#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/04/4310402.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4310402
loop_
_publ_author_name
'Matthew L. Kuhlman'
'Thomas B. Rauchfuss'
_publ_contact_author
; 
Scott R. Wilson 
University of Illinois 
School of Chemical Sciences, Box 59-1 
505 South Mathews Avenue 
Urbana, Illinois  61801 
USA 
;
_publ_contact_author_email       srwilson@uiuc.edu
_publ_contact_author_fax         '1  217 244 8068'
_publ_contact_author_phone       '1  217 244 1708'
_publ_section_title
;
 Hybrid Cluster-Cages Formed via Cyanometalate Condensation:
 Cs@Co4Ru6S2(CN)12, Co4Ru9S6(CN)9, and Rh4Ru9S6(CN)9 Frameworks
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              430
_journal_page_last               435
_journal_paper_doi               10.1021/ic034745s
_journal_volume                  43
_journal_year                    2004
_chemical_formula_moiety
; 
C82 H93 Co4 Cs N12 Ru6 S2, C82 H93 Co4 Cs N12 Ru6 S2, 4(F6 P), 
10(C2 H3 N) 
;
_chemical_formula_sum            'C92 H108 Co4 Cs F12 N17 P2 Ru6 S2'
_chemical_formula_weight         2781.06
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
; 
2003-06-13    text and data added, mlk 
;
_cell_angle_alpha                111.742(6)
_cell_angle_beta                 91.535(7)
_cell_angle_gamma                93.373(6)
_cell_formula_units_Z            4
_cell_length_a                   15.586(4)
_cell_length_b                   26.955(8)
_cell_length_c                   28.378(8)
_cell_measurement_reflns_used    1024
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      16.3
_cell_measurement_theta_min      2.3
_cell_volume                     11040(5)
_computing_cell_refinement       'SAINT V6.22 (Bruker, 2001)'
_computing_data_collection       'SMART V5.625 (Bruker, 2001)'
_computing_data_reduction        'SAINT V6.22 (Bruker, 2001)'
_computing_molecular_graphics    'SHELXTL V6.10 (Bruker, 2001)'
_computing_publication_material  'CIFTAB (Sheldrick, 2001)'
_computing_structure_refinement  'SHELXTL V6.10 (Bruker, 2001)'
_computing_structure_solution    'SHELXTL V6.10 (Bruker, 2001)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device       'Siemens Platform/CCD'
_diffrn_measurement_method       'profile data from ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'normal-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_wavelength_id  p96paps
_diffrn_reflns_av_R_equivalents  0.1554
_diffrn_reflns_av_sigmaI/netI    0.3286
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            26627
_diffrn_reflns_theta_full        17.25
_diffrn_reflns_theta_max         17.25
_diffrn_reflns_theta_min         1.52
_diffrn_standards_decay_%        7.2
_diffrn_standards_interval_time  562
_diffrn_standards_number         85
_exptl_absorpt_coefficient_mu    1.841
_exptl_absorpt_correction_T_max  0.9646
_exptl_absorpt_correction_T_min  0.7666
_exptl_absorpt_correction_type   integration
_exptl_absorpt_process_details   '(Bruker, 2001)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.673
_exptl_crystal_density_meas      ?
_exptl_crystal_description       platy
_exptl_crystal_F_000             5504
_exptl_crystal_id                p96paps
_exptl_crystal_preparation
; 
The data crystal was mounted using oil (Parantone-N, Exxon) to a 
0.3 mm cryo-loop (Hampton Research) with the (??) scattering planes 
roughly normal to the spindle axis. 
;
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.743
_refine_diff_density_min         -0.748
_refine_diff_density_rms         0.142
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.827
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     777
_refine_ls_number_reflns         13345
_refine_ls_number_restraints     894
_refine_ls_restrained_S_all      0.807
_refine_ls_R_factor_all          0.2138
_refine_ls_R_factor_gt           0.0821
_refine_ls_shift/su_max          0.047
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0653P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1596
_refine_ls_wR_factor_ref         0.1944
_reflns_number_gt                4941
_reflns_number_total             13345
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic034745ssi20030630_112819.cif
_cod_data_source_block           p96paps
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        11039(5)
_cod_original_sg_symbol_Hall     '-P 1 '
_cod_original_sg_symbol_H-M      'P -1 '
_cod_database_code               4310402
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.4519(12) 0.2244(9) 0.1364(7) 0.039(8) Uiso 1 1 d DU . .
