#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/39/4083943.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4083943
loop_
_publ_author_name
'Huber, Dominik'
'Kumar, P. G. Anil'
'Pregosin, Paul S.'
'Mezzetti, Antonio'
_publ_section_title
;
 An η2-Aryl−Metal Interaction Turns a Chiral Monodentate
 Phosphoramidite into a Chelating Ligand in
 (Sa,SRu,RC,RC)-[RuCl(η6-p-cymene)
 (O,O‘-(1,1‘-dinaphthyl-2,2‘-diyl)-N-(1-(1,2-η-1-naphthyl)ethyl)-N-(1-(1-naphthyl)ethyl)phosphoramidite-\kP)]PF6
;
_journal_issue                   22
_journal_name_full               Organometallics
_journal_page_first              5221
_journal_paper_doi               10.1021/om050686+
_journal_volume                  24
_journal_year                    2005
_chemical_formula_sum            'C55.5 H48 Cl4 F6 N O2 P2 Ru'
_chemical_formula_weight         1179.76
_chemical_name_systematic        ([RuCl(p-cymene)(phosphoramidite)]PF6
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.8220(10)
_cell_angle_beta                 96.6360(10)
_cell_angle_gamma                111.6590(10)
_cell_formula_units_Z            2
_cell_length_a                   13.3040(8)
_cell_length_b                   13.7074(8)
_cell_length_c                   15.1350(9)
_cell_measurement_reflns_used    14245
_cell_measurement_temperature    201(2)
_cell_measurement_theta_max      28.275
_cell_measurement_theta_min      2.311
_cell_volume                     2489.9(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      201(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'BRUKER APEX'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0169
_diffrn_reflns_av_sigmaI/netI    0.0262
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            25914
_diffrn_reflns_theta_full        28.28
_diffrn_reflns_theta_max         28.28
_diffrn_reflns_theta_min         1.64
_diffrn_source                   'fine-focus sealed tube'
_diffrn_source_type              MoK\a
_exptl_absorpt_coefficient_mu    0.661
_exptl_absorpt_correction_T_max  0.8365
_exptl_absorpt_correction_T_min  0.6334
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   'sadabs vers. 2.03'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.574
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       cube
_exptl_crystal_F_000             1200
_exptl_crystal_size_max          0.76
_exptl_crystal_size_mid          0.49
_exptl_crystal_size_min          0.28
_refine_diff_density_max         1.501
_refine_diff_density_min         -0.865
_refine_diff_density_rms         0.087
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.033
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     715
_refine_ls_number_reflns         12262
_refine_ls_number_restraints     42
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0447
_refine_ls_R_factor_gt           0.0405
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0645P)²+2.0683P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1079
_refine_ls_wR_factor_ref         0.1112
_reflns_number_gt                11071
_reflns_number_total             12262
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om050686%2Bsi20050915_032639.cif
_cod_data_source_block           '[RuCl(p-cymene)(1,2-eta-1-kappaP]+'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not given.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_formula_sum        'C55.50 H48 Cl4 F6 N O2 P2 Ru'
_cod_database_code               4083943
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ru1 Ru 0.097697(13) 0.160603(13) 0.777261(11) 0.02144(6) Uani 1 1 d .
Cl1 Cl -0.01353(4) 0.09123(4) 0.62804(4) 0.02831(11) Uani 1 1 d .
P1 P 0.23350(4) 0.20734(4) 0.69383(3) 0.01863(10) Uani 1 1 d .
O1 O 0.34757(12) 0.23944(12) 0.76307(10) 0.0213(3) Uani 1 1 d .
O2 O 0.24107(12) 0.12127(11) 0.61296(10) 0.0210(3) Uani 1 1 d .
N1 N 0.23490(14) 0.30378(13) 0.64011(11) 0.0206(3) Uani 1 1 d .
C1 C 0.14077(18) 0.34226(17) 0.76590(15) 0.0244(4) Uani 1 1 d .
C2 C 0.03128(19) 0.30041(19) 0.77938(16) 0.0292(4) Uani 1 1 d .
H2 H -0.0241 0.2887 0.7240 0.035 Uiso 1 1 calc R
C3 C 0.0021(2) 0.3380(2) 0.86303(19) 0.0381(6) Uani 1 1 d .
H3 H -0.0725 0.3104 0.8705 0.046 Uiso 1 1 calc R
C4 C 0.0794(2) 0.4115(2) 0.93005(18) 0.0406(6) Uani 1 1 d .
H4 H 0.0582 0.4375 0.9837 0.049 Uiso 1 1 calc R
C5 C 0.1934(2) 0.4521(2) 0.92311(17) 0.0352(5) Uani 1 1 d .
C6 C 0.2744(3) 0.5275(2) 0.99537(19) 0.0474(7) Uani 1 1 d .
H6 H 0.2534 0.5486 1.0507 0.057 Uiso 1 1 calc R
C7 C 0.3823(3) 0.5707(2) 0.98771(19) 0.0492(7) Uani 1 1 d .
H7 H 0.4353 0.6222 1.0370 0.059 Uiso 1 1 calc R
C8 C 0.4150(2) 0.5392(2) 0.90730(19) 0.0397(6) Uani 1 1 d .
H8 H 0.4902 0.5693 0.9019 0.048 Uiso 1 1 calc R
C9 C 0.3376(2) 0.46431(18) 0.83572(16) 0.0290(4) Uani 1 1 d .
H9 H 0.3604 0.4432 0.7813 0.035 Uiso 1 1 calc R
C10 C 0.22623(19) 0.41898(18) 0.84190(15) 0.0271(4) Uani 1 1 d .
C11 C 0.15484(18) 0.34920(17) 0.66791(14) 0.0235(4) Uani 1 1 d .
H11 H 0.0819 0.3043 0.6276 0.028 Uiso 1 1 calc R
C12 C 0.1836(2) 0.46530(19) 0.65805(17) 0.0319(5) Uani 1 1 d .
H12A H 0.1789 0.4683 0.5935 0.048 Uiso 1 1 calc R
H12B H 0.2586 0.5101 0.6910 0.048 Uiso 1 1 calc R
H12C H 0.1317 0.4919 0.6833 0.048 Uiso 1 1 calc R
C13 C 0.25317(17) 0.30745(17) 0.54435(14) 0.0230(4) Uani 1 1 d .
H13 H 0.2597 0.3806 0.5367 0.028 Uiso 1 1 calc R
C14 C 0.1517(2) 0.22925(19) 0.47416(15) 0.0309(5) Uani 1 1 d .
H14A H 0.0867 0.2424 0.4870 0.046 Uiso 1 1 calc R
H14B H 0.1405 0.1553 0.4777 0.046 Uiso 1 1 calc R
H14C H 0.1630 0.2401 0.4130 0.046 Uiso 1 1 calc R
C15 C 0.36145(18) 0.30196(17) 0.52793(14) 0.0250(4) Uani 1 1 d .
C16 C 0.3644(2) 0.21617(19) 0.46941(16) 0.0325(5) Uani 1 1 d .
H16 H 0.2976 0.1566 0.4424 0.039 Uiso 1 1 calc R
C17 C 0.4645(2) 0.2148(2) 0.44866(18) 0.0391(6) Uani 1 1 d .
H17 H 0.4642 0.1549 0.4075 0.047 Uiso 1 1 calc R
C18 C 0.5613(2) 0.2982(2) 0.48678(19) 0.0394(6) Uani 1 1 d .
H18 H 0.6282 0.2958 0.4728 0.047 Uiso 1 1 calc R
C19 C 0.5635(2) 0.3892(2) 0.54741(17) 0.0326(5) Uani 1 1 d .
C20 C 0.6635(2) 0.4772(2) 0.58849(19) 0.0406(6) Uani 1 1 d .
H20 H 0.7310 0.4751 0.5757 0.049 Uiso 1 1 calc R
C21 C 0.6650(2) 0.5646(2) 0.6458(2) 0.0430(6) Uani 1 1 d .
H21 H 0.7331 0.6222 0.6736 0.052 Uiso 1 1 calc R
C22 C 0.5657(2) 0.5695(2) 0.66370(18) 0.0366(5) Uani 1 1 d .
H22 H 0.5665 0.6314 0.7024 0.044 Uiso 1 1 calc R
C23 C 0.46747(19) 0.48557(18) 0.62572(16) 0.0289(4) Uani 1 1 d .
H23 H 0.4010 0.4902 0.6388 0.035 Uiso 1 1 calc R
C24 C 0.46255(18) 0.39189(18) 0.56729(15) 0.0262(4) Uani 1 1 d .
C25 C 0.44743(16) 0.24329(16) 0.73920(13) 0.0199(4) Uani 1 1 d .
C26 C 0.53780(17) 0.34223(16) 0.76930(14) 0.0226(4) Uani 1 1 d .
H26 H 0.5287 0.4026 0.8016 0.027 Uiso 1 1 calc R
C27 C 0.63863(17) 0.35100(17) 0.75191(14) 0.0242(4) Uani 1 1 d .
H27 H 0.7010 0.4162 0.7758 0.029 Uiso 1 1 calc R
C28 C 0.65082(17) 0.26316(17) 0.69835(14) 0.0230(4) Uani 1 1 d .
C29 C 0.75139(18) 0.27492(19) 0.66980(16) 0.0285(4) Uani 1 1 d .
