#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:01:04 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179045 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/07/4300765.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4300765
loop_
_publ_author_name
'Shengming Liu'
'Christine E. Plecnik'
'Edward A. Meyers'
'Sheldon G. Shore'
_publ_section_title
;
Two Distinct Ln(III)-Cu(I) Cyanide Extended Arrays: Structures and
Synthetic Methodology for Inclusion and Layer Complexes
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              282
_journal_page_last               292
_journal_paper_doi               10.1021/ic040113+
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C156 H280 Cu24 Er4 N76 O40'
_chemical_formula_weight         6054.56
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 101.670(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            1
_cell_length_a                   15.0805(10)
_cell_length_b                   15.6823(10)
_cell_length_c                   27.3024(10)
_cell_measurement_temperature    200(2)
_cell_volume                     6323.5(6)
_diffrn_ambient_temperature      200(2)
_exptl_crystal_density_diffrn    1.590
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4300765
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Er1 Er 0.219921(11) 0.383729(11) 0.628853(6) 0.03388(6) Uani 1 1 d . . .
O1 O 0.09493(19) 0.34218(19) 0.66278(11) 0.0509(7) Uani 1 1 d . . .
C1 C 0.0499(4) 0.3802(3) 0.6905(2) 0.0715(16) Uani 1 1 d . A .
H1 H 0.0792 0.4248 0.7112 0.086 Uiso 1 1 calc . . .
N1 N -0.0325(2) 0.3630(3) 0.69291(14) 0.0512(9) Uani 1 1 d . . .
C1A C -0.0851(6) 0.3080(6) 0.6583(3) 0.074(4) Uiso 0.72(2) 1 d P A 1
C1AA C -0.054(2) 0.260(2) 0.6835(13) 0.123(14) Uiso 0.28(2) 1 d P A 2
C1B C -0.0810(4) 0.4126(4) 0.7244(3) 0.093(2) Uani 1 1 d . A .
H1B1 H -0.1425 0.3900 0.7213 0.139 Uiso 1 1 calc . . .
H1B2 H -0.0839 0.4724 0.7138 0.139 Uiso 1 1 calc . . .
H1B3 H -0.0490 0.4086 0.7594 0.139 Uiso 1 1 calc . . .
O2 O 0.2999(2) 0.3466(2) 0.70635(10) 0.0599(9) Uani 1 1 d . . .
C2 C 0.3073(3) 0.3497(3) 0.75211(16) 0.0483(10) Uani 1 1 d . . .
H2 H 0.2719 0.3901 0.7656 0.058 Uiso 1 1 calc . . .
N2 N 0.3619(2) 0.2994(2) 0.78303(12) 0.0416(8) Uani 1 1 d . . .
C2A C 0.3721(3) 0.3070(3) 0.83718(17) 0.0603(13) Uani 1 1 d . . .
H2A1 H 0.4153 0.2641 0.8537 0.090 Uiso 1 1 calc . . .
H2A2 H 0.3133 0.2979 0.8464 0.090 Uiso 1 1 calc . . .
H2A3 H 0.3946 0.3641 0.8478 0.090 Uiso 1 1 calc . . .
C2B C 0.4180(4) 0.2362(3) 0.76464(19) 0.0665(14) Uani 1 1 d . . .
H2B1 H 0.4543 0.2055 0.7930 0.100 Uiso 1 1 calc . . .
H2B2 H 0.4582 0.2648 0.7458 0.100 Uiso 1 1 calc . . .
H2B3 H 0.3791 0.1958 0.7428 0.100 Uiso 1 1 calc . . .
O3 O 0.2110(2) 0.23615(19) 0.62725(11) 0.0553(8) Uani 1 1 d . . .
C3 C 0.1849(4) 0.1811(3) 0.65317(18) 0.0595(13) Uani 1 1 d . . .
H3 H 0.1371 0.1960 0.6695 0.071 Uiso 1 1 calc . . .