C2 C 0.3285(14) 0.2838(6) 0.1843(8) 0.037(8) Uiso 1 1 d DU . .
C3 C 0.2956(13) 0.1851(10) 0.1330(8) 0.064(9) Uiso 1 1 d DU . .
C4 C 0.4394(12) 0.1651(10) -0.0411(7) 0.049(8) Uiso 1 1 d DU . .
C5 C 0.3213(14) 0.1909(6) -0.0939(8) 0.037(8) Uiso 1 1 d DU . .
C6 C 0.2840(12) 0.1263(9) -0.0437(7) 0.041(8) Uiso 1 1 d DU . .
C7 C 0.1205(11) 0.3301(8) 0.0960(6) 0.011(7) Uiso 1 1 d DU . .
C8 C 0.1131(12) 0.2977(9) -0.0065(7) 0.048(8) Uiso 1 1 d DU . .
C9 C 0.0852(17) 0.2282(7) 0.0394(9) 0.076(9) Uiso 1 1 d DU . .
C10 C 0.5051(14) 0.3388(6) 0.0545(8) 0.029(7) Uiso 1 1 d DU . .
C11 C 0.3916(12) 0.4013(10) 0.1047(7) 0.056(8) Uiso 1 1 d DU . .
C12 C 0.3852(12) 0.3655(9) 0.0049(7) 0.039(8) Uiso 1 1 d DU . .
N1 N 0.4938(13) 0.2238(8) 0.1022(7) 0.055(7) Uiso 1 1 d DU . .
N2 N 0.3052(12) 0.3251(6) 0.1857(6) 0.027(6) Uiso 1 1 d DU A .
N3 N 0.2463(12) 0.1622(8) 0.0984(7) 0.054(7) Uiso 1 1 d DU . .
N4 N 0.4892(12) 0.1879(8) -0.0066(7) 0.057(7) Uiso 1 1 d DU . .
N5 N 0.2936(12) 0.2302(7) -0.0954(7) 0.040(6) Uiso 1 1 d DU . .
N6 N 0.2328(12) 0.1221(8) -0.0161(7) 0.053(7) Uiso 1 1 d DU . .
N7 N 0.1673(11) 0.3553(7) 0.1315(6) 0.037(6) Uiso 1 1 d DU A .
N8 N 0.1584(12) 0.3001(7) -0.0378(6) 0.034(6) Uiso 1 1 d DU . .
N9 N 0.1072(16) 0.1883(8) 0.0423(8) 0.089(9) Uiso 1 1 d DU . .
N10 N 0.5251(12) 0.2980(6) 0.0562(6) 0.025(6) Uiso 1 1 d DU . .
N11 N 0.3431(12) 0.4005(8) 0.1353(7) 0.054(7) Uiso 1 1 d DU A .
N12 N 0.3333(12) 0.3399(8) -0.0269(7) 0.050(7) Uiso 1 1 d DU . .
C13 C 0.4122(12) 0.1642(6) 0.2081(5) 0.083(3) Uiso 1 1 d GU . .
H1 H 0.4328 0.1311 0.1873 0.099 Uiso 1 1 calc R . .
C14 C 0.3259(11) 0.1730(8) 0.2218(7) 0.083(3) Uiso 1 1 d GU . .
H2 H 0.2785 0.1468 0.2118 0.099 Uiso 1 1 calc R . .
C15 C 0.3227(13) 0.2279(9) 0.2532(7) 0.083(3) Uiso 1 1 d GU . .
H3 H 0.2728 0.2448 0.2678 0.099 Uiso 1 1 calc R . .
C16 C 0.4071(16) 0.2530(6) 0.2588(6) 0.083(3) Uiso 1 1 d GU . .