H29 H 0.8137 0.3407 0.6913 0.034 Uiso 1 1 calc R
C30 C 0.76025(18) 0.1930(2) 0.61176(17) 0.0314(5) Uani 1 1 d .
H30 H 0.8280 0.2023 0.5924 0.038 Uiso 1 1 calc R
C31 C 0.66815(19) 0.09432(19) 0.58057(16) 0.0295(5) Uani 1 1 d .
H31 H 0.6741 0.0378 0.5394 0.035 Uiso 1 1 calc R
C32 C 0.57064(18) 0.07932(17) 0.60903(15) 0.0253(4) Uani 1 1 d .
H32 H 0.5102 0.0119 0.5887 0.030 Uiso 1 1 calc R
C33 C 0.55859(16) 0.16337(16) 0.66867(14) 0.0216(4) Uani 1 1 d .
C34 C 0.45564(16) 0.15173(16) 0.69567(14) 0.0205(4) Uani 1 1 d .
C35 C 0.36134(16) 0.04582(15) 0.67728(14) 0.0210(4) Uani 1 1 d .
C36 C 0.37212(18) -0.04614(16) 0.70513(15) 0.0239(4) Uani 1 1 d .
C37 C 0.46983(19) -0.03983(18) 0.75900(16) 0.0284(4) Uani 1 1 d .
H37 H 0.5315 0.0270 0.7772 0.034 Uiso 1 1 calc R
C38 C 0.4762(2) -0.1291(2) 0.78500(18) 0.0349(5) Uani 1 1 d .
H38 H 0.5422 -0.1232 0.8213 0.042 Uiso 1 1 calc R
C39 C 0.3871(2) -0.2287(2) 0.7590(2) 0.0389(6) Uani 1 1 d .
H39 H 0.3934 -0.2902 0.7764 0.047 Uiso 1 1 calc R
C40 C 0.2907(2) -0.23735(19) 0.70869(19) 0.0359(5) Uani 1 1 d .
H40 H 0.2303 -0.3051 0.6915 0.043 Uiso 1 1 calc R
C41 C 0.28013(19) -0.14651(17) 0.68184(16) 0.0274(4) Uani 1 1 d .
C42 C 0.17884(19) -0.15387(18) 0.63430(17) 0.0304(5) Uani 1 1 d .
H42 H 0.1181 -0.2214 0.6177 0.036 Uiso 1 1 calc R
C43 C 0.16702(17) -0.06551(17) 0.61189(15) 0.0261(4) Uani 1 1 d .
H43 H 0.0984 -0.0705 0.5810 0.031 Uiso 1 1 calc R
C44 C 0.25860(17) 0.03296(16) 0.63549(14) 0.0211(4) Uani 1 1 d .
C45 C 0.3156(2) 0.2279(3) 0.9550(2) 0.0481(7) Uani 1 1 d .
H45A H 0.3246 0.2207 1.0186 0.072 Uiso 1 1 calc R
H45B H 0.3308 0.3030 0.9529 0.072 Uiso 1 1 calc R
H45C H 0.3671 0.2053 0.9248 0.072 Uiso 1 1 calc R
C46 C 0.1987(2) 0.1579(2) 0.90671(16) 0.0345(5) Uani 1 1 d .
C47 C 0.1713(2) 0.0617(2) 0.84154(17) 0.0331(5) Uani 1 1 d .
H47 H 0.2317 0.0469 0.8163 0.040 Uiso 1 1 calc R
C48 C 0.0618(2) -0.00309(19) 0.80044(17) 0.0312(5) Uani 1 1 d .
H48 H 0.0462 -0.0631 0.7473 0.037 Uiso 1 1 calc R
C49 C -0.02739(19) 0.02211(19) 0.82653(16) 0.0287(4) Uani 1 1 d .
C50 C -0.1443(2) -0.0511(2) 0.78377(19) 0.0376(5) Uani 1 1 d .
H50 H -0.1439 -0.0933 0.7238 0.045 Uiso 1 1 calc R
C51 C -0.1881(3) -0.1307(3) 0.8464(3) 0.0655(10) Uani 1 1 d .
H51A H -0.1926 -0.0913 0.9046 0.098 Uiso 1 1 calc R
H51B H -0.1378 -0.1667 0.8573 0.098 Uiso 1 1 calc R
H51C H -0.2614 -0.1844 0.8170 0.098 Uiso 1 1 calc R
C52 C -0.2195(2) 0.0063(3) 0.7675(2) 0.0511(7) Uani 1 1 d .
H52A H -0.1870 0.0617 0.7333 0.077 Uiso 1 1 calc R
H52B H -0.2293 0.0398 0.8260 0.077 Uiso 1 1 calc R
H52C H -0.2911 -0.0454 0.7324 0.077 Uiso 1 1 calc R
C53 C -0.0008(2) 0.11653(19) 0.89060(16) 0.0303(5) Uani 1 1 d .
H53 H -0.0592 0.1447 0.8993 0.036 Uiso 1 1 calc R
C54 C 0.1115(2) 0.1854(2) 0.92739(16) 0.0329(5) Uani 1 1 d .
H54 H 0.1286 0.2591 0.9632 0.039 Uiso 1 1 calc R
P2 P 0.98205(8) 0.65845(8) 0.81806(6) 0.0552(2) Uani 1 1 d D
F1A F 1.0163(4) 0.7588(5) 0.8957(3) 0.108(3) Uani 0.607(7) 1 d PD
F1B F 1.0768(9) 0.7736(5) 0.8244(8) 0.147(6) Uani 0.393(7) 1 d PD
F6A F 1.0908(3) 0.6949(6) 0.7857(3) 0.184(6) Uani 0.607(7) 1 d PD
F6B F 1.0532(10) 0.6148(6) 0.7757(13) 0.236(11) Uani 0.393(7) 1 d PD
F5A F 0.9278(5) 0.5531(4) 0.7394(4) 0.130(3) Uani 0.607(7) 1 d PD
F5B F 0.9068(7) 0.5450(8) 0.8214(7) 0.151(5) Uani 0.393(7) 1 d PD
F3A F 0.8654(4) 0.6230(5) 0.8482(4) 0.108(3) Uani 0.607(7) 1 d PD
F3B F 0.9200(18) 0.699(2) 0.8784(8) 0.340(19) Uani 0.393(7) 1 d PD
F2A F 0.9417(6) 0.7175(5) 0.7463(4) 0.095(2) Uani 0.607(7) 1 d PD
F2B F 0.9245(8) 0.6835(14) 0.7402(7) 0.176(10) Uani 0.393(7) 1 d PD
F4A F 1.0276(7) 0.6071(7) 0.8820(4) 0.182(6) Uani 0.607(7) 1 d PD
F4B F 1.0482(6) 0.6511(8) 0.9126(6) 0.124(5) Uani 0.393(7) 1 d PD
C56 C 0.0144(4) 0.4512(4) 0.4483(4) 0.0391(11) Uani 0.50 1 d P
Cl4 Cl 0.08197(7) 0.59146(6) 0.47664(6) 0.05424(19) Uani 1 1 d .
C55 C 0.7020(5) 0.1731(4) 1.0273(3) 0.0894(14) Uani 1 1 d .
Cl3A Cl 0.69481(12) 0.20331(9) 0.91866(8) 0.0734(4) Uani 0.891(3) 1 d P
Cl3B Cl 0.5679(17) 0.1526(17) 0.9946(15) 0.145(8) Uiso 0.109(3) 1 d P
Cl2 Cl 0.67353(19) 0.03581(15) 1.02118(11) 0.1305(6) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
C48 Ru1 C47 36.96(9) .
C48 Ru1 C54 77.76(9) .
C47 Ru1 C54 65.49(10) .
C48 Ru1 C46 66.77(10) .
C47 Ru1 C46 36.91(10) .
C54 Ru1 C46 36.41(9) .
C48 Ru1 P1 110.32(6) .
C47 Ru1 P1 90.82(6) .
C54 Ru1 P1 129.16(7) .
C46 Ru1 P1 98.67(6) .
C48 Ru1 C53 64.77(9) .
C47 Ru1 C53 76.76(9) .
C54 Ru1 C53 36.80(9) .
C46 Ru1 C53 65.82(9) .
P1 Ru1 C53 164.49(7) .
C48 Ru1 C49 36.92(8) .
C47 Ru1 C49 66.18(9) .
C54 Ru1 C49 65.49(9) .
C46 Ru1 C49 78.37(9) .
P1 Ru1 C49 145.78(6) .
C53 Ru1 C49 35.21(8) .
C48 Ru1 C1 175.14(8) .
C47 Ru1 C1 140.17(9) .
C54 Ru1 C1 97.44(8) .
C46 Ru1 C1 108.90(9) .
P1 Ru1 C1 72.05(5) .
C53 Ru1 C1 111.79(8) .
C49 Ru1 C1 141.53(8) .
C48 Ru1 C2 145.00(8) .
C47 Ru1 C2 154.01(9) .
C54 Ru1 C2 88.86(9) .
C46 Ru1 C2 118.14(9) .
P1 Ru1 C2 103.25(6) .
C53 Ru1 C2 85.14(8) .
C49 Ru1 C2 108.14(8) .
C1 Ru1 C2 34.36(7) .
C48 Ru1 Cl1 91.47(7) .
C47 Ru1 Cl1 120.11(7) .
