#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/27/4112715.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4112715
loop_
_publ_author_name
'Olivier Tardif'
'Daisuke Hashizume'
'Zhaomin Hou'
_publ_section_title
;
 Hydrogenation of Carbon Dioxide and Aryl Isocyanates by a Tetranuclear
 Tetrahydrido Yttrium Complex. Isolation, Structures, and CO2 Insertion
 Reactions of Methylene Diolate and μ3-Oxo Yttrium Complexes
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              8080
_journal_page_last               8081
_journal_paper_doi               10.1021/ja047889u
_journal_volume                  126
_journal_year                    2004
_chemical_formula_moiety         'C60 H108 O4 Si6 Y4, 1.5(C7 H8)'
_chemical_formula_sum            'C70.5 H120 O4 Si6 Y4'
_chemical_formula_weight         1555.85
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                96.005(2)
_cell_angle_beta                 90.298(2)
_cell_angle_gamma                91.165(2)
_cell_formula_units_Z            2
_cell_length_a                   12.2348(11)
_cell_length_b                   15.2532(13)
_cell_length_c                   21.2206(18)
_cell_measurement_temperature    193
_cell_volume                     3937.5(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193
_diffrn_measured_fraction_theta_full 0.959
_diffrn_measured_fraction_theta_max 0.959
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0514
_diffrn_reflns_av_sigmaI/netI    0.1817
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            24052
_diffrn_reflns_theta_full        27.09
_diffrn_reflns_theta_max         27.09
_diffrn_reflns_theta_min         1.73
_exptl_absorpt_coefficient_mu    3.051
_exptl_absorpt_correction_T_max  0.7501
_exptl_absorpt_correction_T_min  0.3749
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.312
_exptl_crystal_description       block
_exptl_crystal_F_000             1630
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.562
_refine_diff_density_min         -0.651
_refine_diff_density_rms         0.091
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.844
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     768
_refine_ls_number_reflns         16659
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.844
_refine_ls_R_factor_all          0.1501
_refine_ls_R_factor_gt           0.0532
_refine_ls_shift/su_max          0.034
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0446P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0970
_refine_ls_wR_factor_ref         0.1180
_reflns_number_gt                7497
_reflns_number_total             16659
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ja047889urom20040413_031841.cif
_cod_data_source_block           2
_cod_original_formula_sum        'C70.50 H120 O4 Si6 Y4'
_cod_database_code               4112715
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Y1 Y 0.14449(3) 0.19500(2) 0.223872(17) 0.03484(10) Uani 1 1 d . . .
Y2 Y 0.08858(3) 0.43434(2) 0.245114(16) 0.03061(10) Uani 1 1 d . . .
Y3 Y 0.27116(3) 0.33857(2) 0.352527(18) 0.03889(11) Uani 1 1 d . . .
Y4 Y 0.26468(3) 0.34424(2) 0.119545(17) 0.03269(10) Uani 1 1 d . . .
Si1 Si -0.12183(14) 0.03032(9) 0.16825(7) 0.0878(5) Uani 1 1 d . . .
Si2 Si 0.15312(13) 0.70100(9) 0.24980(9) 0.0988(6) Uani 1 1 d . . .
Si3 Si 0.48815(11) 0.18917(9) 0.44811(7) 0.0746(5) Uani 1 1 d . . .
Si4 Si 0.47260(10) 0.18813(8) 0.01009(7) 0.0634(4) Uani 1 1 d . . .
Si5 Si 0.03775(9) 0.29552(8) 0.39286(5) 0.0467(3) Uani 1 1 d . . .
Si6 Si 0.02440(9) 0.30817(8) 0.07458(5) 0.0446(3) Uani 1 1 d . . .
O1 O 0.30427(19) 0.23639(15) 0.17381(11) 0.0410(7) Uani 1 1 d . . .
O2 O 0.30818(19) 0.23380(16) 0.28016(11) 0.0434(8) Uani 1 1 d . . .
O3 O 0.25587(19) 0.45020(15) 0.29850(11) 0.0403(7) Uani 1 1 d . . .
O4 O 0.25317(18) 0.45338(15) 0.19263(11) 0.0381(7) Uani 1 1 d . . .
C1 C 0.0221(4) 0.0473(2) 0.19720(17) 0.0499(13) Uani 1 1 d . . .
C2 C 0.0549(3) 0.0476(2) 0.26140(18) 0.0477(12) Uani 1 1 d . . .
C3 C 0.1662(4) 0.0352(3) 0.2657(2) 0.0618(15) Uani 1 1 d . . .
C4 C 0.2077(4) 0.0269(3) 0.2044(2) 0.0787(17) Uani 1 1 d . . .
C5 C 0.1230(5) 0.0323(3) 0.1636(2) 0.0800(18) Uani 1 1 d . . .
C6 C -0.0239(3) 0.0465(3) 0.31623(18) 0.0663(15) Uani 1 1 d . . .
H6A H 0.0164 0.0361 0.3547 0.100 Uiso 1 1 calc R . .
H6B H -0.0789 -0.0006 0.3065 0.100 Uiso 1 1 calc R . .
H6C H -0.0602 0.1034 0.3230 0.100 Uiso 1 1 calc R . .
C7 C 0.2320(4) 0.0231(3) 0.3247(2) 0.100(2) Uani 1 1 d . . .
H7A H 0.1829 0.0240 0.3612 0.149 Uiso 1 1 calc R . .
H7B H 0.2865 0.0711 0.3323 0.149 Uiso 1 1 calc R . .
H7C H 0.2690 -0.0335 0.3190 0.149 Uiso 1 1 calc R . .
C8 C 0.3242(4) 0.0039(3) 0.1881(3) 0.142(3) Uani 1 1 d . . .
H8A H 0.3420 0.0229 0.1466 0.213 Uiso 1 1 calc R . .
H8B H 0.3326 -0.0601 0.1867 0.213 Uiso 1 1 calc R . .
H8C H 0.3736 0.0338 0.2203 0.213 Uiso 1 1 calc R . .
C9 C 0.1313(5) 0.0094(3) 0.0904(2) 0.132(3) Uani 1 1 d . . .
H9A H 0.1892 0.0458 0.0739 0.198 Uiso 1 1 calc R . .
H9B H 0.0614 0.0211 0.0704 0.198 Uiso 1 1 calc R . .
H9C H 0.1485 -0.0530 0.0809 0.198 Uiso 1 1 calc R . .
C10 C -0.1591(5) -0.0881(3) 0.1704(3) 0.137(3) Uani 1 1 d . . .
H10A H -0.2304 -0.1006 0.1497 0.205 Uiso 1 1 calc R . .
H10B H -0.1631 -0.1014 0.2145 0.205 Uiso 1 1 calc R . .
H10C H -0.1036 -0.1246 0.1480 0.205 Uiso 1 1 calc R . .
C11 C -0.1426(5) 0.0551(4) 0.0848(3) 0.190(3) Uani 1 1 d . . .
H11A H -0.1033 0.0123 0.0561 0.285 Uiso 1 1 calc R . .
H11B H -0.1147 0.1147 0.0801 0.285 Uiso 1 1 calc R . .
H11C H -0.2208 0.0512 0.0743 0.285 Uiso 1 1 calc R . .
C12 C -0.2232(4) 0.0975(4) 0.2150(3) 0.122(3) Uani 1 1 d . . .
H12A H -0.2027 0.1601 0.2159 0.183 Uiso 1 1 calc R . .
H12B H -0.2249 0.0809 0.2583 0.183 Uiso 1 1 calc R . .
H12C H -0.2957 0.0873 0.1954 0.183 Uiso 1 1 calc R . .
C13 C 0.0518(3) 0.6096(2) 0.25572(18) 0.0413(11) Uani 1 1 d . . .
C14 C 0.0108(3) 0.5789(2) 0.31198(18) 0.0438(12) Uani 1 1 d . . .
C15 C -0.0805(3) 0.5244(2) 0.2976(2) 0.0522(13) Uani 1 1 d . . .
C16 C -0.0991(3) 0.5198(3) 0.2325(2) 0.0596(14) Uani 1 1 d . . .
C17 C -0.0196(4) 0.5724(2) 0.20720(19) 0.0552(13) Uani 1 1 d . . .
C18 C 0.0540(4) 0.6092(3) 0.3788(2) 0.090(2) Uani 1 1 d . . .
H18A H 0.0590 0.6738 0.3846 0.135 Uiso 1 1 calc R . .
H18B H 0.1265 0.5850 0.3843 0.135 Uiso 1 1 calc R . .
H18C H 0.0039 0.5884 0.4102 0.135 Uiso 1 1 calc R . .
C19 C -0.1571(3) 0.4884(3) 0.3446(2) 0.0967(19) Uani 1 1 d . . .
H19A H -0.1160 0.4773 0.3826 0.145 Uiso 1 1 calc R . .
H19B H -0.1912 0.4332 0.3255 0.145 Uiso 1 1 calc R . .
H19C H -0.2139 0.5314 0.3562 0.145 Uiso 1 1 calc R . .
C20 C -0.1981(4) 0.4748(3) 0.2007(3) 0.130(2) Uani 1 1 d . . .
H20A H -0.2633 0.5083 0.2134 0.194 Uiso 1 1 calc R . .
H20B H -0.2057 0.4150 0.2132 0.194 Uiso 1 1 calc R . .
H20C H -0.1898 0.4718 0.1546 0.194 Uiso 1 1 calc R . .
C21 C -0.0194(5) 0.5954(3) 0.1394(2) 0.130(3) Uani 1 1 d . . .
H21A H -0.0693 0.5552 0.1137 0.195 Uiso 1 1 calc R . .
H21B H 0.0547 0.5899 0.1223 0.195 Uiso 1 1 calc R . .
H21C H -0.0434 0.6562 0.1384 0.195 Uiso 1 1 calc R . .
C22 C 0.2317(5) 0.6875(4) 0.1728(3) 0.160(3) Uani 1 1 d . . .
H22A H 0.1804 0.6844 0.1370 0.240 Uiso 1 1 calc R . .
H22B H 0.2733 0.6330 0.1706 0.240 Uiso 1 1 calc R . .
H22C H 0.2821 0.7379 0.1711 0.240 Uiso 1 1 calc R . .
C23 C 0.0762(5) 0.8056(3) 0.2506(4) 0.216(4) Uani 1 1 d . . .
H23A H 0.0222 0.7999 0.2161 0.324 Uiso 1 1 calc R . .
H23B H 0.1273 0.8544 0.2448 0.324 Uiso 1 1 calc R . .
H23C H 0.0388 0.8175 0.2912 0.324 Uiso 1 1 calc R . .
C24 C 0.2570(5) 0.7127(4) 0.3167(3) 0.171(3) Uani 1 1 d . . .
H24A H 0.2218 0.7370 0.3559 0.256 Uiso 1 1 calc R . .
H24B H 0.3167 0.7525 0.3064 0.256 Uiso 1 1 calc R . .
H24C H 0.2863 0.6547 0.3225 0.256 Uiso 1 1 calc R . .
C25 C 0.4352(3) 0.2961(3) 0.42715(19) 0.0485(13) Uani 1 1 d . . .
C26 C 0.3708(3) 0.3549(3) 0.46806(19) 0.0515(13) Uani 1 1 d . . .
C27 C 0.3757(4) 0.4391(3) 0.4484(2) 0.0617(14) Uani 1 1 d . . .
C28 C 0.4489(3) 0.4355(3) 0.3969(2) 0.0639(15) Uani 1 1 d . . .
C29 C 0.4851(3) 0.3498(3) 0.3832(2) 0.0562(14) Uani 1 1 d . . .
C30 C 0.3156(4) 0.3329(3) 0.52857(19) 0.0748(17) Uani 1 1 d . . .
H30A H 0.3714 0.3242 0.5605 0.112 Uiso 1 1 calc R . .
H30B H 0.2711 0.2788 0.5198 0.112 Uiso 1 1 calc R . .
H30C H 0.2687 0.3816 0.5445 0.112 Uiso 1 1 calc R . .
C31 C 0.3301(4) 0.5237(3) 0.4815(2) 0.096(2) Uani 1 1 d . . .
H31A H 0.2729 0.5092 0.5111 0.145 Uiso 1 1 calc R . .
H31B H 0.2990 0.5587 0.4499 0.145 Uiso 1 1 calc R . .
H31C H 0.3889 0.5578 0.5048 0.145 Uiso 1 1 calc R . .
C32 C 0.4891(4) 0.5156(3) 0.3661(2) 0.102(2) Uani 1 1 d . . .
H32A H 0.5472 0.5462 0.3924 0.153 Uiso 1 1 calc R . .
H32B H 0.4284 0.5556 0.3622 0.153 Uiso 1 1 calc R . .
H32C H 0.5178 0.4967 0.3240 0.153 Uiso 1 1 calc R . .
C33 C 0.5720(3) 0.3231(3) 0.3358(2) 0.0873(19) Uani 1 1 d . . .
H33A H 0.5753 0.3653 0.3040 0.131 Uiso 1 1 calc R . .
H33B H 0.5545 0.2641 0.3149 0.131 Uiso 1 1 calc R . .
H33C H 0.6428 0.3226 0.3574 0.131 Uiso 1 1 calc R . .
C34 C 0.5470(5) 0.1203(3) 0.3796(3) 0.138(3) Uani 1 1 d . . .
H34A H 0.4911 0.1079 0.3465 0.207 Uiso 1 1 calc R . .
H34B H 0.5719 0.0647 0.3935 0.207 Uiso 1 1 calc R . .
H34C H 0.6091 0.1519 0.3629 0.207 Uiso 1 1 calc R . .
C35 C 0.5991(4) 0.2152(3) 0.5090(2) 0.110(2) Uani 1 1 d . . .
H35A H 0.6553 0.2529 0.4921 0.165 Uiso 1 1 calc R . .
H35B H 0.6320 0.1603 0.5192 0.165 Uiso 1 1 calc R . .
H35C H 0.5681 0.2460 0.5474 0.165 Uiso 1 1 calc R . .
C36 C 0.3860(4) 0.1159(3) 0.4827(3) 0.112(2) Uani 1 1 d . . .
H36A H 0.3573 0.1461 0.5220 0.168 Uiso 1 1 calc R . .
H36B H 0.4211 0.0614 0.4919 0.168 Uiso 1 1 calc R . .
H36C H 0.3259 0.1016 0.4524 0.168 Uiso 1 1 calc R . .
C37 C 0.4279(3) 0.3006(2) 0.03993(18) 0.0441(12) Uani 1 1 d . . .
C38 C 0.4774(3) 0.3573(3) 0.09151(19) 0.0471(12) Uani 1 1 d . . .
C39 C 0.4409(3) 0.4427(2) 0.08885(18) 0.0441(12) Uani 1 1 d . . .
C40 C 0.3688(3) 0.4436(3) 0.03721(19) 0.0540(13) Uani 1 1 d . . .
C41 C 0.3623(3) 0.3562(3) 0.00709(18) 0.0486(12) Uani 1 1 d . . .
C42 C 0.5652(3) 0.3329(3) 0.13465(19) 0.0655(15) Uani 1 1 d . . .
H42A H 0.6361 0.3363 0.1137 0.098 Uiso 1 1 calc R . .
H42B H 0.5517 0.2725 0.1452 0.098 Uiso 1 1 calc R . .
H42C H 0.5657 0.3736 0.1736 0.098 Uiso 1 1 calc R . .
C43 C 0.4834(3) 0.5240(3) 0.1290(2) 0.0694(15) Uani 1 1 d . . .
H43A H 0.5484 0.5474 0.1092 0.104 Uiso 1 1 calc R . .
H43B H 0.5025 0.5087 0.1713 0.104 Uiso 1 1 calc R . .
H43C H 0.4267 0.5688 0.1325 0.104 Uiso 1 1 calc R . .
C44 C 0.3223(4) 0.5250(3) 0.0141(2) 0.0820(17) Uani 1 1 d . . .
H44A H 0.2912 0.5619 0.0499 0.123 Uiso 1 1 calc R . .
H44B H 0.2649 0.5080 -0.0175 0.123 Uiso 1 1 calc R . .
H44C H 0.3805 0.5581 -0.0051 0.123 Uiso 1 1 calc R . .
C45 C 0.3016(4) 0.3309(3) -0.05563(19) 0.0778(17) Uani 1 1 d . . .
H45A H 0.3545 0.3233 -0.0902 0.117 Uiso 1 1 calc R . .
H45B H 0.2511 0.3777 -0.0635 0.117 Uiso 1 1 calc R . .
H45C H 0.2604 0.2756 -0.0533 0.117 Uiso 1 1 calc R . .
C46 C 0.5866(5) 0.1982(4) -0.0435(3) 0.165(3) Uani 1 1 d . . .
H46A H 0.6101 0.1393 -0.0602 0.247 Uiso 1 1 calc R . .
H46B H 0.6475 0.2300 -0.0205 0.247 Uiso 1 1 calc R . .
H46C H 0.5638 0.2306 -0.0786 0.247 Uiso 1 1 calc R . .
C47 C 0.3686(5) 0.1227(4) -0.0329(4) 0.333(5) Uani 1 1 d . . .
H47A H 0.4002 0.0680 -0.0526 0.499 Uiso 1 1 calc R . .
H47B H 0.3382 0.1557 -0.0659 0.499 Uiso 1 1 calc R . .
H47C H 0.3104 0.1084 -0.0039 0.499 Uiso 1 1 calc R . .
C48 C 0.5177(7) 0.1243(4) 0.0722(3) 0.225(4) Uani 1 1 d . . .
H48A H 0.4802 0.1440 0.1117 0.337 Uiso 1 1 calc R . .
H48B H 0.5968 0.1327 0.0784 0.337 Uiso 1 1 calc R . .
H48C H 0.5006 0.0618 0.0602 0.337 Uiso 1 1 calc R . .
C49 C 0.3738(3) 0.2337(3) 0.22673(18) 0.0503(13) Uani 1 1 d . . .
H49A H 0.4179 0.1797 0.2217 0.060 Uiso 1 1 calc R . .
H49B H 0.4241 0.2856 0.2310 0.060 Uiso 1 1 calc R . .
C50 C 0.3160(3) 0.4761(2) 0.24755(17) 0.0412(12) Uani 1 1 d . . .
H50A H 0.3867 0.4455 0.2444 0.049 Uiso 1 1 calc R . .
H50B H 0.3309 0.5405 0.2533 0.049 Uiso 1 1 calc R . .
C51 C 0.1237(3) 0.2114(3) 0.4265(2) 0.0683(15) Uani 1 1 d . . .
H51A H 0.1077 0.1532 0.4040 0.103 Uiso 1 1 calc R . .
H51B H 0.1072 0.2104 0.4716 0.103 Uiso 1 1 calc R . .
H51C H 0.2012 0.2266 0.4217 0.103 Uiso 1 1 calc R . .
C52 C 0.0718(4) 0.3990(3) 0.44629(18) 0.0668(15) Uani 1 1 d . . .
H52A H 0.1479 0.4170 0.4396 0.100 Uiso 1 1 calc R . .
H52B H 0.0622 0.3878 0.4906 0.100 Uiso 1 1 calc R . .
H52C H 0.0232 0.4461 0.4365 0.100 Uiso 1 1 calc R . .
C53 C -0.1081(3) 0.2668(3) 0.40843(19) 0.0757(17) Uani 1 1 d . . .
H53A H -0.1559 0.3072 0.3889 0.114 Uiso 1 1 calc R . .
H53B H -0.1205 0.2719 0.4542 0.114 Uiso 1 1 calc R . .
H53C H -0.1244 0.2061 0.3903 0.114 Uiso 1 1 calc R . .
C54 C 0.0782(3) 0.3062(2) 0.31051(16) 0.0304(10) Uani 1 1 d . . .
C55 C -0.0138(3) 0.2921(2) 0.26580(16) 0.0348(10) Uani 1 1 d . . .
H55 H -0.0822 0.2804 0.2846 0.042 Uiso 1 1 calc R . .
C56 C -0.0171(3) 0.2930(2) 0.19994(16) 0.0347(11) Uani 1 1 d . . .
H56 H -0.0866 0.2809 0.1804 0.042 Uiso 1 1 calc R . .
C57 C 0.0740(3) 0.3103(2) 0.15682(16) 0.0309(10) Uani 1 1 d . . .
C58 C -0.1262(4) 0.3048(4) 0.0598(2) 0.128(3) Uani 1 1 d . . .
H58A H -0.1585 0.2524 0.0761 0.193 Uiso 1 1 calc R . .
H58B H -0.1404 0.3023 0.0141 0.193 Uiso 1 1 calc R . .
