#------------------------------------------------------------------------------
#$Date: 2017-02-04 03:15:38 +0200 (Sat, 04 Feb 2017) $
#$Revision: 191286 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/08/69/4086983.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4086983
loop_
_publ_author_name
'Chen, Yi-Ting'
'Krytchankou, Ilya S.'
'Karttunen, Antti J.'
'Grachova, Elena V.'
'Tunik, Sergey P.'
'Chou, Pi-Tai'
'Koshevoy, Igor O.'
_publ_section_title
;
 Silver Alkynyl-Phosphine Clusters: An Electronic Effect of the Alkynes
 Defines Structural Diversity
;
_journal_issue                   2
_journal_name_full               Organometallics
_journal_page_first              480
_journal_paper_doi               10.1021/acs.organomet.6b00866
_journal_volume                  36
_journal_year                    2017
_chemical_formula_moiety         'C106 H110 Ag8 F6 O8 P6 S2, 2(C F3 O3 S)'
_chemical_formula_sum            'C108 H110 Ag8 F12 O14 P6 S4'
_chemical_formula_weight         3036.97
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                112.562(2)
_cell_angle_beta                 99.276(2)
_cell_angle_gamma                94.822(2)
_cell_formula_units_Z            1
_cell_length_a                   13.8948(9)
_cell_length_b                   14.7416(10)
_cell_length_c                   15.8355(11)
_cell_measurement_reflns_used    9528
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      33.07
_cell_measurement_theta_min      2.24
_cell_volume                     2918.1(3)
_computing_cell_refinement       'SAINT (Bruker AXS, 2009)'
_computing_data_collection       'APEX2 (Bruker AXS, 2010)'
_computing_data_reduction        'SAINT (Bruker AXS, 2009)'
_computing_molecular_graphics    'Diamond v.4.03 (Brandenburg, 2014)'
_computing_publication_material  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device       '62mm x 62mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  'Bruker KAPPA APEX II DUO CCD'
_diffrn_measurement_method       'φ scans and ω scans with κ offset'
_diffrn_radiation_monochromator  'curved graphite crystal'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0467
_diffrn_reflns_av_unetI/netI     0.0349
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            120578
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.999
_diffrn_reflns_theta_min         1.842
_exptl_absorpt_coefficient_mu    1.544
_exptl_absorpt_correction_T_max  0.909
_exptl_absorpt_correction_T_min  0.833
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2008)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.728
_exptl_crystal_description       block
_exptl_crystal_F_000             1508
_exptl_crystal_size_max          0.123
_exptl_crystal_size_mid          0.114
_exptl_crystal_size_min          0.063
_refine_diff_density_max         2.510
_refine_diff_density_min         -1.504
_refine_diff_density_rms         0.133
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     737
_refine_ls_number_reflns         18515
_refine_ls_number_restraints     202
_refine_ls_restrained_S_all      1.052
_refine_ls_R_factor_all          0.0540
_refine_ls_R_factor_gt           0.0390
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0592P)²+2.7933P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1008
_refine_ls_wR_factor_ref         0.1068
_reflns_Friedel_coverage         0.000
_reflns_number_gt                14748
_reflns_number_total             18515
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            8_9.cif
_cod_data_source_block           9
_cod_database_code               4086983
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.833
_shelx_estimated_absorpt_t_max   0.909
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 1.1515(2) 0.4440(2) 0.3989(2) 0.0202(5) Uani 1 1 d . . . . .
C2 C 1.2300(2) 0.4827(2) 0.3942(2) 0.0207(6) Uani 1 1 d . . . . .
C3 C 1.3270(2) 0.5272(2) 0.3878(2) 0.0257(6) Uani 1 1 d . . . . .
C4 C 1.3670(3) 0.6230(3) 0.4759(3) 0.0398(9) Uani 1 1 d . . . . .
H12A H 1.4310 0.6525 0.4718 0.060 Uiso 1 1 calc R U . . .
H12B H 1.3204 0.6702 0.4809 0.060 Uiso 1 1 calc R U . . .
H12C H 1.3750 0.6073 0.5312 0.060 Uiso 1 1 calc R U . . .
C5 C 1.3982(2) 0.4514(3) 0.3800(3) 0.0321(7) Uani 1 1 d . . . . .
H13A H 1.4628 0.4796 0.3757 0.048 Uiso 1 1 calc R U . . .
H13B H 1.4056 0.4360 0.4354 0.048 Uiso 1 1 calc R U . . .
H13C H 1.3717 0.3904 0.3238 0.048 Uiso 1 1 calc R U . . .
C6 C 1.3124(3) 0.5508(3) 0.3004(3) 0.0310(7) Uani 1 1 d . . . . .
H11A H 1.3759 0.5803 0.2953 0.047 Uiso 1 1 calc R U . . .
H11B H 1.2863 0.4894 0.2446 0.047 Uiso 1 1 calc R U . . .
H11C H 1.2655 0.5979 0.3058 0.047 Uiso 1 1 calc R U . . .
C7 C 0.9556(2) 0.3341(2) 0.5272(2) 0.0187(5) Uani 1 1 d . . . . .
C8 C 0.9257(2) 0.2731(2) 0.5559(2) 0.0196(5) Uani 1 1 d . . . . .
C9 C 0.8995(3) 0.1957(2) 0.5895(2) 0.0257(6) Uani 1 1 d . . . . .
C10 C 0.9008(4) 0.2447(3) 0.6944(3) 0.0443(10) Uani 1 1 d . . . . .
H7A H 0.8835 0.1933 0.7168 0.066 Uiso 1 1 calc R U . . .
H7B H 0.9670 0.2813 0.7282 0.066 Uiso 1 1 calc R U . . .
H7C H 0.8528 0.2908 0.7052 0.066 Uiso 1 1 calc R U . . .