C54 Ru1 Cl1 149.75(7) .
C46 Ru1 Cl1 156.88(7) .
P1 Ru1 Cl1 81.066(19) .
C53 Ru1 Cl1 113.11(6) .
C49 Ru1 Cl1 88.88(6) .
C1 Ru1 Cl1 93.11(5) .
C2 Ru1 Cl1 84.04(6) .
O2 P1 O1 101.84(8) .
O2 P1 N1 100.68(8) .
O1 P1 N1 112.17(9) .
O2 P1 Ru1 121.26(6) .
O1 P1 Ru1 106.35(6) .
N1 P1 Ru1 114.00(6) .
C25 O1 P1 126.23(13) .
C44 O2 P1 117.77(12) .
C11 N1 C13 114.55(16) .
C11 N1 P1 110.71(13) .
C13 N1 P1 125.97(13) .
C2 C1 C10 118.4(2) .
C2 C1 C11 115.50(19) .
C10 C1 C11 119.65(19) .
C2 C1 Ru1 73.09(13) .
C10 C1 Ru1 112.50(14) .
C11 C1 Ru1 107.23(13) .
C1 C2 C3 120.8(2) .
C1 C2 Ru1 72.55(12) .
C3 C2 Ru1 117.15(17) .
C1 C2 H2 113.4 .
C3 C2 H2 113.4 .
Ru1 C2 H2 113.4 .
C4 C3 C2 120.4(2) .
C4 C3 H3 119.8 .
C2 C3 H3 119.8 .
C3 C4 C5 121.6(2) .
C3 C4 H4 119.2 .
C5 C4 H4 119.2 .
C6 C5 C10 118.7(2) .
C6 C5 C4 121.0(2) .
C10 C5 C4 120.2(2) .
C7 C6 C5 121.4(3) .
C7 C6 H6 119.3 .
C5 C6 H6 119.3 .
C6 C7 C8 120.1(3) .
C6 C7 H7 120.0 .
C8 C7 H7 120.0 .
C9 C8 C7 119.8(3) .
C9 C8 H8 120.1 .
C7 C8 H8 120.1 .
C8 C9 C10 121.2(2) .
C8 C9 H9 119.4 .
C10 C9 H9 119.4 .
C9 C10 C5 118.7(2) .
C9 C10 C1 122.8(2) .
C5 C10 C1 118.4(2) .
N1 C11 C12 114.21(18) .
N1 C11 C1 111.29(16) .
C12 C11 C1 108.82(17) .
N1 C11 H11 107.4 .
C12 C11 H11 107.4 .
C1 C11 H11 107.4 .
C11 C12 H12A 109.5 .
C11 C12 H12B 109.5 .
H12A C12 H12B 109.5 .
C11 C12 H12C 109.5 .
H12A C12 H12C 109.5 .
H12B C12 H12C 109.5 .
N1 C13 C15 113.82(17) .
N1 C13 C14 111.72(17) .
C15 C13 C14 115.02(18) .
N1 C13 H13 105.0 .
C15 C13 H13 105.0 .
C14 C13 H13 105.0 .
C13 C14 H14A 109.5 .
C13 C14 H14B 109.5 .
H14A C14 H14B 109.5 .
C13 C14 H14C 109.5 .
H14A C14 H14C 109.5 .
H14B C14 H14C 109.5 .
C16 C15 C24 118.8(2) .
C16 C15 C13 121.4(2) .
C24 C15 C13 119.60(19) .
C15 C16 C17 121.4(2) .
C15 C16 H16 119.3 .
C17 C16 H16 119.3 .
C18 C17 C16 120.6(2) .
C18 C17 H17 119.7 .
C16 C17 H17 119.7 .
C17 C18 C19 120.6(2) .
C17 C18 H18 119.7 .
C19 C18 H18 119.7 .
C20 C19 C18 121.7(2) .
C20 C19 C24 119.3(2) .
C18 C19 C24 119.0(2) .
C21 C20 C19 121.4(2) .
C21 C20 H20 119.3 .
C19 C20 H20 119.3 .
C20 C21 C22 119.8(2) .
C20 C21 H21 120.1 .
C22 C21 H21 120.1 .
C23 C22 C21 120.4(3) .
C23 C22 H22 119.8 .
C21 C22 H22 119.8 .
C22 C23 C24 121.6(2) .
C22 C23 H23 119.2 .
C24 C23 H23 119.2 .
C23 C24 C19 117.5(2) .
C23 C24 C15 122.9(2) .
C19 C24 C15 119.5(2) .
C34 C25 O1 120.33(17) .
C34 C25 C26 123.29(18) .
O1 C25 C26 116.15(17) .
C27 C26 C25 119.54(19) .
C27 C26 H26 120.2 .
C25 C26 H26 120.2 .
C26 C27 C28 120.24(19) .
C26 C27 H27 119.9 .
C28 C27 H27 119.9 .
C29 C28 C27 121.00(19) .
C29 C28 C33 119.5(2) .
C27 C28 C33 119.39(19) .
C30 C29 C28 120.9(2) .
C30 C29 H29 119.5 .
C28 C29 H29 119.5 .
C29 C30 C31 119.7(2) .
C29 C30 H30 120.1 .
C31 C30 H30 120.1 .
C32 C31 C30 120.7(2) .
C32 C31 H31 119.6 .
C30 C31 H31 119.6 .
C31 C32 C33 120.8(2) .
C31 C32 H32 119.6 .
C33 C32 H32 119.6 .
C32 C33 C28 118.21(18) .
C32 C33 C34 121.94(19) .
C28 C33 C34 119.78(18) .
C25 C34 C33 116.98(18) .
C25 C34 C35 121.08(18) .
C33 C34 C35 121.94(18) .
C44 C35 C36 117.12(18) .
C44 C35 C34 120.90(18) .
C36 C35 C34 121.95(18) .
C37 C36 C41 118.2(2) .
C37 C36 C35 122.50(19) .
C41 C36 C35 119.2(2) .
C38 C37 C36 120.6(2) .
C38 C37 H37 119.7 .
C36 C37 H37 119.7 .
C37 C38 C39 121.1(2) .
C37 C38 H38 119.5 .
C39 C38 H38 119.5 .
C40 C39 C38 119.9(2) .
C40 C39 H39 120.1 .
C38 C39 H39 120.1 .
C39 C40 C41 120.8(2) .
C39 C40 H40 119.6 .
C41 C40 H40 119.6 .
C42 C41 C40 120.9(2) .
C42 C41 C36 119.8(2) .
C40 C41 C36 119.4(2) .
C43 C42 C41 121.0(2) .
C43 C42 H42 119.5 .
C41 C42 H42 119.5 .
C42 C43 C44 118.5(2) .
C42 C43 H43 120.8 .
C44 C43 H43 120.8 .
C35 C44 O2 119.79(17) .
C35 C44 C43 124.15(19) .
O2 C44 C43 116.05(18) .
C46 C45 H45A 109.5 .
C46 C45 H45B 109.5 .
H45A C45 H45B 109.5 .
C46 C45 H45C 109.5 .
H45A C45 H45C 109.5 .
H45B C45 H45C 109.5 .
C54 C46 C47 116.9(2) .
C54 C46 C45 120.2(3) .
C47 C46 C45 122.9(2) .
C54 C46 Ru1 70.36(14) .
C47 C46 Ru1 69.93(13) .
C45 C46 Ru1 131.84(18) .
C48 C47 C46 121.4(2) .
C48 C47 Ru1 71.21(13) .
C46 C47 Ru1 73.16(14) .
C48 C47 H47 118.8 .
C46 C47 H47 118.8 .
Ru1 C47 H47 118.8 .
C47 C48 C49 121.3(2) .
C47 C48 Ru1 71.83(13) .
C49 C48 Ru1 75.27(13) .
C47 C48 H48 119.2 .
C49 C48 H48 119.2 .
Ru1 C48 H48 119.2 .
C53 C49 C48 117.5(2) .
C53 C49 C50 122.4(2) .
C48 C49 C50 120.1(2) .
C53 C49 Ru1 72.06(13) .
C48 C49 Ru1 67.81(12) .
C50 C49 Ru1 130.26(17) .
C52 C50 C49 114.2(2) .
C52 C50 C51 110.2(2) .
C49 C50 C51 107.7(3) .
C52 C50 H50 108.2 .
C49 C50 H50 108.2 .
C51 C50 H50 108.2 .
C50 C51 H51A 109.5 .
C50 C51 H51B 109.5 .
H51A C51 H51B 109.5 .
C50 C51 H51C 109.5 .
H51A C51 H51C 109.5 .
H51B C51 H51C 109.5 .
C50 C52 H52A 109.5 .
C50 C52 H52B 109.5 .
H52A C52 H52B 109.5 .
C50 C52 H52C 109.5 .
H52A C52 H52C 109.5 .
H52B C52 H52C 109.5 .
C49 C53 C54 120.6(2) .
C49 C53 Ru1 72.73(13) .
C54 C53 Ru1 68.68(12) .
C49 C53 H53 118.9 .
C54 C53 H53 118.9 .
Ru1 C53 H53 118.9 .
C46 C54 C53 122.2(2) .
C46 C54 Ru1 73.23(14) .
C53 C54 Ru1 74.52(13) .
C46 C54 H54 118.7 .
C53 C54 H54 118.7 .
Ru1 C54 H54 118.7 .