H58C H -0.1586 0.3579 0.0814 0.193 Uiso 1 1 calc R . .
C59 C 0.0825(4) 0.2164(3) 0.0205(2) 0.0954(19) Uani 1 1 d . . .
H59A H 0.1621 0.2165 0.0258 0.143 Uiso 1 1 calc R . .
H59B H 0.0643 0.2246 -0.0235 0.143 Uiso 1 1 calc R . .
H59C H 0.0515 0.1600 0.0309 0.143 Uiso 1 1 calc R . .
C60 C 0.0775(4) 0.4098(3) 0.03949(19) 0.0741(16) Uani 1 1 d . . .
H60A H 0.0481 0.4626 0.0632 0.111 Uiso 1 1 calc R . .
H60B H 0.0544 0.4072 -0.0050 0.111 Uiso 1 1 calc R . .
H60C H 0.1575 0.4122 0.0421 0.111 Uiso 1 1 calc R . .
C71 C -0.0528(7) 0.0319(6) 0.5072(4) 0.156(6) Uani 0.50 1 d PG . .
C72 C 0.0512(7) 0.0411(6) 0.5341(4) 0.216(10) Uani 0.50 1 d PG . .
H72 H 0.0683 0.0896 0.5646 0.259 Uiso 0.50 1 calc PR . .
C73 C 0.1302(7) -0.0207(7) 0.5163(5) 0.166(7) Uani 0.50 1 d PG . .
H73 H 0.2013 -0.0144 0.5346 0.200 Uiso 0.50 1 calc PR . .
C74 C 0.1053(8) -0.0916(6) 0.4716(5) 0.231(5) Uani 0.50 1 d PG . .
H74 H 0.1593 -0.1338 0.4594 0.277 Uiso 0.50 1 calc PR . .
C75 C 0.0013(9) -0.1008(6) 0.4447(4) 0.140(6) Uani 0.50 1 d PG . .
H75 H -0.0158 -0.1493 0.4142 0.168 Uiso 0.50 1 calc PR . .
C76 C -0.0778(7) -0.0390(6) 0.4625(4) 0.178(8) Uani 0.50 1 d PG . .
H76 H -0.1488 -0.0452 0.4442 0.214 Uiso 0.50 1 calc PR . .
C77 C -0.1384(8) 0.0989(7) 0.5265(5) 0.319(12) Uani 0.50 1 d PG . .
H77A H -0.1110 0.1394 0.5623 0.478 Uiso 0.50 1 calc PR . .
H77B H -0.2049 0.0686 0.5391 0.478 Uiso 0.50 1 calc PR . .
H77C H -0.1550 0.1322 0.4907 0.478 Uiso 0.50 1 calc PR . .
C81 C 0.5889(5) 0.8230(4) 0.2954(3) 0.185(2) Uani 0.541(4) 1 d PG A 1
C82 C 0.6834(6) 0.8498(5) 0.3293(3) 0.185(2) Uani 0.541(4) 1 d PG A 1
H82 H 0.6864 0.9052 0.3544 0.222 Uiso 0.541(4) 1 calc PR A 1
C83 C 0.7735(6) 0.7955(6) 0.3266(4) 0.185(2) Uani 0.541(4) 1 d PG A 1
H83 H 0.8381 0.8138 0.3497 0.222 Uiso 0.541(4) 1 calc PR A 1
C84 C 0.7691(7) 0.7144(6) 0.2900(5) 0.185(2) Uani 0.541(4) 1 d PG A 1
H84 H 0.8306 0.6773 0.2881 0.222 Uiso 0.541(4) 1 calc PR A 1
C85 C 0.6746(8) 0.6877(4) 0.2560(4) 0.185(2) Uani 0.541(4) 1 d PG A 1
H85 H 0.6716 0.6323 0.2310 0.222 Uiso 0.541(4) 1 calc PR A 1
C86 C 0.5844(7) 0.7420(4) 0.2588(3) 0.185(2) Uani 0.541(4) 1 d PG A 1
H86 H 0.5198 0.7236 0.2357 0.222 Uiso 0.541(4) 1 calc PR A 1
C87 C 0.4913(6) 0.8819(5) 0.2984(4) 0.185(2) Uani 0.541(4) 1 d PG A 1
H87A H 0.4321 0.8532 0.2720 0.277 Uiso 0.541(4) 1 calc PR A 1
H87B H 0.5116 0.9382 0.2828 0.277 Uiso 0.541(4) 1 calc PR A 1
H87C H 0.4666 0.8925 0.3424 0.277 Uiso 0.541(4) 1 calc PR A 1
C91 C 0.7195(6) 0.7796(5) 0.3015(4) 0.185(2) Uani 0.459(4) 1 d PG A 2
C92 C 0.6698(8) 0.7183(5) 0.2567(4) 0.185(2) Uani 0.459(4) 1 d PG A 2
H92 H 0.6994 0.6613 0.2480 0.222 Uiso 0.459(4) 1 calc PR A 2
C93 C 0.5768(8) 0.7406(8) 0.2245(4) 0.185(2) Uani 0.459(4) 1 d PG A 2
H93 H 0.5428 0.6988 0.1939 0.222 Uiso 0.459(4) 1 calc PR A 2
C94 C 0.5336(7) 0.8241(9) 0.2372(5) 0.185(2) Uani 0.459(4) 1 d PG A 2
H94 H 0.4700 0.8394 0.2152 0.222 Uiso 0.459(4) 1 calc PR A 2
C95 C 0.5833(8) 0.8853(6) 0.2820(6) 0.185(2) Uani 0.459(4) 1 d PG A 2
H95 H 0.5537 0.9424 0.2907 0.222 Uiso 0.459(4) 1 calc PR A 2
C96 C 0.6762(8) 0.8631(5) 0.3142(5) 0.185(2) Uani 0.459(4) 1 d PG A 2
H96 H 0.7102 0.9049 0.3448 0.222 Uiso 0.459(4) 1 calc PR A 2
C97 C 0.8202(8) 0.7554(7) 0.3364(5) 0.185(2) Uani 0.459(4) 1 d PG A 2
H97A H 0.8396 0.6946 0.3219 0.277 Uiso 0.459(4) 1 calc PR A 2
H97B H 0.8058 0.7605 0.3820 0.277 Uiso 0.459(4) 1 calc PR A 2
H97C H 0.8809 0.7954 0.3280 0.277 Uiso 0.459(4) 1 calc PR A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Y1 O2 57.57(8) . .
O1 Y1 C54 114.93(9) . .
O2 Y1 C54 78.56(10) . .
O1 Y1 C57 78.55(10) . .
O2 Y1 C57 115.30(10) . .
C54 Y1 C57 80.60(11) . .
O1 Y1 C55 128.61(10) . .
O2 Y1 C55 111.43(9) . .
C54 Y1 C55 33.51(10) . .
C57 Y1 C55 61.08(11) . .
O1 Y1 C56 111.61(10) . .
O2 Y1 C56 129.27(9) . .
C54 Y1 C56 61.34(11) . .
C57 Y1 C56 33.68(10) . .
C55 Y1 C56 31.53(10) . .
O1 Y1 C5 97.34(12) . .
O2 Y1 C5 118.50(14) . .
C54 Y1 C5 147.43(13) . .
C57 Y1 C5 111.55(13) . .
C55 Y1 C5 125.33(14) . .
C56 Y1 C5 111.88(14) . .
O1 Y1 C2 137.60(10) . .
O2 Y1 C2 110.76(11) . .
C54 Y1 C2 99.87(11) . .
C57 Y1 C2 132.94(12) . .
C55 Y1 C2 93.78(12) . .
C56 Y1 C2 105.87(12) . .
C5 Y1 C2 49.25(13) . .
O1 Y1 C4 88.40(12) . .
O2 Y1 C4 90.19(12) . .
C54 Y1 C4 140.98(14) . .
C57 Y1 C4 136.80(14) . .
C55 Y1 C4 142.82(13) . .
C56 Y1 C4 140.54(13) . .
C5 Y1 C4 29.31(15) . .
C2 Y1 C4 49.43(13) . .
O1 Y1 C1 127.86(10) . .
O2 Y1 C1 136.06(11) . .
C54 Y1 C1 117.17(11) . .
C57 Y1 C1 107.92(11) . .
C55 Y1 C1 95.69(12) . .
C56 Y1 C1 91.68(12) . .
C5 Y1 C1 31.12(14) . .
C2 Y1 C1 30.63(11) . .
C4 Y1 C1 50.82(14) . .
O1 Y1 C3 110.49(11) . .
O2 Y1 C3 85.63(11) . .
C54 Y1 C3 111.21(12) . .
C57 Y1 C3 158.18(12) . .
C55 Y1 C3 118.83(12) . .
C56 Y1 C3 135.66(12) . .
C5 Y1 C3 48.86(14) . .
C2 Y1 C3 29.81(12) . .
C4 Y1 C3 30.01(13) . .
C1 Y1 C3 50.61(13) . .
O1 Y1 Y4 34.64(6) . .
O2 Y1 Y4 80.57(6) . .
C54 Y1 Y4 99.32(8) . .
C57 Y1 Y4 44.07(8) . .
C55 Y1 Y4 98.01(8) . .
C56 Y1 Y4 76.98(8) . .
C5 Y1 Y4 110.34(10) . .
C2 Y1 Y4 159.33(8) . .
C4 Y1 Y4 115.68(11) . .
C1 Y1 Y4 130.49(8) . .
C3 Y1 Y4 143.16(10) . .
O3 Y2 O4 57.75(8) . .
O3 Y2 C54 79.13(10) . .
O4 Y2 C54 116.01(10) . .
O3 Y2 C57 115.96(10) . .
O4 Y2 C57 79.11(9) . .
C54 Y2 C57 80.95(11) . .
O3 Y2 C55 112.10(10) . .
O4 Y2 C55 129.74(9) . .
C54 Y2 C55 33.57(10) . .
C57 Y2 C55 61.35(11) . .
O3 Y2 C56 129.87(10) . .
O4 Y2 C56 112.28(9) . .
C54 Y2 C56 61.35(11) . .
C57 Y2 C56 33.75(10) . .
C55 Y2 C56 31.55(10) . .
O3 Y2 C14 91.83(10) . .
O4 Y2 C14 115.97(10) . .
C54 Y2 C14 109.65(11) . .
C57 Y2 C14 151.95(11) . .
C55 Y2 C14 113.29(11) . .
C56 Y2 C14 128.45(11) . .
O3 Y2 C15 117.35(11) . .
O4 Y2 C15 142.07(10) . .
C54 Y2 C15 97.75(12) . .
C57 Y2 C15 125.32(12) . .
C55 Y2 C15 87.96(11) . .
C56 Y2 C15 98.45(11) . .
C14 Y2 C15 30.01(11) . .
O3 Y2 C16 140.90(10) . .
O4 Y2 C16 127.70(12) . .
C54 Y2 C16 115.80(12) . .
C57 Y2 C16 102.41(12) . .
C55 Y2 C16 92.11(12) . .
C56 Y2 C16 86.63(11) . .
C14 Y2 C16 49.54(12) . .
C15 Y2 C16 30.02(12) . .
O3 Y2 C17 122.77(11) . .
O4 Y2 C17 98.82(11) . .
C54 Y2 C17 145.17(12) . .
C57 Y2 C17 107.45(11) . .
C55 Y2 C17 120.88(12) . .
C56 Y2 C17 107.01(12) . .
C14 Y2 C17 49.23(12) . .
C15 Y2 C17 49.33(13) . .
C16 Y2 C17 29.97(12) . .
O3 Y2 C13 94.11(10) . .
O4 Y2 C13 91.71(10) . .
C54 Y2 C13 139.90(11) . .
C57 Y2 C13 135.17(11) . .
C55 Y2 C13 138.08(11) . .
C56 Y2 C13 135.95(11) . .
C14 Y2 C13 30.48(11) . .
C15 Y2 C13 50.36(11) . .
C16 Y2 C13 50.39(11) . .
C17 Y2 C13 30.28(11) . .
O3 Y2 Y4 80.76(6) . .
O4 Y2 Y4 34.92(5) . .
C54 Y2 Y4 99.93(7) . .
C57 Y2 Y4 44.40(8) . .
C55 Y2 Y4 98.64(7) . .
C56 Y2 Y4 77.36(8) . .
C14 Y2 Y4 147.58(8) . .
C15 Y2 Y4 156.86(9) . .
C16 Y2 Y4 127.04(10) . .
C17 Y2 Y4 109.59(9) . .
C13 Y2 Y4 118.10(8) . .
O2 Y3 O3 102.21(9) . .
O2 Y3 C54 81.90(10) . .
O3 Y3 C54 81.73(10) . .
O2 Y3 C25 92.41(10) . .
O3 Y3 C25 129.86(11) . .
C54 Y3 C25 148.25(12) . .
O2 Y3 C29 88.50(11) . .
O3 Y3 C29 101.03(12) . .
C54 Y3 C29 170.38(12) . .
C25 Y3 C29 31.00(12) . .
O2 Y3 C28 113.77(12) . .
O3 Y3 C28 80.32(11) . .
C54 Y3 C28 158.32(12) . .
C25 Y3 C28 50.20(12) . .
C29 Y3 C28 29.81(12) . .
O2 Y3 C27 138.46(11) . .
O3 Y3 C27 91.65(11) . .
C54 Y3 C27 139.27(12) . .
C25 Y3 C27 50.79(12) . .
C29 Y3 C27 50.22(13) . .
C28 Y3 C27 30.23(13) . .
O2 Y3 C26 122.20(11) . .
O3 Y3 C26 121.33(11) . .
C54 Y3 C26 136.13(12) . .
C25 Y3 C26 30.76(11) . .
C29 Y3 C26 49.90(12) . .
C28 Y3 C26 48.95(13) . .
C27 Y3 C26 29.68(12) . .
O2 Y3 Si5 104.32(7) . .
O3 Y3 Si5 105.03(7) . .
C54 Y3 Si5 36.90(8) . .
C25 Y3 Si5 117.38(9) . .
C29 Y3 Si5 147.55(10) . .
C28 Y3 Si5 139.56(10) . .
C27 Y3 Si5 109.55(10) . .
C26 Y3 Si5 99.24(9) . .
O2 Y3 Y2 90.67(7) . .
O3 Y3 Y2 37.93(6) . .
C54 Y3 Y2 43.98(8) . .
C25 Y3 Y2 167.76(9) . .
C29 Y3 Y2 137.39(10) . .
C28 Y3 Y2 117.92(10) . .
C27 Y3 Y2 121.49(9) . .
C26 Y3 Y2 146.95(9) . .
Si5 Y3 Y2 73.16(2) . .
O2 Y3 Y1 38.31(6) . .
O3 Y3 Y1 90.38(6) . .
C54 Y3 Y1 43.78(7) . .
C25 Y3 Y1 125.97(8) . .
C29 Y3 Y1 126.68(9) . .
C28 Y3 Y1 147.93(10) . .
C27 Y3 Y1 176.62(9) . .
C26 Y3 Y1 148.17(9) . .
Si5 Y3 Y1 72.48(2) . .
Y2 Y3 Y1 61.502(11) . .
O4 Y4 O1 102.07(9) . .
O4 Y4 C57 82.24(9) . .
O1 Y4 C57 81.93(10) . .
O4 Y4 C37 129.79(10) . .
O1 Y4 C37 90.27(10) . .
C57 Y4 C37 147.96(11) . .
O4 Y4 C38 99.88(10) . .
O1 Y4 C38 88.11(11) . .
C57 Y4 C38 170.04(12) . .
C37 Y4 C38 31.32(11) . .
O4 Y4 C41 123.68(10) . .
O1 Y4 C41 119.39(11) . .
C57 Y4 C41 136.29(11) . .
C37 Y4 C41 30.51(12) . .
C38 Y4 C41 49.97(12) . .
O4 Y4 C39 80.51(10) . .
O1 Y4 C39 114.26(10) . .
C57 Y4 C39 158.47(11) . .
C37 Y4 C39 50.59(11) . .
C38 Y4 C39 29.83(11) . .
C41 Y4 C39 49.40(11) . .
O4 Y4 C40 93.48(10) . .
O1 Y4 C40 137.25(11) . .
C57 Y4 C40 140.06(12) . .
C37 Y4 C40 50.78(12) . .
C38 Y4 C40 49.79(12) . .
C41 Y4 C40 30.25(11) . .
C39 Y4 C40 29.85(11) . .
O4 Y4 Y2 38.19(6) . .
O1 Y4 Y2 90.17(6) . .
C57 Y4 Y2 44.28(7) . .
C37 Y4 Y2 167.52(8) . .
C38 Y4 Y2 136.25(8) . .
C41 Y4 Y2 150.31(9) . .
C39 Y4 Y2 118.37(7) . .
C40 Y4 Y2 123.82(8) . .
O4 Y4 Y1 90.79(6) . .
O1 Y4 Y1 37.84(6) . .
C57 Y4 Y1 44.27(8) . .
C37 Y4 Y1 123.60(8) . .
C38 Y4 Y1 125.79(9) . .
C41 Y4 Y1 145.16(9) . .
C39 Y4 Y1 148.32(9) . .
C40 Y4 Y1 174.39(9) . .
Y2 Y4 Y1 61.595(11) . .
C12 Si1 C10 108.5(3) . .
C12 Si1 C1 114.6(2) . .
C10 Si1 C1 107.8(2) . .
C12 Si1 C11 105.1(3) . .
C10 Si1 C11 106.6(3) . .
C1 Si1 C11 113.9(2) . .
C13 Si2 C23 107.8(2) . .
C13 Si2 C24 113.3(2) . .
C23 Si2 C24 109.1(3) . .
C13 Si2 C22 112.2(2) . .
C23 Si2 C22 106.9(3) . .
C24 Si2 C22 107.3(3) . .
C34 Si3 C25 113.4(2) . .
C34 Si3 C36 105.1(3) . .
C25 Si3 C36 115.4(2) . .
C34 Si3 C35 108.1(3) . .
C25 Si3 C35 107.3(2) . .
C36 Si3 C35 107.1(2) . .
C47 Si4 C48 106.0(4) . .
C47 Si4 C46 107.2(3) . .
C48 Si4 C46 107.6(3) . .
C47 Si4 C37 113.6(2) . .
C48 Si4 C37 113.4(2) . .
C46 Si4 C37 108.7(2) . .
C54 Si5 C53 118.19(18) . .
C54 Si5 C51 109.81(18) . .
C53 Si5 C51 107.2(2) . .
C54 Si5 C52 111.37(17) . .
C53 Si5 C52 106.4(2) . .
C51 Si5 C52 102.67(19) . .
C54 Si5 Y3 55.88(11) . .
C53 Si5 Y3 173.99(14) . .
C51 Si5 Y3 75.47(13) . .
C52 Si5 Y3 77.90(14) . .
C57 Si6 C58 118.46(19) . .
C57 Si6 C59 113.0(2) . .
C58 Si6 C59 106.5(2) . .
C57 Si6 C60 109.39(17) . .
C58 Si6 C60 105.5(2) . .
C59 Si6 C60 102.64(19) . .
C49 O1 Y4 130.7(2) . .
C49 O1 Y1 96.1(2) . .
Y4 O1 Y1 107.52(9) . .
C49 O2 Y3 130.6(2) . .
C49 O2 Y1 95.6(2) . .
Y3 O2 Y1 107.23(10) . .
C50 O3 Y3 131.3(2) . .
C50 O3 Y2 96.05(19) . .
Y3 O3 Y2 107.33(10) . .
C50 O4 Y4 131.0(2) . .
C50 O4 Y2 95.77(19) . .
Y4 O4 Y2 106.89(9) . .
C2 C1 C5 102.7(4) . .
C2 C1 Si1 124.3(3) . .
C5 C1 Si1 129.7(3) . .
C2 C1 Y1 74.3(2) . .
C5 C1 Y1 74.0(2) . .
Si1 C1 Y1 131.28(19) . .
C3 C2 C1 110.6(4) . .
C3 C2 C6 124.6(4) . .
C1 C2 C6 124.1(4) . .
C3 C2 Y1 75.9(2) . .
C1 C2 Y1 75.1(2) . .
C6 C2 Y1 123.9(3) . .
C2 C3 C4 107.7(4) . .
C2 C3 C7 127.4(4) . .
C4 C3 C7 124.6(4) . .
C2 C3 Y1 74.3(2) . .
C4 C3 Y1 74.5(2) . .
C7 C3 Y1 121.7(3) . .
C5 C4 C3 107.9(4) . .
C5 C4 C8 127.3(5) . .
C3 C4 C8 124.3(5) . .
