb1 141.6(3) .
C31 N1 Yb1 102.1(3) .
CT01 C3 C2 54.2(3) .
CT01 C3 C4 53.8(3) .
C2 C3 C4 108.0(4) .
CT01 C3 C8 175.5(4) .
C2 C3 C8 127.4(4) .
C4 C3 C8 124.4(4) .
CT01 C3 Yb1 62.45(17) .
C2 C3 Yb1 73.9(2) .
C4 C3 Yb1 75.0(2) .
C8 C3 Yb1 121.7(3) .
CT02 C13 C14 54.4(3) .
CT02 C13 C12 54.2(3) .
C14 C13 C12 108.6(4) .
CT02 C13 C18 176.0(4) .
C14 C13 C18 127.6(4) .
C12 C13 C18 123.6(4) .
CT02 C13 Yb1 63.17(19) .
C14 C13 Yb1 75.4(3) .
C12 C13 Yb1 74.9(3) .
C18 C13 Yb1 120.2(3) .
C28 C27 C26 119.0(4) .
N1 C21 C22 122.9(4) .
C22 C23 C24 119.3(4) .
CT02 C11 C15 53.6(3) .
CT02 C11 C12 54.0(3) .
C15 C11 C12 107.6(5) .
CT02 C11 C16 176.5(4) .
C15 C11 C16 125.8(5) .
C12 C11 C16 126.4(5) .
CT02 C11 Yb1 62.60(19) .
C15 C11 Yb1 74.9(3) .
C12 C11 Yb1 74.4(3) .
C16 C11 Yb1 120.8(3) .
N2 C29 C28 123.0(4) .
CT01 C5 C4 53.9(3) .
CT01 C5 C1 53.9(3) .
C4 C5 C1 107.8(4) .
CT01 C5 C10 175.3(4) .
C4 C5 C10 124.6(4) .
C1 C5 C10 127.3(4) .
CT01 C5 Yb1 61.92(18) .
C4 C5 Yb1 74.6(2) .
C1 C5 Yb1 72.9(2) .
C10 C5 Yb1 122.6(3) .
C23 C22 C21 121.3(4) .
CT01 C1 C5 54.2(3) .
CT01 C1 C2 54.1(3) .
C5 C1 C2 108.3(4) .
CT01 C1 C6 175.8(4) .
C5 C1 C6 127.1(4) .
C2 C1 C6 124.4(4) .
CT01 C1 Yb1 63.27(18) .
C5 C1 Yb1 75.4(3) .
C2 C1 Yb1 74.5(3) .
C6 C1 Yb1 120.7(3) .
C27 C26 C25 134.8(4) .
C27 C26 C30 115.8(4) .
C25 C26 C30 109.4(4) .
CT01 C2 C3 54.1(3) .
CT01 C2 C1 53.6(3) .
C3 C2 C1 107.7(4) .
CT01 C2 C7 169.9(4) .
C3 C2 C7 127.5(4) .
C1 C2 C7 123.7(4) .
CT01 C2 Yb1 62.72(19) .
C3 C2 Yb1 74.4(3) .
C1 C2 Yb1 73.5(3) .
C7 C2 Yb1 127.1(3) .
CT02 C14 C15 53.8(3) .
CT02 C14 C13 53.8(3) .
C15 C14 C13 107.6(5) .
CT02 C14 C19 175.9(4) .
C15 C14 C19 125.2(5) .
C13 C14 C19 127.0(5) .
CT02 C14 Yb1 61.95(19) .
C15 C14 Yb1 74.4(3) .
C13 C14 Yb1 73.1(3) .
C19 C14 Yb1 122.1(3) .
CT02 C12 C13 53.6(3) .
CT02 C12 C11 54.0(3) .
C13 C12 C11 107.6(4) .
CT02 C12 C17 170.4(4) .
C13 C12 C17 123.8(4) .
C11 C12 C17 127.7(5) .
CT02 C12 Yb1 62.36(19) .
C13 C12 Yb1 73.4(3) .
C11 C12 Yb1 73.9(3) .
C17 C12 Yb1 127.0(3) .
C2S C1S C6S 120.1(5) .
C1S C2S C3S 119.9(5) .
C5S C6S C1S 119.9(5) .
C4S C3S C2S 119.6(5) .
C5S C4S C3S 120.6(5) .
C4S C5S C6S 119.7(5) .
C1 CT01 C4 143.7(3) .
C1 CT01 C3 144.0(3) .
C4 CT01 C3 72.3(3) .
C1 CT01 C2 72.3(3) .
C4 CT01 C2 144.0(3) .
C3 CT01 C2 71.7(3) .
C1 CT01 C5 71.9(3) .
C4 CT01 C5 71.8(3) .
C3 CT01 C5 144.1(3) .
C2 CT01 C5 144.2(3) .
C1 CT01 Yb1 89.0(2) .
C4 CT01 Yb1 91.1(2) .
C3 CT01 Yb1 89.9(2) .
C2 CT01 Yb1 89.5(2) .
C5 CT01 Yb1 90.5(2) .
C15 CT02 C13 143.7(4) .
C15 CT02 C14 71.8(4) .
C13 CT02 C14 71.9(3) .
C15 CT02 C12 144.2(4) .
C13 CT02 C12 72.2(3) .
C14 CT02 C12 144.0(3) .
C15 CT02 C11 72.2(4) .
C13 CT02 C11 144.1(3) .
C14 CT02 C11 144.0(4) .
C12 CT02 C11 72.0(3) .
C15 CT02 Yb1 90.8(2) .
C13 CT02 Yb1 89.2(2) .
C14 CT02 Yb1 90.5(2) .
C12 CT02 Yb1 90.0(2) .
C11 CT02 Yb1 89.7(2) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C10 C5 1.498(6) .
C7 C2 1.499(7) .
C17 C12 1.500(7) .
C31 N1 1.365(6) .
C31 C30 1.400(6) .
C31 C24 1.444(6) .
C31 Yb1 2.949(5) .
C6 C1 1.499(6) .
Yb1 CT02 2.3027(4) .
Yb1 CT01 2.3055(3) .
Yb1 N1 2.345(4) .
Yb1 N2 2.351(4) .
Yb1 C13 2.580(4) .
Yb1 C1 2.581(4) .
Yb1 C11 2.594(5) .
Yb1 C2 2.594(4) .
Yb1 C12 2.599(5) .
Yb1 C3 2.600(4) .
Yb1 C14 2.609(4) .
Yb1 C15 2.610(5) .
Yb1 C5 2.613(4) .
Yb1 C4 2.621(4) .
C30 N2 1.363(6) .
C30 C26 1.432(6) .
C4 CT01 1.204(5) .
C4 C5 1.415(6) .
C4 C3 1.421(6) .
C4 C9 1.504(6) .
C25 C24 1.410(6) .
C25 C26 1.419(6) .
C25 C25 1.463(9) 2_756
C15 CT02 1.197(5) .
C15 C14 1.409(8) .
C15 C11 1.417(8) .
C15 C20 1.509(7) .
N2 C29 1.328(6) .
C28 C27 1.377(6) .
C28 C29 1.400(6) .
C24 C23 1.416(6) .
N1 C21 1.331(6) .
C3 CT01 1.207(5) .
C3 C2 1.416(6) .
C3 C8 1.506(6) .
C18 C13 1.497(6) .
C13 CT02 1.197(5) .
C13 C14 1.411(7) .
C13 C12 1.416(6) .
C27 C26 1.407(6) .
C19 C14 1.503(7) .
C21 C22 1.396(7) .
C23 C22 1.375(6) .
C11 CT02 1.207(5) .
C11 C12 1.419(7) .
C11 C16 1.509(7) .
C5 CT01 1.208(5) .
C5 C1 1.415(6) .
C1 CT01 1.203(5) .
C1 C2 1.423(6) .
C2 CT01 1.210(5) .
C14 CT02 1.206(5) .
C12 CT02 1.207(5) .
C1S C2S 1.377(7) .
C1S C6S 1.384(7) .
C2S C3S 1.386(7) .
C6S C5S 1.380(7) .
C3S C4S 1.377(7) .
C4S C5S 1.377(7) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
N1 C31 C30 N2 1.0(7) .
C24 C31 C30 N2 -178.7(4) .
Yb1 C31 C30 N2 0.6(4) .
N1 C31 C30 C26 -179.9(4) .
C24 C31 C30 C26 0.3(5) .
Yb1 C31 C30 C26 179.7(3) .