F6B P2 F3B 168.2(9) .
F6B P2 F4A 70.6(8) .
F3B P2 F4A 97.8(5) .
F6B P2 F2B 102.5(10) .
F3B P2 F2B 89.3(5) .
F4A P2 F2B 166.2(7) .
F6B P2 F6A 39.5(3) .
F3B P2 F6A 141.1(11) .
F4A P2 F6A 88.4(4) .
F2B P2 F6A 93.4(5) .
F6B P2 F5B 88.9(4) .
F3B P2 F5B 88.2(11) .
F4A P2 F5B 64.5(6) .
F2B P2 F5B 104.2(7) .
F6A P2 F5B 128.2(5) .
F6B P2 F1A 127.8(6) .
F3B P2 F1A 47.1(11) .
F4A P2 F1A 88.8(4) .
F2B P2 F1A 104.6(8) .
F6A P2 F1A 95.0(2) .
F5B P2 F1A 125.4(5) .
F6B P2 F3A 141.9(4) .
F3B P2 F3A 38.5(11) .
F4A P2 F3A 94.6(3) .
F2B P2 F3A 83.7(6) .
F6A P2 F3A 177.0(3) .
F5B P2 F3A 53.5(5) .
F1A P2 F3A 85.1(4) .
F6B P2 F5A 61.1(6) .
F3B P2 F5A 124.1(11) .
F4A P2 F5A 94.6(3) .
F2B P2 F5A 71.7(7) .
F6A P2 F5A 93.3(2) .
F5B P2 F5A 50.0(4) .
F1A P2 F5A 171.1(3) .
F3A P2 F5A 86.4(3) .
F6B P2 F1B 86.0(4) .
F3B P2 F1B 95.1(11) .
F4A P2 F1B 106.0(5) .
F2B P2 F1B 84.9(4) .
F6A P2 F1B 46.7(4) .
F5B P2 F1B 170.3(6) .
F1A P2 F1B 53.4(5) .
F3A P2 F1B 132.1(5) .
F5A P2 F1B 132.7(5) .
F6B P2 F2A 105.9(8) .
F3B P2 F2A 85.5(6) .
F4A P2 F2A 175.6(5) .
F2B P2 F2A 15.2(7) .
F6A P2 F2A 87.1(4) .
F5B P2 F2A 118.7(5) .
F1A P2 F2A 91.3(3) .
F3A P2 F2A 89.8(2) .
F5A P2 F2A 85.9(3) .
F1B P2 F2A 70.7(4) .
F6B P2 F4B 84.3(9) .
F3B P2 F4B 84.0(3) .
F4A P2 F4B 23.3(5) .
F2B P2 F4B 170.3(8) .
F6A P2 F4B 87.5(4) .
F5B P2 F4B 82.6(4) .
F1A P2 F4B 65.8(5) .
F3A P2 F4B 95.3(4) .
F5A P2 F4B 117.9(4) .
F1B P2 F4B 88.7(5) .
F2A P2 F4B 155.9(4) .
F3B F1A F1B 119.4(7) .
F3B F1A P2 63.3(7) .
F1B F1A P2 65.0(3) .
F3B F1A F4B 88.4(9) .
F1B F1A F4B 91.2(5) .
P2 F1A F4B 59.3(3) .
F6A F1B F1A 116.8(7) .
F6A F1B P2 63.1(3) .
F1A F1B P2 61.5(5) .
F6B F6A F1B 136.8(8) .
F6B F6A P2 66.9(5) .
F1B F6A P2 70.2(5) .
F6A F6B P2 73.6(5) .
F6A F6B F5A 122.8(13) .
P2 F6B F5A 63.9(5) .
F6A F6B F4A 98.2(12) .
P2 F6B F4A 55.5(5) .
F5A F6B F4A 88.0(4) .
F5B F5A F6B 92.7(8) .
F5B F5A P2 62.3(4) .
F6B F5A P2 55.0(4) .
F5A F5B F3A 106.4(10) .
F5A F5B P2 67.8(5) .
F3A F5B P2 65.8(5) .
F5A F5B F4A 101.0(5) .
F3A F5B F4A 97.2(5) .
P2 F5B F4A 56.5(3) .
F3B F3A F5B 118.3(8) .
F3B F3A P2 64.6(6) .
F5B F3A P2 60.7(4) .
F3A F3B F1A 144.6(10) .
F3A F3B P2 76.8(9) .
F1A F3B P2 69.6(6) .
F4B F4A P2 91.4(11) .
F4B F4A F5B 130.8(13) .
P2 F4A F5B 59.0(5) .
F4B F4A F6B 117.2(15) .
P2 F4A F6B 53.9(5) .
F5B F4A F6B 78.3(6) .
F4A F4B P2 65.3(9) .
F4A F4B F1A 119.7(11) .
P2 F4B F1A 54.9(3) .
Cl4 C56 Cl4 109.1(3) 2_566
C56 Cl4 C56 70.9(3) 2_566
Cl3B C55 Cl3A 75.5(7) .
Cl3B C55 Cl2 94.1(8) .
Cl3A C55 Cl2 111.6(2) .
C55 Cl3A Cl3B 51.1(6) .
C55 Cl3B Cl3A 53.5(6) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ru1 C48 2.208(2) .
Ru1 C47 2.216(2) .
Ru1 C54 2.221(2) .
Ru1 C46 2.258(2) .
Ru1 P1 2.2783(5) .
Ru1 C53 2.298(2) .
Ru1 C49 2.306(2) .
Ru1 C1 2.379(2) .
Ru1 C2 2.386(2) .
Ru1 Cl1 2.3926(6) .
P1 O2 1.6041(14) .
P1 O1 1.6103(15) .
P1 N1 1.6504(17) .
O1 C25 1.401(2) .
O2 C44 1.397(2) .
N1 C11 1.487(3) .
N1 C13 1.502(3) .
C1 C2 1.407(3) .
C1 C10 1.472(3) .
C1 C11 1.529(3) .
C2 C3 1.442(3) .
C2 H2 1.0000 .
C3 C4 1.334(4) .
C3 H3 0.9500 .
C4 C5 1.433(4) .
C4 H4 0.9500 .
C5 C6 1.409(4) .
C5 C10 1.417(3) .
C6 C7 1.362(5) .
C6 H6 0.9500 .
C7 C8 1.399(4) .
C7 H7 0.9500 .
C8 C9 1.381(3) .
C8 H8 0.9500 .
C9 C10 1.401(3) .
C9 H9 0.9500 .
C11 C12 1.529(3) .
C11 H11 1.0000 .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 C15 1.516(3) .
C13 C14 1.534(3) .
C13 H13 1.0000 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 C16 1.375(3) .
C15 C24 1.432(3) .
C16 C17 1.409(4) .
C16 H16 0.9500 .
C17 C18 1.355(4) .
C17 H17 0.9500 .
C18 C19 1.419(4) .
C18 H18 0.9500 .
C19 C20 1.417(4) .
C19 C24 1.421(3) .
C20 C21 1.360(4) .
C20 H20 0.9500 .
C21 C22 1.402(4) .
C21 H21 0.9500 .
C22 C23 1.369(3) .
C22 H22 0.9500 .
C23 C24 1.418(3) .
C23 H23 0.9500 .
C25 C34 1.373(3) .
C25 C26 1.404(3) .
C26 C27 1.362(3) .
C26 H26 0.9500 .
C27 C28 1.417(3) .
C27 H27 0.9500 .
C28 C29 1.414(3) .
C28 C33 1.423(3) .
C29 C30 1.366(3) .
C29 H29 0.9500 .
C30 C31 1.415(3) .
C30 H30 0.9500 .
C31 C32 1.367(3) .
C31 H31 0.9500 .
C32 C33 1.421(3) .
C32 H32 0.9500 .
C33 C34 1.434(3) .
C34 C35 1.487(3) .
C35 C44 1.374(3) .
C35 C36 1.439(3) .
C36 C37 1.419(3) .
C36 C41 1.423(3) .
C37 C38 1.369(3) .
C37 H37 0.9500 .
C38 C39 1.399(4) .
C38 H38 0.9500 .
C39 C40 1.368(4) .
C39 H39 0.9500 .
C40 C41 1.417(3) .
C40 H40 0.9500 .
C41 C42 1.413(3) .
C42 C43 1.364(3) .
C42 H42 0.9500 .
C43 C44 1.404(3) .
C43 H43 0.9500 .
C45 C46 1.515(4) .
C45 H45A 0.9800 .
C45 H45B 0.9800 .
C45 H45C 0.9800 .
C46 C54 1.400(4) .
C46 C47 1.417(4) .
C47 C48 1.402(4) .
C47 H47 1.0000 .
C48 C49 1.432(3) .
C48 H48 1.0000 .
C49 C53 1.392(3) .
C49 C50 1.504(3) .
C50 C52 1.504(4) .
C50 C51 1.551(4) .
C50 H50 1.0000 .
C51 H51A 0.9800 .
C51 H51B 0.9800 .
C51 H51C 0.9800 .
C52 H52A 0.9800 .
C52 H52B 0.9800 .
C52 H52C 0.9800 .
C53 C54 1.428(3) .
C53 H53 1.0000 .
C54 H54 1.0000 .
P2 F6B 1.450(7) .
P2 F3B 1.476(7) .
P2 F4A 1.479(5) .