C5 C4 Y1 75.0(3) . .
C3 C4 Y1 75.5(2) . .
C8 C4 Y1 121.6(3) . .
C4 C5 C1 111.1(4) . .
C4 C5 C9 123.8(5) . .
C1 C5 C9 124.4(5) . .
C4 C5 Y1 75.6(3) . .
C1 C5 Y1 74.9(2) . .
C9 C5 Y1 124.7(3) . .
C2 C6 H6A 109.5 . .
C2 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C2 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C3 C7 H7A 109.5 . .
C3 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C3 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
C4 C8 H8A 109.5 . .
C4 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
C4 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
C5 C9 H9A 109.5 . .
C5 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C5 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
Si1 C10 H10A 109.5 . .
Si1 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
Si1 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
Si1 C11 H11A 109.5 . .
Si1 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
Si1 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
Si1 C12 H12A 109.5 . .
Si1 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
Si1 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C17 C13 C14 104.9(3) . .
C17 C13 Si2 126.4(3) . .
C14 C13 Si2 127.0(3) . .
C17 C13 Y2 74.6(2) . .
C14 C13 Y2 74.0(2) . .
Si2 C13 Y2 127.77(17) . .
C15 C14 C13 109.6(3) . .
C15 C14 C18 125.6(4) . .
C13 C14 C18 124.6(4) . .
C15 C14 Y2 75.0(2) . .
C13 C14 Y2 75.5(2) . .
C18 C14 Y2 121.0(3) . .
C14 C15 C16 108.0(4) . .
C14 C15 C19 126.3(4) . .
C16 C15 C19 125.0(4) . .
C14 C15 Y2 75.0(2) . .
C16 C15 Y2 75.0(2) . .
C19 C15 Y2 123.4(3) . .
C15 C16 C17 107.6(4) . .
C15 C16 C20 123.0(4) . .
C17 C16 C20 128.9(5) . .
C15 C16 Y2 74.9(2) . .
C17 C16 Y2 75.4(2) . .
C20 C16 Y2 121.9(3) . .
C16 C17 C13 109.9(4) . .
C16 C17 C21 124.6(4) . .
C13 C17 C21 125.1(4) . .
C16 C17 Y2 74.6(2) . .
C13 C17 Y2 75.1(2) . .
C21 C17 Y2 123.2(3) . .
C14 C18 H18A 109.5 . .
C14 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C14 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C15 C19 H19A 109.5 . .
C15 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
C15 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
C16 C20 H20A 109.5 . .
C16 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C16 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
C17 C21 H21A 109.5 . .
C17 C21 H21B 109.5 . .
H21A C21 H21B 109.5 . .
C17 C21 H21C 109.5 . .
H21A C21 H21C 109.5 . .
H21B C21 H21C 109.5 . .
Si2 C22 H22A 109.5 . .
Si2 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
Si2 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
Si2 C23 H23A 109.5 . .
Si2 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
Si2 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
Si2 C24 H24A 109.5 . .
Si2 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
Si2 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C26 C25 C29 105.4(4) . .
C26 C25 Si3 124.7(3) . .
C29 C25 Si3 125.2(3) . .
C26 C25 Y3 76.0(2) . .
C29 C25 Y3 74.9(2) . .
Si3 C25 Y3 133.35(18) . .
C27 C26 C25 110.1(4) . .
C27 C26 C30 123.8(4) . .
C25 C26 C30 125.7(4) . .
C27 C26 Y3 75.0(2) . .
C25 C26 Y3 73.2(2) . .
C30 C26 Y3 124.0(3) . .
C26 C27 C28 106.6(4) . .
C26 C27 C31 128.1(4) . .
C28 C27 C31 124.5(4) . .
C26 C27 Y3 75.3(2) . .
C28 C27 Y3 74.8(2) . .
C31 C27 Y3 123.7(3) . .
C29 C28 C27 109.7(4) . .
C29 C28 C32 125.8(4) . .
C27 C28 C32 124.2(4) . .
C29 C28 Y3 74.3(2) . .
C27 C28 Y3 75.0(2) . .
C32 C28 Y3 121.9(3) . .
C28 C29 C25 108.1(4) . .
C28 C29 C33 124.5(4) . .
C25 C29 C33 127.0(4) . .
C28 C29 Y3 75.9(2) . .
C25 C29 Y3 74.1(2) . .
C33 C29 Y3 121.9(3) . .
C26 C30 H30A 109.5 . .
C26 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C26 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C27 C31 H31A 109.5 . .
C27 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C27 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C28 C32 H32A 109.5 . .
C28 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C28 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
C29 C33 H33A 109.5 . .
C29 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C29 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
Si3 C34 H34A 109.5 . .
Si3 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
Si3 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
Si3 C35 H35A 109.5 . .
Si3 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
Si3 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
Si3 C36 H36A 109.5 . .
Si3 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
Si3 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C41 C37 C38 105.3(3) . .
C41 C37 Si4 126.5(3) . .
C38 C37 Si4 126.1(3) . .
C41 C37 Y4 75.7(2) . .
C38 C37 Y4 74.7(2) . .
Si4 C37 Y4 127.81(18) . .
C39 C38 C37 108.8(3) . .
C39 C38 C42 124.6(4) . .
C37 C38 C42 126.1(4) . .
C39 C38 Y4 76.8(2) . .
C37 C38 Y4 74.0(2) . .
C42 C38 Y4 122.5(3) . .
C38 C39 C40 109.2(3) . .
C38 C39 C43 125.7(4) . .
C40 C39 C43 124.6(4) . .
C38 C39 Y4 73.4(2) . .
C40 C39 Y4 75.4(2) . .
C43 C39 Y4 124.0(2) . .
C39 C40 C41 106.7(4) . .
C39 C40 C44 125.1(4) . .
C41 C40 C44 127.5(4) . .
C39 C40 Y4 74.7(2) . .
C41 C40 Y4 73.4(2) . .
C44 C40 Y4 124.1(3) . .
C37 C41 C40 110.1(3) . .
C37 C41 C45 126.4(4) . .
C40 C41 C45 123.2(4) . .
C37 C41 Y4 73.8(2) . .
C40 C41 Y4 76.3(2) . .
C45 C41 Y4 121.6(3) . .
C38 C42 H42A 109.5 . .
C38 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C38 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
C39 C43 H43A 109.5 . .
C39 C43 H43B 109.5 . .
H43A C43 H43B 109.5 . .
C39 C43 H43C 109.5 . .
H43A C43 H43C 109.5 . .
H43B C43 H43C 109.5 . .
C40 C44 H44A 109.5 . .
C40 C44 H44B 109.5 . .
H44A C44 H44B 109.5 . .
C40 C44 H44C 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
C41 C45 H45A 109.5 . .
C41 C45 H45B 109.5 . .
H45A C45 H45B 109.5 . .
C41 C45 H45C 109.5 . .
H45A C45 H45C 109.5 . .
H45B C45 H45C 109.5 . .
Si4 C46 H46A 109.5 . .
Si4 C46 H46B 109.5 . .
H46A C46 H46B 109.5 . .
Si4 C46 H46C 109.5 . .
H46A C46 H46C 109.5 . .
H46B C46 H46C 109.5 . .
Si4 C47 H47A 109.5 . .
Si4 C47 H47B 109.5 . .
H47A C47 H47B 109.5 . .
Si4 C47 H47C 109.5 . .
H47A C47 H47C 109.5 . .
H47B C47 H47C 109.5 . .
Si4 C48 H48A 109.5 . .
Si4 C48 H48B 109.5 . .
H48A C48 H48B 109.5 . .
Si4 C48 H48C 109.5 . .
H48A C48 H48C 109.5 . .
H48B C48 H48C 109.5 . .
O2 C49 O1 107.6(3) . .
O2 C49 H49A 110.2 . .
O1 C49 H49A 110.2 . .
O2 C49 H49B 110.2 . .
O1 C49 H49B 110.2 . .
H49A C49 H49B 108.5 . .
O3 C50 O4 107.2(3) . .
O3 C50 H50A 110.3 . .
O4 C50 H50A 110.3 . .
O3 C50 H50B 110.3 . .
O4 C50 H50B 110.3 . .
H50A C50 H50B 108.5 . .
Si5 C51 H51A 109.5 . .
Si5 C51 H51B 109.5 . .
H51A C51 H51B 109.5 . .
Si5 C51 H51C 109.5 . .
H51A C51 H51C 109.5 . .
H51B C51 H51C 109.5 . .
Si5 C52 H52A 109.5 . .
Si5 C52 H52B 109.5 . .
H52A C52 H52B 109.5 . .
Si5 C52 H52C 109.5 . .
H52A C52 H52C 109.5 . .
H52B C52 H52C 109.5 . .
Si5 C53 H53A 109.5 . .
Si5 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
Si5 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C55 C54 Si5 112.6(2) . .
C55 C54 Y2 75.03(19) . .
Si5 C54 Y2 133.28(16) . .
C55 C54 Y1 75.14(18) . .
Si5 C54 Y1 131.71(17) . .
Y2 C54 Y1 95.01(11) . .
C55 C54 Y3 160.1(2) . .
Si5 C54 Y3 87.22(13) . .
Y2 C54 Y3 91.48(11) . .
Y1 C54 Y3 91.95(11) . .
C56 C55 C54 130.4(3) . .
C56 C55 Y2 75.1(2) . .
C54 C55 Y2 71.40(19) . .
C56 C55 Y1 74.8(2) . .
C54 C55 Y1 71.35(18) . .
Y2 C55 Y1 92.62(11) . .
C56 C55 H55 114.8 . .
C54 C55 H55 114.8 . .
Y2 C55 H55 133.3 . .
Y1 C55 H55 133.9 . .
C55 C56 C57 128.2(3) . .
C55 C56 Y1 73.6(2) . .
C57 C56 Y1 71.47(19) . .
C55 C56 Y2 73.32(19) . .
C57 C56 Y2 70.80(18) . .
Y1 C56 Y2 91.74(11) . .
C55 C56 H56 115.9 . .
C57 C56 H56 115.9 . .
Y1 C56 H56 133.4 . .
Y2 C56 H56 134.8 . .
C56 C57 Si6 110.7(2) . .
C56 C57 Y2 75.45(18) . .
Si6 C57 Y2 131.17(17) . .
C56 C57 Y4 160.1(2) . .
Si6 C57 Y4 89.19(13) . .
Y2 C57 Y4 91.32(11) . .
C56 C57 Y1 74.86(19) . .
Si6 C57 Y1 134.49(16) . .
Y2 C57 Y1 94.31(11) . .
Y4 C57 Y1 91.66(11) . .
Si6 C58 H58A 109.5 . .
Si6 C58 H58B 109.5 . .
H58A C58 H58B 109.5 . .
Si6 C58 H58C 109.5 . .
H58A C58 H58C 109.5 . .
H58B C58 H58C 109.5 . .
Si6 C59 H59A 109.5 . .
Si6 C59 H59B 109.5 . .
H59A C59 H59B 109.5 . .
Si6 C59 H59C 109.5 . .
H59A C59 H59C 109.5 . .
H59B C59 H59C 109.5 . .
Si6 C60 H60A 109.5 . .
Si6 C60 H60B 109.5 . .
H60A C60 H60B 109.5 . .
Si6 C60 H60C 109.5 . .
H60A C60 H60C 109.5 . .
H60B C60 H60C 109.5 . .
C73 C71 C74 76.3(10) 2_556 2_556
C73 C71 C72 69.3(9) 2_556 2_556
C74 C71 C72 145.5(14) 2_556 2_556
C73 C71 C76 55.3(10) 2_556 .
C74 C71 C76 131.6(10) 2_556 .
C72 C71 C76 14.0(8) 2_556 .
C73 C71 C72 175.2(10) 2_556 .
C74 C71 C72 108.4(10) 2_556 .
C72 C71 C72 106.1(8) 2_556 .
C76 C71 C72 120.0 . .
C73 C71 C77 64.7(10) 2_556 .
C74 C71 C77 11.6(10) 2_556 .
C72 C71 C77 134.0(8) 2_556 .
C76 C71 C77 120.0 . .
C72 C71 C77 120.0 . .
C73 C71 C75 137.0(14) 2_556 2_556
C74 C71 C75 60.8(7) 2_556 2_556
C72 C71 C75 153.7(13) 2_556 2_556
C76 C71 C75 167.6(8) . 2_556
C72 C71 C75 47.6(8) . 2_556
C77 C71 C75 72.4(8) . 2_556
C73 C71 C71 123.6(13) 2_556 2_556
C74 C71 C71 160.1(14) 2_556 2_556
C72 C71 C71 54.3(6) 2_556 2_556
C76 C71 C71 68.3(6) . 2_556
C72 C71 C71 51.7(6) . 2_556
C77 C71 C71 171.7(6) . 2_556
C75 C71 C71 99.3(10) 2_556 2_556
C73 C71 C76 172.2(14) 2_556 2_556
C74 C71 C76 111.3(11) 2_556 2_556
C72 C71 C76 103.1(10) 2_556 2_556
C76 C71 C76 117.1(6) . 2_556
C72 C71 C76 3.0(7) . 2_556
C77 C71 C76 122.9(7) . 2_556
C75 C71 C76 50.6(5) 2_556 2_556
C71 C71 C76 48.8(5) 2_556 2_556
C73 C72 C71 120.0 . .
C73 C72 H72 120.0 . .
C71 C72 H72 120.0 . .
C72 C73 C74 120.0 . .
C72 C73 H73 120.0 . .
C74 C73 H73 120.0 . .
C75 C74 C73 120.0 . .
C75 C74 H74 120.0 . .
C73 C74 H74 120.0 . .
C74 C75 C76 120.0 . .
C74 C75 H75 120.0 . .
C76 C75 H75 120.0 . .
C71 C76 C75 120.0 . .
C71 C76 H76 120.0 . .
C75 C76 H76 120.0 . .
C71 C77 H77A 109.5 . .
C71 C77 H77B 109.5 . .
H77A C77 H77B 109.5 . .
C71 C77 H77C 109.5 . .
H77A C77 H77C 109.5 . .
H77B C77 H77C 109.5 . .
C82 C81 C86 120.0 . .
C82 C81 C87 120.0 . .
C86 C81 C87 120.0 . .
C81 C82 C83 120.0 . .
C81 C82 H82 120.0 . .
C83 C82 H82 120.0 . .
C84 C83 C82 120.0 . .
C84 C83 H83 120.0 . .
C82 C83 H83 120.0 . .
C83 C84 C85 120.0 . .
C83 C84 H84 120.0 . .
C85 C84 H84 120.0 . .
C86 C85 C84 120.0 . .
C86 C85 H85 120.0 . .
C84 C85 H85 120.0 . .
C85 C86 C81 120.0 . .
C85 C86 H86 120.0 . .
C81 C86 H86 120.0 . .
C81 C87 H87A 109.5 . .
C81 C87 H87B 109.5 . .
H87A C87 H87B 109.5 . .
C81 C87 H87C 109.5 . .
H87A C87 H87C 109.5 . .
H87B C87 H87C 109.5 . .
C96 C91 C92 120.0 . .
C96 C91 C97 120.0 . .
C92 C91 C97 120.0 . .
C93 C92 C91 120.0 . .
C93 C92 H92 120.0 . .
C91 C92 H92 120.0 . .
C92 C93 C94 120.0 . .
C92 C93 H93 120.0 . .
C94 C93 H93 120.0 . .
C95 C94 C93 120.0 . .
C95 C94 H94 120.0 . .
C93 C94 H94 120.0 . .
C96 C95 C94 120.0 . .
C96 C95 H95 120.0 . .
C94 C95 H95 120.0 . .
C95 C96 C91 120.0 . .
C95 C96 H96 120.0 . .
C91 C96 H96 120.0 . .
C91 C97 H97A 109.5 . .
C91 C97 H97B 109.5 . .
H97A C97 H97B 109.5 . .
C91 C97 H97C 109.5 . .
H97A C97 H97C 109.5 . .
H97B C97 H97C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Y1 O1 2.337(2) .
Y1 O2 2.359(2) .
Y1 C54 2.517(3) .
Y1 C57 2.537(3) .
Y1 C55 2.568(3) .
Y1 C56 2.583(4) .
Y1 C5 2.677(4) .
Y1 C2 2.678(4) .
Y1 C4 2.684(4) .
Y1 C1 2.689(4) .
Y1 C3 2.697(4) .
Y1 Y4 3.6328(5) .
Y2 O3 2.330(2) .
Y2 O4 2.334(2) .
Y2 C54 2.514(3) .
Y2 C57 2.522(3) .
Y2 C55 2.562(3) .
Y2 C56 2.585(3) .
Y2 C14 2.687(3) .
Y2 C15 2.688(4) .
Y2 C16 2.689(4) .
Y2 C17 2.700(4) .
Y2 C13 2.707(3) .
Y2 Y4 3.6117(5) .
Y3 O2 2.154(2) .
Y3 O3 2.160(2) .
Y3 C54 2.539(3) .
Y3 C25 2.681(4) .
Y3 C29 2.691(4) .
Y3 C28 2.712(4) .
Y3 C27 2.715(4) .
Y3 C26 2.718(4) .
Y3 Si5 3.0636(12) .
Y4 O4 2.161(2) .
Y4 O1 2.166(2) .
Y4 C57 2.528(3) .
Y4 C37 2.672(4) .
Y4 C38 2.681(4) .
Y4 C41 2.696(4) .
Y4 C39 2.724(4) .
Y4 C40 2.733(4) .
Si1 C12 1.851(5) .
Si1 C10 1.859(5) .
Si1 C1 1.866(4) .
Si1 C11 1.866(5) .
Si2 C13 1.861(4) .
Si2 C23 1.868(5) .
Si2 C24 1.893(6) .
Si2 C22 1.894(6) .
Si3 C34 1.859(5) .
Si3 C25 1.863(4) .
Si3 C36 1.864(5) .
Si3 C35 1.877(5) .
Si4 C47 1.787(6) .
Si4 C48 1.809(6) .
Si4 C46 1.818(5) .
Si4 C37 1.859(4) .
Si5 C54 1.842(3) .
Si5 C53 1.868(4) .
Si5 C51 1.871(4) .
Si5 C52 1.883(4) .
Si6 C57 1.842(4) .
Si6 C58 1.866(4) .
Si6 C59 1.869(4) .
Si6 C60 1.893(4) .
O1 C49 1.410(4) .
O2 C49 1.392(4) .
O3 C50 1.397(4) .
O4 C50 1.401(4) .
C1 C2 1.418(5) .
C1 C5 1.439(6) .
C2 C3 1.383(6) .
C2 C6 1.516(5) .
C3 C4 1.393(6) .
C3 C7 1.515(6) .
C4 C5 1.356(7) .
C4 C8 1.508(6) .
C5 C9 1.561(6) .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 H8A 0.9800 .
C8 H8B 0.9800 .
C8 H8C 0.9800 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 H11A 0.9800 .
C11 H11B 0.9800 .
C11 H11C 0.9800 .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 C17 1.412(5) .
C13 C14 1.418(5) .
C14 C15 1.392(5) .
C14 C18 1.532(5) .
C15 C16 1.393(6) .
C15 C19 1.510(6) .
C16 C17 1.394(6) .
C16 C20 1.501(6) .
C17 C21 1.516(6) .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 H21A 0.9800 .
C21 H21B 0.9800 .
C21 H21C 0.9800 .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
C25 C26 1.432(5) .
C25 C29 1.436(6) .
C26 C27 1.391(6) .
C26 C30 1.519(6) .
C27 C28 1.415(6) .
C27 C31 1.521(6) .
C28 C29 1.390(6) .
C28 C32 1.519(6) .
C29 C33 1.500(6) .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
C35 H35A 0.9800 .
C35 H35B 0.9800 .
C35 H35C 0.9800 .
C36 H36A 0.9800 .
C36 H36B 0.9800 .
C36 H36C 0.9800 .
C37 C41 1.412(5) .
C37 C38 1.445(5) .
C38 C39 1.392(5) .
C38 C42 1.486(5) .
C39 C40 1.405(5) .
C39 C43 1.511(5) .
C40 C41 1.417(5) .
C40 C44 1.503(6) .
C41 C45 1.530(5) .
C42 H42A 0.9800 .
C42 H42B 0.9800 .
C42 H42C 0.9800 .
C43 H43A 0.9800 .
C43 H43B 0.9800 .
C43 H43C 0.9800 .
C44 H44A 0.9800 .
C44 H44B 0.9800 .
C44 H44C 0.9800 .
C45 H45A 0.9800 .
C45 H45B 0.9800 .
C45 H45C 0.9800 .
C46 H46A 0.9800 .