N1 C31 C30 Yb1 0.4(4) .
C24 C31 C30 Yb1 -179.3(3) .
CT02 Yb1 C30 N2 -87.2(3) .
CT01 Yb1 C30 N2 83.2(3) .
N1 Yb1 C30 N2 -179.6(3) .
C13 Yb1 C30 N2 -116.6(3) .
C1 Yb1 C30 N2 55.0(3) .
C11 Yb1 C30 N2 -58.1(3) .
C2 Yb1 C30 N2 67.0(3) .
C12 Yb1 C30 N2 -88.6(3) .
C3 Yb1 C30 N2 107.5(3) .
C14 Yb1 C30 N2 -102.2(3) .
C15 Yb1 C30 N2 -70.9(3) .
C5 Yb1 C30 N2 78.6(3) .
C4 Yb1 C30 N2 107.2(3) .
CT02 Yb1 C30 C31 92.1(2) .
CT01 Yb1 C30 C31 -97.4(2) .
N1 Yb1 C30 C31 -0.3(2) .
N2 Yb1 C30 C31 179.4(4) .
C13 Yb1 C30 C31 62.8(3) .
C1 Yb1 C30 C31 -125.6(2) .
C11 Yb1 C30 C31 121.3(2) .
C2 Yb1 C30 C31 -113.6(3) .
C12 Yb1 C30 C31 90.7(3) .
C3 Yb1 C30 C31 -73.2(3) .
C14 Yb1 C30 C31 77.2(3) .
C15 Yb1 C30 C31 108.5(3) .
C5 Yb1 C30 C31 -102.0(2) .
C4 Yb1 C30 C31 -73.4(2) .
CT02 Yb1 C30 C26 -84(5) .
CT01 Yb1 C30 C26 87(4) .
N1 Yb1 C30 C26 -176(5) .
N2 Yb1 C30 C26 4(4) .
C13 Yb1 C30 C26 -113(4) .
C1 Yb1 C30 C26 59(5) .
C11 Yb1 C30 C26 -54(5) .
C2 Yb1 C30 C26 71(5) .
C12 Yb1 C30 C26 -85(5) .
C3 Yb1 C30 C26 111(4) .
C14 Yb1 C30 C26 -99(5) .
C15 Yb1 C30 C26 -67(4) .
C5 Yb1 C30 C26 82(5) .
C4 Yb1 C30 C26 111(4) .
CT02 Yb1 C4 CT01 87.8(3) .
N1 Yb1 C4 CT01 -175.2(2) .
N2 Yb1 C4 CT01 -96.7(2) .
C13 Yb1 C4 CT01 111.1(2) .
C1 Yb1 C4 CT01 -20.45(18) .
C11 Yb1 C4 CT01 33.0(4) .
C2 Yb1 C4 CT01 20.30(18) .
C12 Yb1 C4 CT01 70.7(3) .
C3 Yb1 C4 CT01 57.6(3) .
C14 Yb1 C4 CT01 147.6(3) .
C15 Yb1 C4 CT01 6(4) .
C5 Yb1 C4 CT01 -57.6(3) .
CT02 Yb1 C4 C5 145.4(2) .
CT01 Yb1 C4 C5 57.6(3) .
N1 Yb1 C4 C5 -117.7(3) .
N2 Yb1 C4 C5 -39.1(3) .
C13 Yb1 C4 C5 168.7(3) .
C1 Yb1 C4 C5 37.1(3) .
C11 Yb1 C4 C5 90.6(4) .
C2 Yb1 C4 C5 77.9(3) .
C12 Yb1 C4 C5 128.2(3) .
C3 Yb1 C4 C5 115.1(4) .
C14 Yb1 C4 C5 -154.8(3) .
C15 Yb1 C4 C5 64(4) .
CT02 Yb1 C4 C3 30.2(4) .
CT01 Yb1 C4 C3 -57.6(3) .
N1 Yb1 C4 C3 127.2(3) .
N2 Yb1 C4 C3 -154.3(3) .
C13 Yb1 C4 C3 53.5(3) .
C1 Yb1 C4 C3 -78.0(3) .
C11 Yb1 C4 C3 -24.6(4) .
C2 Yb1 C4 C3 -37.3(3) .
C12 Yb1 C4 C3 13.1(3) .
C14 Yb1 C4 C3 90.0(4) .
C15 Yb1 C4 C3 -52(4) .
C5 Yb1 C4 C3 -115.1(4) .
CT02 Yb1 C4 C9 -93.2(4) .
CT01 Yb1 C4 C9 179.1(6) .
N1 Yb1 C4 C9 3.8(4) .
N2 Yb1 C4 C9 82.4(4) .
C13 Yb1 C4 C9 -69.9(4) .
C1 Yb1 C4 C9 158.6(5) .
C11 Yb1 C4 C9 -148.0(4) .
C2 Yb1 C4 C9 -160.6(5) .
C12 Yb1 C4 C9 -110.3(4) .
C3 Yb1 C4 C9 -123.4(5) .
C14 Yb1 C4 C9 -33.3(6) .
C15 Yb1 C4 C9 -175(3) .
C5 Yb1 C4 C9 121.5(5) .
CT01 Yb1 C15 CT02 92.1(3) .
N1 Yb1 C15 CT02 -92.2(3) .
N2 Yb1 C15 CT02 -170.2(3) .
C13 Yb1 C15 CT02 -20.4(2) .
C1 Yb1 C15 CT02 112.2(3) .
C11 Yb1 C15 CT02 57.8(3) .
C2 Yb1 C15 CT02 72.7(3) .
C12 Yb1 C15 CT02 20.2(2) .
C3 Yb1 C15 CT02 38.0(5) .
C14 Yb1 C15 CT02 -57.6(3) .
C5 Yb1 C15 CT02 146.6(2) .
C4 Yb1 C15 CT02 87(4) .
CT02 Yb1 C15 C14 57.6(3) .
CT01 Yb1 C15 C14 149.7(2) .
N1 Yb1 C15 C14 -34.6(3) .
N2 Yb1 C15 C14 -112.6(3) .
C13 Yb1 C15 C14 37.2(3) .
C1 Yb1 C15 C14 169.8(3) .
C11 Yb1 C15 C14 115.4(4) .
C2 Yb1 C15 C14 130.3(3) .
C12 Yb1 C15 C14 77.8(3) .
C3 Yb1 C15 C14 95.6(4) .
C5 Yb1 C15 C14 -155.8(3) .
C4 Yb1 C15 C14 144(3) .
CT02 Yb1 C15 C11 -57.8(3) .
CT01 Yb1 C15 C11 34.3(4) .
N1 Yb1 C15 C11 -150.0(3) .
N2 Yb1 C15 C11 132.0(3) .
C13 Yb1 C15 C11 -78.2(3) .
C1 Yb1 C15 C11 54.4(3) .
C2 Yb1 C15 C11 14.9(4) .
C12 Yb1 C15 C11 -37.6(3) .
C3 Yb1 C15 C11 -19.8(5) .
C14 Yb1 C15 C11 -115.4(4) .
C5 Yb1 C15 C11 88.8(4) .
C4 Yb1 C15 C11 29(4) .
CT02 Yb1 C15 C20 179.6(8) .
CT01 Yb1 C15 C20 -88.3(6) .
N1 Yb1 C15 C20 87.4(6) .
N2 Yb1 C15 C20 9.4(5) .
C13 Yb1 C15 C20 159.2(6) .
C1 Yb1 C15 C20 -68.2(6) .
C11 Yb1 C15 C20 -122.6(7) .
C2 Yb1 C15 C20 -107.7(6) .
C12 Yb1 C15 C20 -160.2(6) .
C3 Yb1 C15 C20 -142.4(5) .
C14 Yb1 C15 C20 122.0(7) .
C5 Yb1 C15 C20 -33.8(7) .
C4 Yb1 C15 C20 -94(4) .
C31 C30 N2 C29 -179.2(4) .
C26 C30 N2 C29 1.9(6) .
Yb1 C30 N2 C29 -178.4(4) .
C31 C30 N2 Yb1 -0.8(5) .
C26 C30 N2 Yb1 -179.7(4) .
CT02 Yb1 N2 C29 -80.9(5) .
CT01 Yb1 N2 C29 73.3(5) .
N1 Yb1 N2 C29 178.1(5) .
C13 Yb1 N2 C29 -104.6(5) .
C1 Yb1 N2 C29 51.0(5) .
C11 Yb1 N2 C29 -53.0(5) .