H4 H 0.4236 0.2897 0.2778 0.099 Uiso 1 1 calc R . .
C17 C 0.4624(11) 0.2136(8) 0.2309(7) 0.083(3) Uiso 1 1 d GU . .
H5 H 0.5224 0.2194 0.2281 0.099 Uiso 1 1 calc R . .
C18 C 0.3881(13) 0.0491(6) -0.1214(5) 0.083(3) Uiso 1 1 d GU . .
H6 H 0.3928 0.0284 -0.1008 0.099 Uiso 1 1 calc R . .
C19 C 0.4567(11) 0.0791(8) -0.1330(7) 0.083(3) Uiso 1 1 d GU . .
H7 H 0.5152 0.0820 -0.1215 0.099 Uiso 1 1 calc R . .
C20 C 0.4223(15) 0.1040(7) -0.1648(7) 0.083(3) Uiso 1 1 d GU . .
H8 H 0.4538 0.1265 -0.1783 0.099 Uiso 1 1 calc R . .
C21 C 0.3325(15) 0.0894(8) -0.1729(7) 0.083(3) Uiso 1 1 d GU . .
H9 H 0.2935 0.1003 -0.1928 0.099 Uiso 1 1 calc R . .
C22 C 0.3114(11) 0.0554(8) -0.1461(7) 0.083(3) Uiso 1 1 d GU . .
H10 H 0.2558 0.0397 -0.1449 0.099 Uiso 1 1 calc R . .
C23 C -0.0468(10) 0.3543(6) 0.0652(7) 0.083(3) Uiso 1 1 d GU . .
H11 H -0.0320 0.3916 0.0817 0.099 Uiso 1 1 calc R . .
C24 C -0.0554(12) 0.3256(8) 0.0118(7) 0.083(3) Uiso 1 1 d GU . .
H12 H -0.0474 0.3403 -0.0135 0.099 Uiso 1 1 calc R . .
C25 C -0.0781(13) 0.2710(7) 0.0031(7) 0.083(3) Uiso 1 1 d GU . .
H13 H -0.0880 0.2428 -0.0292 0.099 Uiso 1 1 calc R . .
C26 C -0.0835(12) 0.2659(7) 0.0510(8) 0.083(3) Uiso 1 1 d GU . .
H14 H -0.0976 0.2338 0.0564 0.099 Uiso 1 1 calc R . .
C27 C -0.0641(12) 0.3174(8) 0.0894(6) 0.083(3) Uiso 1 1 d GU . .
H15 H -0.0630 0.3257 0.1250 0.099 Uiso 1 1 calc R . .
C28 C 0.4989(12) 0.4821(7) 0.0956(6) 0.083(3) Uiso 1 1 d GU . .
H16 H 0.4791 0.5025 0.1279 0.099 Uiso 1 1 calc R . .
C29 C 0.5725(12) 0.4519(8) 0.0864(7) 0.083(3) Uiso 1 1 d GU . .
H17 H 0.6106 0.4485 0.1115 0.099 Uiso 1 1 calc R . .
C30 C 0.5792(13) 0.4276(8) 0.0330(8) 0.083(3) Uiso 1 1 d GU . .
H18 H 0.6226 0.4051 0.0162 0.099 Uiso 1 1 calc R . .
C31 C 0.5097(14) 0.4428(8) 0.0092(6) 0.083(3) Uiso 1 1 d GU . .
H19 H 0.4984 0.4323 -0.0264 0.099 Uiso 1 1 calc R . .
C32 C 0.4601(12) 0.4765(8) 0.0478(7) 0.083(3) Uiso 1 1 d GU . .
H20 H 0.4098 0.4925 0.0427 0.099 Uiso 1 1 calc R . .