N3 N 0.2169(3) 0.1049(2) 0.66000(14) 0.0572(11) Uani 1 1 d . . .
C3A C 0.2917(5) 0.0801(4) 0.6371(3) 0.095(2) Uani 1 1 d . . .
H3A1 H 0.3093 0.0212 0.6465 0.142 Uiso 1 1 calc . . .
H3A2 H 0.3433 0.1181 0.6488 0.142 Uiso 1 1 calc . . .
H3A3 H 0.2732 0.0842 0.6007 0.142 Uiso 1 1 calc . . .
C3B C 0.1810(5) 0.0420(3) 0.6907(2) 0.0820(18) Uani 1 1 d . . .
H3B1 H 0.2145 -0.0116 0.6911 0.123 Uiso 1 1 calc . . .
H3B2 H 0.1168 0.0320 0.6767 0.123 Uiso 1 1 calc . . .
H3B3 H 0.1879 0.0636 0.7250 0.123 Uiso 1 1 calc . . .
O4 O 0.36528(19) 0.3437(2) 0.61842(11) 0.0566(8) Uani 1 1 d . . .
C4 C 0.4416(3) 0.3406(3) 0.64530(16) 0.0451(10) Uani 1 1 d . . .
H4 H 0.4503 0.3688 0.6767 0.054 Uiso 1 1 calc . . .
N4 N 0.5112(2) 0.3014(2) 0.63398(13) 0.0488(9) Uani 1 1 d . . .
C4A C 0.5033(4) 0.2569(6) 0.5868(2) 0.128(3) Uani 1 1 d . . .
H4A1 H 0.5615 0.2308 0.5849 0.192 Uiso 1 1 calc . . .
H4A2 H 0.4859 0.2974 0.5592 0.192 Uiso 1 1 calc . . .
H4A3 H 0.4569 0.2124 0.5843 0.192 Uiso 1 1 calc . . .
C4B C 0.5995(3) 0.2984(3) 0.66715(18) 0.0555(12) Uani 1 1 d . . .
H4B1 H 0.6413 0.2652 0.6514 0.083 Uiso 1 1 calc . . .
H4B2 H 0.5940 0.2715 0.6988 0.083 Uiso 1 1 calc . . .
H4B3 H 0.6229 0.3565 0.6736 0.083 Uiso 1 1 calc . . .
O5 O 0.21263(18) 0.34586(18) 0.54558(10) 0.0429(6) Uani 1 1 d . . .
C5 C 0.2161(2) 0.2755(3) 0.52422(14) 0.0394(9) Uani 1 1 d . . .
H5 H 0.1890 0.2277 0.5368 0.047 Uiso 1 1 calc . . .
N5 N 0.2544(2) 0.2632(2) 0.48591(11) 0.0394(7) Uani 1 1 d . . .
C5A C 0.3014(4) 0.3317(3) 0.46581(18) 0.0635(13) Uani 1 1 d . . .
H5A1 H 0.3249 0.3105 0.4372 0.095 Uiso 1 1 calc . . .
H5A2 H 0.3517 0.3520 0.4917 0.095 Uiso 1 1 calc . . .
H5A3 H 0.2592 0.3787 0.4550 0.095 Uiso 1 1 calc . . .
C5B C 0.2515(4) 0.1806(3) 0.46103(18) 0.0605(13) Uani 1 1 d . . .
H5B1 H 0.2839 0.1843 0.4334 0.091 Uiso 1 1 calc . . .
H5B2 H 0.1883 0.1646 0.4479 0.091 Uiso 1 1 calc . . .
H5B3 H 0.2802 0.1375 0.4851 0.091 Uiso 1 1 calc . . .
O6 O 0.29126(18) 0.50626(18) 0.60678(11) 0.0470(7) Uani 1 1 d . . .
C6 C 0.3387(3) 0.5188(3) 0.57520(16) 0.0458(10) Uani 1 1 d . . .
H6 H 0.3250 0.4871 0.5450 0.055 Uiso 1 1 calc . . .