P2 F2B 1.484(9) .
P2 F6A 1.513(4) .
P2 F5B 1.520(9) .
P2 F1A 1.548(4) .
P2 F3A 1.590(5) .
P2 F5A 1.590(4) .
P2 F1B 1.596(8) .
P2 F2A 1.606(6) .
P2 F4B 1.628(8) .
F1A F3B 1.21(3) .
F1A F1B 1.414(13) .
F1A F4B 1.725(12) .
F1B F6A 1.233(9) .
F6A F6B 1.002(8) .
F6B F5A 1.551(14) .
F6B F4A 1.694(17) .
F5A F5B 1.316(10) .
F5B F3A 1.402(13) .
F5B F4A 1.601(10) .
F3A F3B 1.02(3) .
F4A F4B 0.645(12) .
C56 Cl4 1.752(5) .
C56 Cl4 1.807(6) 2_566
Cl4 C56 1.807(6) 2_566
C55 Cl3B 1.70(2) .
C55 Cl3A 1.757(5) .
C55 Cl2 1.763(6) .
Cl3A Cl3B 2.12(2) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C48 Ru1 P1 O2 37.45(10) . .
C47 Ru1 P1 O2 69.58(10) . .
C54 Ru1 P1 O2 128.02(11) . .
C46 Ru1 P1 O2 105.80(10) . .
C53 Ru1 P1 O2 106.0(2) . .
C49 Ru1 P1 O2 23.77(13) . .
C1 Ru1 P1 O2 -147.04(9) . .
C2 Ru1 P1 O2 -132.46(9) . .
Cl1 Ru1 P1 O2 -50.79(7) . .
C48 Ru1 P1 O1 -77.91(9) . .
C47 Ru1 P1 O1 -45.78(9) . .
C54 Ru1 P1 O1 12.66(11) . .
C46 Ru1 P1 O1 -9.56(9) . .
C53 Ru1 P1 O1 -9.3(2) . .
C49 Ru1 P1 O1 -91.59(12) . .
C1 Ru1 P1 O1 97.60(8) . .
C2 Ru1 P1 O1 112.18(8) . .
Cl1 Ru1 P1 O1 -166.15(6) . .
C48 Ru1 P1 N1 157.96(10) . .
C47 Ru1 P1 N1 -169.91(10) . .
C54 Ru1 P1 N1 -111.47(11) . .
C46 Ru1 P1 N1 -133.69(10) . .
C53 Ru1 P1 N1 -133.5(2) . .
C49 Ru1 P1 N1 144.28(13) . .
C1 Ru1 P1 N1 -26.53(9) . .
C2 Ru1 P1 N1 -11.95(9) . .
Cl1 Ru1 P1 N1 69.71(7) . .
O2 P1 O1 C25 32.32(17) . .
N1 P1 O1 C25 -74.53(17) . .
Ru1 P1 O1 C25 160.21(14) . .
O1 P1 O2 C44 55.02(15) . .
N1 P1 O2 C44 170.60(14) . .
Ru1 P1 O2 C44 -62.62(15) . .
O2 P1 N1 C11 138.80(14) . .
O1 P1 N1 C11 -113.61(14) . .
Ru1 P1 N1 C11 7.34(15) . .
O2 P1 N1 C13 -6.63(18) . .
O1 P1 N1 C13 100.97(17) . .
Ru1 P1 N1 C13 -138.08(15) . .
C48 Ru1 C1 C2 -85.8(9) . .
C47 Ru1 C1 C2 -137.12(15) . .
C54 Ru1 C1 C2 -76.89(15) . .
C46 Ru1 C1 C2 -112.48(14) . .
P1 Ru1 C1 C2 154.27(14) . .
C53 Ru1 C1 C2 -41.72(15) . .
C49 Ru1 C1 C2 -17.4(2) . .
Cl1 Ru1 C1 C2 74.71(13) . .
C48 Ru1 C1 C10 28.5(10) . .
C47 Ru1 C1 C10 -22.8(2) . .
C54 Ru1 C1 C10 37.41(16) . .
C46 Ru1 C1 C10 1.81(17) . .
P1 Ru1 C1 C10 -91.43(15) . .
C53 Ru1 C1 C10 72.58(17) . .
C49 Ru1 C1 C10 96.87(18) . .
C2 Ru1 C1 C10 114.3(2) . .
Cl1 Ru1 C1 C10 -171.00(14) . .
C48 Ru1 C1 C11 162.0(9) . .
C47 Ru1 C1 C11 110.74(16) . .
C54 Ru1 C1 C11 170.97(14) . .
C46 Ru1 C1 C11 135.38(14) . .
P1 Ru1 C1 C11 42.13(12) . .
C53 Ru1 C1 C11 -153.86(14) . .
C49 Ru1 C1 C11 -129.56(15) . .
C2 Ru1 C1 C11 -112.1(2) . .
Cl1 Ru1 C1 C11 -37.43(13) . .
C10 C1 C2 C3 4.8(3) . .
C11 C1 C2 C3 -146.9(2) . .
Ru1 C1 C2 C3 111.7(2) . .
C10 C1 C2 Ru1 -106.89(19) . .
C11 C1 C2 Ru1 101.42(17) . .
C48 Ru1 C2 C1 171.54(15) . .
C47 Ru1 C2 C1 96.0(2) . .
C54 Ru1 C2 C1 105.00(14) . .
C46 Ru1 C2 C1 82.45(15) . .
P1 Ru1 C2 C1 -25.10(14) . .
C53 Ru1 C2 C1 141.67(14) . .
C49 Ru1 C2 C1 168.70(13) . .
Cl1 Ru1 C2 C1 -104.44(13) . .
C48 Ru1 C2 C3 55.3(3) . .
C47 Ru1 C2 C3 -20.3(3) . .
C54 Ru1 C2 C3 -11.3(2) . .
C46 Ru1 C2 C3 -33.8(2) . .
P1 Ru1 C2 C3 -141.36(18) . .
C53 Ru1 C2 C3 25.41(19) . .
C49 Ru1 C2 C3 52.4(2) . .
C1 Ru1 C2 C3 -116.3(3) . .
Cl1 Ru1 C2 C3 139.30(19) . .
C1 C2 C3 C4 -1.7(4) . .
Ru1 C2 C3 C4 83.4(3) . .
C2 C3 C4 C5 -2.6(4) . .
C3 C4 C5 C6 -178.2(3) . .
C3 C4 C5 C10 3.4(4) . .
C10 C5 C6 C7 1.8(4) . .
C4 C5 C6 C7 -176.6(3) . .
C5 C6 C7 C8 -1.0(5) . .
C6 C7 C8 C9 0.1(5) . .
C7 C8 C9 C10 0.1(4) . .
C8 C9 C10 C5 0.6(4) . .
C8 C9 C10 C1 177.5(2) . .
C6 C5 C10 C9 -1.5(4) . .
C4 C5 C10 C9 176.8(2) . .
C6 C5 C10 C1 -178.5(2) . .
C4 C5 C10 C1 -0.2(3) . .
C2 C1 C10 C9 179.3(2) . .
C11 C1 C10 C9 -30.2(3) . .
Ru1 C1 C10 C9 97.0(2) . .
C2 C1 C10 C5 -3.8(3) . .
C11 C1 C10 C5 146.7(2) . .
Ru1 C1 C10 C5 -86.1(2) . .
C13 N1 C11 C12 -56.4(2) . .
P1 N1 C11 C12 153.92(16) . .
C13 N1 C11 C1 179.89(17) . .
P1 N1 C11 C1 30.2(2) . .
C2 C1 C11 N1 -131.91(19) . .
C10 C1 C11 N1 76.8(2) . .
Ru1 C1 C11 N1 -52.83(19) . .
C2 C1 C11 C12 101.4(2) . .
C10 C1 C11 C12 -49.9(3) . .
Ru1 C1 C11 C12 -179.54(14) . .
C11 N1 C13 C15 157.99(17) . .
P1 N1 C13 C15 -57.7(2) . .
C11 N1 C13 C14 -69.7(2) . .
P1 N1 C13 C14 74.6(2) . .
N1 C13 C15 C16 115.0(2) . .
C14 C13 C15 C16 -15.7(3) . .
N1 C13 C15 C24 -70.9(2) . .
C14 C13 C15 C24 158.43(19) . .
C24 C15 C16 C17 0.8(3) . .
C13 C15 C16 C17 175.0(2) . .
C15 C16 C17 C18 0.6(4) . .
C16 C17 C18 C19 -0.9(4) . .
C17 C18 C19 C20 179.7(2) . .
C17 C18 C19 C24 -0.3(4) . .
C18 C19 C20 C21 179.3(2) . .
C24 C19 C20 C21 -0.7(4) . .
C19 C20 C21 C22 -1.2(4) . .
C20 C21 C22 C23 1.7(4) . .
C21 C22 C23 C24 -0.2(4) . .
C22 C23 C24 C19 -1.6(3) . .
C22 C23 C24 C15 178.8(2) . .
C20 C19 C24 C23 2.1(3) . .
C18 C19 C24 C23 -177.9(2) . .
C20 C19 C24 C15 -178.3(2) . .
C18 C19 C24 C15 1.7(3) . .
C16 C15 C24 C23 177.7(2) . .
C13 C15 C24 C23 3.4(3) . .
C16 C15 C24 C19 -1.9(3) . .