C33 C 0.3093(13) 0.4686(8) 0.2526(7) 0.129(2) Uiso 0.662(14) 1 d PGU A 1
C34 C 0.2625(15) 0.4343(8) 0.2721(8) 0.129(2) Uiso 0.662(14) 1 d PGU A 1
C35 C 0.1747(14) 0.4306(9) 0.2556(9) 0.129(2) Uiso 0.662(14) 1 d PGU A 1
C36 C 0.1673(14) 0.4626(9) 0.2259(8) 0.129(2) Uiso 0.662(14) 1 d PGU A 1
C37 C 0.2505(15) 0.4861(8) 0.2240(8) 0.129(2) Uiso 0.662(14) 1 d PGU A 1
C38 C 0.4049(13) 0.4838(11) 0.2608(10) 0.138(2) Uiso 0.662(14) 1 d PGU A 1
H167 H 0.4158 0.5167 0.2910 0.207 Uiso 0.662(14) 1 calc PR A 1
H168 H 0.4265 0.4897 0.2311 0.207 Uiso 0.662(14) 1 calc PR A 1
H169 H 0.4344 0.4548 0.2657 0.207 Uiso 0.662(14) 1 calc PR A 1
C39 C 0.2995(19) 0.4066(11) 0.3047(10) 0.138(2) Uiso 0.662(14) 1 d PGU A 1
H170 H 0.2976 0.4297 0.3406 0.207 Uiso 0.662(14) 1 calc PR A 1
H171 H 0.3593 0.3995 0.2965 0.207 Uiso 0.662(14) 1 calc PR A 1
H172 H 0.2657 0.3727 0.2982 0.207 Uiso 0.662(14) 1 calc PR A 1
C40 C 0.1021(17) 0.3983(12) 0.2675(12) 0.138(2) Uiso 0.662(14) 1 d PGU A 1
H173 H 0.0757 0.4207 0.2985 0.207 Uiso 0.662(14) 1 calc PR A 1
H174 H 0.1246 0.3674 0.2727 0.207 Uiso 0.662(14) 1 calc PR A 1
H175 H 0.0588 0.3858 0.2392 0.207 Uiso 0.662(14) 1 calc PR A 1
C41 C 0.0854(16) 0.4703(13) 0.2006(12) 0.138(2) Uiso 0.662(14) 1 d PGU A 1
H176 H 0.0583 0.5013 0.2239 0.207 Uiso 0.662(14) 1 calc PR A 1
H177 H 0.0459 0.4382 0.1921 0.207 Uiso 0.662(14) 1 calc PR A 1
H178 H 0.0988 0.4764 0.1696 0.207 Uiso 0.662(14) 1 calc PR A 1
C42 C 0.273(2) 0.5232(11) 0.1965(11) 0.138(2) Uiso 0.662(14) 1 d PGU A 1
H179 H 0.2665 0.5603 0.2192 0.207 Uiso 0.662(14) 1 calc PR A 1
H180 H 0.2335 0.5140 0.1664 0.207 Uiso 0.662(14) 1 calc PR A 1
H181 H 0.3320 0.5193 0.1861 0.207 Uiso 0.662(14) 1 calc PR A 1
C185 C 0.297(3) 0.4449(16) 0.2664(14) 0.129(2) Uiso 0.338(14) 1 d PGU A 2
C186 C 0.214(3) 0.4204(17) 0.2664(15) 0.129(2) Uiso 0.338(14) 1 d PGU A 2
C187 C 0.156(3) 0.4388(19) 0.2381(17) 0.129(2) Uiso 0.338(14) 1 d PGU A 2
C188 C 0.203(3) 0.4747(19) 0.2206(16) 0.129(2) Uiso 0.338(14) 1 d PGU A 2
C189 C 0.290(3) 0.4785(17) 0.2381(15) 0.129(2) Uiso 0.338(14) 1 d PGU A 2
C190 C 0.378(3) 0.437(2) 0.2920(19) 0.138(2) Uiso 0.338(14) 1 d PGU A 2
H182 H 0.3849 0.4633 0.3268 0.207 Uiso 0.338(14) 1 calc PR A 2
H183 H 0.4279 0.4410 0.2731 0.207 Uiso 0.338(14) 1 calc PR A 2