N6 N 0.4062(2) 0.5727(2) 0.58076(14) 0.0470(9) Uani 1 1 d . . .
C6A C 0.4290(4) 0.6253(4) 0.6254(2) 0.0760(16) Uani 1 1 d . . .
H6A1 H 0.4804 0.6622 0.6230 0.114 Uiso 1 1 calc . . .
H6A2 H 0.4452 0.5886 0.6549 0.114 Uiso 1 1 calc . . .
H6A3 H 0.3767 0.6606 0.6285 0.114 Uiso 1 1 calc . . .
C6B C 0.4596(4) 0.5849(4) 0.5428(2) 0.0787(17) Uani 1 1 d . . .
H6B1 H 0.5062 0.6281 0.5541 0.118 Uiso 1 1 calc . . .
H6B2 H 0.4202 0.6040 0.5117 0.118 Uiso 1 1 calc . . .
H6B3 H 0.4885 0.5310 0.5369 0.118 Uiso 1 1 calc . . .
O7 O 0.09575(18) 0.45615(18) 0.58281(11) 0.0472(7) Uani 1 1 d . . .
C7 C 0.0838(3) 0.5324(3) 0.57154(15) 0.0420(9) Uani 1 1 d . . .
H7 H 0.1358 0.5669 0.5725 0.050 Uiso 1 1 calc . . .
N7 N 0.0049(2) 0.5682(2) 0.55848(13) 0.0425(8) Uani 1 1 d . . .
C7A C -0.0782(3) 0.5219(3) 0.5577(2) 0.0625(13) Uani 1 1 d . . .
H7A1 H -0.1300 0.5597 0.5464 0.094 Uiso 1 1 calc . . .
H7A2 H -0.0793 0.5011 0.5914 0.094 Uiso 1 1 calc . . .
H7A3 H -0.0817 0.4733 0.5348 0.094 Uiso 1 1 calc . . .
C7B C -0.0055(3) 0.6575(3) 0.5452(2) 0.0756(17) Uani 1 1 d . . .
H7B1 H -0.0701 0.6718 0.5367 0.113 Uiso 1 1 calc . . .
H7B2 H 0.0223 0.6688 0.5164 0.113 Uiso 1 1 calc . . .
H7B3 H 0.0242 0.6924 0.5736 0.113 Uiso 1 1 calc . . .
O8 O 0.1918(2) 0.49647(19) 0.68069(11) 0.0508(7) Uani 1 1 d . . .
C8 C 0.2295(3) 0.5627(3) 0.69918(16) 0.0476(10) Uani 1 1 d . . .
H8 H 0.2922 0.5688 0.6995 0.057 Uiso 1 1 calc . . .
N8 N 0.1897(2) 0.6243(2) 0.71819(13) 0.0463(9) Uani 1 1 d . . .
C8A C 0.2394(3) 0.6973(3) 0.74170(17) 0.0571(12) Uani 1 1 d . . .
H8A1 H 0.1978 0.7362 0.7539 0.086 Uiso 1 1 calc . . .
H8A2 H 0.2678 0.7270 0.7173 0.086 Uiso 1 1 calc . . .
H8A3 H 0.2862 0.6782 0.7699 0.086 Uiso 1 1 calc . . .
C8B C 0.0943(4) 0.6175(3) 0.7200(2) 0.0694(15) Uani 1 1 d . . .
H8B1 H 0.0753 0.6686 0.7358 0.104 Uiso 1 1 calc . . .
H8B2 H 0.0847 0.5671 0.7395 0.104 Uiso 1 1 calc . . .
H8B3 H 0.0584 0.6122 0.6859 0.104 Uiso 1 1 calc . . .
O O 0.4795(3) 0.1918(3) 0.46179(16) 0.0867(12) Uani 1 1 d . . .
C C 0.5538(4) 0.1588(4) 0.47559(19) 0.0638(13) Uani 1 1 d . . .