C46 H46B 0.9800 .
C46 H46C 0.9800 .
C47 H47A 0.9800 .
C47 H47B 0.9800 .
C47 H47C 0.9800 .
C48 H48A 0.9800 .
C48 H48B 0.9800 .
C48 H48C 0.9800 .
C49 H49A 0.9900 .
C49 H49B 0.9900 .
C50 H50A 0.9900 .
C50 H50B 0.9900 .
C51 H51A 0.9800 .
C51 H51B 0.9800 .
C51 H51C 0.9800 .
C52 H52A 0.9800 .
C52 H52B 0.9800 .
C52 H52C 0.9800 .
C53 H53A 0.9800 .
C53 H53B 0.9800 .
C53 H53C 0.9800 .
C54 C55 1.467(5) .
C55 C56 1.400(5) .
C55 H55 0.9500 .
C56 C57 1.484(5) .
C56 H56 0.9500 .
C58 H58A 0.9800 .
C58 H58B 0.9800 .
C58 H58C 0.9800 .
C59 H59A 0.9800 .
C59 H59B 0.9800 .
C59 H59C 0.9800 .
C60 H60A 0.9800 .
C60 H60B 0.9800 .
C60 H60C 0.9800 .
C71 C73 1.070(17) 2_556
C71 C74 1.177(16) 2_556
C71 C72 1.344(17) 2_556
C71 C76 1.3897 .
C71 C72 1.3902 .
C71 C77 1.5059 .
C71 C75 1.511(17) 2_556
C71 C71 1.645(16) 2_556
C71 C76 1.716(16) 2_556
C72 C73 1.3898 .
C72 H72 0.9500 .
C73 C74 1.3900 .
C73 H73 0.9500 .
C74 C75 1.3897 .
C74 H74 0.9500 .
C75 C76 1.3904 .
C75 H75 0.9500 .
C76 H76 0.9500 .
C77 H77A 0.9800 .
C77 H77B 0.9800 .
C77 H77C 0.9800 .
C81 C82 1.3900 .
C81 C86 1.3902 .
C81 C87 1.5061 .
C82 C83 1.3901 .
C82 H82 0.9500 .
C83 C84 1.3898 .
C83 H83 0.9500 .
C84 C85 1.3901 .
C84 H84 0.9500 .
C85 C86 1.3899 .
C85 H85 0.9500 .
C86 H86 0.9500 .
C87 H87A 0.9800 .
C87 H87B 0.9800 .
C87 H87C 0.9800 .
C91 C96 1.3898 .
C91 C92 1.3902 .
C91 C97 1.5060 .
C92 C93 1.3898 .
C92 H92 0.9500 .
C93 C94 1.3900 .
C93 H93 0.9500 .
C94 C95 1.3900 .
C94 H94 0.9500 .
C95 C96 1.3894 .
C95 H95 0.9500 .
C96 H96 0.9500 .
C97 H97A 0.9800 .
C97 H97B 0.9800 .
C97 H97C 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O3 Y2 Y3 O2 -109.21(12) .
O4 Y2 Y3 O2 -65.09(8) .
C54 Y2 Y3 O2 77.58(12) .
C57 Y2 Y3 O2 11.99(10) .
C55 Y2 Y3 O2 69.28(10) .
C56 Y2 Y3 O2 46.21(10) .
C14 Y2 Y3 O2 -179.69(11) .
C15 Y2 Y3 O2 150.47(11) .
C16 Y2 Y3 O2 143.76(17) .
C17 Y2 Y3 O2 -156.9(2) .
C13 Y2 Y3 O2 -151.49(11) .
Y4 Y2 Y3 O2 -30.39(7) .
O4 Y2 Y3 O3 44.12(11) .
C54 Y2 Y3 O3 -173.21(14) .
C57 Y2 Y3 O3 121.20(13) .
C55 Y2 Y3 O3 178.49(13) .
C56 Y2 Y3 O3 155.42(13) .
C14 Y2 Y3 O3 -70.48(13) .
C15 Y2 Y3 O3 -100.32(14) .
C16 Y2 Y3 O3 -107.04(18) .
C17 Y2 Y3 O3 -47.7(2) .
C13 Y2 Y3 O3 -42.28(14) .
Y4 Y2 Y3 O3 78.82(10) .
O3 Y2 Y3 C54 173.21(14) .
O4 Y2 Y3 C54 -142.68(12) .
C57 Y2 Y3 C54 -65.60(13) .
C55 Y2 Y3 C54 -8.30(13) .
C56 Y2 Y3 C54 -31.37(13) .
C14 Y2 Y3 C54 102.73(13) .
C15 Y2 Y3 C54 72.89(14) .
C16 Y2 Y3 C54 66.17(18) .
C17 Y2 Y3 C54 125.6(2) .
C13 Y2 Y3 C54 130.93(14) .
Y4 Y2 Y3 C54 -107.97(10) .
O3 Y2 Y3 C25 -4.6(4) .
O4 Y2 Y3 C25 39.5(4) .
C54 Y2 Y3 C25 -177.8(4) .
C57 Y2 Y3 C25 116.6(4) .
C55 Y2 Y3 C25 173.9(4) .
C56 Y2 Y3 C25 150.8(4) .
C14 Y2 Y3 C25 -75.1(4) .
C15 Y2 Y3 C25 -104.9(4) .
C16 Y2 Y3 C25 -111.6(4) .
C17 Y2 Y3 C25 -52.3(4) .
C13 Y2 Y3 C25 -46.9(4) .
Y4 Y2 Y3 C25 74.2(4) .
O3 Y2 Y3 C29 -20.70(17) .
O4 Y2 Y3 C29 23.42(15) .
C54 Y2 Y3 C29 166.10(17) .
C57 Y2 Y3 C29 100.50(16) .
C55 Y2 Y3 C29 157.79(16) .
C56 Y2 Y3 C29 134.73(16) .
C14 Y2 Y3 C29 -91.17(16) .
C15 Y2 Y3 C29 -121.01(16) .
C16 Y2 Y3 C29 -127.7(2) .
C17 Y2 Y3 C29 -68.4(2) .
C13 Y2 Y3 C29 -62.97(17) .
Y4 Y2 Y3 C29 58.13(14) .
O3 Y2 Y3 C28 8.33(15) .
O4 Y2 Y3 C28 52.45(12) .
C54 Y2 Y3 C28 -164.87(15) .
C57 Y2 Y3 C28 129.53(14) .
C55 Y2 Y3 C28 -173.18(13) .
C56 Y2 Y3 C28 163.75(13) .
C14 Y2 Y3 C28 -62.14(14) .
C15 Y2 Y3 C28 -91.98(14) .
C16 Y2 Y3 C28 -98.70(19) .
C17 Y2 Y3 C28 -39.3(2) .
C13 Y2 Y3 C28 -33.95(14) .
Y4 Y2 Y3 C28 87.15(11) .
O3 Y2 Y3 C27 43.04(15) .
O4 Y2 Y3 C27 87.16(13) .
C54 Y2 Y3 C27 -130.17(15) .
C57 Y2 Y3 C27 164.24(14) .
C55 Y2 Y3 C27 -138.47(14) .
C56 Y2 Y3 C27 -161.54(14) .
C14 Y2 Y3 C27 -27.44(14) .
C15 Y2 Y3 C27 -57.28(15) .
C16 Y2 Y3 C27 -64.00(19) .
C17 Y2 Y3 C27 -4.6(2) .
C13 Y2 Y3 C27 0.76(15) .
Y4 Y2 Y3 C27 121.86(11) .
O3 Y2 Y3 C26 65.09(19) .
O4 Y2 Y3 C26 109.20(17) .
C54 Y2 Y3 C26 -108.12(19) .
C57 Y2 Y3 C26 -173.72(18) .
C55 Y2 Y3 C26 -116.42(18) .
C56 Y2 Y3 C26 -139.49(18) .
C14 Y2 Y3 C26 -5.39(19) .
C15 Y2 Y3 C26 -35.23(19) .
C16 Y2 Y3 C26 -41.9(2) .
C17 Y2 Y3 C26 17.4(3) .
C13 Y2 Y3 C26 22.81(19) .
Y4 Y2 Y3 C26 143.91(16) .
O3 Y2 Y3 Si5 146.02(10) .
O4 Y2 Y3 Si5 -169.86(6) .
C54 Y2 Y3 Si5 -27.19(11) .
C57 Y2 Y3 Si5 -92.78(8) .
C55 Y2 Y3 Si5 -35.49(8) .
C56 Y2 Y3 Si5 -58.56(8) .
C14 Y2 Y3 Si5 75.54(9) .
C15 Y2 Y3 Si5 45.70(10) .
C16 Y2 Y3 Si5 38.99(16) .
C17 Y2 Y3 Si5 98.4(2) .
C13 Y2 Y3 Si5 103.74(10) .
Y4 Y2 Y3 Si5 -135.16(2) .
O3 Y2 Y3 Y1 -135.14(10) .
O4 Y2 Y3 Y1 -91.03(6) .
C54 Y2 Y3 Y1 51.65(10) .
C57 Y2 Y3 Y1 -13.95(8) .
C55 Y2 Y3 Y1 43.35(8) .
C56 Y2 Y3 Y1 20.28(8) .
C14 Y2 Y3 Y1 154.38(9) .
C15 Y2 Y3 Y1 124.54(9) .
C16 Y2 Y3 Y1 117.82(15) .
C17 Y2 Y3 Y1 177.2(2) .
C13 Y2 Y3 Y1 -177.42(9) .
Y4 Y2 Y3 Y1 -56.323(11) .
O1 Y1 Y3 O2 -44.81(12) .
C54 Y1 Y3 O2 172.96(15) .
C57 Y1 Y3 O2 -121.30(13) .
C55 Y1 Y3 O2 -178.44(13) .
C56 Y1 Y3 O2 -155.41(13) .
C5 Y1 Y3 O2 43.4(2) .
C2 Y1 Y3 O2 93.06(14) .
C4 Y1 Y3 O2 37.90(16) .
C1 Y1 Y3 O2 99.72(19) .
C3 Y1 Y3 O2 64.29(14) .
Y4 Y1 Y3 O2 -79.25(11) .
O1 Y1 Y3 O3 64.62(9) .
O2 Y1 Y3 O3 109.44(12) .
C54 Y1 Y3 O3 -77.60(13) .
C57 Y1 Y3 O3 -11.86(10) .
C55 Y1 Y3 O3 -69.01(10) .
C56 Y1 Y3 O3 -45.97(10) .
C5 Y1 Y3 O3 152.9(2) .
C2 Y1 Y3 O3 -157.51(11) .
C4 Y1 Y3 O3 147.34(13) .
C1 Y1 Y3 O3 -150.84(16) .
C3 Y1 Y3 O3 173.73(12) .
Y4 Y1 Y3 O3 30.19(6) .
O1 Y1 Y3 C54 142.23(13) .
O2 Y1 Y3 C54 -172.96(15) .
C57 Y1 Y3 C54 65.74(14) .
C55 Y1 Y3 C54 8.60(14) .
C56 Y1 Y3 C54 31.63(14) .
C5 Y1 Y3 C54 -129.5(2) .
C2 Y1 Y3 C54 -79.91(15) .
C4 Y1 Y3 C54 -135.06(16) .
C1 Y1 Y3 C54 -73.24(19) .
C3 Y1 Y3 C54 -108.67(15) .
Y4 Y1 Y3 C54 107.79(11) .
O1 Y1 Y3 C25 -78.20(12) .
O2 Y1 Y3 C25 -33.39(15) .
C54 Y1 Y3 C25 139.57(15) .
C57 Y1 Y3 C25 -154.69(13) .
C55 Y1 Y3 C25 148.17(13) .
C56 Y1 Y3 C25 171.20(13) .
C5 Y1 Y3 C25 10.0(2) .
C2 Y1 Y3 C25 59.66(14) .
C4 Y1 Y3 C25 4.51(16) .
C1 Y1 Y3 C25 66.33(19) .
C3 Y1 Y3 C25 30.90(15) .
Y4 Y1 Y3 C25 -112.64(11) .
O1 Y1 Y3 C29 -39.46(13) .
O2 Y1 Y3 C29 5.35(16) .
C54 Y1 Y3 C29 178.31(16) .
C57 Y1 Y3 C29 -115.95(14) .
C55 Y1 Y3 C29 -173.10(14) .
C56 Y1 Y3 C29 -150.06(14) .
C5 Y1 Y3 C29 48.8(2) .
C2 Y1 Y3 C29 98.40(15) .
C4 Y1 Y3 C29 43.25(17) .
C1 Y1 Y3 C29 105.07(19) .
C3 Y1 Y3 C29 69.64(16) .
Y4 Y1 Y3 C29 -73.90(12) .
O1 Y1 Y3 C28 -7.55(19) .
O2 Y1 Y3 C28 37.3(2) .
C54 Y1 Y3 C28 -149.8(2) .
C57 Y1 Y3 C28 -84.0(2) .
C55 Y1 Y3 C28 -141.2(2) .
C56 Y1 Y3 C28 -118.1(2) .
C5 Y1 Y3 C28 80.7(3) .
C2 Y1 Y3 C28 130.3(2) .
C4 Y1 Y3 C28 75.2(2) .
C1 Y1 Y3 C28 137.0(2) .
C3 Y1 Y3 C28 101.6(2) .
Y4 Y1 Y3 C28 -41.99(18) .
O1 Y1 Y3 C27 -62.3(17) .
O2 Y1 Y3 C27 -17.5(17) .
C54 Y1 Y3 C27 155.4(17) .
C57 Y1 Y3 C27 -138.8(17) .
C55 Y1 Y3 C27 164.0(17) .
C56 Y1 Y3 C27 -172.9(17) .
C5 Y1 Y3 C27 25.9(17) .
C2 Y1 Y3 C27 75.5(17) .
C4 Y1 Y3 C27 20.4(17) .
C1 Y1 Y3 C27 82.2(17) .
C3 Y1 Y3 C27 46.8(17) .
Y4 Y1 Y3 C27 -96.8(17) .
O1 Y1 Y3 C26 -110.63(18) .
O2 Y1 Y3 C26 -65.8(2) .
C54 Y1 Y3 C26 107.1(2) .
C57 Y1 Y3 C26 172.88(18) .
C55 Y1 Y3 C26 115.74(18) .
C56 Y1 Y3 C26 138.77(18) .
C5 Y1 Y3 C26 -22.4(3) .
C2 Y1 Y3 C26 27.24(19) .
C4 Y1 Y3 C26 -27.9(2) .
C1 Y1 Y3 C26 33.9(2) .
C3 Y1 Y3 C26 -1.53(19) .
Y4 Y1 Y3 C26 -145.07(17) .
O1 Y1 Y3 Si5 170.28(6) .
O2 Y1 Y3 Si5 -144.91(11) .
C54 Y1 Y3 Si5 28.05(11) .
C57 Y1 Y3 Si5 93.79(8) .
C55 Y1 Y3 Si5 36.65(8) .
C56 Y1 Y3 Si5 59.69(8) .
C5 Y1 Y3 Si5 -101.5(2) .
C2 Y1 Y3 Si5 -51.85(10) .
C4 Y1 Y3 Si5 -107.01(12) .
C1 Y1 Y3 Si5 -45.18(15) .
C3 Y1 Y3 Si5 -80.61(10) .
Y4 Y1 Y3 Si5 135.84(3) .
O1 Y1 Y3 Y2 90.32(6) .
O2 Y1 Y3 Y2 135.13(11) .
C54 Y1 Y3 Y2 -51.91(11) .
C57 Y1 Y3 Y2 13.83(8) .
C55 Y1 Y3 Y2 -43.31(8) .
C56 Y1 Y3 Y2 -20.28(8) .
C5 Y1 Y3 Y2 178.5(2) .
C2 Y1 Y3 Y2 -131.82(10) .
C4 Y1 Y3 Y2 173.03(12) .
C1 Y1 Y3 Y2 -125.15(15) .
C3 Y1 Y3 Y2 -160.58(10) .
Y4 Y1 Y3 Y2 55.882(11) .
O3 Y2 Y4 O4 -44.65(12) .
C54 Y2 Y4 O4 -121.79(13) .
C57 Y2 Y4 O4 172.23(15) .
C55 Y2 Y4 O4 -155.80(13) .
C56 Y2 Y4 O4 -179.24(13) .
C14 Y2 Y4 O4 34.07(19) .
C15 Y2 Y4 O4 98.9(2) .
C16 Y2 Y4 O4 104.92(15) .
C17 Y2 Y4 O4 76.97(14) .
C13 Y2 Y4 O4 45.09(14) .
O3 Y2 Y4 O1 64.90(9) .
O4 Y2 Y4 O1 109.55(12) .
C54 Y2 Y4 O1 -12.24(10) .
C57 Y2 Y4 O1 -78.22(13) .
C55 Y2 Y4 O1 -46.25(10) .
C56 Y2 Y4 O1 -69.69(10) .
C14 Y2 Y4 O1 143.62(17) .
C15 Y2 Y4 O1 -151.6(2) .
C16 Y2 Y4 O1 -145.53(12) .
C17 Y2 Y4 O1 -173.48(11) .
C13 Y2 Y4 O1 154.64(11) .
O3 Y2 Y4 C57 143.12(13) .
O4 Y2 Y4 C57 -172.23(15) .
C54 Y2 Y4 C57 65.98(14) .
C55 Y2 Y4 C57 31.97(14) .
C56 Y2 Y4 C57 8.53(14) .
C14 Y2 Y4 C57 -138.16(19) .
C15 Y2 Y4 C57 -73.3(2) .
C16 Y2 Y4 C57 -67.31(16) .
C17 Y2 Y4 C57 -95.26(15) .
C13 Y2 Y4 C57 -127.14(14) .
O3 Y2 Y4 C37 -27.1(4) .
O4 Y2 Y4 C37 17.5(4) .
C54 Y2 Y4 C37 -104.2(4) .
C57 Y2 Y4 C37 -170.2(4) .
C55 Y2 Y4 C37 -138.2(4) .
C56 Y2 Y4 C37 -161.7(4) .
C14 Y2 Y4 C37 51.6(4) .
C15 Y2 Y4 C37 116.4(4) .
C16 Y2 Y4 C37 122.5(4) .
C17 Y2 Y4 C37 94.5(4) .
C13 Y2 Y4 C37 62.6(4) .
O3 Y2 Y4 C38 -22.54(14) .
O4 Y2 Y4 C38 22.11(16) .
C54 Y2 Y4 C38 -99.68(15) .
C57 Y2 Y4 C38 -165.66(17) .
C55 Y2 Y4 C38 -133.69(15) .
C56 Y2 Y4 C38 -157.13(15) .
C14 Y2 Y4 C38 56.2(2) .
C15 Y2 Y4 C38 121.0(2) .
C16 Y2 Y4 C38 127.03(17) .
C17 Y2 Y4 C38 99.08(16) .
C13 Y2 Y4 C38 67.20(16) .
O3 Y2 Y4 C41 -109.92(18) .
O4 Y2 Y4 C41 -65.3(2) .
C54 Y2 Y4 C41 172.94(19) .
C57 Y2 Y4 C41 107.0(2) .
C55 Y2 Y4 C41 138.93(19) .
C56 Y2 Y4 C41 115.49(19) .
C14 Y2 Y4 C41 -31.2(2) .
C15 Y2 Y4 C41 33.6(3) .
C16 Y2 Y4 C41 39.6(2) .
C17 Y2 Y4 C41 11.70(19) .
C13 Y2 Y4 C41 -20.18(19) .
O3 Y2 Y4 C39 -53.03(11) .
O4 Y2 Y4 C39 -8.38(14) .
C54 Y2 Y4 C39 -130.17(12) .
C57 Y2 Y4 C39 163.85(15) .
C55 Y2 Y4 C39 -164.18(12) .
C56 Y2 Y4 C39 172.38(13) .
C14 Y2 Y4 C39 25.69(18) .
C15 Y2 Y4 C39 90.5(2) .
C16 Y2 Y4 C39 96.54(15) .
C17 Y2 Y4 C39 68.59(14) .
C13 Y2 Y4 C39 36.71(13) .
O3 Y2 Y4 C40 -87.47(12) .
O4 Y2 Y4 C40 -42.82(15) .
C54 Y2 Y4 C40 -164.61(13) .
C57 Y2 Y4 C40 129.41(15) .
C55 Y2 Y4 C40 161.39(13) .
C56 Y2 Y4 C40 137.94(13) .
C14 Y2 Y4 C40 -8.75(19) .
C15 Y2 Y4 C40 56.1(2) .
C16 Y2 Y4 C40 62.10(15) .