H184 H 0.3745 0.4007 0.2928 0.207 Uiso 0.338(14) 1 calc PR A 2
C191 C 0.191(4) 0.382(2) 0.292(2) 0.138(2) Uiso 0.338(14) 1 d PGU A 2
H185 H 0.1743 0.4014 0.3266 0.207 Uiso 0.338(14) 1 calc PR A 2
H186 H 0.2410 0.3616 0.2933 0.207 Uiso 0.338(14) 1 calc PR A 2
H187 H 0.1430 0.3565 0.2727 0.207 Uiso 0.338(14) 1 calc PR A 2
C192 C 0.061(3) 0.423(3) 0.228(2) 0.138(2) Uiso 0.338(14) 1 d PGU A 2
H188 H 0.0290 0.4481 0.2552 0.207 Uiso 0.338(14) 1 calc PR A 2
H189 H 0.0490 0.3867 0.2279 0.207 Uiso 0.338(14) 1 calc PR A 2
H190 H 0.0418 0.4239 0.1954 0.207 Uiso 0.338(14) 1 calc PR A 2
C193 C 0.167(4) 0.504(3) 0.189(2) 0.138(2) Uiso 0.338(14) 1 d PGU A 2
H191 H 0.1478 0.5381 0.2114 0.207 Uiso 0.338(14) 1 calc PR A 2
H192 H 0.1182 0.4818 0.1673 0.207 Uiso 0.338(14) 1 calc PR A 2
H193 H 0.2117 0.5099 0.1678 0.207 Uiso 0.338(14) 1 calc PR A 2
C194 C 0.363(4) 0.512(2) 0.228(2) 0.138(2) Uiso 0.338(14) 1 d PGU A 2
H194 H 0.3676 0.5480 0.2552 0.207 Uiso 0.338(14) 1 calc PR A 2
H195 H 0.3524 0.5152 0.1954 0.207 Uiso 0.338(14) 1 calc PR A 2
H196 H 0.4174 0.4954 0.2282 0.207 Uiso 0.338(14) 1 calc PR A 2
C43 C 0.6990(8) 0.2339(5) 0.0145(5) 0.129(2) Uiso 1 1 d GU . .
C44 C 0.7087(8) 0.2683(5) 0.0664(5) 0.129(2) Uiso 1 1 d GU . .
C45 C 0.6996(9) 0.2362(6) 0.0962(5) 0.129(2) Uiso 1 1 d GU . .
C46 C 0.6842(9) 0.1820(6) 0.0626(5) 0.129(2) Uiso 1 1 d GU . .
C47 C 0.6838(8) 0.1806(5) 0.0121(5) 0.129(2) Uiso 1 1 d GU . .
C48 C 0.7038(11) 0.2511(7) -0.0304(5) 0.138(2) Uiso 1 1 d GU . .
H21 H 0.7626 0.2485 -0.0422 0.207 Uiso 1 1 calc R . .
H22 H 0.6884 0.2882 -0.0203 0.207 Uiso 1 1 calc R . .
H23 H 0.6638 0.2277 -0.0579 0.207 Uiso 1 1 calc R . .
C49 C 0.7258(13) 0.3284(5) 0.0865(6) 0.138(2) Uiso 1 1 d GU . .
H24 H 0.7880 0.3376 0.0901 0.207 Uiso 1 1 calc R . .
H25 H 0.7009 0.3441 0.1197 0.207 Uiso 1 1 calc R . .
H26 H 0.6995 0.3426 0.0628 0.207 Uiso 1 1 calc R . .
C50 C 0.7052(13) 0.2562(8) 0.1535(5) 0.138(2) Uiso 1 1 d GU . .
H27 H 0.7642 0.2544 0.1653 0.207 Uiso 1 1 calc R . .
H28 H 0.6657 0.2338 0.1649 0.207 Uiso 1 1 calc R . .
H29 H 0.6895 0.2933 0.1675 0.207 Uiso 1 1 calc R . .
C51 C 0.6706(13) 0.1342(7) 0.0780(7) 0.138(2) Uiso 1 1 d GU . .
H30 H 0.7258 0.1190 0.0791 0.207 Uiso 1 1 calc R . .
H31 H 0.6306 0.1071 0.0531 0.207 Uiso 1 1 calc R . .