H0 H 0.5987 0.1921 0.4966 0.077 Uiso 1 1 calc . . .
N N 0.5777(3) 0.0817(3) 0.46424(14) 0.0571(10) Uani 1 1 d . . .
C1' C 0.6702(5) 0.0532(4) 0.4802(3) 0.100(2) Uani 1 1 d . . .
H1'1 H 0.6755 -0.0058 0.4692 0.150 Uiso 1 1 calc . . .
H1'2 H 0.6874 0.0559 0.5167 0.150 Uiso 1 1 calc . . .
H1'3 H 0.7104 0.0900 0.4655 0.150 Uiso 1 1 calc . . .
C1'' C 0.5149(5) 0.0276(4) 0.4316(2) 0.0875(18) Uani 1 1 d . . .
H1'4 H 0.5438 -0.0273 0.4278 0.131 Uiso 1 1 calc . . .
H1'5 H 0.4971 0.0550 0.3988 0.131 Uiso 1 1 calc . . .
H1'6 H 0.4611 0.0184 0.4459 0.131 Uiso 1 1 calc . . .
O' O 0.1347(3) 0.0668(3) 0.53103(17) 0.0985(14) Uani 1 1 d . . .
C' C 0.0786(4) 0.0391(4) 0.5529(2) 0.0760(15) Uani 1 1 d . . .
H' H 0.0942 -0.0126 0.5707 0.091 Uiso 1 1 calc . . .
N' N -0.0048(3) 0.0724(3) 0.55538(19) 0.0806(14) Uani 1 1 d . . .
C2' C -0.0647(5) 0.0300(5) 0.5804(3) 0.107(2) Uani 1 1 d . . .
H2'1 H -0.1200 0.0639 0.5781 0.160 Uiso 1 1 calc . . .
H2'2 H -0.0358 0.0224 0.6157 0.160 Uiso 1 1 calc . . .
H2'3 H -0.0801 -0.0259 0.5650 0.160 Uiso 1 1 calc . . .
C2'' C -0.0334(5) 0.1518(5) 0.5308(3) 0.117(3) Uani 1 1 d . . .
H2'4 H -0.0939 0.1665 0.5362 0.175 Uiso 1 1 calc . . .
H2'5 H -0.0354 0.1461 0.4948 0.175 Uiso 1 1 calc . . .
H2'6 H 0.0094 0.1969 0.5445 0.175 Uiso 1 1 calc . . .
Cu1 Cu 0.76766(4) 0.20010(4) 0.37804(2) 0.05480(15) Uani 1 1 d . . .
Cu2 Cu 0.72727(4) 0.55630(4) 0.65726(2) 0.05594(15) Uani 1 1 d . . .
Cu3 Cu 0.92650(4) -0.19126(4) 0.66536(2) 0.05839(16) Uani 1 1 d . . .
Cu4 Cu 0.46980(4) -0.02370(4) 0.72561(2) 0.04998(14) Uani 1 1 d . . .
Cu5 Cu 0.73131(4) 0.06474(3) 0.65330(2) 0.04860(14) Uani 1 1 d . . .
Cu6 Cu 0.74503(4) 0.31784(4) 0.54250(2) 0.05325(15) Uani 1 1 d . . .
C9A C 1.0424(3) -0.1881(3) 0.64810(17) 0.0483(10) Uani 1 1 d . . .
N9A N 1.1125(3) -0.1876(3) 0.63696(15) 0.0636(11) Uani 1 1 d . . .
C9B C 0.8141(3) -0.3553(3) 0.66845(17) 0.0512(11) Uani 1 1 d . . .
N9B N 0.8620(3) -0.2967(3) 0.67151(18) 0.0709(12) Uani 1 1 d . . .
C9C C 0.3367(3) -0.1523(3) 0.66259(17) 0.0484(10) Uani 1 1 d . . .
N9C N 0.3964(3) -0.1167(2) 0.68747(16) 0.0579(10) Uani 1 1 d . . .