C17 Y2 Y4 C40 34.15(14) .
C13 Y2 Y4 C40 2.27(14) .
O3 Y2 Y4 Y1 90.82(6) .
O4 Y2 Y4 Y1 135.47(10) .
C54 Y2 Y4 Y1 13.68(8) .
C57 Y2 Y4 Y1 -52.30(11) .
C55 Y2 Y4 Y1 -20.33(8) .
C56 Y2 Y4 Y1 -43.77(8) .
C14 Y2 Y4 Y1 169.54(16) .
C15 Y2 Y4 Y1 -125.6(2) .
C16 Y2 Y4 Y1 -119.61(11) .
C17 Y2 Y4 Y1 -147.56(10) .
C13 Y2 Y4 Y1 -179.45(9) .
O1 Y1 Y4 O4 -108.86(12) .
O2 Y1 Y4 O4 -64.58(8) .
C54 Y1 Y4 O4 12.07(10) .
C57 Y1 Y4 O4 78.02(12) .
C55 Y1 Y4 O4 45.95(10) .
C56 Y1 Y4 O4 69.61(10) .
C5 Y1 Y4 O4 178.40(14) .
C2 Y1 Y4 O4 170.1(3) .
C4 Y1 Y4 O4 -150.21(14) .
C1 Y1 Y4 O4 150.53(13) .
C3 Y1 Y4 O4 -134.07(17) .
O2 Y1 Y4 O1 44.28(11) .
C54 Y1 Y4 O1 120.93(13) .
C57 Y1 Y4 O1 -173.12(14) .
C55 Y1 Y4 O1 154.81(13) .
C56 Y1 Y4 O1 178.47(12) .
C5 Y1 Y4 O1 -72.74(16) .
C2 Y1 Y4 O1 -81.0(3) .
C4 Y1 Y4 O1 -41.35(16) .
C1 Y1 Y4 O1 -100.61(16) .
C3 Y1 Y4 O1 -25.21(19) .
O1 Y1 Y4 C57 173.12(14) .
O2 Y1 Y4 C57 -142.60(12) .
C54 Y1 Y4 C57 -65.95(13) .
C55 Y1 Y4 C57 -32.07(13) .
C56 Y1 Y4 C57 -8.41(13) .
C5 Y1 Y4 C57 100.38(17) .
C2 Y1 Y4 C57 92.1(3) .
C4 Y1 Y4 C57 131.77(16) .
C1 Y1 Y4 C57 72.51(16) .
C3 Y1 Y4 C57 147.91(19) .
O1 Y1 Y4 C37 32.19(14) .
O2 Y1 Y4 C37 76.47(11) .
C54 Y1 Y4 C37 153.12(12) .
C57 Y1 Y4 C37 -140.93(14) .
C55 Y1 Y4 C37 -173.00(12) .
C56 Y1 Y4 C37 -149.34(12) .
C5 Y1 Y4 C37 -40.55(16) .
C2 Y1 Y4 C37 -48.8(3) .
C4 Y1 Y4 C37 -9.16(16) .
C1 Y1 Y4 C37 -68.42(15) .
C3 Y1 Y4 C37 6.97(19) .
O1 Y1 Y4 C38 -6.06(14) .
O2 Y1 Y4 C38 38.22(11) .
C54 Y1 Y4 C38 114.87(13) .
C57 Y1 Y4 C38 -179.18(14) .
C55 Y1 Y4 C38 148.75(13) .
C56 Y1 Y4 C38 172.41(12) .
C5 Y1 Y4 C38 -78.80(17) .
C2 Y1 Y4 C38 -87.1(3) .
C4 Y1 Y4 C38 -47.41(16) .
C1 Y1 Y4 C38 -106.67(15) .
C3 Y1 Y4 C38 -31.27(19) .
O1 Y1 Y4 C41 63.32(18) .
O2 Y1 Y4 C41 107.60(16) .
C54 Y1 Y4 C41 -175.75(17) .
C57 Y1 Y4 C41 -109.80(19) .
C55 Y1 Y4 C41 -141.87(17) .
C56 Y1 Y4 C41 -118.21(17) .
C5 Y1 Y4 C41 -9.4(2) .
C2 Y1 Y4 C41 -17.7(3) .
C4 Y1 Y4 C41 22.0(2) .
C1 Y1 Y4 C41 -37.3(2) .
C3 Y1 Y4 C41 38.1(2) .
O1 Y1 Y4 C39 -35.81(17) .
O2 Y1 Y4 C39 8.47(15) .
C54 Y1 Y4 C39 85.12(16) .
C57 Y1 Y4 C39 151.07(18) .
C55 Y1 Y4 C39 119.00(16) .
C56 Y1 Y4 C39 142.66(16) .
C5 Y1 Y4 C39 -108.55(19) .
C2 Y1 Y4 C39 -116.8(3) .
C4 Y1 Y4 C39 -77.16(19) .
C1 Y1 Y4 C39 -136.42(19) .
C3 Y1 Y4 C39 -61.0(2) .
O1 Y1 Y4 C40 30.7(9) .
O2 Y1 Y4 C40 75.0(9) .
C54 Y1 Y4 C40 151.6(9) .
C57 Y1 Y4 C40 -142.4(9) .
C55 Y1 Y4 C40 -174.5(9) .
C56 Y1 Y4 C40 -150.8(9) .
C5 Y1 Y4 C40 -42.0(9) .
C2 Y1 Y4 C40 -50.3(9) .
C4 Y1 Y4 C40 -10.6(9) .
C1 Y1 Y4 C40 -69.9(9) .
C3 Y1 Y4 C40 5.5(9) .
O1 Y1 Y4 Y2 -134.56(10) .
O2 Y1 Y4 Y2 -90.28(6) .
C54 Y1 Y4 Y2 -13.63(8) .
C57 Y1 Y4 Y2 52.32(10) .
C55 Y1 Y4 Y2 20.25(8) .
C56 Y1 Y4 Y2 43.91(8) .
C5 Y1 Y4 Y2 152.70(13) .
C2 Y1 Y4 Y2 144.4(3) .
C4 Y1 Y4 Y2 -175.91(13) .
C1 Y1 Y4 Y2 124.83(12) .
C3 Y1 Y4 Y2 -159.78(16) .
O2 Y3 Si5 C54 -54.39(14) .
O3 Y3 Si5 C54 52.73(14) .
C25 Y3 Si5 C54 -154.83(15) .
C29 Y3 Si5 C54 -165.0(2) .
C28 Y3 Si5 C54 145.41(19) .
C27 Y3 Si5 C54 150.03(16) .
C26 Y3 Si5 C54 178.83(15) .
Y2 Y3 Si5 C54 31.90(12) .
Y1 Y3 Si5 C54 -32.82(12) .
O2 Y3 Si5 C53 -44.6(15) .
O3 Y3 Si5 C53 62.6(15) .
C54 Y3 Si5 C53 9.8(15) .
C25 Y3 Si5 C53 -145.0(15) .
C29 Y3 Si5 C53 -155.1(15) .
C28 Y3 Si5 C53 155.2(15) .
C27 Y3 Si5 C53 159.9(15) .
C26 Y3 Si5 C53 -171.3(15) .
Y2 Y3 Si5 C53 41.7(15) .
Y1 Y3 Si5 C53 -23.0(15) .
O2 Y3 Si5 C51 72.37(15) .
O3 Y3 Si5 C51 179.49(15) .
C54 Y3 Si5 C51 126.76(19) .
C25 Y3 Si5 C51 -28.07(17) .
C29 Y3 Si5 C51 -38.2(2) .
C28 Y3 Si5 C51 -87.8(2) .
C27 Y3 Si5 C51 -83.21(17) .
C26 Y3 Si5 C51 -54.41(16) .
Y2 Y3 Si5 C51 158.66(14) .
Y1 Y3 Si5 C51 93.95(14) .
O2 Y3 Si5 C52 179.07(15) .
O3 Y3 Si5 C52 -73.81(15) .
C54 Y3 Si5 C52 -126.54(19) .
C25 Y3 Si5 C52 78.63(16) .
C29 Y3 Si5 C52 68.5(2) .
C28 Y3 Si5 C52 18.9(2) .
C27 Y3 Si5 C52 23.49(17) .
C26 Y3 Si5 C52 52.29(16) .
Y2 Y3 Si5 C52 -94.64(14) .
Y1 Y3 Si5 C52 -159.35(14) .
O4 Y4 O1 C49 -39.3(3) .
C57 Y4 O1 C49 -119.6(3) .
C37 Y4 O1 C49 91.6(3) .
C38 Y4 O1 C49 60.4(3) .
C41 Y4 O1 C49 101.2(3) .
C39 Y4 O1 C49 45.6(3) .
C40 Y4 O1 C49 69.5(3) .
Y2 Y4 O1 C49 -75.9(3) .
Y1 Y4 O1 C49 -114.7(3) .
O4 Y4 O1 Y1 75.38(10) .
C57 Y4 O1 Y1 -4.84(10) .
C37 Y4 O1 Y1 -153.66(11) .
C38 Y4 O1 Y1 175.08(11) .
C41 Y4 O1 Y1 -144.13(11) .
C39 Y4 O1 Y1 160.30(10) .
C40 Y4 O1 Y1 -175.78(13) .
Y2 Y4 O1 Y1 38.81(8) .
O2 Y1 O1 C49 10.89(19) .
C54 Y1 O1 C49 67.2(2) .
C57 Y1 O1 C49 141.1(2) .
C55 Y1 O1 C49 103.6(2) .
C56 Y1 O1 C49 134.6(2) .
C5 Y1 O1 C49 -108.3(2) .
C2 Y1 O1 C49 -74.9(2) .
C4 Y1 O1 C49 -80.4(2) .
C1 Y1 O1 C49 -115.0(2) .
C3 Y1 O1 C49 -59.6(2) .
Y4 Y1 O1 C49 136.2(2) .
O2 Y1 O1 Y4 -125.31(13) .
C54 Y1 O1 Y4 -68.98(13) .
C57 Y1 O1 Y4 4.88(10) .
C55 Y1 O1 Y4 -32.64(16) .
C56 Y1 O1 Y4 -1.60(13) .
C5 Y1 O1 Y4 115.47(14) .
C2 Y1 O1 Y4 148.87(13) .
C4 Y1 O1 Y4 143.44(14) .
C1 Y1 O1 Y4 108.76(14) .
C3 Y1 O1 Y4 164.18(12) .
O3 Y3 O2 C49 38.8(3) .
C54 Y3 O2 C49 118.5(3) .
C25 Y3 O2 C49 -92.9(3) .
C29 Y3 O2 C49 -62.1(3) .
C28 Y3 O2 C49 -45.9(3) .
C27 Y3 O2 C49 -68.0(3) .
C26 Y3 O2 C49 -101.1(3) .
Si5 Y3 O2 C49 148.0(3) .
Y2 Y3 O2 C49 75.3(3) .
Y1 Y3 O2 C49 113.6(3) .
O3 Y3 O2 Y1 -74.75(11) .
C54 Y3 O2 Y1 4.91(11) .
C25 Y3 O2 Y1 153.53(12) .
C29 Y3 O2 Y1 -175.71(13) .
C28 Y3 O2 Y1 -159.44(12) .
C27 Y3 O2 Y1 178.47(14) .
C26 Y3 O2 Y1 145.35(12) .
Si5 Y3 O2 Y1 34.46(10) .
Y2 Y3 O2 Y1 -38.32(8) .
O1 Y1 O2 C49 -11.02(19) .
C54 Y1 O2 C49 -140.7(2) .
C57 Y1 O2 C49 -66.9(2) .
C55 Y1 O2 C49 -134.0(2) .
C56 Y1 O2 C49 -103.6(2) .
C5 Y1 O2 C49 69.0(2) .
C2 Y1 O2 C49 123.0(2) .
C4 Y1 O2 C49 77.0(2) .
C1 Y1 O2 C49 101.9(2) .
C3 Y1 O2 C49 106.7(2) .
Y4 Y1 O2 C49 -39.06(19) .
O1 Y1 O2 Y3 124.64(13) .
C54 Y1 O2 Y3 -5.01(11) .
C57 Y1 O2 Y3 68.73(13) .
C55 Y1 O2 Y3 1.63(14) .
C56 Y1 O2 Y3 32.10(17) .
C5 Y1 O2 Y3 -155.30(13) .
C2 Y1 O2 Y3 -101.35(12) .
C4 Y1 O2 Y3 -147.38(14) .
C1 Y1 O2 Y3 -122.48(14) .
C3 Y1 O2 Y3 -117.69(13) .
Y4 Y1 O2 Y3 96.59(9) .
O2 Y3 O3 C50 -39.9(3) .
C54 Y3 O3 C50 -119.7(3) .
C25 Y3 O3 C50 63.8(3) .
C29 Y3 O3 C50 51.0(3) .
C28 Y3 O3 C50 72.5(3) .
C27 Y3 O3 C50 100.7(3) .
C26 Y3 O3 C50 100.4(3) .
Si5 Y3 O3 C50 -148.6(3) .
Y2 Y3 O3 C50 -114.9(3) .
Y1 Y3 O3 C50 -76.6(3) .
O2 Y3 O3 Y2 75.04(11) .
C54 Y3 O3 Y2 -4.76(10) .
C25 Y3 O3 Y2 178.73(11) .
C29 Y3 O3 Y2 165.89(11) .
C28 Y3 O3 Y2 -172.54(13) .
C27 Y3 O3 Y2 -144.39(12) .
C26 Y3 O3 Y2 -144.62(11) .
Si5 Y3 O3 Y2 -33.63(10) .
Y1 Y3 O3 Y2 38.31(8) .
O4 Y2 O3 C50 11.16(18) .
C54 Y2 O3 C50 141.6(2) .
C57 Y2 O3 C50 67.4(2) .
C55 Y2 O3 C50 135.20(19) .
C56 Y2 O3 C50 104.4(2) .
C14 Y2 O3 C50 -108.7(2) .
C15 Y2 O3 C50 -125.2(2) .
C16 Y2 O3 C50 -100.6(2) .
C17 Y2 O3 C50 -67.9(2) .
C13 Y2 O3 C50 -78.3(2) .
Y4 Y2 O3 C50 39.56(18) .
O4 Y2 O3 Y3 -125.63(12) .
C54 Y2 O3 Y3 4.85(10) .
C57 Y2 O3 Y3 -69.39(13) .
C55 Y2 O3 Y3 -1.59(13) .
C56 Y2 O3 Y3 -32.36(16) .
C14 Y2 O3 Y3 114.51(12) .
C15 Y2 O3 Y3 98.02(13) .
C16 Y2 O3 Y3 122.64(18) .
C17 Y2 O3 Y3 155.36(12) .
C13 Y2 O3 Y3 144.94(11) .
Y4 Y2 O3 Y3 -97.23(8) .
O1 Y4 O4 C50 39.3(3) .
C57 Y4 O4 C50 119.2(3) .
C37 Y4 O4 C50 -61.4(3) .
C38 Y4 O4 C50 -50.9(3) .
C41 Y4 O4 C50 -99.0(3) .
C39 Y4 O4 C50 -73.7(3) .
C40 Y4 O4 C50 -100.7(3) .
Y2 Y4 O4 C50 113.8(3) .
Y1 Y4 O4 C50 75.7(3) .
O1 Y4 O4 Y2 -74.51(11) .
C57 Y4 O4 Y2 5.47(11) .
C37 Y4 O4 Y2 -175.14(12) .
C38 Y4 O4 Y2 -164.68(11) .
C41 Y4 O4 Y2 147.27(12) .
C39 Y4 O4 Y2 172.53(13) .
C40 Y4 O4 Y2 145.55(12) .
Y1 Y4 O4 Y2 -38.09(8) .
O3 Y2 O4 C50 -11.12(18) .
C54 Y2 O4 C50 -67.3(2) .
C57 Y2 O4 C50 -141.5(2) .
C55 Y2 O4 C50 -104.2(2) .
C56 Y2 O4 C50 -135.22(19) .
C14 Y2 O4 C50 63.5(2) .
C15 Y2 O4 C50 83.1(3) .
C16 Y2 O4 C50 121.1(2) .
C17 Y2 O4 C50 112.2(2) .
C13 Y2 O4 C50 82.7(2) .
Y4 Y2 O4 C50 -136.0(2) .
O3 Y2 O4 Y4 124.90(13) .
C54 Y2 O4 Y4 68.68(13) .
C57 Y2 O4 Y4 -5.53(11) .
C55 Y2 O4 Y4 31.81(16) .
C56 Y2 O4 Y4 0.80(14) .
C14 Y2 O4 Y4 -160.48(11) .
C15 Y2 O4 Y4 -140.84(16) .
C16 Y2 O4 Y4 -102.88(14) .
C17 Y2 O4 Y4 -111.74(12) .
C13 Y2 O4 Y4 -141.32(12) .
C12 Si1 C1 C2 47.7(4) .
C10 Si1 C1 C2 -73.2(4) .
C11 Si1 C1 C2 168.7(4) .
C12 Si1 C1 C5 -156.3(4) .
C10 Si1 C1 C5 82.8(4) .
C11 Si1 C1 C5 -35.3(5) .
C12 Si1 C1 Y1 -51.7(3) .
C10 Si1 C1 Y1 -172.6(3) .
C11 Si1 C1 Y1 69.3(3) .
O1 Y1 C1 C2 121.5(2) .
O2 Y1 C1 C2 41.4(3) .
C54 Y1 C1 C2 -60.8(3) .
C57 Y1 C1 C2 -149.2(2) .
C55 Y1 C1 C2 -87.8(2) .
C56 Y1 C1 C2 -119.2(2) .
C5 Y1 C1 C2 108.6(4) .
C4 Y1 C1 C2 74.3(3) .
C3 Y1 C1 C2 35.2(2) .
Y4 Y1 C1 C2 166.57(19) .
O1 Y1 C1 C5 12.9(3) .
O2 Y1 C1 C5 -67.1(3) .
C54 Y1 C1 C5 -169.3(2) .
C57 Y1 C1 C5 102.2(3) .
C55 Y1 C1 C5 163.6(3) .
C56 Y1 C1 C5 132.3(3) .
C2 Y1 C1 C5 -108.6(4) .
C4 Y1 C1 C5 -34.3(3) .
C3 Y1 C1 C5 -73.3(3) .
Y4 Y1 C1 C5 58.0(3) .
O1 Y1 C1 Si1 -116.3(2) .
O2 Y1 C1 Si1 163.61(18) .
C54 Y1 C1 Si1 61.4(3) .
C57 Y1 C1 Si1 -27.0(3) .
C55 Y1 C1 Si1 34.4(3) .
C56 Y1 C1 Si1 3.0(2) .
C5 Y1 C1 Si1 -129.2(4) .
C2 Y1 C1 Si1 122.2(4) .
C4 Y1 C1 Si1 -163.5(3) .
C3 Y1 C1 Si1 157.4(3) .
Y4 Y1 C1 Si1 -71.2(3) .
C5 C1 C2 C3 0.8(4) .
Si1 C1 C2 C3 162.1(3) .
Y1 C1 C2 C3 -68.3(3) .
C5 C1 C2 C6 -169.9(4) .
Si1 C1 C2 C6 -8.6(5) .
Y1 C1 C2 C6 121.1(4) .
C5 C1 C2 Y1 69.1(2) .
Si1 C1 C2 Y1 -129.6(3) .
O1 Y1 C2 C3 29.8(3) .
O2 Y1 C2 C3 -34.4(3) .
C54 Y1 C2 C3 -115.8(3) .
C57 Y1 C2 C3 157.9(2) .
C55 Y1 C2 C3 -149.0(3) .
C56 Y1 C2 C3 -178.6(2) .
C5 Y1 C2 C3 75.9(3) .
C4 Y1 C2 C3 37.0(3) .
C1 Y1 C2 C3 116.2(4) .
Y4 Y1 C2 C3 86.2(3) .
O1 Y1 C2 C1 -86.4(3) .
O2 Y1 C2 C1 -150.6(2) .
C54 Y1 C2 C1 128.0(2) .
C57 Y1 C2 C1 41.7(3) .
C55 Y1 C2 C1 94.8(2) .
C56 Y1 C2 C1 65.2(2) .
C5 Y1 C2 C1 -40.3(3) .
C4 Y1 C2 C1 -79.3(3) .
C3 Y1 C2 C1 -116.2(4) .
Y4 Y1 C2 C1 -30.0(4) .
O1 Y1 C2 C6 152.3(3) .
O2 Y1 C2 C6 88.1(3) .
C54 Y1 C2 C6 6.7(3) .