C11 C 0.9753(3) 0.1246(3) 0.5708(3) 0.0399(9) Uani 1 1 d . . . . .
H5A H 0.9593 0.0725 0.5926 0.060 Uiso 1 1 calc R U . . .
H5B H 0.9736 0.0942 0.5035 0.060 Uiso 1 1 calc R U . . .
H5C H 1.0414 0.1617 0.6042 0.060 Uiso 1 1 calc R U . . .
C12 C 0.7955(3) 0.1391(3) 0.5361(3) 0.0445(10) Uani 1 1 d . . . . .
H6A H 0.7776 0.0875 0.5581 0.067 Uiso 1 1 calc R U . . .
H6B H 0.7479 0.1856 0.5472 0.067 Uiso 1 1 calc R U . . .
H6C H 0.7946 0.1081 0.4690 0.067 Uiso 1 1 calc R U . . .
C13 C 0.81284(19) 0.31774(19) 0.17693(19) 0.0139(5) Uani 1 1 d . . . . .
H1 H 0.7644 0.2974 0.1164 0.017 Uiso 1 1 calc R U . . .
C14 C 0.9053(2) 0.16665(19) 0.04201(19) 0.0165(5) Uani 1 1 d . . . . .
C15 C 0.9957(2) 0.1419(2) 0.0217(2) 0.0219(6) Uani 1 1 d . . . . .
H15 H 1.0516 0.1578 0.0711 0.026 Uiso 1 1 calc R U . . .
C16 C 1.0048(3) 0.0935(2) -0.0711(2) 0.0288(7) Uani 1 1 d . . . . .
H16 H 1.0668 0.0769 -0.0846 0.035 Uiso 1 1 calc R U . . .
C17 C 0.9238(3) 0.0700(2) -0.1430(2) 0.0282(7) Uani 1 1 d . . . . .
H17 H 0.9300 0.0371 -0.2060 0.034 Uiso 1 1 calc R U . . .
C18 C 0.8334(3) 0.0945(2) -0.1231(2) 0.0265(6) Uani 1 1 d . . . . .
H18 H 0.7777 0.0785 -0.1727 0.032 Uiso 1 1 calc R U . . .
C19 C 0.8238(2) 0.1423(2) -0.0308(2) 0.0212(6) Uani 1 1 d . . . . .
H19 H 0.7615 0.1584 -0.0175 0.025 Uiso 1 1 calc R U . . .
C20 C 0.8463(2) 0.12239(19) 0.1878(2) 0.0168(5) Uani 1 1 d . . . . .
C21 C 0.8903(2) 0.1092(2) 0.2664(2) 0.0236(6) Uani 1 1 d . . . . .
H21 H 0.9449 0.1562 0.3094 0.028 Uiso 1 1 calc R U . . .
C22 C 0.8548(3) 0.0269(3) 0.2828(3) 0.0322(7) Uani 1 1 d . . . . .
H22 H 0.8859 0.0174 0.3361 0.039 Uiso 1 1 calc R U . . .
C23 C 0.7743(3) -0.0401(2) 0.2212(3) 0.0340(8) Uani 1 1 d . . . . .
H23 H 0.7491 -0.0950 0.2331 0.041 Uiso 1 1 calc R U . . .
C24 C 0.7297(2) -0.0282(2) 0.1420(2) 0.0265(7) Uani 1 1 d . . . . .
H24 H 0.6744 -0.0748 0.0998 0.032 Uiso 1 1 calc R U . . .
C25 C 0.7663(2) 0.0522(2) 0.1246(2) 0.0202(6) Uani 1 1 d . . . . .
H25 H 0.7369 0.0596 0.0696 0.024 Uiso 1 1 calc R U . . .
C26 C 0.6467(4) 0.2173(4) 0.2227(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
C27 C 0.6216(4) 0.1704(4) 0.2791(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
H27 H 0.6573 0.1926 0.3417 0.033 Uiso 0.522(9) 1 calc R U P A 3
C28 C 0.5441(4) 0.0911(4) 0.2439(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
H28 H 0.5269 0.0590 0.2825 0.033 Uiso 0.522(9) 1 calc R U P A 3
C29 C 0.4917(3) 0.0586(3) 0.1523(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
H29 H 0.4388 0.0044 0.1282 0.033 Uiso 0.522(9) 1 calc R U P A 3
C30 C 0.5168(4) 0.1055(4) 0.0958(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
H30 H 0.4811 0.0833 0.0332 0.033 Uiso 0.522(9) 1 calc R U P A 3
C31 C 0.5943(5) 0.1848(5) 0.1310(5) 0.0277(6) Uani 0.522(9) 1 d G . P A 3
H31 H 0.6115 0.2169 0.0924 0.033 Uiso 0.522(9) 1 calc R U P A 3
C271 C 0.6454(5) 0.1798(5) 0.2987(5) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
H271 H 0.6903 0.2057 0.3576 0.033 Uiso 0.478(9) 1 calc R U P A 4
C281 C 0.5707(5) 0.1007(4) 0.2769(5) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
H281 H 0.5644 0.0724 0.3209 0.033 Uiso 0.478(9) 1 calc R U P A 4
C291 C 0.5051(4) 0.0628(4) 0.1908(6) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
H291 H 0.4540 0.0087 0.1759 0.033 Uiso 0.478(9) 1 calc R U P A 4
C301 C 0.5143(4) 0.1041(4) 0.1264(5) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
H301 H 0.4694 0.0783 0.0675 0.033 Uiso 0.478(9) 1 calc R U P A 4
C311 C 0.5891(5) 0.1833(5) 0.1482(5) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
H311 H 0.5954 0.2115 0.1042 0.033 Uiso 0.478(9) 1 calc R U P A 4
C261 C 0.6546(4) 0.2211(5) 0.2343(6) 0.0277(6) Uani 0.478(9) 1 d G U P A 4
C32 C 0.6780(2) 0.4305(2) 0.2847(2) 0.0186(5) Uani 1 1 d . . . . .