C2 Yb1 N2 C29 48.1(5) .
C12 Yb1 N2 C29 -65.6(5) .
C3 Yb1 N2 C29 84.1(5) .
C14 Yb1 N2 C29 -105.0(5) .
C15 Yb1 N2 C29 -76.3(5) .
C5 Yb1 N2 C29 81.5(5) .
C4 Yb1 N2 C29 101.2(5) .
CT02 Yb1 N2 C30 101.3(2) .
CT01 Yb1 N2 C30 -104.5(2) .
N1 Yb1 N2 C30 0.3(3) .
C13 Yb1 N2 C30 77.6(3) .
C1 Yb1 N2 C30 -126.8(3) .
C11 Yb1 N2 C30 129.2(3) .
C2 Yb1 N2 C30 -129.7(3) .
C12 Yb1 N2 C30 116.7(3) .
C3 Yb1 N2 C30 -93.7(3) .
C14 Yb1 N2 C30 77.2(3) .
C15 Yb1 N2 C30 105.9(3) .
C5 Yb1 N2 C30 -96.2(3) .
C4 Yb1 N2 C30 -76.6(3) .
C26 C25 C24 C23 177.0(5) .
C25 C25 C24 C23 -3.1(9) 2_756
C26 C25 C24 C31 0.3(5) .
C25 C25 C24 C31 -179.8(5) 2_756
N1 C31 C24 C25 179.8(4) .
C30 C31 C24 C25 -0.4(5) .
Yb1 C31 C24 C25 -170(5) .
N1 C31 C24 C23 2.3(6) .
C30 C31 C24 C23 -177.9(4) .
Yb1 C31 C24 C23 12(5) .
C30 C31 N1 C21 -179.9(4) .
C24 C31 N1 C21 -0.1(6) .
Yb1 C31 N1 C21 -179.3(4) .
C30 C31 N1 Yb1 -0.6(5) .
C24 C31 N1 Yb1 179.2(4) .
CT02 Yb1 N1 C21 74.8(5) .
CT01 Yb1 N1 C21 -79.4(5) .
N2 Yb1 N1 C21 179.1(5) .
C13 Yb1 N1 C21 54.1(5) .
C1 Yb1 N1 C21 -101.6(5) .
C11 Yb1 N1 C21 82.9(5) .
C2 Yb1 N1 C21 -61.2(5) .
C12 Yb1 N1 C21 48.7(5) .
C3 Yb1 N1 C21 -52.1(5) .
C14 Yb1 N1 C21 85.3(5) .
C15 Yb1 N1 C21 102.8(5) .
C5 Yb1 N1 C21 -104.6(5) .
C4 Yb1 N1 C21 -77.1(5) .
CT02 Yb1 N1 C31 -104.2(2) .
CT01 Yb1 N1 C31 101.6(2) .
N2 Yb1 N1 C31 0.1(3) .
C13 Yb1 N1 C31 -124.9(3) .
C1 Yb1 N1 C31 79.4(3) .
C11 Yb1 N1 C31 -96.1(3) .
C2 Yb1 N1 C31 119.7(3) .
C12 Yb1 N1 C31 -130.3(3) .
C3 Yb1 N1 C31 128.9(3) .
C14 Yb1 N1 C31 -93.8(3) .
C15 Yb1 N1 C31 -76.2(3) .
C5 Yb1 N1 C31 76.4(3) .
C4 Yb1 N1 C31 103.9(3) .
C5 C4 C3 CT01 0.2(3) .
C9 C4 C3 CT01 -174.1(5) .
Yb1 C4 C3 CT01 66.57(16) .
CT01 C4 C3 C2 0.6(3) .
C5 C4 C3 C2 0.8(5) .
C9 C4 C3 C2 -173.5(4) .
Yb1 C4 C3 C2 67.2(3) .
CT01 C4 C3 C8 175.0(5) .
C5 C4 C3 C8 175.2(4) .
C9 C4 C3 C8 0.9(7) .
Yb1 C4 C3 C8 -118.4(4) .
CT01 C4 C3 Yb1 -66.57(16) .
C5 C4 C3 Yb1 -66.3(3) .
C9 C4 C3 Yb1 119.3(4) .
CT02 Yb1 C3 CT01 139.53(15) .
N1 Yb1 C3 CT01 -108.9(2) .
N2 Yb1 C3 CT01 -23.2(3) .
C13 Yb1 C3 CT01 164.4(2) .
C1 Yb1 C3 CT01 20.17(18) .
C11 Yb1 C3 CT01 108.4(2) .
C2 Yb1 C3 CT01 57.6(3) .
C12 Yb1 C3 CT01 133.9(2) .
C14 Yb1 C3 CT01 170.5(2) .
C15 Yb1 C3 CT01 119.8(3) .
C5 Yb1 C3 CT01 -20.05(18) .
C4 Yb1 C3 CT01 -56.6(3) .
CT02 Yb1 C3 C2 81.9(3) .
CT01 Yb1 C3 C2 -57.6(3) .
N1 Yb1 C3 C2 -166.5(3) .
N2 Yb1 C3 C2 -80.8(3) .
C13 Yb1 C3 C2 106.8(3) .
C1 Yb1 C3 C2 -37.4(3) .
C11 Yb1 C3 C2 50.9(3) .
C12 Yb1 C3 C2 76.3(3) .
C14 Yb1 C3 C2 112.9(3) .
C15 Yb1 C3 C2 62.2(4) .
C5 Yb1 C3 C2 -77.6(3) .
C4 Yb1 C3 C2 -114.2(4) .
CT02 Yb1 C3 C4 -163.9(2) .
CT01 Yb1 C3 C4 56.6(3) .
N1 Yb1 C3 C4 -52.3(3) .
N2 Yb1 C3 C4 33.4(3) .
C13 Yb1 C3 C4 -139.0(3) .
C1 Yb1 C3 C4 76.8(3) .
C11 Yb1 C3 C4 165.0(3) .
C2 Yb1 C3 C4 114.2(4) .
C12 Yb1 C3 C4 -169.5(3) .
C14 Yb1 C3 C4 -133.0(3) .
C15 Yb1 C3 C4 176.4(3) .
C5 Yb1 C3 C4 36.5(3) .
CT02 Yb1 C3 C8 -42.4(4) .
CT01 Yb1 C3 C8 178.0(5) .
N1 Yb1 C3 C8 69.1(4) .
N2 Yb1 C3 C8 154.8(3) .
C13 Yb1 C3 C8 -17.6(4) .
C1 Yb1 C3 C8 -161.8(5) .
C11 Yb1 C3 C8 -73.5(4) .
C2 Yb1 C3 C8 -124.4(5) .
C12 Yb1 C3 C8 -48.1(4) .
C14 Yb1 C3 C8 -11.5(5) .
C15 Yb1 C3 C8 -62.1(5) .
C5 Yb1 C3 C8 158.0(5) .
C4 Yb1 C3 C8 121.4(5) .
CT01 Yb1 C13 CT02 -120.80(17) .
N1 Yb1 C13 CT02 132.0(2) .
N2 Yb1 C13 CT02 56.4(3) .
C1 Yb1 C13 CT02 -81.2(3) .
C11 Yb1 C13 CT02 -20.1(2) .
C2 Yb1 C13 CT02 -97.6(2) .
C12 Yb1 C13 CT02 -57.2(3) .
C3 Yb1 C13 CT02 -130.7(2) .
C14 Yb1 C13 CT02 57.1(3) .
C15 Yb1 C13 CT02 20.2(2) .
C5 Yb1 C13 CT02 -140.4(3) .
C4 Yb1 C13 CT02 -156.77(18) .
CT02 Yb1 C13 C14 -57.1(3) .
CT01 Yb1 C13 C14 -177.9(2) .
N1 Yb1 C13 C14 74.9(3) .
N2 Yb1 C13 C14 -0.8(4) .
C1 Yb1 C13 C14 -138.3(3) .
C11 Yb1 C13 C14 -77.2(3) .
C2 Yb1 C13 C14 -154.7(3) .
C12 Yb1 C13 C14 -114.3(4) .
C3 Yb1 C13 C14 172.2(3) .
C15 Yb1 C13 C14 -37.0(3) .
C5 Yb1 C13 C14 162.5(4) .
C4 Yb1 C13 C14 146.1(3) .
CT02 Yb1 C13 C12 57.2(3) .
CT01 Yb1 C13 C12 -63.6(3) .
N1 Yb1 C13 C12 -170.8(3) .
N2 Yb1 C13 C12 113.5(3) .