C13 C15 C24 C19 -176.23(19) . .
P1 O1 C25 C34 -62.8(2) . .
P1 O1 C25 C26 122.52(17) . .
C34 C25 C26 C27 2.9(3) . .
O1 C25 C26 C27 177.35(18) . .
C25 C26 C27 C28 4.4(3) . .
C26 C27 C28 C29 171.8(2) . .
C26 C27 C28 C33 -4.7(3) . .
C27 C28 C29 C30 -174.3(2) . .
C33 C28 C29 C30 2.2(3) . .
C28 C29 C30 C31 -0.9(4) . .
C29 C30 C31 C32 -1.0(4) . .
C30 C31 C32 C33 1.7(4) . .
C31 C32 C33 C28 -0.4(3) . .
C31 C32 C33 C34 176.6(2) . .
C29 C28 C33 C32 -1.5(3) . .
C27 C28 C33 C32 174.99(19) . .
C29 C28 C33 C34 -178.5(2) . .
C27 C28 C33 C34 -2.0(3) . .
O1 C25 C34 C33 176.38(17) . .
C26 C25 C34 C33 -9.3(3) . .
O1 C25 C34 C35 -3.3(3) . .
C26 C25 C34 C35 170.97(19) . .
C32 C33 C34 C25 -168.2(2) . .
C28 C33 C34 C25 8.7(3) . .
C32 C33 C34 C35 11.5(3) . .
C28 C33 C34 C35 -171.58(19) . .
C25 C34 C35 C44 51.0(3) . .
C33 C34 C35 C44 -128.7(2) . .
C25 C34 C35 C36 -126.7(2) . .
C33 C34 C35 C36 53.7(3) . .
C44 C35 C36 C37 -171.8(2) . .
C34 C35 C36 C37 5.9(3) . .
C44 C35 C36 C41 5.2(3) . .
C34 C35 C36 C41 -177.13(19) . .
C41 C36 C37 C38 2.2(3) . .
C35 C36 C37 C38 179.2(2) . .
C36 C37 C38 C39 0.2(4) . .
C37 C38 C39 C40 -1.6(4) . .
C38 C39 C40 C41 0.4(4) . .
C39 C40 C41 C42 -176.4(2) . .
C39 C40 C41 C36 2.1(4) . .
C37 C36 C41 C42 175.1(2) . .
C35 C36 C41 C42 -1.9(3) . .
C37 C36 C41 C40 -3.3(3) . .
C35 C36 C41 C40 179.6(2) . .
C40 C41 C42 C43 177.1(2) . .
C36 C41 C42 C43 -1.4(3) . .
C41 C42 C43 C44 1.3(3) . .
C36 C35 C44 O2 175.27(17) . .
C34 C35 C44 O2 -2.5(3) . .
C36 C35 C44 C43 -5.5(3) . .
C34 C35 C44 C43 176.75(19) . .
P1 O2 C44 C35 -75.2(2) . .
P1 O2 C44 C43 105.53(18) . .
C42 C43 C44 C35 2.3(3) . .
C42 C43 C44 O2 -178.43(19) . .
C48 Ru1 C46 C54 -101.14(16) . .
C47 Ru1 C46 C54 -129.9(2) . .
P1 Ru1 C46 C54 150.40(14) . .
C53 Ru1 C46 C54 -29.54(14) . .
C49 Ru1 C46 C54 -64.26(15) . .
C1 Ru1 C46 C54 76.50(15) . .
C2 Ru1 C46 C54 40.25(17) . .
Cl1 Ru1 C46 C54 -122.06(18) . .
C48 Ru1 C46 C47 28.77(13) . .
C54 Ru1 C46 C47 129.9(2) . .
P1 Ru1 C46 C47 -79.70(13) . .
C53 Ru1 C46 C47 100.36(15) . .
C49 Ru1 C46 C47 65.65(14) . .
C1 Ru1 C46 C47 -153.60(13) . .
C2 Ru1 C46 C47 170.15(13) . .
Cl1 Ru1 C46 C47 7.8(2) . .
C48 Ru1 C46 C45 145.5(3) . .
C47 Ru1 C46 C45 116.7(3) . .
C54 Ru1 C46 C45 -113.4(3) . .
P1 Ru1 C46 C45 37.0(3) . .
C53 Ru1 C46 C45 -142.9(3) . .
C49 Ru1 C46 C45 -177.6(3) . .
C1 Ru1 C46 C45 -36.9(3) . .
C2 Ru1 C46 C45 -73.1(3) . .
Cl1 Ru1 C46 C45 124.6(3) . .
C54 C46 C47 C48 -0.5(3) . .
C45 C46 C47 C48 177.8(2) . .
Ru1 C46 C47 C48 -54.6(2) . .
C54 C46 C47 Ru1 54.10(19) . .
C45 C46 C47 Ru1 -127.6(2) . .
C54 Ru1 C47 C48 102.61(15) . .
C46 Ru1 C47 C48 132.6(2) . .
P1 Ru1 C47 C48 -123.95(13) . .
C53 Ru1 C47 C48 65.44(14) . .
C49 Ru1 C47 C48 29.90(13) . .
C1 Ru1 C47 C48 173.69(13) . .
C2 Ru1 C47 C48 112.5(2) . .
Cl1 Ru1 C47 C48 -43.81(15) . .
C48 Ru1 C47 C46 -132.6(2) . .
C54 Ru1 C47 C46 -30.03(14) . .
P1 Ru1 C47 C46 103.41(13) . .
C53 Ru1 C47 C46 -67.20(14) . .
C49 Ru1 C47 C46 -102.74(15) . .
C1 Ru1 C47 C46 41.05(19) . .
C2 Ru1 C47 C46 -20.1(3) . .
Cl1 Ru1 C47 C46 -176.45(11) . .
C46 C47 C48 C49 -3.6(3) . .
Ru1 C47 C48 C49 -59.2(2) . .
C46 C47 C48 Ru1 55.5(2) . .
C54 Ru1 C48 C47 -65.31(15) . .
C46 Ru1 C48 C47 -28.73(14) . .
P1 Ru1 C48 C47 62.19(14) . .
C53 Ru1 C48 C47 -101.84(16) . .
C49 Ru1 C48 C47 -130.6(2) . .
C1 Ru1 C48 C47 -56.2(10) . .
C2 Ru1 C48 C47 -135.10(16) . .
Cl1 Ru1 C48 C47 143.20(13) . .
C47 Ru1 C48 C49 130.6(2) . .
C54 Ru1 C48 C49 65.30(15) . .
C46 Ru1 C48 C49 101.88(16) . .
P1 Ru1 C48 C49 -167.20(12) . .
C53 Ru1 C48 C49 28.77(14) . .
C1 Ru1 C48 C49 74.4(10) . .
C2 Ru1 C48 C49 -4.5(2) . .
Cl1 Ru1 C48 C49 -86.19(14) . .
C47 C48 C49 C53 3.5(3) . .
Ru1 C48 C49 C53 -54.06(19) . .
C47 C48 C49 C50 -177.7(2) . .
Ru1 C48 C49 C50 124.8(2) . .
C47 C48 C49 Ru1 57.54(19) . .
C48 Ru1 C49 C53 131.0(2) . .
C47 Ru1 C49 C53 101.04(16) . .
C54 Ru1 C49 C53 28.32(15) . .
C46 Ru1 C49 C53 64.31(15) . .
P1 Ru1 C49 C53 152.64(12) . .
C1 Ru1 C49 C53 -41.5(2) . .
C2 Ru1 C49 C53 -51.75(16) . .
Cl1 Ru1 C49 C53 -135.11(14) . .
C47 Ru1 C49 C48 -29.93(15) . .
C54 Ru1 C49 C48 -102.64(16) . .
C46 Ru1 C49 C48 -66.66(15) . .
P1 Ru1 C49 C48 21.7(2) . .
C53 Ru1 C49 C48 -131.0(2) . .
C1 Ru1 C49 C48 -172.47(14) . .
C2 Ru1 C49 C48 177.29(14) . .
Cl1 Ru1 C49 C48 93.93(14) . .
C48 Ru1 C49 C50 -111.3(3) . .
C47 Ru1 C49 C50 -141.3(2) . .
C54 Ru1 C49 C50 146.0(2) . .
C46 Ru1 C49 C50 -178.0(2) . .
P1 Ru1 C49 C50 -89.7(2) . .
C53 Ru1 C49 C50 117.7(3) . .
C1 Ru1 C49 C50 76.2(3) . .
C2 Ru1 C49 C50 65.9(2) . .
Cl1 Ru1 C49 C50 -17.4(2) . .
C53 C49 C50 C52 35.3(3) . .
C48 C49 C50 C52 -143.5(2) . .
Ru1 C49 C50 C52 -58.2(3) . .
C53 C49 C50 C51 -87.5(3) . .
C48 C49 C50 C51 93.7(3) . .
Ru1 C49 C50 C51 179.0(2) . .
C48 C49 C53 C54 0.8(3) . .
C50 C49 C53 C54 -178.0(2) . .
Ru1 C49 C53 C54 -51.2(2) . .
C48 C49 C53 Ru1 52.00(18) . .
C50 C49 C53 Ru1 -126.8(2) . .
C48 Ru1 C53 C49 -30.09(14) . .
C47 Ru1 C53 C49 -67.29(15) . .