C57 Y1 C2 C6 -79.6(3) .
C55 Y1 C2 C6 -26.5(3) .
C56 Y1 C2 C6 -56.1(3) .
C5 Y1 C2 C6 -161.6(4) .
C4 Y1 C2 C6 159.5(4) .
C1 Y1 C2 C6 -121.3(4) .
C3 Y1 C2 C6 122.5(4) .
Y4 Y1 C2 C6 -151.3(2) .
C1 C2 C3 C4 0.2(5) .
C6 C2 C3 C4 170.8(4) .
Y1 C2 C3 C4 -67.6(3) .
C1 C2 C3 C7 -174.0(4) .
C6 C2 C3 C7 -3.4(7) .
Y1 C2 C3 C7 118.2(4) .
C1 C2 C3 Y1 67.8(3) .
C6 C2 C3 Y1 -121.6(4) .
O1 Y1 C3 C2 -159.0(2) .
O2 Y1 C3 C2 148.0(2) .
C54 Y1 C3 C2 72.1(3) .
C57 Y1 C3 C2 -47.7(5) .
C55 Y1 C3 C2 35.9(3) .
C56 Y1 C3 C2 1.9(3) .
C5 Y1 C3 C2 -77.4(3) .
C4 Y1 C3 C2 -114.0(4) .
C1 Y1 C3 C2 -36.3(2) .
Y4 Y1 C3 C2 -144.03(19) .
O1 Y1 C3 C4 -45.0(3) .
O2 Y1 C3 C4 -98.0(3) .
C54 Y1 C3 C4 -173.9(3) .
C57 Y1 C3 C4 66.2(5) .
C55 Y1 C3 C4 149.9(3) .
C56 Y1 C3 C4 115.9(3) .
C5 Y1 C3 C4 36.6(3) .
C2 Y1 C3 C4 114.0(4) .
C1 Y1 C3 C4 77.7(3) .
Y4 Y1 C3 C4 -30.0(4) .
O1 Y1 C3 C7 76.4(4) .
O2 Y1 C3 C7 23.5(4) .
C54 Y1 C3 C7 -52.5(4) .
C57 Y1 C3 C7 -172.3(3) .
C55 Y1 C3 C7 -88.6(4) .
C56 Y1 C3 C7 -122.6(3) .
C5 Y1 C3 C7 158.1(4) .
C2 Y1 C3 C7 -124.6(5) .
C4 Y1 C3 C7 121.5(5) .
C1 Y1 C3 C7 -160.8(4) .
Y4 Y1 C3 C7 91.4(4) .
C2 C3 C4 C5 -1.2(5) .
C7 C3 C4 C5 173.2(4) .
Y1 C3 C4 C5 -68.7(3) .
C2 C3 C4 C8 -173.9(4) .
C7 C3 C4 C8 0.6(7) .
Y1 C3 C4 C8 118.7(4) .
C2 C3 C4 Y1 67.5(3) .
C7 C3 C4 Y1 -118.1(4) .
O1 Y1 C4 C5 -108.1(3) .
O2 Y1 C4 C5 -165.7(3) .
C54 Y1 C4 C5 122.4(3) .
C57 Y1 C4 C5 -36.8(4) .
C55 Y1 C4 C5 66.8(4) .
C56 Y1 C4 C5 15.0(4) .
C2 Y1 C4 C5 76.7(3) .
C1 Y1 C4 C5 36.5(3) .
C3 Y1 C4 C5 113.4(4) .
Y4 Y1 C4 C5 -86.1(3) .
O1 Y1 C4 C3 138.5(3) .
O2 Y1 C4 C3 80.9(3) .
C54 Y1 C4 C3 9.0(4) .
C57 Y1 C4 C3 -150.2(3) .
C55 Y1 C4 C3 -46.6(4) .
C56 Y1 C4 C3 -98.5(3) .
C5 Y1 C4 C3 -113.4(4) .
C2 Y1 C4 C3 -36.7(3) .
C1 Y1 C4 C3 -76.9(3) .
Y4 Y1 C4 C3 160.5(2) .
O1 Y1 C4 C8 16.8(4) .
O2 Y1 C4 C8 -40.8(4) .
C54 Y1 C4 C8 -112.6(4) .
C57 Y1 C4 C8 88.1(5) .
C55 Y1 C4 C8 -168.3(4) .
C56 Y1 C4 C8 139.9(4) .
C5 Y1 C4 C8 124.9(6) .
C2 Y1 C4 C8 -158.4(5) .
C1 Y1 C4 C8 161.4(5) .
C3 Y1 C4 C8 -121.7(6) .
Y4 Y1 C4 C8 38.9(5) .
C3 C4 C5 C1 1.8(5) .
C8 C4 C5 C1 174.1(4) .
Y1 C4 C5 C1 -67.2(3) .
C3 C4 C5 C9 -168.6(4) .
C8 C4 C5 C9 3.8(7) .
Y1 C4 C5 C9 122.4(4) .
C3 C4 C5 Y1 69.0(3) .
C8 C4 C5 Y1 -118.6(5) .
C2 C1 C5 C4 -1.6(4) .
Si1 C1 C5 C4 -161.5(3) .
Y1 C1 C5 C4 67.7(3) .
C2 C1 C5 C9 168.7(4) .
Si1 C1 C5 C9 8.8(6) .
Y1 C1 C5 C9 -122.0(4) .
C2 C1 C5 Y1 -69.3(2) .
Si1 C1 C5 Y1 130.8(3) .
O1 Y1 C5 C4 73.3(3) .
O2 Y1 C5 C4 16.3(3) .
C54 Y1 C5 C4 -99.2(4) .
C57 Y1 C5 C4 153.8(3) .
C55 Y1 C5 C4 -137.1(3) .
C56 Y1 C5 C4 -169.8(3) .
C2 Y1 C5 C4 -77.4(3) .
C1 Y1 C5 C4 -117.0(4) .
C3 Y1 C5 C4 -37.5(3) .
Y4 Y1 C5 C4 106.5(3) .
O1 Y1 C5 C1 -169.7(2) .
O2 Y1 C5 C1 133.3(2) .
C54 Y1 C5 C1 17.8(4) .
C57 Y1 C5 C1 -89.2(3) .
C55 Y1 C5 C1 -20.1(3) .
C56 Y1 C5 C1 -52.9(3) .
C2 Y1 C5 C1 39.6(2) .
C4 Y1 C5 C1 117.0(4) .
C3 Y1 C5 C1 79.4(3) .
Y4 Y1 C5 C1 -136.5(2) .
O1 Y1 C5 C9 -48.1(5) .
O2 Y1 C5 C9 -105.0(5) .
C54 Y1 C5 C9 139.4(4) .
C57 Y1 C5 C9 32.5(5) .
C55 Y1 C5 C9 101.5(5) .
C56 Y1 C5 C9 68.8(5) .
C2 Y1 C5 C9 161.3(6) .
C4 Y1 C5 C9 -121.4(6) .
C1 Y1 C5 C9 121.7(6) .
C3 Y1 C5 C9 -158.9(6) .
Y4 Y1 C5 C9 -14.9(5) .
C23 Si2 C13 C17 73.9(4) .
C24 Si2 C13 C17 -165.3(3) .
C22 Si2 C13 C17 -43.5(4) .
C23 Si2 C13 C14 -88.8(4) .
C24 Si2 C13 C14 32.0(4) .
C22 Si2 C13 C14 153.7(4) .
C23 Si2 C13 Y2 172.7(3) .
C24 Si2 C13 Y2 -66.5(3) .
C22 Si2 C13 Y2 55.3(3) .
O3 Y2 C13 C17 162.5(2) .
O4 Y2 C13 C17 104.7(2) .
C54 Y2 C13 C17 -119.6(3) .
C57 Y2 C13 C17 28.4(3) .
C55 Y2 C13 C17 -67.4(3) .
C56 Y2 C13 C17 -20.5(3) .
C14 Y2 C13 C17 -110.9(3) .
C15 Y2 C13 C17 -75.0(3) .
C16 Y2 C13 C17 -35.7(2) .
Y4 Y2 C13 C17 80.7(2) .
O3 Y2 C13 C14 -86.6(2) .
O4 Y2 C13 C14 -144.4(2) .
C54 Y2 C13 C14 -8.7(3) .
C57 Y2 C13 C14 139.4(2) .
C55 Y2 C13 C14 43.5(3) .
C56 Y2 C13 C14 90.4(3) .
C15 Y2 C13 C14 36.0(2) .
C16 Y2 C13 C14 75.3(2) .
C17 Y2 C13 C14 110.9(3) .
Y4 Y2 C13 C14 -168.35(19) .
O3 Y2 C13 Si2 38.1(2) .
O4 Y2 C13 Si2 -19.7(2) .
C54 Y2 C13 Si2 116.1(2) .
C57 Y2 C13 Si2 -95.9(3) .
C55 Y2 C13 Si2 168.21(19) .
C56 Y2 C13 Si2 -144.9(2) .
C14 Y2 C13 Si2 124.7(4) .
C15 Y2 C13 Si2 160.7(3) .
C16 Y2 C13 Si2 -160.0(3) .
C17 Y2 C13 Si2 -124.4(4) .
Y4 Y2 C13 Si2 -43.6(3) .
C17 C13 C14 C15 0.8(4) .
Si2 C13 C14 C15 166.5(3) .
Y2 C13 C14 C15 -68.0(3) .
C17 C13 C14 C18 -173.3(4) .
Si2 C13 C14 C18 -7.6(6) .
Y2 C13 C14 C18 118.0(4) .
C17 C13 C14 Y2 68.7(2) .
Si2 C13 C14 Y2 -125.6(3) .
O3 Y2 C14 C15 -149.7(2) .
O4 Y2 C14 C15 155.6(2) .
C54 Y2 C14 C15 -70.6(3) .
C57 Y2 C14 C15 37.7(4) .
C55 Y2 C14 C15 -34.7(3) .
C56 Y2 C14 C15 -2.1(3) .
C16 Y2 C14 C15 37.0(2) .
C17 Y2 C14 C15 76.8(3) .
C13 Y2 C14 C15 115.3(3) .
Y4 Y2 C14 C15 134.7(2) .
O3 Y2 C14 C13 95.0(2) .
O4 Y2 C14 C13 40.3(2) .
C54 Y2 C14 C13 174.1(2) .
C57 Y2 C14 C13 -77.6(3) .
C55 Y2 C14 C13 -150.0(2) .
C56 Y2 C14 C13 -117.4(2) .
C15 Y2 C14 C13 -115.3(3) .
C16 Y2 C14 C13 -78.3(2) .
C17 Y2 C14 C13 -38.4(2) .
Y4 Y2 C14 C13 19.4(3) .
O3 Y2 C14 C18 -26.9(3) .
O4 Y2 C14 C18 -81.6(3) .
C54 Y2 C14 C18 52.2(3) .
C57 Y2 C14 C18 160.5(3) .
C55 Y2 C14 C18 88.1(3) .
C56 Y2 C14 C18 120.7(3) .
C15 Y2 C14 C18 122.8(4) .
C16 Y2 C14 C18 159.8(4) .
C17 Y2 C14 C18 -160.3(4) .
C13 Y2 C14 C18 -121.9(4) .
Y4 Y2 C14 C18 -102.5(3) .
C13 C14 C15 C16 -0.1(4) .
C18 C14 C15 C16 173.9(4) .
Y2 C14 C15 C16 -68.4(3) .
C13 C14 C15 C19 -171.0(4) .
C18 C14 C15 C19 3.0(6) .
Y2 C14 C15 C19 120.7(4) .
C13 C14 C15 Y2 68.3(3) .
C18 C14 C15 Y2 -117.7(4) .
O3 Y2 C15 C14 34.6(3) .
O4 Y2 C15 C14 -37.2(3) .
C54 Y2 C15 C14 116.3(2) .
C57 Y2 C15 C14 -159.4(2) .
C55 Y2 C15 C14 148.5(2) .
C56 Y2 C15 C14 178.3(2) .
C16 Y2 C15 C14 -113.8(4) .
C17 Y2 C15 C14 -76.5(3) .
C13 Y2 C15 C14 -36.5(2) .
Y4 Y2 C15 C14 -104.1(3) .
O3 Y2 C15 C16 148.3(2) .
O4 Y2 C15 C16 76.6(3) .
C54 Y2 C15 C16 -130.0(2) .
C57 Y2 C15 C16 -45.6(3) .
C55 Y2 C15 C16 -97.8(2) .
C56 Y2 C15 C16 -67.9(2) .
C14 Y2 C15 C16 113.8(4) .
C17 Y2 C15 C16 37.3(2) .
C13 Y2 C15 C16 77.2(3) .
Y4 Y2 C15 C16 9.7(4) .
O3 Y2 C15 C19 -89.3(3) .
O4 Y2 C15 C19 -161.0(3) .
C54 Y2 C15 C19 -7.6(4) .
C57 Y2 C15 C19 76.8(4) .
C55 Y2 C15 C19 24.6(3) .
C56 Y2 C15 C19 54.5(4) .
C14 Y2 C15 C19 -123.9(5) .
C16 Y2 C15 C19 122.4(5) .
C17 Y2 C15 C19 159.6(4) .
C13 Y2 C15 C19 -160.4(4) .
Y4 Y2 C15 C19 132.0(3) .
C14 C15 C16 C17 -0.6(4) .
C19 C15 C16 C17 170.4(4) .
Y2 C15 C16 C17 -69.0(3) .
C14 C15 C16 C20 -173.1(4) .
C19 C15 C16 C20 -2.1(6) .
Y2 C15 C16 C20 118.5(4) .
C14 C15 C16 Y2 68.3(3) .
C19 C15 C16 Y2 -120.6(4) .
O3 Y2 C16 C15 -47.7(3) .
O4 Y2 C16 C15 -130.9(2) .
C54 Y2 C16 C15 57.5(3) .
C57 Y2 C16 C15 143.4(2) .
C55 Y2 C16 C15 82.3(2) .
C56 Y2 C16 C15 113.3(2) .
C14 Y2 C16 C15 -37.0(2) .
C17 Y2 C16 C15 -113.2(3) .
C13 Y2 C16 C15 -77.1(2) .
Y4 Y2 C16 C15 -175.27(19) .
O3 Y2 C16 C17 65.5(3) .
O4 Y2 C16 C17 -17.8(3) .
C54 Y2 C16 C17 170.7(2) .
C57 Y2 C16 C17 -103.5(2) .
C55 Y2 C16 C17 -164.6(2) .
C56 Y2 C16 C17 -133.5(2) .
C14 Y2 C16 C17 76.2(2) .
C15 Y2 C16 C17 113.2(3) .
C13 Y2 C16 C17 36.0(2) .
Y4 Y2 C16 C17 -62.1(3) .
O3 Y2 C16 C20 -167.5(3) .
O4 Y2 C16 C20 109.3(4) .
C54 Y2 C16 C20 -62.3(4) .
C57 Y2 C16 C20 23.6(4) .
C55 Y2 C16 C20 -37.5(4) .
C56 Y2 C16 C20 -6.5(4) .
C14 Y2 C16 C20 -156.8(5) .
C15 Y2 C16 C20 -119.8(5) .
C17 Y2 C16 C20 127.0(5) .
C13 Y2 C16 C20 163.1(5) .
Y4 Y2 C16 C20 64.9(4) .
C15 C16 C17 C13 1.2(5) .
C20 C16 C17 C13 173.1(4) .
Y2 C16 C17 C13 -67.5(3) .
C15 C16 C17 C21 -171.4(4) .
C20 C16 C17 C21 0.5(7) .
Y2 C16 C17 C21 120.0(4) .
C15 C16 C17 Y2 68.7(3) .
C20 C16 C17 Y2 -119.4(4) .
C14 C13 C17 C16 -1.2(4) .
Si2 C13 C17 C16 -167.0(3) .
Y2 C13 C17 C16 67.1(3) .
C14 C13 C17 C21 171.3(4) .
Si2 C13 C17 C21 5.5(6) .
Y2 C13 C17 C21 -120.4(4) .
C14 C13 C17 Y2 -68.3(2) .
Si2 C13 C17 Y2 125.9(3) .
O3 Y2 C17 C16 -137.0(2) .
O4 Y2 C17 C16 165.9(2) .
C54 Y2 C17 C16 -14.8(4) .
C57 Y2 C17 C16 84.6(3) .
C55 Y2 C17 C16 18.0(3) .
C56 Y2 C17 C16 49.2(3) .
C14 Y2 C17 C16 -77.3(3) .
C15 Y2 C17 C16 -37.3(2) .
C13 Y2 C17 C16 -116.0(4) .
Y4 Y2 C17 C16 131.5(2) .
O3 Y2 C17 C13 -21.0(3) .
O4 Y2 C17 C13 -78.1(2) .
C54 Y2 C17 C13 101.2(3) .
C57 Y2 C17 C13 -159.4(2) .
C55 Y2 C17 C13 134.0(2) .
C56 Y2 C17 C13 165.2(2) .
C14 Y2 C17 C13 38.7(2) .
C15 Y2 C17 C13 78.7(2) .
C16 Y2 C17 C13 116.0(4) .
Y4 Y2 C17 C13 -112.5(2) .
O3 Y2 C17 C21 101.5(4) .
O4 Y2 C17 C21 44.4(4) .
C54 Y2 C17 C21 -136.3(4) .
C57 Y2 C17 C21 -36.9(4) .
C55 Y2 C17 C21 -103.5(4) .
C56 Y2 C17 C21 -72.3(4) .
C14 Y2 C17 C21 161.2(5) .
C15 Y2 C17 C21 -158.8(4) .
C16 Y2 C17 C21 -121.5(5) .
C13 Y2 C17 C21 122.5(5) .
Y4 Y2 C17 C21 10.0(4) .
C34 Si3 C25 C26 169.7(4) .
C36 Si3 C25 C26 48.3(4) .
C35 Si3 C25 C26 -71.0(4) .
C34 Si3 C25 C29 -38.0(4) .
C36 Si3 C25 C29 -159.4(4) .
C35 Si3 C25 C29 81.4(4) .
C34 Si3 C25 Y3 65.1(3) .
C36 Si3 C25 Y3 -56.2(3) .
C35 Si3 C25 Y3 -175.5(3) .
O2 Y3 C25 C26 -166.4(2) .
O3 Y3 C25 C26 85.5(3) .
C54 Y3 C25 C26 -87.9(3) .
C29 Y3 C25 C26 110.5(3) .
C28 Y3 C25 C26 74.3(3) .
C27 Y3 C25 C26 34.8(2) .
Si5 Y3 C25 C26 -58.9(2) .
Y2 Y3 C25 C26 89.2(5) .
Y1 Y3 C25 C26 -146.4(2) .
O2 Y3 C25 C29 83.1(2) .
O3 Y3 C25 C29 -25.1(3) .
C54 Y3 C25 C29 161.5(2) .
C28 Y3 C25 C29 -36.3(2) .
C27 Y3 C25 C29 -75.8(3) .
C26 Y3 C25 C29 -110.5(3) .
Si5 Y3 C25 C29 -169.4(2) .
Y2 Y3 C25 C29 -21.4(6) .
Y1 Y3 C25 C29 103.0(2) .
O2 Y3 C25 Si3 -41.4(3) .
O3 Y3 C25 Si3 -149.6(2) .
C54 Y3 C25 Si3 37.0(4) .
C29 Y3 C25 Si3 -124.5(4) .
C28 Y3 C25 Si3 -160.8(3) .
C27 Y3 C25 Si3 159.7(3) .
C26 Y3 C25 Si3 125.0(4) .
Si5 Y3 C25 Si3 66.1(3) .
Y2 Y3 C25 Si3 -145.9(2) .
Y1 Y3 C25 Si3 -21.5(3) .
C29 C25 C26 C27 3.1(4) .
Si3 C25 C26 C27 159.9(3) .
Y3 C25 C26 C27 -66.6(3) .
C29 C25 C26 C30 -170.2(4) .
Si3 C25 C26 C30 -13.4(6) .
Y3 C25 C26 C30 120.1(4) .
C29 C25 C26 Y3 69.7(3) .
Si3 C25 C26 Y3 -133.5(3) .
O2 Y3 C26 C27 133.0(2) .
O3 Y3 C26 C27 0.5(3) .
C54 Y3 C26 C27 -112.5(3) .
C25 Y3 C26 C27 116.8(4) .
C29 Y3 C26 C27 77.8(3) .
C28 Y3 C26 C27 38.2(3) .
Si5 Y3 C26 C27 -113.5(2) .
Y2 Y3 C26 C27 -40.3(3) .
Y1 Y3 C26 C27 174.9(2) .