C1 Yb1 C13 C12 -24.0(4) .
C11 Yb1 C13 C12 37.1(3) .
C2 Yb1 C13 C12 -40.4(3) .
C3 Yb1 C13 C12 -73.5(3) .
C14 Yb1 C13 C12 114.3(4) .
C15 Yb1 C13 C12 77.4(3) .
C5 Yb1 C13 C12 -83.2(5) .
C4 Yb1 C13 C12 -99.6(3) .
CT02 Yb1 C13 C18 177.6(5) .
CT01 Yb1 C13 C18 56.8(4) .
N1 Yb1 C13 C18 -50.4(4) .
N2 Yb1 C13 C18 -126.0(3) .
C1 Yb1 C13 C18 96.4(4) .
C11 Yb1 C13 C18 157.5(4) .
C2 Yb1 C13 C18 80.0(4) .
C12 Yb1 C13 C18 120.4(5) .
C3 Yb1 C13 C18 46.9(4) .
C14 Yb1 C13 C18 -125.3(5) .
C15 Yb1 C13 C18 -162.2(4) .
C5 Yb1 C13 C18 37.2(6) .
C4 Yb1 C13 C18 20.8(4) .
C29 C28 C27 C26 2.0(7) .
C31 N1 C21 C22 -1.5(6) .
Yb1 N1 C21 C22 179.6(3) .
C25 C24 C23 C22 -179.6(5) .
C31 C24 C23 C22 -2.9(6) .
C14 C15 C11 CT02 0.3(3) .
C20 C15 C11 CT02 -173.6(6) .
Yb1 C15 C11 CT02 66.87(17) .
CT02 C15 C11 C12 0.9(3) .
C14 C15 C11 C12 1.2(5) .
C20 C15 C11 C12 -172.7(5) .
Yb1 C15 C11 C12 67.8(3) .
CT02 C15 C11 C16 175.8(5) .
C14 C15 C11 C16 176.1(4) .
C20 C15 C11 C16 2.2(8) .
Yb1 C15 C11 C16 -117.3(5) .
CT02 C15 C11 Yb1 -66.87(17) .
C14 C15 C11 Yb1 -66.6(3) .
C20 C15 C11 Yb1 119.6(5) .
CT01 Yb1 C11 CT02 142.75(19) .
N1 Yb1 C11 CT02 -17.2(4) .
N2 Yb1 C11 CT02 -104.3(2) .
C13 Yb1 C11 CT02 20.04(19) .
C1 Yb1 C11 CT02 166.6(2) .
C2 Yb1 C11 CT02 135.7(3) .
C12 Yb1 C11 CT02 57.2(3) .
C3 Yb1 C11 CT02 111.6(3) .
C14 Yb1 C11 CT02 -20.1(2) .
C15 Yb1 C11 CT02 -56.5(3) .
C5 Yb1 C11 CT02 173.56(18) .
C4 Yb1 C11 CT02 125.7(3) .
CT02 Yb1 C11 C15 56.5(3) .
CT01 Yb1 C11 C15 -160.8(3) .
N1 Yb1 C11 C15 39.3(4) .
N2 Yb1 C11 C15 -47.8(3) .
C13 Yb1 C11 C15 76.5(3) .
C1 Yb1 C11 C15 -137.0(3) .
C2 Yb1 C11 C15 -167.8(3) .
C12 Yb1 C11 C15 113.6(4) .
C3 Yb1 C11 C15 168.1(3) .
C14 Yb1 C11 C15 36.4(3) .
C5 Yb1 C11 C15 -130.0(3) .
C4 Yb1 C11 C15 -177.8(3) .
CT02 Yb1 C11 C12 -57.2(3) .
CT01 Yb1 C11 C12 85.6(3) .
N1 Yb1 C11 C12 -74.4(4) .
N2 Yb1 C11 C12 -161.5(3) .
C13 Yb1 C11 C12 -37.1(3) .
C1 Yb1 C11 C12 109.4(3) .
C2 Yb1 C11 C12 78.5(3) .
C3 Yb1 C11 C12 54.5(3) .
C14 Yb1 C11 C12 -77.2(3) .
C15 Yb1 C11 C12 -113.6(4) .
C5 Yb1 C11 C12 116.4(3) .
C4 Yb1 C11 C12 68.5(4) .
CT02 Yb1 C11 C16 179.4(7) .
CT01 Yb1 C11 C16 -37.9(5) .
N1 Yb1 C11 C16 162.2(4) .
N2 Yb1 C11 C16 75.1(5) .
C13 Yb1 C11 C16 -160.6(6) .
C1 Yb1 C11 C16 -14.0(5) .
C2 Yb1 C11 C16 -44.9(5) .
C12 Yb1 C11 C16 -123.5(6) .
C3 Yb1 C11 C16 -69.0(5) .
C14 Yb1 C11 C16 159.3(6) .
C15 Yb1 C11 C16 122.9(6) .
C5 Yb1 C11 C16 -7.1(6) .
C4 Yb1 C11 C16 -54.9(6) .
C30 N2 C29 C28 -2.4(6) .
Yb1 N2 C29 C28 -179.9(3) .
C27 C28 C29 N2 0.5(7) .
C3 C4 C5 CT01 -0.2(3) .
C9 C4 C5 CT01 174.2(5) .
Yb1 C4 C5 CT01 -66.18(16) .
CT01 C4 C5 C1 0.2(3) .
C3 C4 C5 C1 0.0(5) .
C9 C4 C5 C1 174.5(4) .
Yb1 C4 C5 C1 -65.9(3) .
CT01 C4 C5 C10 -174.5(5) .
C3 C4 C5 C10 -174.7(4) .
C9 C4 C5 C10 -0.3(7) .
Yb1 C4 C5 C10 119.3(4) .
CT01 C4 C5 Yb1 66.18(16) .
C3 C4 C5 Yb1 66.0(3) .
C9 C4 C5 Yb1 -119.6(4) .
CT02 Yb1 C5 CT01 -60.5(5) .
N1 Yb1 C5 CT01 117.7(2) .
N2 Yb1 C5 CT01 -162.4(2) .
C13 Yb1 C5 CT01 31.9(5) .
C1 Yb1 C5 CT01 -57.7(3) .
C11 Yb1 C5 CT01 -70.6(3) .
C2 Yb1 C5 CT01 -20.14(18) .
C12 Yb1 C5 CT01 -23.1(4) .
C3 Yb1 C5 CT01 20.12(18) .
C14 Yb1 C5 CT01 166.7(6) .
C15 Yb1 C5 CT01 -118.9(3) .
C4 Yb1 C5 CT01 56.9(3) .
CT02 Yb1 C5 C4 -117.4(4) .
CT01 Yb1 C5 C4 -56.9(3) .
N1 Yb1 C5 C4 60.7(3) .
N2 Yb1 C5 C4 140.7(3) .
C13 Yb1 C5 C4 -25.1(6) .
C1 Yb1 C5 C4 -114.6(4) .
C11 Yb1 C5 C4 -127.6(3) .
C2 Yb1 C5 C4 -77.1(3) .
C12 Yb1 C5 C4 -80.0(3) .
C3 Yb1 C5 C4 -36.8(3) .
C14 Yb1 C5 C4 109.8(7) .
C15 Yb1 C5 C4 -175.8(3) .
CT02 Yb1 C5 C1 -2.8(5) .
CT01 Yb1 C5 C1 57.7(3) .
N1 Yb1 C5 C1 175.3(3) .
N2 Yb1 C5 C1 -104.7(3) .
C13 Yb1 C5 C1 89.5(5) .
C11 Yb1 C5 C1 -13.0(4) .
C2 Yb1 C5 C1 37.5(2) .
C12 Yb1 C5 C1 34.6(4) .
C3 Yb1 C5 C1 77.8(3) .
C14 Yb1 C5 C1 -135.6(7) .
C15 Yb1 C5 C1 -61.3(4) .
C4 Yb1 C5 C1 114.6(4) .
CT02 Yb1 C5 C10 121.0(4) .
CT01 Yb1 C5 C10 -178.5(5) .
N1 Yb1 C5 C10 -60.8(4) .
N2 Yb1 C5 C10 19.1(4) .
C13 Yb1 C5 C10 -146.6(4) .
C1 Yb1 C5 C10 123.8(5) .
C11 Yb1 C5 C10 110.9(4) .
C2 Yb1 C5 C10 161.4(5) .
C12 Yb1 C5 C10 158.4(3) .