C33 C 0.6088(2) 0.4314(2) 0.2112(2) 0.0241(6) Uani 1 1 d . . . . .
H33 H 0.5936 0.3755 0.1527 0.029 Uiso 1 1 calc R U . . .
C34 C 0.5617(3) 0.5133(3) 0.2227(3) 0.0348(8) Uani 1 1 d . . . . .
H34 H 0.5149 0.5137 0.1721 0.042 Uiso 1 1 calc R U . . .
C35 C 0.5831(3) 0.5944(3) 0.3079(4) 0.0490(12) Uani 1 1 d . . . . .
H35 H 0.5524 0.6514 0.3155 0.059 Uiso 1 1 calc R U . . .
C36 C 0.6492(3) 0.5924(3) 0.3821(4) 0.0525(13) Uani 1 1 d . . . . .
H36 H 0.6619 0.6470 0.4413 0.063 Uiso 1 1 calc R U . . .
C37 C 0.6968(3) 0.5115(3) 0.3704(3) 0.0333(8) Uani 1 1 d . . . . .
H37 H 0.7430 0.5112 0.4214 0.040 Uiso 1 1 calc R U . . .
C38 C 0.8121(2) 0.5271(2) 0.1854(2) 0.0171(5) Uani 1 1 d . . . . .
C39 C 0.7444(2) 0.5031(2) 0.1013(2) 0.0235(6) Uani 1 1 d . . . . .
H39 H 0.7327 0.4375 0.0539 0.028 Uiso 1 1 calc R U . . .
C40 C 0.6946(2) 0.5757(3) 0.0874(3) 0.0286(7) Uani 1 1 d . . . . .
H40 H 0.6482 0.5592 0.0306 0.034 Uiso 1 1 calc R U . . .
C41 C 0.7121(2) 0.6717(3) 0.1554(3) 0.0338(8) Uani 1 1 d . . . . .
H41 H 0.6794 0.7213 0.1443 0.041 Uiso 1 1 calc R U . . .
C42 C 0.7766(3) 0.6957(3) 0.2393(3) 0.0373(9) Uani 1 1 d . . . . .
H42 H 0.7870 0.7612 0.2868 0.045 Uiso 1 1 calc R U . . .
C43 C 0.8270(2) 0.6227(2) 0.2542(2) 0.0255(6) Uani 1 1 d . . . . .
H43 H 0.8716 0.6391 0.3120 0.031 Uiso 1 1 calc R U . . .
C44 C 0.9581(2) 0.41415(19) 0.11259(19) 0.0147(5) Uani 1 1 d . . . . .
C45 C 0.9103(2) 0.3671(2) 0.0189(2) 0.0193(5) Uani 1 1 d . . . . .
H45 H 0.8408 0.3461 0.0027 0.023 Uiso 1 1 calc R U . . .
C46 C 0.9641(2) 0.3506(2) -0.0510(2) 0.0239(6) Uani 1 1 d . . . . .
H46 H 0.9312 0.3174 -0.1148 0.029 Uiso 1 1 calc R U . . .
C47 C 1.0639(3) 0.3820(2) -0.0287(2) 0.0266(7) Uani 1 1 d . . . . .
H47 H 1.1000 0.3705 -0.0769 0.032 Uiso 1 1 calc R U . . .
C48 C 1.1127(2) 0.4306(2) 0.0643(2) 0.0254(6) Uani 1 1 d . . . . .
H48 H 1.1819 0.4531 0.0796 0.030 Uiso 1 1 calc R U . . .
C49 C 1.0602(2) 0.4463(2) 0.1354(2) 0.0193(5) Uani 1 1 d . . . . .
H49 H 1.0936 0.4786 0.1991 0.023 Uiso 1 1 calc R U . . .
C52 C 1.2503(3) 0.1431(3) 0.1286(3) 0.0345(8) Uani 1 1 d . . . . .
H52A H 1.2987 0.1120 0.0927 0.052 Uiso 1 1 calc R U . . .
H52B H 1.2647 0.1409 0.1904 0.052 Uiso 1 1 calc R U . . .
H52C H 1.1838 0.1070 0.0954 0.052 Uiso 1 1 calc R U . . .
C53 C 1.2561(2) 0.2490(2) 0.1399(2) 0.0256(6) Uani 1 1 d . . . . .
C54 C 1.3314(3) 0.2856(3) 0.0976(3) 0.0470(11) Uani 1 1 d . . . . .
H54A H 1.3667 0.2315 0.0667 0.071 Uiso 1 1 calc R U . . .
H54B H 1.2982 0.3084 0.0516 0.071 Uiso 1 1 calc R U . . .
H54C H 1.3785 0.3411 0.1469 0.071 Uiso 1 1 calc R U . . .
O1 O 1.1397(2) 0.17532(19) 0.30609(19) 0.0359(6) Uani 1 1 d . . . . .
O2 O 1.16611(19) 0.25010(19) 0.47540(18) 0.0339(5) Uani 1 1 d . . . . .
O7 O 1.20272(16) 0.30368(16) 0.18238(16) 0.0249(5) Uani 1 1 d . . . . .