C54 Ru1 C53 C49 -133.9(2) . .
C46 Ru1 C53 C49 -104.65(16) . .
P1 Ru1 C53 C49 -104.9(2) . .
C1 Ru1 C53 C49 153.64(14) . .
C2 Ru1 C53 C49 131.50(15) . .
Cl1 Ru1 C53 C49 50.10(15) . .
C48 Ru1 C53 C54 103.80(17) . .
C47 Ru1 C53 C54 66.61(16) . .
C46 Ru1 C53 C54 29.25(15) . .
P1 Ru1 C53 C54 29.0(3) . .
C49 Ru1 C53 C54 133.9(2) . .
C1 Ru1 C53 C54 -72.46(16) . .
C2 Ru1 C53 C54 -94.60(15) . .
Cl1 Ru1 C53 C54 -176.00(13) . .
C47 C46 C54 C53 4.9(3) . .
C45 C46 C54 C53 -173.5(2) . .
Ru1 C46 C54 C53 58.7(2) . .
C47 C46 C54 Ru1 -53.89(19) . .
C45 C46 C54 Ru1 127.7(2) . .
C49 C53 C54 C46 -5.1(4) . .
Ru1 C53 C54 C46 -58.1(2) . .
C49 C53 C54 Ru1 53.1(2) . .
C48 Ru1 C54 C46 67.31(15) . .
C47 Ru1 C54 C46 30.42(15) . .
P1 Ru1 C54 C46 -39.04(18) . .
C53 Ru1 C54 C46 131.3(2) . .
C49 Ru1 C54 C46 104.17(16) . .
C1 Ru1 C54 C46 -111.91(15) . .
C2 Ru1 C54 C46 -145.26(15) . .
Cl1 Ru1 C54 C46 138.65(14) . .
C48 Ru1 C54 C53 -64.02(15) . .
C47 Ru1 C54 C53 -100.91(16) . .
C46 Ru1 C54 C53 -131.3(2) . .
P1 Ru1 C54 C53 -170.37(11) . .
C49 Ru1 C54 C53 -27.17(14) . .
C1 Ru1 C54 C53 116.76(14) . .
C2 Ru1 C54 C53 83.41(15) . .
Cl1 Ru1 C54 C53 7.3(2) . .
F6B P2 F1A F3B -166.0(10) . .
F4A P2 F1A F3B -101.8(8) . .
F2B P2 F1A F3B 75.1(8) . .
F6A P2 F1A F3B 169.9(8) . .
F5B P2 F1A F3B -44.7(10) . .
F3A P2 F1A F3B -7.1(8) . .
F5A P2 F1A F3B 11(3) . .
F1B P2 F1A F3B 147.2(9) . .
F2A P2 F1A F3B 82.6(8) . .
F4B P2 F1A F3B -105.2(8) . .
F6B P2 F1A F1B 46.8(10) . .
F3B P2 F1A F1B -147.2(9) . .
F4A P2 F1A F1B 111.0(6) . .
F2B P2 F1A F1B -72.1(4) . .
F6A P2 F1A F1B 22.7(5) . .
F5B P2 F1A F1B 168.1(7) . .
F3A P2 F1A F1B -154.3(5) . .
F5A P2 F1A F1B -136(2) . .
F2A P2 F1A F1B -64.6(6) . .
F4B P2 F1A F1B 107.6(5) . .
F6B P2 F1A F4B -60.8(9) . .
F3B P2 F1A F4B 105.2(8) . .
F4A P2 F1A F4B 3.4(6) . .
F2B P2 F1A F4B -179.8(5) . .
F6A P2 F1A F4B -85.0(4) . .
F5B P2 F1A F4B 60.5(7) . .
F3A P2 F1A F4B 98.1(4) . .
F5A P2 F1A F4B 116(2) . .
F1B P2 F1A F4B -107.6(5) . .
F2A P2 F1A F4B -172.2(4) . .
F3B F1A F1B F6A -65.6(14) . .
P2 F1A F1B F6A -31.8(7) . .
F4B F1A F1B F6A 23.3(9) . .
F3B F1A F1B P2 -33.8(10) . .
F4B F1A F1B P2 55.1(3) . .
F6B P2 F1B F6A 3.4(10) . .
F3B P2 F1B F6A 171.6(6) . .
F4A P2 F1B F6A 72.0(6) . .
F2B P2 F1B F6A -99.5(8) . .
F5B P2 F1B F6A 61(4) . .
F1A P2 F1B F6A 148.1(7) . .
F3A P2 F1B F6A -176.2(4) . .
F5A P2 F1B F6A -40.3(8) . .
F2A P2 F1B F6A -104.9(7) . .
F4B P2 F1B F6A 87.8(6) . .
F6B P2 F1B F1A -144.7(9) . .
F3B P2 F1B F1A 23.5(6) . .
F4A P2 F1B F1A -76.2(5) . .
F2B P2 F1B F1A 112.4(8) . .
F6A P2 F1B F1A -148.1(7) . .
F5B P2 F1B F1A -87(4) . .
F3A P2 F1B F1A 35.6(7) . .
F5A P2 F1B F1A 171.6(4) . .
F2A P2 F1B F1A 106.9(5) . .
F4B P2 F1B F1A -60.4(5) . .
F1A F1B F6A F6B 24(2) . .
P2 F1B F6A F6B -7(2) . .
F1A F1B F6A P2 31.3(7) . .
F3B P2 F6A F6B 161.3(14) . .
F4A P2 F6A F6B 60.7(14) . .
F2B P2 F6A F6B -105.6(16) . .
F5B P2 F6A F6B 5.5(15) . .
F1A P2 F6A F6B 149.4(14) . .
F3A P2 F6A F6B -118(7) . .
F5A P2 F6A F6B -33.8(14) . .
F1B P2 F6A F6B 174.6(16) . .
F2A P2 F6A F6B -119.5(14) . .
F4B P2 F6A F6B 84.0(14) . .
F6B P2 F6A F1B -174.6(16) . .
F3B P2 F6A F1B -13.3(10) . .
F4A P2 F6A F1B -113.9(6) . .
F2B P2 F6A F1B 79.8(8) . .
F5B P2 F6A F1B -169.2(7) . .
F1A P2 F6A F1B -25.2(7) . .
F3A P2 F6A F1B 67(6) . .
F5A P2 F6A F1B 151.6(6) . .
F2A P2 F6A F1B 65.9(6) . .
F4B P2 F6A F1B -90.6(7) . .
F1B F6A F6B P2 7(2) . .
F1B F6A F6B F5A 50(3) . .
P2 F6A F6B F5A 42.7(9) . .
F1B F6A F6B F4A -43(2) . .
P2 F6A F6B F4A -50.3(4) . .
F3B P2 F6B F6A -100(5) . .
F4A P2 F6B F6A -112.4(13) . .
F2B P2 F6B F6A 80.0(13) . .
F5B P2 F6B F6A -175.7(12) . .
F1A P2 F6B F6A -39.9(16) . .
F3A P2 F6B F6A 175.6(5) . .
F5A P2 F6B F6A 140.6(15) . .
F1B P2 F6B F6A -3.9(11) . .
F2A P2 F6B F6A 64.7(12) . .
F4B P2 F6B F6A -93.0(12) . .
F3B P2 F6B F5A 119(6) . .
F4A P2 F6B F5A 106.9(4) . .
F2B P2 F6B F5A -60.7(7) . .
F6A P2 F6B F5A -140.6(15) . .
F5B P2 F6B F5A 43.6(6) . .
F1A P2 F6B F5A 179.5(5) . .
F3A P2 F6B F5A 35.0(15) . .
F1B P2 F6B F5A -144.6(6) . .
F2A P2 F6B F5A -76.0(4) . .
F4B P2 F6B F5A 126.3(5) . .
F3B P2 F6B F4A 13(5) . .
F2B P2 F6B F4A -167.6(7) . .
F6A P2 F6B F4A 112.4(13) . .
F5B P2 F6B F4A -63.3(5) . .
F1A P2 F6B F4A 72.6(7) . .
F3A P2 F6B F4A -71.9(13) . .
F5A P2 F6B F4A -106.9(4) . .
F1B P2 F6B F4A 108.5(6) . .
F2A P2 F6B F4A 177.1(4) . .
F4B P2 F6B F4A 19.4(5) . .
F6A F6B F5A F5B -99.4(16) . .
P2 F6B F5A F5B -53.0(8) . .
F4A F6B F5A F5B -0.9(7) . .
F6A F6B F5A P2 -46.4(11) . .
F4A F6B F5A P2 52.1(4) . .
F6B P2 F5A F5B 115.7(10) . .
F3B P2 F5A F5B -51.9(9) . .
F4A P2 F5A F5B 50.8(7) . .
F2B P2 F5A F5B -128.0(8) . .
F6A P2 F5A F5B 139.5(8) . .
F1A P2 F5A F5B -62(2) . .
F3A P2 F5A F5B -43.5(7) . .
F1B P2 F5A F5B 167.6(8) . .
F2A P2 F5A F5B -133.6(8) . .
F4B P2 F5A F5B 50.6(9) . .
F3B P2 F5A F6B -167.6(9) . .
F4A P2 F5A F6B -64.9(8) . .
F2B P2 F5A F6B 116.3(9) . .
F6A P2 F5A F6B 23.8(8) . .