C3 Yb1 C5 C10 -158.4(5) .
C14 Yb1 C5 C10 -11.8(9) .
C15 Yb1 C5 C10 62.6(5) .
C4 Yb1 C5 C10 -121.6(5) .
C24 C23 C22 C21 1.6(7) .
N1 C21 C22 C23 0.8(7) .
C4 C5 C1 CT01 -0.2(3) .
C10 C5 C1 CT01 174.3(5) .
Yb1 C5 C1 CT01 -67.32(17) .
CT01 C5 C1 C2 -0.6(3) .
C4 C5 C1 C2 -0.8(5) .
C10 C5 C1 C2 173.7(4) .
Yb1 C5 C1 C2 -67.9(3) .
CT01 C5 C1 C6 -175.0(5) .
C4 C5 C1 C6 -175.2(4) .
C10 C5 C1 C6 -0.7(7) .
Yb1 C5 C1 C6 117.7(4) .
CT01 C5 C1 Yb1 67.32(17) .
C4 C5 C1 Yb1 67.1(3) .
C10 C5 C1 Yb1 -118.4(4) .
CT02 Yb1 C1 CT01 -124.17(16) .
N1 Yb1 C1 CT01 51.2(3) .
N2 Yb1 C1 CT01 127.8(2) .
C13 Yb1 C1 CT01 -86.6(3) .
C11 Yb1 C1 CT01 -132.4(2) .
C2 Yb1 C1 CT01 -57.1(2) .
C12 Yb1 C1 CT01 -100.0(2) .
C3 Yb1 C1 CT01 -20.09(18) .
C14 Yb1 C1 CT01 -145.5(3) .
C15 Yb1 C1 CT01 -158.51(19) .
C5 Yb1 C1 CT01 57.0(3) .
C4 Yb1 C1 CT01 20.13(18) .
CT02 Yb1 C1 C5 178.9(2) .
CT01 Yb1 C1 C5 -57.0(3) .
N1 Yb1 C1 C5 -5.8(3) .
N2 Yb1 C1 C5 70.8(3) .
C13 Yb1 C1 C5 -143.6(3) .
C11 Yb1 C1 C5 170.6(3) .
C2 Yb1 C1 C5 -114.1(4) .
C12 Yb1 C1 C5 -157.0(3) .
C3 Yb1 C1 C5 -77.0(3) .
C14 Yb1 C1 C5 157.6(3) .
C15 Yb1 C1 C5 144.5(3) .
C4 Yb1 C1 C5 -36.8(3) .
CT02 Yb1 C1 C2 -67.0(3) .
CT01 Yb1 C1 C2 57.1(2) .
N1 Yb1 C1 C2 108.3(3) .
N2 Yb1 C1 C2 -175.1(3) .
C13 Yb1 C1 C2 -29.5(4) .
C11 Yb1 C1 C2 -75.3(3) .
C12 Yb1 C1 C2 -42.9(3) .
C3 Yb1 C1 C2 37.1(3) .
C14 Yb1 C1 C2 -88.3(4) .
C15 Yb1 C1 C2 -101.4(3) .
C5 Yb1 C1 C2 114.1(4) .
C4 Yb1 C1 C2 77.3(3) .
CT02 Yb1 C1 C6 54.1(4) .
CT01 Yb1 C1 C6 178.3(5) .
N1 Yb1 C1 C6 -130.5(3) .
N2 Yb1 C1 C6 -53.9(4) .
C13 Yb1 C1 C6 91.7(4) .
C11 Yb1 C1 C6 45.9(4) .
C2 Yb1 C1 C6 121.2(5) .
C12 Yb1 C1 C6 78.3(4) .
C3 Yb1 C1 C6 158.2(4) .
C14 Yb1 C1 C6 32.9(6) .
C15 Yb1 C1 C6 19.8(4) .
C5 Yb1 C1 C6 -124.7(5) .
C4 Yb1 C1 C6 -161.6(4) .
C28 C27 C26 C25 179.7(5) .
C28 C27 C26 C30 -2.4(6) .
C24 C25 C26 C27 177.9(5) .
C25 C25 C26 C27 -2.0(9) 2_756
C24 C25 C26 C30 0.0(5) .
C25 C25 C26 C30 -180.0(5) 2_756
N2 C30 C26 C27 0.5(6) .
C31 C30 C26 C27 -178.6(4) .
Yb1 C30 C26 C27 -3(5) .
N2 C30 C26 C25 178.9(4) .
C31 C30 C26 C25 -0.2(5) .
Yb1 C30 C26 C25 175(4) .
C4 C3 C2 CT01 -0.6(3) .
C8 C3 C2 CT01 -174.8(5) .
Yb1 C3 C2 CT01 67.31(16) .
CT01 C3 C2 C1 -0.7(3) .
C4 C3 C2 C1 -1.3(5) .
C8 C3 C2 C1 -175.5(4) .
Yb1 C3 C2 C1 66.6(3) .
CT01 C3 C2 C7 167.5(5) .
C4 C3 C2 C7 167.0(4) .
C8 C3 C2 C7 -7.2(8) .
Yb1 C3 C2 C7 -125.1(5) .
CT01 C3 C2 Yb1 -67.31(16) .
C4 C3 C2 Yb1 -67.9(3) .
C8 C3 C2 Yb1 117.9(5) .
C5 C1 C2 CT01 0.6(3) .
C6 C1 C2 CT01 175.2(5) .
Yb1 C1 C2 CT01 -67.92(17) .
CT01 C1 C2 C3 0.7(3) .
C5 C1 C2 C3 1.3(5) .
C6 C1 C2 C3 175.9(4) .
Yb1 C1 C2 C3 -67.2(3) .
CT01 C1 C2 C7 -168.1(5) .
C5 C1 C2 C7 -167.5(4) .
C6 C1 C2 C7 7.1(7) .
Yb1 C1 C2 C7 124.0(4) .
CT01 C1 C2 Yb1 67.92(17) .
C5 C1 C2 Yb1 68.5(3) .
C6 C1 C2 Yb1 -116.9(4) .
CT02 Yb1 C2 CT01 -172.14(15) .
N1 Yb1 C2 CT01 -39.8(3) .
N2 Yb1 C2 CT01 62.7(2) .
C13 Yb1 C2 CT01 -141.97(19) .
C1 Yb1 C2 CT01 57.1(3) .
C11 Yb1 C2 CT01 167.1(2) .
C12 Yb1 C2 CT01 -161.9(2) .
C3 Yb1 C2 CT01 -57.2(3) .
C14 Yb1 C2 CT01 -162.4(2) .
C15 Yb1 C2 CT01 159.27(19) .
C5 Yb1 C2 CT01 19.96(18) .
C4 Yb1 C2 CT01 -19.98(18) .
CT02 Yb1 C2 C3 -115.0(3) .
CT01 Yb1 C2 C3 57.2(3) .
N1 Yb1 C2 C3 17.4(3) .
N2 Yb1 C2 C3 119.9(3) .
C13 Yb1 C2 C3 -84.8(3) .
C1 Yb1 C2 C3 114.3(4) .
C11 Yb1 C2 C3 -135.8(3) .
C12 Yb1 C2 C3 -104.7(3) .
C14 Yb1 C2 C3 -105.2(3) .
C15 Yb1 C2 C3 -143.6(3) .
C5 Yb1 C2 C3 77.1(3) .
C4 Yb1 C2 C3 37.2(3) .
CT02 Yb1 C2 C1 130.8(2) .
CT01 Yb1 C2 C1 -57.1(3) .
N1 Yb1 C2 C1 -96.9(3) .
N2 Yb1 C2 C1 5.6(3) .
C13 Yb1 C2 C1 160.9(3) .
C11 Yb1 C2 C1 110.0(3) .
C12 Yb1 C2 C1 141.0(3) .
C3 Yb1 C2 C1 -114.3(4) .
C14 Yb1 C2 C1 140.5(3) .
C15 Yb1 C2 C1 102.2(3) .
C5 Yb1 C2 C1 -37.1(3) .
C4 Yb1 C2 C1 -77.1(3) .
CT02 Yb1 C2 C7 10.6(4) .
CT01 Yb1 C2 C7 -177.3(6) .
N1 Yb1 C2 C7 142.9(4) .
N2 Yb1 C2 C7 -114.6(4) .
C13 Yb1 C2 C7 40.8(4) .
C1 Yb1 C2 C7 -120.2(5) .
C11 Yb1 C2 C7 -10.2(4) .