C50 C 1.2946(11) 0.1454(10) 0.4056(9) 0.043(3) Uani 0.68(3) 1 d . U P B 1
F1 F 1.3514(6) 0.2203(7) 0.4032(9) 0.061(3) Uani 0.68(3) 1 d . U P B 1
F2 F 1.3050(9) 0.0613(9) 0.3367(9) 0.067(3) Uani 0.68(3) 1 d . U P B 1
F3 F 1.3264(8) 0.1375(8) 0.4847(5) 0.064(3) Uani 0.68(3) 1 d . U P B 1
O3 O 1.1130(9) 0.0717(10) 0.3867(9) 0.044(2) Uani 0.68(3) 1 d . U P B 1
F31 F 1.3528(13) 0.1699(15) 0.4667(11) 0.053(5) Uani 0.32(3) 1 d . U P B 2
F11 F 1.3380(11) 0.2371(10) 0.3699(15) 0.045(4) Uani 0.32(3) 1 d . U P B 2
F21 F 1.3128(15) 0.0801(15) 0.3174(14) 0.040(3) Uani 0.32(3) 1 d . U P B 2
C501 C 1.300(2) 0.1594(17) 0.3841(17) 0.029(4) Uani 0.32(3) 1 d . U P B 2
O31 O 1.142(2) 0.069(2) 0.394(2) 0.046(5) Uani 0.32(3) 1 d . U P B 2
P1 P 0.90253(5) 0.22613(5) 0.16585(5) 0.01310(12) Uani 1 1 d . . . . .
P2 P 0.74667(5) 0.32838(6) 0.27286(5) 0.01794(14) Uani 1 1 d . . . . .
P3 P 0.89042(5) 0.44110(5) 0.20658(5) 0.01270(12) Uani 1 1 d . . . . .
S1 S 1.16614(6) 0.16250(6) 0.39187(6) 0.02710(16) Uani 1 1 d . . . . .
Ag1 Ag 1.06563(2) 0.30433(2) 0.26596(2) 0.01641(5) Uani 1 1 d . . . . .
Ag2 Ag 0.85489(16) 0.3430(3) 0.40981(18) 0.0268(3) Uani 0.653(18) 1 d . . P A 7
Ag21 Ag 0.8567(3) 0.3706(9) 0.4264(6) 0.0300(9) Uani 0.347(18) 1 d . . P A 8
Ag3 Ag 1.00572(2) 0.50272(2) 0.35787(2) 0.01734(5) Uani 1 1 d . . . . .
Ag4 Ag 1.06408(2) 0.38225(2) 0.46678(2) 0.01811(5) Uani 1 1 d . . . . .
S2 S 0.55381(9) 0.26782(10) 0.91489(10) 0.0328(3) Uani 0.769(2) 1 d D U P C 5
F4 F 0.6563(5) 0.2646(5) 0.7910(4) 0.1149(11) Uani 0.769(2) 1 d D U P C 5
F5 F 0.4940(5) 0.2015(5) 0.7323(4) 0.1149(11) Uani 0.769(2) 1 d D U P C 5
F6 F 0.6043(6) 0.1238(5) 0.7743(5) 0.1149(11) Uani 0.769(2) 1 d D U P C 5
O4 O 0.5360(3) 0.3653(3) 0.9273(4) 0.0663(15) Uani 0.769(2) 1 d D U P C 5
O5 O 0.4712(3) 0.2035(5) 0.9103(4) 0.0536(15) Uani 0.769(2) 1 d D U P C 5
O6 O 0.6424(5) 0.2648(6) 0.9729(5) 0.0415(16) Uani 0.769(2) 1 d D U P C 5
C51 C 0.5803(6) 0.2132(6) 0.8003(6) 0.082(2) Uani 0.769(2) 1 d D U P C 5
S21 S 0.5708(3) 0.2308(3) 0.9066(3) 0.0328(3) Uani 0.231(2) 1 d D . P C 6
F51 F 0.5597(18) 0.2789(14) 0.7622(9) 0.1149(11) Uani 0.231(2) 1 d D U P C 6
F41 F 0.6897(12) 0.3402(14) 0.8621(15) 0.1149(11) Uani 0.231(2) 1 d D U P C 6
F61 F 0.5660(19) 0.4072(9) 0.9129(14) 0.1149(11) Uani 0.231(2) 1 d D U P C 6
O41 O 0.5987(13) 0.1427(10) 0.8356(11) 0.079(5) Uani 0.231(2) 1 d D U P C 6
O51 O 0.4684(8) 0.1874(13) 0.8694(10) 0.037(4) Uani 0.231(2) 1 d D U P C 6
O61 O 0.6362(18) 0.263(3) 0.9968(11) 0.041(6) Uani 0.231(2) 1 d D U P C 6
C511 C 0.5914(12) 0.3201(10) 0.8570(10) 0.082(2) Uani 0.231(2) 1 d D U P C 6
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C2 C1 Ag4 151.4(3) . .
C2 C1 Ag1 117.4(2) . .
Ag4 C1 Ag1 82.27(10) . .
C2 C1 Ag3 119.1(2) . .
Ag4 C1 Ag3 83.68(10) . .
Ag1 C1 Ag3 78.45(9) . .
C1 C2 C3 178.3(3) . .
C2 C3 C4 109.3(3) . .
C2 C3 C5 108.3(3) . .
C4 C3 C5 110.1(3) . .
C2 C3 C6 108.5(3) . .
C4 C3 C6 110.0(3) . .
C5 C3 C6 110.4(3) . .
C3 C4 H12A 109.5 . .
C3 C4 H12B 109.5 . .
H12A C4 H12B 109.5 . .
C3 C4 H12C 109.5 . .
H12A C4 H12C 109.5 . .
H12B C4 H12C 109.5 . .
C3 C5 H13A 109.5 . .
C3 C5 H13B 109.5 . .
H13A C5 H13B 109.5 . .
C3 C5 H13C 109.5 . .
H13A C5 H13C 109.5 . .
H13B C5 H13C 109.5 . .
C3 C6 H11A 109.5 . .
C3 C6 H11B 109.5 . .
H11A C6 H11B 109.5 . .