C9D C 0.3600(3) 0.0273(3) 0.80417(17) 0.0503(11) Uani 1 1 d . . .
N9D N 0.4082(3) 0.0067(3) 0.77840(16) 0.0658(11) Uani 1 1 d . . .
C9E C 0.7598(3) 0.2891(3) 0.47794(17) 0.0460(10) Uani 1 1 d . . .
N9E N 0.7650(3) 0.2626(3) 0.43866(17) 0.0651(11) Uani 1 1 d . . .
C9F C 0.8629(3) -0.0879(3) 0.67209(17) 0.0458(10) Uani 1 1 d . . .
N9F N 0.8182(3) -0.0274(3) 0.66896(16) 0.0670(11) Uani 1 1 d . . .
C9G C 0.7278(3) 0.4207(3) 0.57571(17) 0.0507(11) Uani 1 1 d . . .
N9G N 0.7225(3) 0.4789(3) 0.60060(16) 0.0646(11) Uani 1 1 d . . .
C9H C 0.5685(3) 0.0222(3) 0.70194(15) 0.0435(10) Uani 1 1 d . . .
N9H N 0.6281(3) 0.0459(2) 0.68538(14) 0.0511(9) Uani 1 1 d . . .
C9I C 0.7395(3) 0.1582(3) 0.61066(16) 0.0457(10) Uani 1 1 d . . .
N9I N 0.7446(3) 0.2164(3) 0.58529(14) 0.0553(10) Uani 1 1 d . . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Er1 O2 2.289(3) . ?
Er1 O3 2.318(3) . ?
Er1 O7 2.329(3) . ?
Er1 O5 2.331(3) . ?
Er1 O6 2.340(3) . ?
Er1 O4 2.352(3) . ?
Er1 O1 2.354(3) . ?
Er1 O8 2.356(3) . ?
O1 C1 1.264(6) . ?
C1 N1 1.287(6) . ?
C1 H1 0.9500 . ?
N1 C1A 1.401(9) . ?
N1 C1B 1.460(7) . ?
N1 C1AA 1.66(4) . ?
C1B H1B1 0.9800 . ?
C1B H1B2 0.9800 . ?
C1B H1B3 0.9800 . ?
O2 C2 1.233(5) . ?
C2 N2 1.316(5) . ?
C2 H2 0.9500 . ?
N2 C2B 1.456(6) . ?
N2 C2A 1.460(5) . ?
C2A H2A1 0.9800 . ?
C2A H2A2 0.9800 . ?
C2A H2A3 0.9800 . ?
C2B H2B1 0.9800 . ?
C2B H2B2 0.9800 . ?
C2B H2B3 0.9800 . ?
O3 C3 1.231(5) . ?
C3 N3 1.287(6) . ?
C3 H3 0.9500 . ?
N3 C3A 1.449(7) . ?
N3 C3B 1.468(7) . ?
C3A H3A1 0.9800 . ?
C3A H3A2 0.9800 . ?
C3A H3A3 0.9800 . ?
C3B H3B1 0.9800 . ?
C3B H3B2 0.9800 . ?
C3B H3B3 0.9800 . ?
O4 C4 1.234(5) . ?
C4 N4 1.307(5) . ?
C4 H4 0.9500 . ?
N4 C4A 1.449(7) . ?
N4 C4B 1.452(5) . ?
C4A H4A1 0.9800 . ?
C4A H4A2 0.9800 . ?
C4A H4A3 0.9800 . ?
C4B H4B1 0.9800 . ?
C4B H4B2 0.9800 . ?
C4B H4B3 0.9800 . ?
O5 C5 1.254(5) . ?
C5 N5 1.307(5) . ?
C5 H5 0.9500 . ?
N5 C5A 1.455(5) . ?
N5 C5B 1.459(6) . ?
C5A H5A1 0.9800 . ?
C5A H5A2 0.9800 . ?
C5A H5A3 0.9800 . ?