C12 Yb1 C2 C7 20.8(4) .
C3 Yb1 C2 C7 125.5(5) .
C14 Yb1 C2 C7 20.3(5) .
C15 Yb1 C2 C7 -18.0(5) .
C5 Yb1 C2 C7 -157.3(5) .
C4 Yb1 C2 C7 162.8(5) .
C11 C15 C14 CT02 -0.3(3) .
C20 C15 C14 CT02 173.6(6) .
Yb1 C15 C14 CT02 -66.39(17) .
CT02 C15 C14 C13 0.3(3) .
C11 C15 C14 C13 0.0(5) .
C20 C15 C14 C13 173.9(5) .
Yb1 C15 C14 C13 -66.1(3) .
CT02 C15 C14 C19 -175.1(5) .
C11 C15 C14 C19 -175.4(4) .
C20 C15 C14 C19 -1.4(8) .
Yb1 C15 C14 C19 118.5(5) .
CT02 C15 C14 Yb1 66.39(17) .
C11 C15 C14 Yb1 66.1(3) .
C20 C15 C14 Yb1 -120.0(5) .
C12 C13 C14 CT02 -0.9(3) .
C18 C13 C14 CT02 -175.6(5) .
Yb1 C13 C14 CT02 67.26(17) .
CT02 C13 C14 C15 -0.3(3) .
C12 C13 C14 C15 -1.2(5) .
C18 C13 C14 C15 -175.9(4) .
Yb1 C13 C14 C15 67.0(3) .
CT02 C13 C14 C19 175.0(5) .
C12 C13 C14 C19 174.1(4) .
C18 C13 C14 C19 -0.7(8) .
Yb1 C13 C14 C19 -117.8(5) .
CT02 C13 C14 Yb1 -67.26(17) .
C12 C13 C14 Yb1 -68.1(3) .
C18 C13 C14 Yb1 117.1(5) .
CT01 Yb1 C14 CT02 -51.7(6) .
N1 Yb1 C14 CT02 -157.5(3) .
N2 Yb1 C14 CT02 121.9(2) .
C13 Yb1 C14 CT02 -57.4(3) .
C1 Yb1 C14 CT02 36.2(5) .
C11 Yb1 C14 CT02 20.2(2) .
C2 Yb1 C14 CT02 -19.5(4) .
C12 Yb1 C14 CT02 -20.16(19) .
C3 Yb1 C14 CT02 -68.6(3) .
C15 Yb1 C14 CT02 56.9(3) .
C5 Yb1 C14 CT02 151.9(6) .
C4 Yb1 C14 CT02 -120.1(3) .
CT02 Yb1 C14 C15 -56.9(3) .
CT01 Yb1 C14 C15 -108.6(5) .
N1 Yb1 C14 C15 145.6(3) .
N2 Yb1 C14 C15 65.0(3) .
C13 Yb1 C14 C15 -114.4(5) .
C1 Yb1 C14 C15 -20.7(5) .
C11 Yb1 C14 C15 -36.7(3) .
C2 Yb1 C14 C15 -76.4(4) .
C12 Yb1 C14 C15 -77.1(3) .
C3 Yb1 C14 C15 -125.5(3) .
C5 Yb1 C14 C15 95.0(8) .
C4 Yb1 C14 C15 -177.0(3) .
CT02 Yb1 C14 C13 57.4(3) .
CT01 Yb1 C14 C13 5.7(7) .
N1 Yb1 C14 C13 -100.1(3) .
N2 Yb1 C14 C13 179.4(3) .
C1 Yb1 C14 C13 93.7(4) .
C11 Yb1 C14 C13 77.7(3) .
C2 Yb1 C14 C13 37.9(4) .
C12 Yb1 C14 C13 37.3(3) .
C3 Yb1 C14 C13 -11.2(4) .
C15 Yb1 C14 C13 114.4(5) .
C5 Yb1 C14 C13 -150.6(6) .
C4 Yb1 C14 C13 -62.7(4) .
CT02 Yb1 C14 C19 -179.0(6) .
CT01 Yb1 C14 C19 129.3(4) .
N1 Yb1 C14 C19 23.5(4) .
N2 Yb1 C14 C19 -57.1(4) .
C13 Yb1 C14 C19 123.5(6) .
C1 Yb1 C14 C19 -142.8(4) .
C11 Yb1 C14 C19 -158.8(5) .
C2 Yb1 C14 C19 161.5(4) .
C12 Yb1 C14 C19 160.8(5) .
C3 Yb1 C14 C19 112.4(4) .
C15 Yb1 C14 C19 -122.1(6) .
C5 Yb1 C14 C19 -27.1(10) .
C4 Yb1 C14 C19 60.9(6) .
C14 C13 C12 CT02 0.9(3) .
C18 C13 C12 CT02 175.9(5) .
Yb1 C13 C12 CT02 -67.57(17) .
CT02 C13 C12 C11 1.0(3) .
C14 C13 C12 C11 1.9(5) .
C18 C13 C12 C11 176.9(4) .
Yb1 C13 C12 C11 -66.6(3) .
CT02 C13 C12 C17 -168.7(5) .
C14 C13 C12 C17 -167.8(4) .
C18 C13 C12 C17 7.2(7) .
Yb1 C13 C12 C17 123.7(4) .
CT02 C13 C12 Yb1 67.57(17) .
C14 C13 C12 Yb1 68.5(3) .
C18 C13 C12 Yb1 -116.5(4) .
C15 C11 C12 CT02 -0.9(3) .
C16 C11 C12 CT02 -175.7(5) .
Yb1 C11 C12 CT02 67.21(17) .
CT02 C11 C12 C13 -1.0(3) .
C15 C11 C12 C13 -1.9(5) .
C16 C11 C12 C13 -176.8(4) .
Yb1 C11 C12 C13 66.2(3) .
CT02 C11 C12 C17 168.2(5) .
C15 C11 C12 C17 167.3(4) .
C16 C11 C12 C17 -7.6(8) .
Yb1 C11 C12 C17 -124.6(5) .
CT02 C11 C12 Yb1 -67.21(17) .
C15 C11 C12 Yb1 -68.1(3) .
C16 C11 C12 Yb1 117.1(5) .
CT01 Yb1 C12 CT02 -168.66(15) .
N1 Yb1 C12 CT02 67.3(2) .
N2 Yb1 C12 CT02 -33.3(3) .
C13 Yb1 C12 CT02 57.1(3) .
C1 Yb1 C12 CT02 -138.4(2) .
C11 Yb1 C12 CT02 -57.4(3) .
C2 Yb1 C12 CT02 -159.5(2) .
C3 Yb1 C12 CT02 169.8(2) .
C14 Yb1 C12 CT02 20.1(2) .
C15 Yb1 C12 CT02 -19.9(2) .
C5 Yb1 C12 CT02 -157.19(19) .
C4 Yb1 C12 CT02 162.96(18) .
CT02 Yb1 C12 C13 -57.1(3) .
CT01 Yb1 C12 C13 134.2(2) .
N1 Yb1 C12 C13 10.2(3) .
N2 Yb1 C12 C13 -90.4(3) .
C1 Yb1 C12 C13 164.5(3) .
C11 Yb1 C12 C13 -114.5(4) .
C2 Yb1 C12 C13 143.4(3) .
C3 Yb1 C12 C13 112.7(3) .
C14 Yb1 C12 C13 -37.1(3) .
C15 Yb1 C12 C13 -77.0(3) .
C5 Yb1 C12 C13 145.7(3) .
C4 Yb1 C12 C13 105.8(3) .
CT02 Yb1 C12 C11 57.4(3) .
CT01 Yb1 C12 C11 -111.3(3) .
N1 Yb1 C12 C11 124.6(3) .
N2 Yb1 C12 C11 24.1(4) .
C13 Yb1 C12 C11 114.5(4) .
C1 Yb1 C12 C11 -81.1(3) .
C2 Yb1 C12 C11 -102.2(3) .
C3 Yb1 C12 C11 -132.8(3) .
C14 Yb1 C12 C11 77.4(3) .
C15 Yb1 C12 C11 37.5(3) .
C5 Yb1 C12 C11 -99.8(4) .
C4 Yb1 C12 C11 -139.7(3) .
CT02 Yb1 C12 C17 -177.2(6) .
CT01 Yb1 C12 C17 14.1(4) .
N1 Yb1 C12 C17 -109.9(4) .
N2 Yb1 C12 C17 149.5(4) .
C13 Yb1 C12 C17 -120.1(5) .