C3 C6 H11C 109.5 . .
H11A C6 H11C 109.5 . .
H11B C6 H11C 109.5 . .
C8 C7 Ag4 147.5(2) . .
C8 C7 Ag21 120.8(3) . .
Ag4 C7 Ag21 81.83(14) . .
C8 C7 Ag2 115.8(2) . .
Ag4 C7 Ag2 82.32(12) . .
C8 C7 Ag3 113.5(2) . 2_766
Ag4 C7 Ag3 84.60(10) . 2_766
Ag21 C7 Ag3 95.1(3) . 2_766
Ag2 C7 Ag3 105.18(16) . 2_766
C7 C8 C9 174.0(3) . .
C8 C9 C11 108.1(3) . .
C8 C9 C10 109.4(3) . .
C11 C9 C10 110.6(3) . .
C8 C9 C12 109.0(3) . .
C11 C9 C12 110.2(3) . .
C10 C9 C12 109.6(3) . .
C9 C10 H7A 109.5 . .
C9 C10 H7B 109.5 . .
H7A C10 H7B 109.5 . .
C9 C10 H7C 109.5 . .
H7A C10 H7C 109.5 . .
H7B C10 H7C 109.5 . .
C9 C11 H5A 109.5 . .
C9 C11 H5B 109.5 . .
H5A C11 H5B 109.5 . .
C9 C11 H5C 109.5 . .
H5A C11 H5C 109.5 . .
H5B C11 H5C 109.5 . .
C9 C12 H6A 109.5 . .
C9 C12 H6B 109.5 . .
H6A C12 H6B 109.5 . .
C9 C12 H6C 109.5 . .
H6A C12 H6C 109.5 . .
H6B C12 H6C 109.5 . .
P2 C13 P3 109.13(13) . .
P2 C13 P1 111.27(14) . .
P3 C13 P1 105.66(13) . .
P2 C13 H1 110.2 . .
P3 C13 H1 110.2 . .
P1 C13 H1 110.2 . .
C15 C14 C19 119.4(3) . .
C15 C14 P1 115.9(2) . .
C19 C14 P1 124.6(2) . .
C14 C15 C16 120.3(3) . .
C14 C15 H15 119.8 . .
C16 C15 H15 119.8 . .
C17 C16 C15 120.0(3) . .
C17 C16 H16 120.0 . .
C15 C16 H16 120.0 . .
C16 C17 C18 119.9(3) . .
C16 C17 H17 120.0 . .
C18 C17 H17 120.0 . .
C17 C18 C19 120.3(3) . .
C17 C18 H18 119.8 . .
C19 C18 H18 119.8 . .
C14 C19 C18 120.0(3) . .
C14 C19 H19 120.0 . .
C18 C19 H19 120.0 . .
C21 C20 C25 119.2(3) . .
C21 C20 P1 118.1(2) . .
C25 C20 P1 122.5(2) . .
C20 C21 C22 120.4(3) . .
C20 C21 H21 119.8 . .
C22 C21 H21 119.8 . .
C23 C22 C21 119.6(3) . .
C23 C22 H22 120.2 . .
C21 C22 H22 120.2 . .
C22 C23 C24 120.6(3) . .
C22 C23 H23 119.7 . .
C24 C23 H23 119.7 . .
C23 C24 C25 119.7(3) . .
C23 C24 H24 120.1 . .
C25 C24 H24 120.1 . .
C24 C25 C20 120.3(3) . .
C24 C25 H25 119.8 . .
C20 C25 H25 119.8 . .
C27 C26 C31 120.0 . .
C27 C26 P2 119.5(4) . .
C31 C26 P2 120.4(4) . .
C28 C27 C26 120.0 . .
C28 C27 H27 120.0 . .
C26 C27 H27 120.0 . .
C27 C28 C29 120.0 . .
C27 C28 H28 120.0 . .
C29 C28 H28 120.0 . .
C30 C29 C28 120.0 . .
C30 C29 H29 120.0 . .
C28 C29 H29 120.0 . .
C31 C30 C29 120.0 . .
C31 C30 H30 120.0 . .
C29 C30 H30 120.0 . .
C30 C31 C26 120.0 . .
C30 C31 H31 120.0 . .
C26 C31 H31 120.0 . .
C281 C271 C261 120.0 . .
C281 C271 H271 120.0 . .
C261 C271 H271 120.0 . .
C291 C281 C271 120.0 . .
C291 C281 H281 120.0 . .
C271 C281 H281 120.0 . .
C301 C291 C281 120.0 . .
C301 C291 H291 120.0 . .
C281 C291 H291 120.0 . .
C291 C301 C311 120.0 . .
C291 C301 H301 120.0 . .
C311 C301 H301 120.0 . .
C261 C311 C301 120.0 . .
C261 C311 H311 120.0 . .
C301 C311 H311 120.0 . .
C311 C261 C271 120.0 . .
C311 C261 P2 123.6(4) . .
C271 C261 P2 116.2(4) . .
C37 C32 C33 118.9(3) . .
C37 C32 P2 118.3(3) . .
C33 C32 P2 122.7(2) . .
C34 C33 C32 120.4(3) . .
C34 C33 H33 119.8 . .
C32 C33 H33 119.8 . .
C35 C34 C33 119.9(4) . .
C35 C34 H34 120.0 . .
C33 C34 H34 120.0 . .
C36 C35 C34 119.9(4) . .
C36 C35 H35 120.1 . .
C34 C35 H35 120.1 . .
C37 C36 C35 120.2(4) . .
C37 C36 H36 119.9 . .
C35 C36 H36 119.9 . .
C36 C37 C32 120.6(4) . .
C36 C37 H37 119.7 . .
C32 C37 H37 119.7 . .