C5B H5B1 0.9800 . ?
C5B H5B2 0.9800 . ?
C5B H5B3 0.9800 . ?
O6 C6 1.242(5) . ?
C6 N6 1.308(5) . ?
C6 H6 0.9500 . ?
N6 C6B 1.449(6) . ?
N6 C6A 1.455(7) . ?
C6A H6A1 0.9800 . ?
C6A H6A2 0.9800 . ?
C6A H6A3 0.9800 . ?
C6B H6B1 0.9800 . ?
C6B H6B2 0.9800 . ?
C6B H6B3 0.9800 . ?
O7 C7 1.238(5) . ?
C7 N7 1.299(5) . ?
C7 H7 0.9500 . ?
N7 C7A 1.446(6) . ?
N7 C7B 1.447(6) . ?
C7A H7A1 0.9800 . ?
C7A H7A2 0.9800 . ?
C7A H7A3 0.9800 . ?
C7B H7B1 0.9800 . ?
C7B H7B2 0.9800 . ?
C7B H7B3 0.9800 . ?
O8 C8 1.242(5) . ?
C8 N8 1.300(5) . ?
C8 H8 0.9500 . ?
N8 C8A 1.445(6) . ?
N8 C8B 1.454(6) . ?
C8A H8A1 0.9800 . ?
C8A H8A2 0.9800 . ?
C8A H8A3 0.9800 . ?
C8B H8B1 0.9800 . ?
C8B H8B2 0.9800 . ?
C8B H8B3 0.9800 . ?
O C 1.222(6) . ?
C N 1.317(6) . ?
C H0 0.9500 . ?
N C1'' 1.438(7) . ?
N C1' 1.446(7) . ?
C1' H1'1 0.9800 . ?
C1' H1'2 0.9800 . ?
C1' H1'3 0.9800 . ?
C1'' H1'4 0.9800 . ?
C1'' H1'5 0.9800 . ?
C1'' H1'6 0.9800 . ?
O' C' 1.210(7) . ?
C' N' 1.376(7) . ?
C' H' 0.9500 . ?
N' C2' 1.406(7) . ?
N' C2'' 1.439(8) . ?
C2' H2'1 0.9800 . ?
C2' H2'2 0.9800 . ?
C2' H2'3 0.9800 . ?
C2'' H2'4 0.9800 . ?
C2'' H2'5 0.9800 . ?
C2'' H2'6 0.9800 . ?
Cu1 C9C 1.888(5) 3_656 ?
Cu1 N9E 1.931(5) . ?
Cu1 N9A 1.943(4) 3_756 ?
Cu2 C9B 1.888(5) 1_565 ?
Cu2 C9D 1.899(4) 2_656 ?
Cu2 N9G 1.956(4) . ?
Cu3 C9A 1.900(5) . ?
Cu3 C9F 1.911(5) . ?
Cu3 N9B 1.943(5) . ?
Cu4 C9H 1.881(4) . ?
Cu4 N9D 1.926(5) . ?
Cu4 N9C 1.992(4) . ?
Cu5 C9I 1.891(5) . ?
Cu5 N9F 1.940(5) . ?
Cu5 N9H 1.957(4) . ?
Cu6 C9E 1.876(4) . ?
Cu6 C9G 1.893(5) . ?
Cu6 N9I 1.975(4) . ?
C9A N9A 1.158(6) . ?
N9A Cu1 1.943(4) 3_756 ?
C9B N9B 1.162(6) . ?
C9B Cu2 1.888(5) 1_545 ?
C9C N9C 1.156(6) . ?
C9C Cu1 1.888(5) 3_656 ?
C9D N9D 1.155(6) . ?
C9D Cu2 1.899(4) 2_646 ?
C9E N9E 1.167(6) . ?
C9F N9F 1.157(6) . ?
C9G N9G 1.151(6) . ?
C9H N9H 1.147(5) . ?
C9I N9I 1.158(5) . ?