O2 Y3 C26 C25 16.1(3) .
O3 Y3 C26 C25 -116.4(2) .
C54 Y3 C26 C25 130.6(2) .
C29 Y3 C26 C25 -39.1(2) .
C28 Y3 C26 C25 -78.7(3) .
C27 Y3 C26 C25 -116.8(4) .
Si5 Y3 C26 C25 129.6(2) .
Y2 Y3 C26 C25 -157.13(18) .
Y1 Y3 C26 C25 58.1(3) .
O2 Y3 C26 C30 -106.0(3) .
O3 Y3 C26 C30 121.4(3) .
C54 Y3 C26 C30 8.5(4) .
C25 Y3 C26 C30 -122.2(4) .
C29 Y3 C26 C30 -161.3(4) .
C28 Y3 C26 C30 159.2(4) .
C27 Y3 C26 C30 121.0(5) .
Si5 Y3 C26 C30 7.5(3) .
Y2 Y3 C26 C30 80.7(4) .
Y1 Y3 C26 C30 -64.1(4) .
C25 C26 C27 C28 -3.4(5) .
C30 C26 C27 C28 170.1(4) .
Y3 C26 C27 C28 -68.8(3) .
C25 C26 C27 C31 -173.0(4) .
C30 C26 C27 C31 0.4(7) .
Y3 C26 C27 C31 121.5(5) .
C25 C26 C27 Y3 65.4(3) .
C30 C26 C27 Y3 -121.1(4) .
O2 Y3 C27 C26 -69.0(3) .
O3 Y3 C27 C26 -179.6(3) .
C54 Y3 C27 C26 101.2(3) .
C25 Y3 C27 C26 -36.1(2) .
C29 Y3 C27 C26 -76.6(3) .
C28 Y3 C27 C26 -112.2(4) .
Si5 Y3 C27 C26 73.8(3) .
Y2 Y3 C27 C26 155.6(2) .
Y1 Y3 C27 C26 -52.7(18) .
O2 Y3 C27 C28 43.1(3) .
O3 Y3 C27 C28 -67.5(3) .
C54 Y3 C27 C28 -146.7(2) .
C25 Y3 C27 C28 76.1(3) .
C29 Y3 C27 C28 35.5(2) .
C26 Y3 C27 C28 112.2(4) .
Si5 Y3 C27 C28 -174.0(2) .
Y2 Y3 C27 C28 -92.3(3) .
Y1 Y3 C27 C28 59.5(17) .
O2 Y3 C27 C31 164.7(3) .
O3 Y3 C27 C31 54.1(4) .
C54 Y3 C27 C31 -25.1(5) .
C25 Y3 C27 C31 -162.4(4) .
C29 Y3 C27 C31 157.1(4) .
C28 Y3 C27 C31 121.6(5) .
C26 Y3 C27 C31 -126.3(5) .
Si5 Y3 C27 C31 -52.5(4) .
Y2 Y3 C27 C31 29.3(4) .
Y1 Y3 C27 C31 -179(100) .
C26 C27 C28 C29 2.4(5) .
C31 C27 C28 C29 172.5(4) .
Y3 C27 C28 C29 -66.8(3) .
C26 C27 C28 C32 -172.1(4) .
C31 C27 C28 C32 -2.0(7) .
Y3 C27 C28 C32 118.7(4) .
C26 C27 C28 Y3 69.2(3) .
C31 C27 C28 Y3 -120.7(4) .
O2 Y3 C28 C29 -34.3(3) .
O3 Y3 C28 C29 -133.5(3) .
C54 Y3 C28 C29 -168.0(3) .
C25 Y3 C28 C29 37.8(2) .
C27 Y3 C28 C29 116.0(4) .
C26 Y3 C28 C29 78.6(3) .
Si5 Y3 C28 C29 124.7(2) .
Y2 Y3 C28 C29 -138.6(2) .
Y1 Y3 C28 C29 -58.5(3) .
O2 Y3 C28 C27 -150.3(2) .
O3 Y3 C28 C27 110.5(3) .
C54 Y3 C28 C27 76.0(4) .
C25 Y3 C28 C27 -78.2(3) .
C29 Y3 C28 C27 -116.0(4) .
C26 Y3 C28 C27 -37.4(2) .
Si5 Y3 C28 C27 8.7(3) .
Y2 Y3 C28 C27 105.3(2) .
Y1 Y3 C28 C27 -174.51(18) .
O2 Y3 C28 C32 88.5(4) .
O3 Y3 C28 C32 -10.7(3) .
C54 Y3 C28 C32 -45.2(6) .
C25 Y3 C28 C32 160.6(4) .
C29 Y3 C28 C32 122.8(5) .
C27 Y3 C28 C32 -121.2(5) .
C26 Y3 C28 C32 -158.7(4) .
Si5 Y3 C28 C32 -112.5(3) .
Y2 Y3 C28 C32 -15.9(4) .
Y1 Y3 C28 C32 64.3(4) .
C27 C28 C29 C25 -0.5(5) .
C32 C28 C29 C25 173.9(4) .
Y3 C28 C29 C25 -67.7(3) .
C27 C28 C29 C33 -173.5(4) .
C32 C28 C29 C33 0.9(7) .
Y3 C28 C29 C33 119.2(4) .
C27 C28 C29 Y3 67.3(3) .
C32 C28 C29 Y3 -118.3(4) .
C26 C25 C29 C28 -1.6(4) .
Si3 C25 C29 C28 -158.2(3) .
Y3 C25 C29 C28 68.9(3) .
C26 C25 C29 C33 171.3(4) .
Si3 C25 C29 C33 14.6(6) .
Y3 C25 C29 C33 -118.2(4) .
C26 C25 C29 Y3 -70.5(3) .
Si3 C25 C29 Y3 132.8(3) .
O2 Y3 C29 C28 148.9(3) .
O3 Y3 C29 C28 46.8(3) .
C54 Y3 C29 C28 152.7(7) .
C25 Y3 C29 C28 -113.9(4) .
C27 Y3 C29 C28 -36.1(2) .
C26 Y3 C29 C28 -75.1(3) .
Si5 Y3 C29 C28 -96.2(3) .
Y2 Y3 C29 C28 59.6(3) .
Y1 Y3 C29 C28 145.6(2) .
O2 Y3 C29 C25 -97.2(2) .
O3 Y3 C29 C25 160.7(2) .
C54 Y3 C29 C25 -93.5(8) .
C28 Y3 C29 C25 113.9(4) .
C27 Y3 C29 C25 77.8(3) .
C26 Y3 C29 C25 38.8(2) .
Si5 Y3 C29 C25 17.6(3) .
Y2 Y3 C29 C25 173.45(17) .
Y1 Y3 C29 C25 -100.5(2) .
O2 Y3 C29 C33 26.9(4) .
O3 Y3 C29 C33 -75.3(4) .
C54 Y3 C29 C33 30.6(10) .
C25 Y3 C29 C33 124.0(5) .
C28 Y3 C29 C33 -122.1(5) .
C27 Y3 C29 C33 -158.2(4) .
C26 Y3 C29 C33 162.8(4) .
Si5 Y3 C29 C33 141.7(3) .
Y2 Y3 C29 C33 -62.5(4) .
Y1 Y3 C29 C33 23.5(4) .
C47 Si4 C37 C41 -40.5(5) .
C48 Si4 C37 C41 -161.7(4) .
C46 Si4 C37 C41 78.8(4) .
C47 Si4 C37 C38 158.8(5) .
C48 Si4 C37 C38 37.7(5) .
C46 Si4 C37 C38 -81.9(4) .
C47 Si4 C37 Y4 60.1(4) .
C48 Si4 C37 Y4 -61.1(4) .
C46 Si4 C37 Y4 179.4(3) .
O4 Y4 C37 C41 -90.5(2) .
O1 Y4 C37 C41 163.5(2) .
C57 Y4 C37 C41 88.4(3) .
C38 Y4 C37 C41 -110.6(3) .
C39 Y4 C37 C41 -74.6(2) .
C40 Y4 C37 C41 -35.8(2) .
Y2 Y4 C37 C41 -104.5(4) .
Y1 Y4 C37 C41 144.42(19) .
O4 Y4 C37 C38 20.1(3) .
O1 Y4 C37 C38 -85.9(2) .
C57 Y4 C37 C38 -161.0(2) .
C41 Y4 C37 C38 110.6(3) .
C39 Y4 C37 C38 35.9(2) .
C40 Y4 C37 C38 74.8(2) .
Y2 Y4 C37 C38 6.1(6) .
Y1 Y4 C37 C38 -105.0(2) .
O4 Y4 C37 Si4 144.21(19) .
O1 Y4 C37 Si4 38.2(2) .
C57 Y4 C37 Si4 -36.9(4) .
C38 Y4 C37 Si4 124.1(4) .
C41 Y4 C37 Si4 -125.3(4) .
C39 Y4 C37 Si4 160.0(3) .
C40 Y4 C37 Si4 -161.1(3) .
Y2 Y4 C37 Si4 130.2(3) .
Y1 Y4 C37 Si4 19.1(3) .
C41 C37 C38 C39 0.5(4) .
Si4 C37 C38 C39 164.4(3) .
Y4 C37 C38 C39 -69.6(3) .
C41 C37 C38 C42 -171.1(4) .
Si4 C37 C38 C42 -7.1(6) .
Y4 C37 C38 C42 118.8(4) .
C41 C37 C38 Y4 70.1(3) .
Si4 C37 C38 Y4 -125.9(3) .
O4 Y4 C38 C39 -50.2(2) .
O1 Y4 C38 C39 -152.1(2) .
C57 Y4 C38 C39 -151.7(6) .
C37 Y4 C38 C39 114.3(3) .
C41 Y4 C38 C39 75.9(2) .
C40 Y4 C38 C39 36.0(2) .
Y2 Y4 C38 C39 -63.9(3) .
Y1 Y4 C38 C39 -148.40(19) .
O4 Y4 C38 C37 -164.4(2) .
O1 Y4 C38 C37 93.6(2) .
C57 Y4 C38 C37 94.0(7) .
C41 Y4 C38 C37 -38.4(2) .
C39 Y4 C38 C37 -114.3(3) .
C40 Y4 C38 C37 -78.3(2) .
Y2 Y4 C38 C37 -178.11(17) .
Y1 Y4 C38 C37 97.3(2) .
O4 Y4 C38 C42 72.6(3) .
O1 Y4 C38 C42 -29.3(3) .
C57 Y4 C38 C42 -28.9(8) .
C37 Y4 C38 C42 -123.0(4) .
C41 Y4 C38 C42 -161.3(4) .
C39 Y4 C38 C42 122.8(4) .
C40 Y4 C38 C42 158.8(4) .
Y2 Y4 C38 C42 58.9(3) .
Y1 Y4 C38 C42 -25.6(3) .
C37 C38 C39 C40 0.2(4) .
C42 C38 C39 C40 171.9(4) .
Y4 C38 C39 C40 -67.6(3) .
C37 C38 C39 C43 -172.0(3) .
C42 C38 C39 C43 -0.3(6) .
Y4 C38 C39 C43 120.2(4) .
C37 C38 C39 Y4 67.8(3) .
C42 C38 C39 Y4 -120.6(4) .
O4 Y4 C39 C38 129.9(2) .
O1 Y4 C39 C38 30.8(2) .
C57 Y4 C39 C38 167.1(3) .
C37 Y4 C39 C38 -37.8(2) .
C41 Y4 C39 C38 -78.0(2) .
C40 Y4 C39 C38 -115.6(3) .
Y2 Y4 C39 C38 135.1(2) .
Y1 Y4 C39 C38 54.0(3) .
O4 Y4 C39 C40 -114.5(2) .
O1 Y4 C39 C40 146.4(2) .
C57 Y4 C39 C40 -77.3(4) .
C37 Y4 C39 C40 77.7(2) .
C38 Y4 C39 C40 115.6(3) .
C41 Y4 C39 C40 37.6(2) .
Y2 Y4 C39 C40 -109.3(2) .
Y1 Y4 C39 C40 169.61(17) .
O4 Y4 C39 C43 7.7(3) .
O1 Y4 C39 C43 -91.4(3) .
C57 Y4 C39 C43 44.9(5) .
C37 Y4 C39 C43 -160.1(4) .
C38 Y4 C39 C43 -122.2(4) .
C41 Y4 C39 C43 159.8(4) .
C40 Y4 C39 C43 122.2(4) .
Y2 Y4 C39 C43 12.9(4) .
Y1 Y4 C39 C43 -68.2(4) .
C38 C39 C40 C41 -0.8(4) .
C43 C39 C40 C41 171.5(4) .
Y4 C39 C40 C41 -67.0(3) .
C38 C39 C40 C44 -172.6(4) .
C43 C39 C40 C44 -0.3(6) .
Y4 C39 C40 C44 121.2(4) .
C38 C39 C40 Y4 66.2(3) .
C43 C39 C40 Y4 -121.5(4) .
O4 Y4 C40 C39 64.0(2) .
O1 Y4 C40 C39 -48.0(3) .
C57 Y4 C40 C39 146.1(2) .
C37 Y4 C40 C39 -77.0(2) .
C38 Y4 C40 C39 -36.0(2) .
C41 Y4 C40 C39 -113.1(3) .
Y2 Y4 C40 C39 88.9(2) .
Y1 Y4 C40 C39 -75.5(10) .
O4 Y4 C40 C41 177.2(2) .
O1 Y4 C40 C41 65.2(3) .
C57 Y4 C40 C41 -100.8(3) .
C37 Y4 C40 C41 36.1(2) .
C38 Y4 C40 C41 77.2(3) .
C39 Y4 C40 C41 113.1(3) .
Y2 Y4 C40 C41 -157.9(2) .
Y1 Y4 C40 C41 37.7(10) .
O4 Y4 C40 C44 -58.3(3) .
O1 Y4 C40 C44 -170.3(3) .
C57 Y4 C40 C44 23.7(4) .
C37 Y4 C40 C44 160.6(4) .
C38 Y4 C40 C44 -158.3(4) .
C41 Y4 C40 C44 124.5(5) .
C39 Y4 C40 C44 -122.4(4) .
Y2 Y4 C40 C44 -33.4(4) .
Y1 Y4 C40 C44 162.2(7) .
C38 C37 C41 C40 -1.0(4) .
Si4 C37 C41 C40 -164.9(3) .
Y4 C37 C41 C40 68.4(3) .
C38 C37 C41 C45 173.1(4) .
Si4 C37 C41 C45 9.1(6) .
Y4 C37 C41 C45 -117.6(4) .
C38 C37 C41 Y4 -69.4(2) .
Si4 C37 C41 Y4 126.7(3) .
C39 C40 C41 C37 1.1(4) .
C44 C40 C41 C37 172.6(4) .
Y4 C40 C41 C37 -66.8(3) .
C39 C40 C41 C45 -173.1(3) .
C44 C40 C41 C45 -1.6(7) .
Y4 C40 C41 C45 119.0(4) .
C39 C40 C41 Y4 67.9(3) .
C44 C40 C41 Y4 -120.6(4) .
O4 Y4 C41 C37 112.6(2) .
O1 Y4 C41 C37 -19.0(2) .
C57 Y4 C41 C37 -129.9(2) .
C38 Y4 C41 C37 39.5(2) .
C39 Y4 C41 C37 78.9(2) .
C40 Y4 C41 C37 116.0(3) .
Y2 Y4 C41 C37 155.02(17) .
Y1 Y4 C41 C37 -58.0(3) .
O4 Y4 C41 C40 -3.4(3) .
O1 Y4 C41 C40 -135.0(2) .
C57 Y4 C41 C40 114.1(2) .
C37 Y4 C41 C40 -116.0(3) .
C38 Y4 C41 C40 -76.5(3) .
C39 Y4 C41 C40 -37.1(2) .
Y2 Y4 C41 C40 39.0(3) .
Y1 Y4 C41 C40 -173.99(18) .
O4 Y4 C41 C45 -124.2(3) .
O1 Y4 C41 C45 104.2(3) .
C57 Y4 C41 C45 -6.7(4) .
C37 Y4 C41 C45 123.2(4) .
C38 Y4 C41 C45 162.7(4) .
C39 Y4 C41 C45 -157.9(4) .
C40 Y4 C41 C45 -120.8(4) .
Y2 Y4 C41 C45 -81.8(4) .
Y1 Y4 C41 C45 65.2(4) .
Y3 O2 C49 O1 -102.1(3) .
Y1 O2 C49 O1 16.3(3) .
Y4 O1 C49 O2 102.9(3) .
Y1 O1 C49 O2 -16.5(3) .
Y3 O3 C50 O4 102.9(3) .
Y2 O3 C50 O4 -16.6(3) .
Y4 O4 C50 O3 -101.8(3) .
Y2 O4 C50 O3 16.5(3) .
C53 Si5 C54 C55 1.3(3) .
C51 Si5 C54 C55 124.6(3) .
C52 Si5 C54 C55 -122.4(3) .
Y3 Si5 C54 C55 -179.9(3) .
C53 Si5 C54 Y2 91.8(3) .
C51 Si5 C54 Y2 -144.9(2) .
C52 Si5 C54 Y2 -31.9(3) .
Y3 Si5 C54 Y2 -89.4(2) .
C53 Si5 C54 Y1 -88.7(3) .
C51 Si5 C54 Y1 34.6(3) .
C52 Si5 C54 Y1 147.7(2) .
Y3 Si5 C54 Y1 90.1(2) .
C53 Si5 C54 Y3 -178.84(18) .
C51 Si5 C54 Y3 -55.51(17) .
C52 Si5 C54 Y3 57.52(18) .
O3 Y2 C54 C55 -169.17(19) .
O4 Y2 C54 C55 -123.46(18) .
C57 Y2 C54 C55 -50.36(19) .
C56 Y2 C54 C55 -21.10(18) .
C14 Y2 C54 C55 102.78(19) .
C15 Y2 C54 C55 74.3(2) .
C16 Y2 C54 C55 49.1(2) .
C17 Y2 C54 C55 57.3(3) .
C13 Y2 C54 C55 107.4(2) .
Y4 Y2 C54 C55 -90.68(17) .
O3 Y2 C54 Si5 83.6(2) .
O4 Y2 C54 Si5 129.3(2) .
C57 Y2 C54 Si5 -157.5(2) .
C55 Y2 C54 Si5 -107.2(3) .
C56 Y2 C54 Si5 -128.3(3) .
C14 Y2 C54 Si5 -4.4(3) .
C15 Y2 C54 Si5 -32.9(2) .
C16 Y2 C54 Si5 -58.1(3) .
C17 Y2 C54 Si5 -49.9(3) .
C13 Y2 C54 Si5 0.2(3) .
Y4 Y2 C54 Si5 162.1(2) .
O3 Y2 C54 Y1 -96.02(10) .
O4 Y2 C54 Y1 -50.31(13) .
C57 Y2 C54 Y1 22.79(11) .
C55 Y2 C54 Y1 73.15(18) .
C56 Y2 C54 Y1 52.05(11) .
C14 Y2 C54 Y1 175.93(10) .
C15 Y2 C54 Y1 147.49(12) .
C16 Y2 C54 Y1 122.27(12) .
C17 Y2 C54 Y1 130.42(17) .
C13 Y2 C54 Y1 -179.42(12) .
Y4 Y2 C54 Y1 -17.54(10) .
O3 Y2 C54 Y3 -3.94(8) .
O4 Y2 C54 Y3 41.78(12) .
C57 Y2 C54 Y3 114.88(11) .
C55 Y2 C54 Y3 165.2(2) .
C56 Y2 C54 Y3 144.14(14) .
C14 Y2 C54 Y3 -91.99(12) .
C15 Y2 C54 Y3 -120.43(11) .
C16 Y2 C54 Y3 -145.64(11) .
C17 Y2 C54 Y3 -137.49(17) .
C13 Y2 C54 Y3 -87.34(17) .
Y4 Y2 C54 Y3 74.55(8) .
O1 Y1 C54 C55 122.98(18) .
O2 Y1 C54 C55 168.8(2) .
C57 Y1 C54 C55 50.37(19) .
C56 Y1 C54 C55 20.92(18) .
C5 Y1 C54 C55 -65.2(3) .
C2 Y1 C54 C55 -81.9(2) .
C4 Y1 C54 C55 -115.4(2) .
C1 Y1 C54 C55 -55.0(2) .
C3 Y1 C54 C55 -110.5(2) .
Y4 Y1 C54 C55 90.45(18) .
O1 Y1 C54 Si5 -129.7(2) .
O2 Y1 C54 Si5 -84.0(2) .
C57 Y1 C54 Si5 157.7(2) .