C43 C38 C39 119.3(3) . .
C43 C38 P3 117.2(2) . .
C39 C38 P3 123.3(2) . .
C40 C39 C38 119.8(3) . .
C40 C39 H39 120.1 . .
C38 C39 H39 120.1 . .
C41 C40 C39 120.5(3) . .
C41 C40 H40 119.7 . .
C39 C40 H40 119.7 . .
C42 C41 C40 120.3(3) . .
C42 C41 H41 119.8 . .
C40 C41 H41 119.8 . .
C41 C42 C43 119.5(3) . .
C41 C42 H42 120.2 . .
C43 C42 H42 120.2 . .
C38 C43 C42 120.5(3) . .
C38 C43 H43 119.7 . .
C42 C43 H43 119.7 . .
C45 C44 C49 119.4(3) . .
C45 C44 P3 121.7(2) . .
C49 C44 P3 118.8(2) . .
C46 C45 C44 120.1(3) . .
C46 C45 H45 120.0 . .
C44 C45 H45 120.0 . .
C47 C46 C45 120.6(3) . .
C47 C46 H46 119.7 . .
C45 C46 H46 119.7 . .
C46 C47 C48 120.2(3) . .
C46 C47 H47 119.9 . .
C48 C47 H47 119.9 . .
C47 C48 C49 120.0(3) . .
C47 C48 H48 120.0 . .
C49 C48 H48 120.0 . .
C48 C49 C44 119.7(3) . .
C48 C49 H49 120.1 . .
C44 C49 H49 120.1 . .
C53 C52 H52A 109.5 . .
C53 C52 H52B 109.5 . .
H52A C52 H52B 109.5 . .
C53 C52 H52C 109.5 . .
H52A C52 H52C 109.5 . .
H52B C52 H52C 109.5 . .
O7 C53 C52 121.8(3) . .
O7 C53 C54 121.4(3) . .
C52 C53 C54 116.8(3) . .
C53 C54 H54A 109.5 . .
C53 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C53 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
S1 O1 Ag1 133.55(15) . .
S1 O2 Ag4 120.55(14) . .
C53 O7 Ag1 141.9(2) . .
F3 C50 F1 108.5(10) . .
F3 C50 F2 107.1(10) . .
F1 C50 F2 108.5(11) . .
F3 C50 S1 111.5(9) . .
F1 C50 S1 111.1(8) . .
F2 C50 S1 110.0(10) . .
F21 C501 F11 107.4(19) . .
F21 C501 F31 111(2) . .
F11 C501 F31 104.7(18) . .
F21 C501 S1 112.8(18) . .
F11 C501 S1 111.2(17) . .
F31 C501 S1 109.1(15) . .
C14 P1 C20 102.20(13) . .
C14 P1 C13 106.70(12) . .
C20 P1 C13 108.26(12) . .
C14 P1 Ag1 113.28(9) . .
C20 P1 Ag1 113.19(10) . .
C13 P1 Ag1 112.50(8) . .
C261 P2 C32 104.8(3) . .
C261 P2 C13 108.9(3) . .
C32 P2 C13 105.42(12) . .
C32 P2 C26 102.7(3) . .
C13 P2 C26 105.5(2) . .
C32 P2 Ag2 115.77(14) . .
C13 P2 Ag2 111.95(10) . .
C32 P2 Ag21 107.3(3) . .
C13 P2 Ag21 114.23(15) . .
C44 P3 C38 102.18(12) . .
C44 P3 C13 103.19(12) . .
C38 P3 C13 109.90(12) . .
C44 P3 Ag3 110.13(9) . .
C38 P3 Ag3 116.92(10) . .
C13 P3 Ag3 113.08(9) . .
O31 S1 O1 120.3(13) . .
O1 S1 O3 111.5(6) . .
O31 S1 O2 117.5(13) . .
O1 S1 O2 114.28(15) . .
O3 S1 O2 114.8(6) . .
O1 S1 C50 107.4(5) . .
O3 S1 C50 104.7(6) . .
O2 S1 C50 103.0(4) . .
O31 S1 C501 99.2(12) . .
O1 S1 C501 93.6(8) . .
O2 S1 C501 105.6(7) . .
C1 Ag1 P1 143.86(7) . .
C1 Ag1 O1 97.63(10) . .
P1 Ag1 O1 107.21(7) . .
C1 Ag1 O7 91.96(9) . .
P1 Ag1 O7 115.45(6) . .
O1 Ag1 O7 85.30(8) . .
C1 Ag1 Ag4 45.25(7) . .
P1 Ag1 Ag4 113.241(18) . .
O1 Ag1 Ag4 80.30(6) . .
O7 Ag1 Ag4 131.31(5) . .
C1 Ag1 Ag3 50.87(7) . .
P1 Ag1 Ag3 94.518(18) . .
O1 Ag1 Ag3 140.38(6) . .
O7 Ag1 Ag3 115.06(5) . .
Ag4 Ag1 Ag3 60.562(7) . .
C7 Ag2 P2 172.0(2) . .
C7 Ag2 Ag4 47.74(8) . .
P2 Ag2 Ag4 132.68(8) . .
C7 Ag21 P2 153.1(6) . .
C7 Ag21 Ag4 48.01(11) . .
P2 Ag21 Ag4 127.9(3) . .
C7 Ag21 Ag3 104.19(17) . .
P2 Ag21 Ag3 84.92(10) . .
Ag4 Ag21 Ag3 57.69(7) . .
C7 Ag21 Ag3 44.21(19) . 2_766
P2 Ag21 Ag3 162.6(4) . 2_766
Ag4 Ag21 Ag3 57.61(12) . 2_766
Ag3 Ag21 Ag3 86.53(19) . 2_766
C7 Ag21 Ag4 95.1(3) . 2_766
P2 Ag21 Ag4 110.3(2) . 2_766
Ag4 Ag21 Ag4 77.4(2) . 2_766
Ag3 Ag21 Ag4 53.59(13) . 2_766
Ag3 Ag21 Ag4 52.83(17) 2_766 2_766
C7 Ag3 C1 98.59(10) 2_766 .