F5B P2 F5A F6B -115.7(10) . .
F1A P2 F5A F6B -177(2) . .
F3A P2 F5A F6B -159.2(8) . .
F1B P2 F5A F6B 51.9(9) . .
F2A P2 F5A F6B 110.7(8) . .
F4B P2 F5A F6B -65.1(8) . .
F6B F5A F5B F3A 102.0(6) . .
P2 F5A F5B F3A 54.4(4) . .
F6B F5A F5B P2 47.6(5) . .
F6B F5A F5B F4A 1.0(8) . .
P2 F5A F5B F4A -46.7(4) . .
F6B P2 F5B F5A -52.1(10) . .
F3B P2 F5B F5A 139.3(8) . .
F4A P2 F5B F5A -121.1(6) . .
F2B P2 F5B F5A 50.5(8) . .
F6A P2 F5B F5A -55.6(8) . .
F1A P2 F5B F5A 170.4(4) . .
F3A P2 F5B F5A 121.3(8) . .
F1B P2 F5B F5A -110(3) . .
F2A P2 F5B F5A 55.4(8) . .
F4B P2 F5B F5A -136.5(8) . .
F6B P2 F5B F3A -173.4(9) . .
F3B P2 F5B F3A 18.1(7) . .
F4A P2 F5B F3A 117.6(5) . .
F2B P2 F5B F3A -70.8(8) . .
F6A P2 F5B F3A -176.8(4) . .
F1A P2 F5B F3A 49.1(7) . .
F5A P2 F5B F3A -121.3(8) . .
F1B P2 F5B F3A 129(4) . .
F2A P2 F5B F3A -65.9(5) . .
F4B P2 F5B F3A 102.3(5) . .
F6B P2 F5B F4A 69.0(9) . .
F3B P2 F5B F4A -99.5(6) . .
F2B P2 F5B F4A 171.6(7) . .
F6A P2 F5B F4A 65.6(5) . .
F1A P2 F5B F4A -68.5(6) . .
F3A P2 F5B F4A -117.6(5) . .
F5A P2 F5B F4A 121.1(6) . .
F1B P2 F5B F4A 11(4) . .
F2A P2 F5B F4A 176.5(4) . .
F4B P2 F5B F4A -15.3(5) . .
F5A F5B F3A F3B -86.3(12) . .
P2 F5B F3A F3B -30.7(10) . .
F4A F5B F3A F3B 17.5(12) . .
F5A F5B F3A P2 -55.6(4) . .
F4A F5B F3A P2 48.2(4) . .
F6B P2 F3A F3B 160.9(15) . .
F4A P2 F3A F3B 96.8(8) . .
F2B P2 F3A F3B -96.9(8) . .
F6A P2 F3A F3B -85(7) . .
F5B P2 F3A F3B 150.2(10) . .
F1A P2 F3A F3B 8.4(8) . .
F5A P2 F3A F3B -168.9(8) . .
F1B P2 F3A F3B -19.7(10) . .
F2A P2 F3A F3B -83.0(8) . .
F4B P2 F3A F3B 73.4(7) . .
F6B P2 F3A F5B 10.8(15) . .
F3B P2 F3A F5B -150.2(10) . .
F4A P2 F3A F5B -53.3(6) . .
F2B P2 F3A F5B 112.9(9) . .
F6A P2 F3A F5B 125(6) . .
F1A P2 F3A F5B -141.8(6) . .
F5A P2 F3A F5B 41.0(6) . .
F1B P2 F3A F5B -169.8(7) . .
F2A P2 F3A F5B 126.8(6) . .
F4B P2 F3A F5B -76.7(5) . .
F5B F3A F3B F1A 11(3) . .
P2 F3A F3B F1A -18.7(19) . .
F5B F3A F3B P2 29.5(10) . .
F1B F1A F3B F3A 54(3) . .
P2 F1A F3B F3A 19.4(19) . .
F4B F1A F3B F3A -37(2) . .
F1B F1A F3B P2 34.3(9) . .
F4B F1A F3B P2 -56.2(4) . .
F6B P2 F3B F3A -99(5) . .
F4A P2 F3B F3A -87.5(7) . .
F2B P2 F3B F3A 80.7(9) . .
F6A P2 F3B F3A 175.2(5) . .
F5B P2 F3B F3A -23.6(8) . .
F1A P2 F3B F3A -168.6(12) . .
F5A P2 F3B F3A 13.5(10) . .
F1B P2 F3B F3A 165.5(7) . .
F2A P2 F3B F3A 95.4(7) . .
F4B P2 F3B F3A -106.4(7) . .
F6B P2 F3B F1A 69(6) . .
F4A P2 F3B F1A 81.1(8) . .
F2B P2 F3B F1A -110.7(9) . .
F6A P2 F3B F1A -16.2(10) . .
F5B P2 F3B F1A 145.0(7) . .
F3A P2 F3B F1A 168.6(12) . .
F5A P2 F3B F1A -177.9(5) . .
F1B P2 F3B F1A -25.9(7) . .
F2A P2 F3B F1A -96.0(7) . .
F4B P2 F3B F1A 62.2(7) . .
F6B P2 F4A F4B 123.2(15) . .
F3B P2 F4A F4B -54.2(15) . .
F2B P2 F4A F4B -175(2) . .
F6A P2 F4A F4B 87.2(13) . .
F5B P2 F4A F4B -138.5(14) . .
F1A P2 F4A F4B -7.8(13) . .
F3A P2 F4A F4B -92.8(13) . .
F5A P2 F4A F4B -179.6(13) . .
F1B P2 F4A F4B 43.5(15) . .
F2A P2 F4A F4B 85(5) . .
F6B P2 F4A F5B -98.3(5) . .
F3B P2 F4A F5B 84.3(11) . .
F2B P2 F4A F5B -36(3) . .
F6A P2 F4A F5B -134.3(4) . .
F1A P2 F4A F5B 130.7(5) . .
F3A P2 F4A F5B 45.6(5) . .
F5A P2 F4A F5B -41.1(4) . .
F1B P2 F4A F5B -178.1(6) . .
F2A P2 F4A F5B -137(5) . .
F4B P2 F4A F5B 138.5(14) . .
F3B P2 F4A F6B -177.4(12) . .
F2B P2 F4A F6B 62(3) . .
F6A P2 F4A F6B -36.0(5) . .
F5B P2 F4A F6B 98.3(5) . .
F1A P2 F4A F6B -131.0(5) . .
F3A P2 F4A F6B 143.9(5) . .
F5A P2 F4A F6B 57.2(5) . .
F1B P2 F4A F6B -79.8(6) . .
F2A P2 F4A F6B -38(5) . .
F4B P2 F4A F6B -123.2(15) . .
F5A F5B F4A F4B 115.0(18) . .
F3A F5B F4A F4B 7(2) . .
P2 F5B F4A F4B 61.2(18) . .
F5A F5B F4A P2 53.8(6) . .
F3A F5B F4A P2 -54.6(6) . .
F5A F5B F4A F6B -0.9(7) . .
F3A F5B F4A F6B -109.3(6) . .
P2 F5B F4A F6B -54.7(4) . .
F6A F6B F4A F4B -6(2) . .
P2 F6B F4A F4B -70.1(14) . .
F5A F6B F4A F4B -129.3(13) . .
F6A F6B F4A P2 63.6(9) . .
F5A F6B F4A P2 -59.3(5) . .
F6A F6B F4A F5B 123.7(12) . .
P2 F6B F4A F5B 60.0(6) . .
F5A F6B F4A F5B 0.8(6) . .
F5B F4A F4B P2 -48.7(12) . .
F6B F4A F4B P2 49.4(8) . .
P2 F4A F4B F1A 8.1(13) . .
F5B F4A F4B F1A -41(2) . .
F6B F4A F4B F1A 57.5(18) . .
F6B P2 F4B F4A -52.5(13) . .
F3B P2 F4B F4A 126.1(16) . .
F2B P2 F4B F4A 173(3) . .
F6A P2 F4B F4A -91.9(14) . .
F5B P2 F4B F4A 37.1(13) . .
F1A P2 F4B F4A 171.4(14) . .
F3A P2 F4B F4A 89.2(13) . .
F5A P2 F4B F4A 0.5(15) . .
F1B P2 F4B F4A -138.6(14) . .
F2A P2 F4B F4A -169.1(11) . .
F6B P2 F4B F1A 136.1(4) . .
F3B P2 F4B F1A -45.3(11) . .
F4A P2 F4B F1A -171.4(14) . .
F2B P2 F4B F1A 1(3) . .
F6A P2 F4B F1A 96.6(3) . .
F5B P2 F4B F1A -134.3(6) . .
F3A P2 F4B F1A -82.2(4) . .
F5A P2 F4B F1A -171.0(4) . .
F1B P2 F4B F1A 50.0(5) . .
F2A P2 F4B F1A 19.4(12) . .
F3B F1A F4B F4A 50.6(16) . .
F1B F1A F4B F4A -68.7(17) . .
P2 F1A F4B F4A -8.9(15) . .
F3B F1A F4B P2 59.6(5) . .
F1B F1A F4B P2 -59.8(5) . .
Cl4 C56 Cl4 C56 0.0 2_566 2_566
Cl2 C55 Cl3A Cl3B 88.7(8) . .
Cl2 C55 Cl3B Cl3A -111.3(3) . .