C55 Y1 C54 Si5 107.3(3) .
C56 Y1 C54 Si5 128.2(3) .
C5 Y1 C54 Si5 42.0(4) .
C2 Y1 C54 Si5 25.4(2) .
C4 Y1 C54 Si5 -8.1(3) .
C1 Y1 C54 Si5 52.3(3) .
C3 Y1 C54 Si5 -3.3(3) .
Y4 Y1 C54 Si5 -162.3(2) .
O1 Y1 C54 Y2 49.93(13) .
O2 Y1 C54 Y2 95.71(10) .
C57 Y1 C54 Y2 -22.68(11) .
C55 Y1 C54 Y2 -73.05(19) .
C56 Y1 C54 Y2 -52.13(11) .
C5 Y1 C54 Y2 -138.3(2) .
C2 Y1 C54 Y2 -154.91(11) .
C4 Y1 C54 Y2 171.57(17) .
C1 Y1 C54 Y2 -128.07(12) .
C3 Y1 C54 Y2 176.40(12) .
Y4 Y1 C54 Y2 17.40(10) .
O1 Y1 C54 Y3 -41.73(13) .
O2 Y1 C54 Y3 4.06(9) .
C57 Y1 C54 Y3 -114.33(11) .
C55 Y1 C54 Y3 -164.7(2) .
C56 Y1 C54 Y3 -143.78(14) .
C5 Y1 C54 Y3 130.0(2) .
C2 Y1 C54 Y3 113.44(12) .
C4 Y1 C54 Y3 79.9(2) .
C1 Y1 C54 Y3 140.27(11) .
C3 Y1 C54 Y3 84.75(14) .
Y4 Y1 C54 Y3 -74.26(8) .
O2 Y3 C54 C55 -53.0(7) .
O3 Y3 C54 C55 50.6(7) .
C25 Y3 C54 C55 -134.4(6) .
C29 Y3 C54 C55 -56.8(12) .
C28 Y3 C54 C55 85.0(8) .
C27 Y3 C54 C55 133.5(7) .
C26 Y3 C54 C55 178.0(6) .
Si5 Y3 C54 C55 179.7(8) .
Y2 Y3 C54 C55 46.4(6) .
Y1 Y3 C54 C55 -48.6(6) .
O2 Y3 C54 Si5 127.28(13) .
O3 Y3 C54 Si5 -129.04(13) .
C25 Y3 C54 Si5 45.9(3) .
C29 Y3 C54 Si5 123.5(7) .
C28 Y3 C54 Si5 -94.6(3) .
C27 Y3 C54 Si5 -46.2(2) .
C26 Y3 C54 Si5 -1.7(2) .
Y2 Y3 C54 Si5 -133.26(16) .
Y1 Y3 C54 Si5 131.68(17) .
O2 Y3 C54 Y2 -99.46(10) .
O3 Y3 C54 Y2 4.21(9) .
C25 Y3 C54 Y2 179.12(16) .
C29 Y3 C54 Y2 -103.2(7) .
C28 Y3 C54 Y2 38.6(4) .
C27 Y3 C54 Y2 87.09(19) .
C26 Y3 C54 Y2 131.59(14) .
Si5 Y3 C54 Y2 133.26(16) .
Y1 Y3 C54 Y2 -95.06(12) .
O2 Y3 C54 Y1 -4.40(10) .
O3 Y3 C54 Y1 99.28(10) .
C25 Y3 C54 Y1 -85.8(2) .
C29 Y3 C54 Y1 -8.1(8) .
C28 Y3 C54 Y1 133.7(3) .
C27 Y3 C54 Y1 -177.85(14) .
C26 Y3 C54 Y1 -133.34(14) .
Si5 Y3 C54 Y1 -131.68(17) .
Y2 Y3 C54 Y1 95.06(12) .
Si5 C54 C55 C56 -178.9(3) .
Y2 C54 C55 C56 50.0(3) .
Y1 C54 C55 C56 -49.4(3) .
Y3 C54 C55 C56 1.5(9) .
Si5 C54 C55 Y2 131.1(2) .
Y1 C54 C55 Y2 -99.46(9) .
Y3 C54 C55 Y2 -48.6(7) .
Si5 C54 C55 Y1 -129.4(2) .
Y2 C54 C55 Y1 99.47(9) .
Y3 C54 C55 Y1 50.9(7) .
O3 Y2 C55 C56 -131.38(19) .
O4 Y2 C55 C56 -65.7(2) .
C54 Y2 C55 C56 -142.9(3) .
C57 Y2 C55 C56 -22.92(19) .
C14 Y2 C55 C56 126.4(2) .
C15 Y2 C55 C56 109.8(2) .
C16 Y2 C55 C56 80.1(2) .
C17 Y2 C55 C56 71.2(2) .
C13 Y2 C55 C56 104.0(2) .
Y4 Y2 C55 C56 -47.9(2) .
O3 Y2 C55 C54 11.5(2) .
O4 Y2 C55 C54 77.2(2) .
C57 Y2 C55 C54 119.9(2) .
C56 Y2 C55 C54 142.9(3) .
C14 Y2 C55 C54 -90.8(2) .
C15 Y2 C55 C54 -107.3(2) .
C16 Y2 C55 C54 -137.1(2) .
C17 Y2 C55 C54 -145.96(18) .
C13 Y2 C55 C54 -113.1(2) .
Y4 Y2 C55 C54 94.97(17) .
O3 Y2 C55 Y1 -57.84(12) .
O4 Y2 C55 Y1 7.87(16) .
C54 Y2 C55 Y1 -69.32(17) .
C57 Y2 C55 Y1 50.62(11) .
C56 Y2 C55 Y1 73.54(19) .
C14 Y2 C55 Y1 -160.09(10) .
C15 Y2 C55 Y1 -176.64(13) .
C16 Y2 C55 Y1 153.62(12) .
C17 Y2 C55 Y1 144.72(11) .
C13 Y2 C55 Y1 177.57(12) .
Y4 Y2 C55 Y1 25.65(9) .
O1 Y1 C55 C56 66.4(2) .
O2 Y1 C55 C56 131.35(19) .
C54 Y1 C55 C56 143.2(3) .
C57 Y1 C55 C56 23.43(19) .
C5 Y1 C55 C56 -73.6(2) .
C2 Y1 C55 C56 -114.6(2) .
C4 Y1 C55 C56 -107.1(3) .
C1 Y1 C55 C56 -83.9(2) .
C3 Y1 C55 C56 -131.6(2) .
Y4 Y1 C55 C56 48.38(19) .
O1 Y1 C55 C54 -76.8(2) .
O2 Y1 C55 C54 -11.8(2) .
C57 Y1 C55 C54 -119.8(2) .
C56 Y1 C55 C54 -143.2(3) .
C5 Y1 C55 C54 143.2(2) .
C2 Y1 C55 C54 102.2(2) .
C4 Y1 C55 C54 109.7(3) .
C1 Y1 C55 C54 132.9(2) .
C3 Y1 C55 C54 85.2(2) .
Y4 Y1 C55 C54 -94.81(18) .
O1 Y1 C55 Y2 -7.41(16) .
O2 Y1 C55 Y2 57.52(12) .
C54 Y1 C55 Y2 69.36(18) .
C57 Y1 C55 Y2 -50.39(11) .
C56 Y1 C55 Y2 -73.82(19) .
C5 Y1 C55 Y2 -147.45(13) .
C2 Y1 C55 Y2 171.58(11) .
C4 Y1 C55 Y2 179.08(19) .
C1 Y1 C55 Y2 -157.74(11) .
C3 Y1 C55 Y2 154.58(12) .
Y4 Y1 C55 Y2 -25.44(9) .
C54 C55 C56 C57 -1.0(6) .
Y2 C55 C56 C57 47.7(3) .
Y1 C55 C56 C57 -49.2(3) .
C54 C55 C56 Y1 48.2(3) .
Y2 C55 C56 Y1 96.95(9) .
C54 C55 C56 Y2 -48.7(3) .
Y1 C55 C56 Y2 -96.95(9) .
O1 Y1 C56 C55 -129.62(19) .
O2 Y1 C56 C55 -64.5(2) .
C54 Y1 C56 C55 -22.15(19) .
C57 Y1 C56 C55 -141.1(3) .
C5 Y1 C56 C55 122.5(2) .
C2 Y1 C56 C55 70.6(2) .
C4 Y1 C56 C55 114.7(3) .
C1 Y1 C56 C55 98.1(2) .
C3 Y1 C56 C55 69.6(3) .
Y4 Y1 C56 C55 -130.6(2) .
O1 Y1 C56 C57 11.5(2) .
O2 Y1 C56 C57 76.6(2) .
C54 Y1 C56 C57 119.0(2) .
C55 Y1 C56 C57 141.1(3) .
C5 Y1 C56 C57 -96.4(2) .
C2 Y1 C56 C57 -148.28(18) .
C4 Y1 C56 C57 -104.2(3) .
C1 Y1 C56 C57 -120.73(19) .
C3 Y1 C56 C57 -149.3(2) .
Y4 Y1 C56 C57 10.57(16) .
O1 Y1 C56 Y2 -57.57(12) .
O2 Y1 C56 Y2 7.53(16) .
C54 Y1 C56 Y2 49.91(10) .
C57 Y1 C56 Y2 -69.07(17) .
C55 Y1 C56 Y2 72.05(19) .
C5 Y1 C56 Y2 -165.46(12) .
C2 Y1 C56 Y2 142.65(10) .
C4 Y1 C56 Y2 -173.28(17) .
C1 Y1 C56 Y2 170.20(11) .
C3 Y1 C56 Y2 141.66(15) .
Y4 Y1 C56 Y2 -58.50(7) .
O3 Y2 C56 C55 64.9(2) .
O4 Y2 C56 C55 130.79(19) .
C54 Y2 C56 C55 22.36(19) .
C57 Y2 C56 C55 142.0(3) .
C14 Y2 C56 C55 -70.8(2) .
C15 Y2 C56 C55 -71.9(2) .
C16 Y2 C56 C55 -99.6(2) .
C17 Y2 C56 C55 -121.8(2) .
C13 Y2 C56 C55 -111.2(2) .
Y4 Y2 C56 C55 131.3(2) .
O3 Y2 C56 C57 -77.1(2) .
O4 Y2 C56 C57 -11.2(2) .
C54 Y2 C56 C57 -119.7(2) .
C55 Y2 C56 C57 -142.0(3) .
C14 Y2 C56 C57 147.15(19) .
C15 Y2 C56 C57 146.1(2) .
C16 Y2 C56 C57 118.4(2) .
C17 Y2 C56 C57 96.1(2) .
C13 Y2 C56 C57 106.8(2) .
Y4 Y2 C56 C57 -10.77(17) .
O3 Y2 C56 Y1 -7.41(16) .
O4 Y2 C56 Y1 58.44(12) .
C54 Y2 C56 Y1 -49.99(10) .
C57 Y2 C56 Y1 69.68(18) .
C55 Y2 C56 Y1 -72.35(19) .
C14 Y2 C56 Y1 -143.17(12) .
C15 Y2 C56 Y1 -144.25(12) .
C16 Y2 C56 Y1 -171.92(13) .
C17 Y2 C56 Y1 165.81(11) .
C13 Y2 C56 Y1 176.46(11) .
Y4 Y2 C56 Y1 58.91(7) .
C55 C56 C57 Si6 -177.6(3) .
Y1 C56 C57 Si6 132.36(19) .
Y2 C56 C57 Si6 -129.0(2) .
C55 C56 C57 Y2 -48.6(3) .
Y1 C56 C57 Y2 -98.67(9) .
C55 C56 C57 Y4 1.2(9) .
Y1 C56 C57 Y4 -48.9(7) .
Y2 C56 C57 Y4 49.8(7) .
C55 C56 C57 Y1 50.0(3) .
Y2 C56 C57 Y1 98.67(9) .
C58 Si6 C57 C56 10.1(4) .
C59 Si6 C57 C56 -115.4(3) .
C60 Si6 C57 C56 131.0(3) .
C58 Si6 C57 Y2 -78.4(3) .
C59 Si6 C57 Y2 156.1(2) .
C60 Si6 C57 Y2 42.4(3) .
C58 Si6 C57 Y4 -169.5(2) .
C59 Si6 C57 Y4 65.03(19) .
C60 Si6 C57 Y4 -48.62(18) .
C58 Si6 C57 Y1 99.0(3) .
C59 Si6 C57 Y1 -26.5(3) .
C60 Si6 C57 Y1 -140.2(2) .
O3 Y2 C57 C56 123.69(19) .
O4 Y2 C57 C56 169.4(2) .
C54 Y2 C57 C56 50.6(2) .
C55 Y2 C57 C56 21.52(18) .
C14 Y2 C57 C56 -64.6(3) .
C15 Y2 C57 C56 -42.6(2) .
C16 Y2 C57 C56 -64.0(2) .
C17 Y2 C57 C56 -94.7(2) .
C13 Y2 C57 C56 -109.2(2) .
Y4 Y2 C57 C56 164.9(2) .
O3 Y2 C57 Si6 -131.3(2) .
O4 Y2 C57 Si6 -85.6(2) .
C54 Y2 C57 Si6 155.6(2) .
C55 Y2 C57 Si6 126.5(3) .
C56 Y2 C57 Si6 105.0(3) .
C14 Y2 C57 Si6 40.4(4) .
C15 Y2 C57 Si6 62.4(3) .
C16 Y2 C57 Si6 41.0(2) .
C17 Y2 C57 Si6 10.4(3) .
C13 Y2 C57 Si6 -4.2(3) .
Y4 Y2 C57 Si6 -90.1(2) .
O3 Y2 C57 Y4 -41.21(13) .
O4 Y2 C57 Y4 4.52(9) .
C54 Y2 C57 Y4 -114.35(11) .
C55 Y2 C57 Y4 -143.38(15) .
C56 Y2 C57 Y4 -164.9(2) .
C14 Y2 C57 Y4 130.5(2) .
C15 Y2 C57 Y4 152.52(12) .
C16 Y2 C57 Y4 131.06(12) .
C17 Y2 C57 Y4 100.44(13) .
C13 Y2 C57 Y4 85.86(16) .
O3 Y2 C57 Y1 50.56(13) .
O4 Y2 C57 Y1 96.29(10) .
C54 Y2 C57 Y1 -22.58(10) .
C55 Y2 C57 Y1 -51.61(11) .
C56 Y2 C57 Y1 -73.13(19) .
C14 Y2 C57 Y1 -137.7(2) .
C15 Y2 C57 Y1 -115.71(14) .
C16 Y2 C57 Y1 -137.18(12) .
C17 Y2 C57 Y1 -167.79(12) .
C13 Y2 C57 Y1 177.63(11) .
Y4 Y2 C57 Y1 91.77(12) .
O4 Y4 C57 C56 -52.5(7) .
O1 Y4 C57 C56 50.9(7) .
C37 Y4 C57 C56 128.3(7) .
C38 Y4 C57 C56 50.5(11) .
C41 Y4 C57 C56 175.6(6) .
C39 Y4 C57 C56 -89.5(8) .
C40 Y4 C57 C56 -138.7(7) .
Y2 Y4 C57 C56 -47.7(6) .
Y1 Y4 C57 C56 46.7(7) .
O4 Y4 C57 Si6 126.33(13) .
O1 Y4 C57 Si6 -130.23(13) .
C37 Y4 C57 Si6 -52.8(3) .
C38 Y4 C57 Si6 -130.6(6) .
C41 Y4 C57 Si6 -5.5(2) .
C39 Y4 C57 Si6 89.3(3) .
C40 Y4 C57 Si6 40.2(2) .
Y2 Y4 C57 Si6 131.16(17) .
Y1 Y4 C57 Si6 -134.48(16) .
O4 Y4 C57 Y2 -4.84(10) .
O1 Y4 C57 Y2 98.61(10) .
C37 Y4 C57 Y2 176.03(17) .
C38 Y4 C57 Y2 98.2(6) .
C41 Y4 C57 Y2 -136.71(14) .
C39 Y4 C57 Y2 -41.8(3) .
C40 Y4 C57 Y2 -90.98(18) .
Y1 Y4 C57 Y2 94.35(12) .
O4 Y4 C57 Y1 -99.19(10) .
O1 Y4 C57 Y1 4.26(9) .
C37 Y4 C57 Y1 81.7(2) .
C38 Y4 C57 Y1 3.8(7) .
C41 Y4 C57 Y1 128.93(15) .
C39 Y4 C57 Y1 -136.2(3) .
C40 Y4 C57 Y1 174.67(13) .
Y2 Y4 C57 Y1 -94.35(12) .
O1 Y1 C57 C56 -169.09(19) .
O2 Y1 C57 C56 -123.59(18) .
C54 Y1 C57 C56 -51.09(18) .
C55 Y1 C57 C56 -22.02(17) .
C5 Y1 C57 C56 97.5(2) .
C2 Y1 C57 C56 43.7(2) .
C4 Y1 C57 C56 115.8(2) .
C1 Y1 C57 C56 64.6(2) .
C3 Y1 C57 C56 73.9(4) .
Y4 Y1 C57 C56 -165.1(2) .
O1 Y1 C57 Si6 86.5(2) .
O2 Y1 C57 Si6 132.0(2) .
C54 Y1 C57 Si6 -155.5(3) .
C55 Y1 C57 Si6 -126.4(3) .
C56 Y1 C57 Si6 -104.4(3) .
C5 Y1 C57 Si6 -6.9(3) .
C2 Y1 C57 Si6 -60.7(3) .
C4 Y1 C57 Si6 11.4(3) .
C1 Y1 C57 Si6 -39.8(3) .
C3 Y1 C57 Si6 -30.5(5) .
Y4 Y1 C57 Si6 90.5(2) .
O1 Y1 C57 Y2 -95.43(10) .
O2 Y1 C57 Y2 -49.93(13) .
C54 Y1 C57 Y2 22.57(10) .
C55 Y1 C57 Y2 51.64(11) .
C56 Y1 C57 Y2 73.66(18) .
C5 Y1 C57 Y2 171.11(13) .
C2 Y1 C57 Y2 117.35(14) .
C4 Y1 C57 Y2 -170.51(15) .
C1 Y1 C57 Y2 138.22(11) .
C3 Y1 C57 Y2 147.5(3) .
Y4 Y1 C57 Y2 -91.45(11) .
O1 Y1 C57 Y4 -3.98(8) .
O2 Y1 C57 Y4 41.52(12) .
C54 Y1 C57 Y4 114.02(11) .
C55 Y1 C57 Y4 143.09(14) .
C56 Y1 C57 Y4 165.1(2) .
C5 Y1 C57 Y4 -97.44(15) .
C2 Y1 C57 Y4 -151.20(12) .
C4 Y1 C57 Y4 -79.06(19) .
C1 Y1 C57 Y4 -130.33(11) .
C3 Y1 C57 Y4 -121.0(3) .
C73 C71 C72 C73 -11(13) 2_556
C74 C71 C72 C73 -179.1(10) 2_556
C72 C71 C72 C73 -0.8(7) 2_556
C76 C71 C72 C73 0.0 .
C77 C71 C72 C73 180.0 .
C75 C71 C72 C73 -179.1(11) 2_556
C71 C71 C72 C73 -0.8(7) 2_556
C76 C71 C72 C73 -11(13) 2_556
C71 C72 C73 C74 0.0 .
C72 C73 C74 C75 0.0 .
C73 C74 C75 C76 0.0 .
C73 C71 C76 C75 178.9(12) 2_556
C74 C71 C76 C75 178.9(13) 2_556
C72 C71 C76 C75 3(3) 2_556
C72 C71 C76 C75 0.0 .
C77 C71 C76 C75 180.0 .
C75 C71 C76 C75 3(4) 2_556
C71 C71 C76 C75 0.6(6) 2_556
C76 C71 C76 C75 0.6(7) 2_556
C74 C75 C76 C71 0.0 .
C86 C81 C82 C83 0.0 .
C87 C81 C82 C83 180.0 .
C81 C82 C83 C84 0.0 .
C82 C83 C84 C85 0.0 .
C83 C84 C85 C86 -0.1 .
C84 C85 C86 C81 0.1 .
C82 C81 C86 C85 -0.1 .
C87 C81 C86 C85 180.0 .
C96 C91 C92 C93 0.0 .
C97 C91 C92 C93 180.0 .
C91 C92 C93 C94 0.0 .
C92 C93 C94 C95 0.0 .
C93 C94 C95 C96 0.0 .
C94 C95 C96 C91 0.0 .
C92 C91 C96 C95 0.0 .
C97 C91 C96 C95 -180.0 .