C7 Ag3 P3 127.86(8) 2_766 .
C1 Ag3 P3 128.53(7) . .
C7 Ag3 Ag1 149.19(7) 2_766 .
C1 Ag3 Ag1 50.68(7) . .
P3 Ag3 Ag1 80.293(17) . .
C7 Ag3 Ag4 102.54(7) 2_766 .
C1 Ag3 Ag4 44.54(7) . .
P3 Ag3 Ag4 125.740(18) . .
Ag1 Ag3 Ag4 59.043(8) . .
C7 Ag3 Ag4 44.56(7) 2_766 2_766
C1 Ag3 Ag4 108.82(7) . 2_766
P3 Ag3 Ag4 119.426(18) . 2_766
Ag1 Ag3 Ag4 138.292(9) . 2_766
Ag4 Ag3 Ag4 80.993(9) . 2_766
C7 Ag3 Ag21 108.4(2) 2_766 .
C1 Ag3 Ag21 96.72(12) . .
P3 Ag3 Ag21 89.04(12) . .
Ag1 Ag3 Ag21 81.1(2) . .
Ag4 Ag3 Ag21 53.04(8) . .
Ag4 Ag3 Ag21 64.3(2) 2_766 .
C7 Ag3 Ag21 40.68(17) 2_766 2_766
C1 Ag3 Ag21 62.51(17) . 2_766
P3 Ag3 Ag21 168.32(16) . 2_766
Ag1 Ag3 Ag21 111.36(16) . 2_766
Ag4 Ag3 Ag21 63.93(14) . 2_766
Ag4 Ag3 Ag21 52.43(12) 2_766 2_766
Ag21 Ag3 Ag21 93.47(19) . 2_766
C1 Ag4 C7 169.28(12) . .
C1 Ag4 O2 97.95(10) . .
C7 Ag4 O2 92.32(10) . .
C1 Ag4 Ag21 119.74(11) . .
C7 Ag4 Ag21 50.16(11) . .
O2 Ag4 Ag21 129.4(2) . .
C1 Ag4 Ag2 120.70(9) . .
C7 Ag4 Ag2 49.94(9) . .
O2 Ag4 Ag2 122.76(10) . .
C1 Ag4 Ag1 52.49(8) . .
C7 Ag4 Ag1 125.52(8) . .
O2 Ag4 Ag1 87.05(6) . .
Ag21 Ag4 Ag1 90.52(18) . .
Ag2 Ag4 Ag1 85.88(5) . .
C1 Ag4 Ag3 51.78(8) . .
C7 Ag4 Ag3 117.53(8) . .
O2 Ag4 Ag3 144.39(6) . .
Ag21 Ag4 Ag3 69.27(10) . .
Ag2 Ag4 Ag3 72.27(6) . .
Ag1 Ag4 Ag3 60.394(8) . .
C1 Ag4 Ag3 125.67(8) . 2_766
C7 Ag4 Ag3 50.84(7) . 2_766
O2 Ag4 Ag3 115.51(6) . 2_766
Ag21 Ag4 Ag3 70.0(2) . 2_766
Ag2 Ag4 Ag3 76.04(6) . 2_766
Ag1 Ag4 Ag3 156.332(10) . 2_766
Ag3 Ag4 Ag3 99.008(9) . 2_766
C1 Ag4 Ag21 63.66(13) . 2_766
C7 Ag4 Ag21 112.52(13) . 2_766
O2 Ag4 Ag21 124.99(10) . 2_766
Ag21 Ag4 Ag21 102.6(2) . 2_766
Ag1 Ag4 Ag21 111.87(9) . 2_766
Ag3 Ag4 Ag21 63.24(7) . 2_766
Ag3 Ag4 Ag21 62.14(10) 2_766 2_766
O5 S2 O4 114.6(3) . .
O5 S2 O6 114.4(4) . .
O4 S2 O6 114.5(4) . .
O5 S2 C51 103.6(4) . .
O4 S2 C51 105.7(3) . .
O6 S2 C51 102.0(4) . .
F4 C51 F6 102.4(8) . .
F4 C51 F5 111.6(6) . .
F6 C51 F5 103.9(7) . .
F4 C51 S2 112.4(6) . .
F6 C51 S2 117.1(5) . .
F5 C51 S2 109.1(6) . .
O51 S21 O61 134.8(13) . .
O51 S21 O41 89.6(10) . .
O61 S21 O41 111.9(17) . .
O51 S21 C511 104.9(9) . .
O61 S21 C511 109.6(14) . .
O41 S21 C511 99.7(9) . .
F41 C511 F51 99.2(17) . .
F41 C511 F61 105.7(18) . .
F51 C511 F61 122.6(16) . .
F41 C511 S21 108.6(8) . .
F51 C511 S21 111.6(9) . .
F61 C511 S21 107.9(8) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C2 1.214(4) .
C1 Ag4 2.108(3) .
C1 Ag1 2.355(3) .
C1 Ag3 2.362(3) .
C2 C3 1.484(4) .
C3 C4 1.535(5) .
C3 C5 1.537(5) .
C3 C6 1.540(5) .
C4 H12A 0.9800 .
C4 H12B 0.9800 .
C4 H12C 0.9800 .
C5 H13A 0.9800 .
C5 H13B 0.9800 .
C5 H13C 0.9800 .
C6 H11A 0.9800 .
C6 H11B 0.9800 .
C6 H11C 0.9800 .
C7 C8 1.223(4) .