C1 Yb1 C12 C17 44.4(4) .
C11 Yb1 C12 C17 125.4(6) .
C2 Yb1 C12 C17 23.3(4) .
C3 Yb1 C12 C17 -7.4(4) .
C14 Yb1 C12 C17 -157.1(5) .
C15 Yb1 C12 C17 162.9(5) .
C5 Yb1 C12 C17 25.6(5) .
C4 Yb1 C12 C17 -14.2(5) .
C6S C1S C2S C3S -0.1(8) .
C2S C1S C6S C5S 0.1(8) .
C1S C2S C3S C4S -0.3(8) .
C2S C3S C4S C5S 0.6(7) .
C3S C4S C5S C6S -0.6(7) .
C1S C6S C5S C4S 0.2(7) .
C5 C1 CT01 C4 0.5(5) .
C2 C1 CT01 C4 179.7(4) .
C6 C1 CT01 C4 110(6) .
Yb1 C1 CT01 C4 -90.5(4) .
C5 C1 CT01 C3 179.3(5) .
C2 C1 CT01 C3 -1.4(5) .
C6 C1 CT01 C3 -71(6) .
Yb1 C1 CT01 C3 88.4(4) .
C5 C1 CT01 C2 -179.3(3) .
C6 C1 CT01 C2 -70(6) .
Yb1 C1 CT01 C2 89.8(2) .
C2 C1 CT01 C5 179.3(3) .
C6 C1 CT01 C5 109(6) .
Yb1 C1 CT01 C5 -90.9(2) .
C5 C1 CT01 Yb1 90.9(2) .
C2 C1 CT01 Yb1 -89.8(2) .
C6 C1 CT01 Yb1 -160(6) .
C5 C4 CT01 C1 -0.5(5) .
C3 C4 CT01 C1 179.3(4) .
C9 C4 CT01 C1 -81(6) .
Yb1 C4 CT01 C1 89.7(4) .
C5 C4 CT01 C3 -179.7(3) .
C9 C4 CT01 C3 100(6) .
Yb1 C4 CT01 C3 -89.5(2) .
C5 C4 CT01 C2 179.1(5) .
C3 C4 CT01 C2 -1.1(5) .
C9 C4 CT01 C2 99(6) .
Yb1 C4 CT01 C2 -90.7(4) .
C3 C4 CT01 C5 179.7(3) .
C9 C4 CT01 C5 -80(6) .
Yb1 C4 CT01 C5 90.2(2) .
C5 C4 CT01 Yb1 -90.2(2) .
C3 C4 CT01 Yb1 89.5(2) .
C9 C4 CT01 Yb1 -171(6) .
C2 C3 CT01 C1 1.4(5) .
C4 C3 CT01 C1 -179.3(5) .
C8 C3 CT01 C1 114(6) .
Yb1 C3 CT01 C1 -88.1(4) .
C2 C3 CT01 C4 -179.3(3) .
C8 C3 CT01 C4 -67(6) .
Yb1 C3 CT01 C4 91.2(2) .
C4 C3 CT01 C2 179.3(3) .
C8 C3 CT01 C2 112(6) .
Yb1 C3 CT01 C2 -89.5(2) .
C2 C3 CT01 C5 -179.7(5) .
C4 C3 CT01 C5 -0.4(5) .
C8 C3 CT01 C5 -67(6) .
Yb1 C3 CT01 C5 90.8(4) .
C2 C3 CT01 Yb1 89.5(2) .
C4 C3 CT01 Yb1 -91.2(2) .
C8 C3 CT01 Yb1 -158(6) .
C3 C2 CT01 C1 -179.1(3) .
C7 C2 CT01 C1 78(3) .
Yb1 C2 CT01 C1 -89.1(2) .
C3 C2 CT01 C4 1.1(5) .
C1 C2 CT01 C4 -179.7(4) .
C7 C2 CT01 C4 -101(3) .
Yb1 C2 CT01 C4 91.2(4) .
C1 C2 CT01 C3 179.1(3) .
C7 C2 CT01 C3 -102(3) .
Yb1 C2 CT01 C3 90.1(2) .
C3 C2 CT01 C5 179.7(5) .
C1 C2 CT01 C5 -1.2(5) .
C7 C2 CT01 C5 77(3) .
Yb1 C2 CT01 C5 -90.2(4) .
C3 C2 CT01 Yb1 -90.1(2) .
C1 C2 CT01 Yb1 89.1(2) .
C7 C2 CT01 Yb1 167(3) .
C4 C5 CT01 C1 179.7(3) .
C10 C5 CT01 C1 -107(6) .
Yb1 C5 CT01 C1 88.7(2) .
C1 C5 CT01 C4 -179.7(3) .
C10 C5 CT01 C4 74(6) .
Yb1 C5 CT01 C4 -91.0(2) .
C4 C5 CT01 C3 0.4(5) .
C1 C5 CT01 C3 -179.3(5) .
C10 C5 CT01 C3 74(6) .
Yb1 C5 CT01 C3 -90.6(4) .
C4 C5 CT01 C2 -179.1(5) .
C1 C5 CT01 C2 1.2(5) .
C10 C5 CT01 C2 -106(6) .
Yb1 C5 CT01 C2 89.9(4) .
C4 C5 CT01 Yb1 91.0(2) .
C1 C5 CT01 Yb1 -88.7(2) .
C10 C5 CT01 Yb1 164(6) .
CT02 Yb1 CT01 C1 83.8(2) .
N1 Yb1 CT01 C1 -138.8(2) .
N2 Yb1 CT01 C1 -54.2(2) .
C13 Yb1 CT01 C1 123.3(3) .
C11 Yb1 CT01 C1 57.1(3) .
C2 Yb1 CT01 C1 72.3(3) .
C12 Yb1 CT01 C1 92.2(2) .
C3 Yb1 CT01 C1 144.0(3) .
C14 Yb1 CT01 C1 119.2(5) .
C15 Yb1 CT01 C1 36.8(3) .
C5 Yb1 CT01 C1 -71.9(3) .
C4 Yb1 CT01 C1 -143.7(3) .
CT02 Yb1 CT01 C4 -132.5(2) .
N1 Yb1 CT01 C4 4.9(2) .
N2 Yb1 CT01 C4 89.5(2) .
C13 Yb1 CT01 C4 -93.0(3) .
C1 Yb1 CT01 C4 143.7(3) .
C11 Yb1 CT01 C4 -159.2(3) .
C2 Yb1 CT01 C4 -144.0(3) .
C12 Yb1 CT01 C4 -124.1(3) .
C3 Yb1 CT01 C4 -72.2(3) .
C14 Yb1 CT01 C4 -97.1(5) .
C15 Yb1 CT01 C4 -179.5(3) .
C5 Yb1 CT01 C4 71.8(3) .
CT02 Yb1 CT01 C3 -60.2(2) .
N1 Yb1 CT01 C3 77.1(2) .
N2 Yb1 CT01 C3 161.7(2) .
C13 Yb1 CT01 C3 -20.7(3) .
C1 Yb1 CT01 C3 -144.0(3) .
C11 Yb1 CT01 C3 -86.9(3) .
C2 Yb1 CT01 C3 -71.7(3) .
C12 Yb1 CT01 C3 -51.8(3) .
C14 Yb1 CT01 C3 -24.8(5) .
C15 Yb1 CT01 C3 -107.2(3) .
C5 Yb1 CT01 C3 144.1(3) .
C4 Yb1 CT01 C3 72.2(3) .
CT02 Yb1 CT01 C2 11.5(2) .
N1 Yb1 CT01 C2 148.8(2) .
N2 Yb1 CT01 C2 -126.5(2) .
C13 Yb1 CT01 C2 51.0(3) .
C1 Yb1 CT01 C2 -72.3(3) .
C11 Yb1 CT01 C2 -15.2(3) .
C12 Yb1 CT01 C2 19.9(2) .
C3 Yb1 CT01 C2 71.7(3) .
C14 Yb1 CT01 C2 46.9(5) .
C15 Yb1 CT01 C2 -35.5(3) .
C5 Yb1 CT01 C2 -144.2(3) .
C4 Yb1 CT01 C2 144.0(3) .
CT02 Yb1 CT01 C5 155.7(2) .
N1 Yb1 CT01 C5 -67.0(2) .
N2 Yb1 CT01 C5 17.7(2) .
C13 Yb1 CT01 C5 -164.8(3) .
C1 Yb1 CT01 C5 71.9(3) .
C11 Yb1 CT01 C5 129.0(3) .