C7 Ag4 2.121(3) .
C7 Ag21 2.192(5) .
C7 Ag2 2.194(4) .
C7 Ag3 2.344(3) 2_766
C8 C9 1.476(4) .
C9 C11 1.529(5) .
C9 C10 1.533(5) .
C9 C12 1.537(5) .
C10 H7A 0.9800 .
C10 H7B 0.9800 .
C10 H7C 0.9800 .
C11 H5A 0.9800 .
C11 H5B 0.9800 .
C11 H5C 0.9800 .
C12 H6A 0.9800 .
C12 H6B 0.9800 .
C12 H6C 0.9800 .
C13 P2 1.863(3) .
C13 P3 1.882(3) .
C13 P1 1.892(3) .
C13 H1 1.0000 .
C14 C15 1.390(4) .
C14 C19 1.390(4) .
C14 P1 1.824(3) .
C15 C16 1.398(4) .
C15 H15 0.9500 .
C16 C17 1.379(5) .
C16 H16 0.9500 .
C17 C18 1.388(5) .
C17 H17 0.9500 .
C18 C19 1.393(4) .
C18 H18 0.9500 .
C19 H19 0.9500 .
C20 C21 1.385(4) .
C20 C25 1.401(4) .
C20 P1 1.834(3) .
C21 C22 1.403(4) .
C21 H21 0.9500 .
C22 C23 1.379(5) .
C22 H22 0.9500 .
C23 C24 1.388(5) .
C23 H23 0.9500 .
C24 C25 1.390(4) .
C24 H24 0.9500 .
C25 H25 0.9500 .
C26 C27 1.3900 .
C26 C31 1.3900 .
C26 P2 1.873(4) .
C27 C28 1.3900 .
C27 H27 0.9500 .
C28 C29 1.3900 .
C28 H28 0.9500 .
C29 C30 1.3900 .
C29 H29 0.9500 .
C30 C31 1.3900 .
C30 H30 0.9500 .
C31 H31 0.9500 .
C271 C281 1.3900 .
C271 C261 1.3900 .
C271 H271 0.9500 .
C281 C291 1.3900 .
C281 H281 0.9500 .
C291 C301 1.3900 .
C291 H291 0.9500 .
C301 C311 1.3900 .
C301 H301 0.9500 .
C311 C261 1.3900 .
C311 H311 0.9500 .
C261 P2 1.782(4) .
C32 C37 1.388(4) .
C32 C33 1.390(5) .
C32 P2 1.815(3) .
C33 C34 1.385(4) .
C33 H33 0.9500 .
C34 C35 1.383(6) .
C34 H34 0.9500 .
C35 C36 1.380(7) .
C35 H35 0.9500 .
C36 C37 1.377(6) .
C36 H36 0.9500 .
C37 H37 0.9500 .
C38 C43 1.385(4) .
C38 C39 1.401(4) .
C38 P3 1.829(3) .
C39 C40 1.388(4) .
C39 H39 0.9500 .
C40 C41 1.383(5) .
C40 H40 0.9500 .
C41 C42 1.377(6) .
C41 H41 0.9500 .
C42 C43 1.403(4) .
C42 H42 0.9500 .
C43 H43 0.9500 .
C44 C45 1.392(4) .
C44 C49 1.399(4) .
C44 P3 1.821(3) .
C45 C46 1.391(4) .
C45 H45 0.9500 .
C46 C47 1.368(5) .
C46 H46 0.9500 .
C47 C48 1.389(5) .
C47 H47 0.9500 .
C48 C49 1.396(4) .
C48 H48 0.9500 .
C49 H49 0.9500 .
C52 C53 1.496(5) .
C52 H52A 0.9800 .
C52 H52B 0.9800 .
C52 H52C 0.9800 .
C53 O7 1.224(4) .
C53 C54 1.497(5) .
C54 H54A 0.9800 .
C54 H54B 0.9800 .
C54 H54C 0.9800 .
O1 S1 1.436(3) .
O1 Ag1 2.475(2) .
O2 S1 1.451(3) .
O2 Ag4 2.536(2) .
O7 Ag1 2.487(2) .
C50 F3 1.312(13) .
C50 F1 1.318(13) .
C50 F2 1.338(16) .
C50 S1 1.813(15) .
O3 S1 1.440(14) .
F31 C501 1.34(2) .
F11 C501 1.33(2) .
F21 C501 1.29(3) .
C501 S1 1.89(3) .
O31 S1 1.41(3) .
P1 Ag1 2.4449(7) .
P2 Ag2 2.355(2) .
P2 Ag21 2.473(6) .
P3 Ag3 2.4453(7) .
Ag1 Ag4 2.9421(4) .
Ag1 Ag3 2.9829(3) .
Ag2 Ag4 2.840(2) .
Ag21 Ag4 2.825(4) .
Ag21 Ag3 3.306(4) .
Ag21 Ag3 3.348(9) 2_766
Ag21 Ag4 3.368(11) 2_766
Ag3 C7 2.344(3) 2_766
Ag3 Ag4 2.9879(3) .
Ag3 Ag4 3.0096(3) 2_766
Ag3 Ag21 3.348(9) 2_766
Ag4 Ag3 3.0097(3) 2_766
Ag4 Ag21 3.368(11) 2_766
S2 O5 1.399(5) .
S2 O4 1.422(4) .
S2 O6 1.427(6) .
S2 C51 1.794(10) .
F4 C51 1.309(9) .
F5 C51 1.427(9) .
F6 C51 1.311(9) .
S21 O51 1.439(9) .
S21 O61 1.442(10) .
S21 O41 1.485(9) .
S21 C511 1.798(9) .
F51 C511 1.364(9) .
F41 C511 1.355(10) .
F61 C511 1.364(10) .