C2 Yb1 CT01 C5 144.2(3) .
C12 Yb1 CT01 C5 164.1(3) .
C3 Yb1 CT01 C5 -144.1(3) .
C14 Yb1 CT01 C5 -168.9(5) .
C15 Yb1 CT01 C5 108.7(3) .
C4 Yb1 CT01 C5 -71.8(3) .
C14 C15 CT02 C13 -0.6(6) .
C11 C15 CT02 C13 179.1(5) .
C20 C15 CT02 C13 -87(7) .
Yb1 C15 CT02 C13 89.7(5) .
C11 C15 CT02 C14 179.7(4) .
C20 C15 CT02 C14 -86(7) .
Yb1 C15 CT02 C14 90.3(2) .
C14 C15 CT02 C12 178.7(5) .
C11 C15 CT02 C12 -1.7(6) .
C20 C15 CT02 C12 92(7) .
Yb1 C15 CT02 C12 -91.1(5) .
C14 C15 CT02 C11 -179.7(4) .
C20 C15 CT02 C11 94(7) .
Yb1 C15 CT02 C11 -89.4(2) .
C14 C15 CT02 Yb1 -90.3(2) .
C11 C15 CT02 Yb1 89.4(2) .
C20 C15 CT02 Yb1 -177(100) .
C14 C13 CT02 C15 0.6(6) .
C12 C13 CT02 C15 179.5(5) .
C18 C13 CT02 C15 121(6) .
Yb1 C13 CT02 C15 -90.2(5) .
C12 C13 CT02 C14 179.0(3) .
C18 C13 CT02 C14 120(7) .
Yb1 C13 CT02 C14 -90.8(2) .
C14 C13 CT02 C12 -179.0(3) .
C18 C13 CT02 C12 -59(7) .
Yb1 C13 CT02 C12 90.2(2) .
C14 C13 CT02 C11 179.1(5) .
C12 C13 CT02 C11 -2.0(6) .
C18 C13 CT02 C11 -61(7) .
Yb1 C13 CT02 C11 88.3(5) .
C14 C13 CT02 Yb1 90.8(2) .
C12 C13 CT02 Yb1 -90.2(2) .
C18 C13 CT02 Yb1 -149(7) .
C13 C14 CT02 C15 -179.6(4) .
C19 C14 CT02 C15 78(7) .
Yb1 C14 CT02 C15 -90.7(2) .
C15 C14 CT02 C13 179.6(4) .
C19 C14 CT02 C13 -103(7) .
Yb1 C14 CT02 C13 89.0(2) .
C15 C14 CT02 C12 -178.7(5) .
C13 C14 CT02 C12 1.7(6) .
C19 C14 CT02 C12 -101(7) .
Yb1 C14 CT02 C12 90.7(5) .
C15 C14 CT02 C11 0.6(6) .
C13 C14 CT02 C11 -179.1(5) .
C19 C14 CT02 C11 78(7) .
Yb1 C14 CT02 C11 -90.1(5) .
C15 C14 CT02 Yb1 90.7(2) .
C13 C14 CT02 Yb1 -89.0(2) .
C19 C14 CT02 Yb1 168(7) .
C13 C12 CT02 C15 -179.5(5) .
C11 C12 CT02 C15 1.7(6) .
C17 C12 CT02 C15 -102(3) .
Yb1 C12 CT02 C15 91.3(5) .
C11 C12 CT02 C13 -178.8(3) .
C17 C12 CT02 C13 77(3) .
Yb1 C12 CT02 C13 -89.1(2) .
C13 C12 CT02 C14 -1.7(6) .
C11 C12 CT02 C14 179.5(5) .
C17 C12 CT02 C14 76(3) .
Yb1 C12 CT02 C14 -90.8(5) .
C13 C12 CT02 C11 178.8(3) .
C17 C12 CT02 C11 -104(3) .
Yb1 C12 CT02 C11 89.7(2) .
C13 C12 CT02 Yb1 89.1(2) .
C11 C12 CT02 Yb1 -89.7(2) .
C17 C12 CT02 Yb1 167(3) .
C12 C11 CT02 C15 -179.0(4) .
C16 C11 CT02 C15 -80(10) .
Yb1 C11 CT02 C15 91.0(2) .
C15 C11 CT02 C13 -179.1(5) .
C12 C11 CT02 C13 2.0(6) .
C16 C11 CT02 C13 101(9) .
Yb1 C11 CT02 C13 -88.1(5) .
C15 C11 CT02 C14 -0.6(6) .
C12 C11 CT02 C14 -179.5(5) .
C16 C11 CT02 C14 -81(10) .
Yb1 C11 CT02 C14 90.4(5) .
C15 C11 CT02 C12 179.0(4) .
C16 C11 CT02 C12 99(10) .
Yb1 C11 CT02 C12 -90.1(2) .
C15 C11 CT02 Yb1 -91.0(2) .
C12 C11 CT02 Yb1 90.1(2) .
C16 C11 CT02 Yb1 -171(10) .
CT01 Yb1 CT02 C15 -127.5(3) .
N1 Yb1 CT02 C15 94.3(3) .
N2 Yb1 CT02 C15 9.9(3) .
C13 Yb1 CT02 C15 143.7(4) .
C1 Yb1 CT02 C15 -89.6(3) .
C11 Yb1 CT02 C15 -72.2(4) .
C2 Yb1 CT02 C15 -121.7(3) .
C12 Yb1 CT02 C15 -144.2(4) .
C3 Yb1 CT02 C15 -156.3(3) .
C14 Yb1 CT02 C15 71.8(4) .
C5 Yb1 CT02 C15 -87.6(5) .
C4 Yb1 CT02 C15 -174.6(4) .
CT01 Yb1 CT02 C13 88.8(2) .
N1 Yb1 CT02 C13 -49.4(2) .
N2 Yb1 CT02 C13 -133.7(2) .
C1 Yb1 CT02 C13 126.8(3) .
C11 Yb1 CT02 C13 144.2(3) .
C2 Yb1 CT02 C13 94.6(2) .
C12 Yb1 CT02 C13 72.2(3) .
C3 Yb1 CT02 C13 60.1(3) .
C14 Yb1 CT02 C13 -71.9(3) .
C15 Yb1 CT02 C13 -143.7(4) .
C5 Yb1 CT02 C13 128.7(4) .
C4 Yb1 CT02 C13 41.7(3) .
CT01 Yb1 CT02 C14 160.7(2) .
N1 Yb1 CT02 C14 22.5(3) .
N2 Yb1 CT02 C14 -61.9(3) .
C13 Yb1 CT02 C14 71.9(3) .
C1 Yb1 CT02 C14 -161.4(3) .
C11 Yb1 CT02 C14 -144.0(4) .
C2 Yb1 CT02 C14 166.5(3) .
C12 Yb1 CT02 C14 144.0(3) .
C3 Yb1 CT02 C14 131.9(3) .
C15 Yb1 CT02 C14 -71.8(4) .
C5 Yb1 CT02 C14 -159.4(4) .
C4 Yb1 CT02 C14 113.6(3) .
CT01 Yb1 CT02 C12 16.6(2) .
N1 Yb1 CT02 C12 -121.5(2) .
N2 Yb1 CT02 C12 154.1(2) .
C13 Yb1 CT02 C12 -72.2(3) .
C1 Yb1 CT02 C12 54.6(3) .
C11 Yb1 CT02 C12 72.0(3) .
C2 Yb1 CT02 C12 22.5(3) .
C3 Yb1 CT02 C12 -12.1(3) .
C14 Yb1 CT02 C12 -144.0(3) .
C15 Yb1 CT02 C12 144.2(4) .
C5 Yb1 CT02 C12 56.6(4) .
C4 Yb1 CT02 C12 -30.4(3) .
CT01 Yb1 CT02 C11 -55.4(3) .
N1 Yb1 CT02 C11 166.5(3) .
N2 Yb1 CT02 C11 82.1(3) .
C13 Yb1 CT02 C11 -144.2(3) .
C1 Yb1 CT02 C11 -17.4(3) .
C2 Yb1 CT02 C11 -49.5(3) .
C12 Yb1 CT02 C11 -72.0(3) .
C3 Yb1 CT02 C11 -84.1(3) .
C14 Yb1 CT02 C11 144.0(4) .
C15 Yb1 CT02 C11 72.2(4) .
C5 Yb1 CT02 C11 -15.4(4) .
C4 Yb1 CT02 C11 -102.4(3) .