H32 H 0.6466 0.1455 0.1116 0.207 Uiso 1 1 calc R . .
C52 C 0.6697(12) 0.1310(6) -0.0357(6) 0.138(2) Uiso 1 1 d GU . .
H33 H 0.7250 0.1158 -0.0458 0.207 Uiso 1 1 calc R . .
H34 H 0.6445 0.1406 -0.0629 0.207 Uiso 1 1 calc R . .
H35 H 0.6306 0.1046 -0.0294 0.207 Uiso 1 1 calc R . .
C53 C 0.0760(9) 0.0739(5) 0.0751(5) 0.129(2) Uiso 1 1 d GU . .
C54 C 0.1485(9) 0.0441(5) 0.0571(5) 0.129(2) Uiso 1 1 d GU . .
C55 C 0.1477(9) 0.0297(6) 0.0036(5) 0.129(2) Uiso 1 1 d GU . .
C56 C 0.0748(9) 0.0506(5) -0.0114(5) 0.129(2) Uiso 1 1 d GU . .
C57 C 0.0304(9) 0.0779(5) 0.0328(5) 0.129(2) Uiso 1 1 d GU . .
C58 C 0.0516(11) 0.0972(7) 0.1297(5) 0.138(2) Uiso 1 1 d GU . .
H36 H 0.0174 0.0700 0.1379 0.207 Uiso 1 1 calc R . .
H37 H 0.0176 0.1280 0.1347 0.207 Uiso 1 1 calc R . .
H38 H 0.1038 0.1087 0.1521 0.207 Uiso 1 1 calc R . .
C59 C 0.2147(11) 0.0302(8) 0.0891(6) 0.138(2) Uiso 1 1 d GU . .
H39 H 0.1963 -0.0041 0.0917 0.207 Uiso 1 1 calc R . .
H40 H 0.2204 0.0583 0.1232 0.207 Uiso 1 1 calc R . .
H41 H 0.2702 0.0273 0.0733 0.207 Uiso 1 1 calc R . .
C60 C 0.2130(12) -0.0022(8) -0.0312(6) 0.138(2) Uiso 1 1 d GU . .
H42 H 0.1970 -0.0406 -0.0410 0.207 Uiso 1 1 calc R . .
H43 H 0.2700 0.0065 -0.0135 0.207 Uiso 1 1 calc R . .
H44 H 0.2145 0.0067 -0.0617 0.207 Uiso 1 1 calc R . .
C61 C 0.0490(13) 0.0447(8) -0.0649(5) 0.138(2) Uiso 1 1 d GU . .
H45 H 0.0129 0.0113 -0.0815 0.207 Uiso 1 1 calc R . .
H46 H 0.1007 0.0440 -0.0840 0.207 Uiso 1 1 calc R . .
H47 H 0.0165 0.0751 -0.0640 0.207 Uiso 1 1 calc R . .
C62 C -0.0508(11) 0.1062(8) 0.0345(7) 0.138(2) Uiso 1 1 d GU . .
H48 H -0.1009 0.0815 0.0322 0.207 Uiso 1 1 calc R . .
H49 H -0.0540 0.1182 0.0059 0.207 Uiso 1 1 calc R . .
H50 H -0.0503 0.1372 0.0665 0.207 Uiso 1 1 calc R . .
C63 C 0.32871(8) 0.232038(16) -0.24273(4) 0.105(3) Uiso 1 1 d GDU . .
C64 C 0.3977(3) 0.26858(13) -0.2185(3) 0.105(3) Uiso 1 1 d GDU . .
H51 H 0.4427 0.2584 -0.2015 0.126 Uiso 1 1 calc R . .
C65 C 0.4007(3) 0.31998(13) -0.2191(3) 0.105(3) Uiso 1 1 d GDU . .
H52 H 0.4478 0.3450 -0.2025 0.126 Uiso 1 1 calc R . .
C66 C 0.33477(10) 0.33483(2) -0.24396(6) 0.105(3) Uiso 1 1 d GDU . .
C67 C 0.2658(3) 0.29829(14) -0.2682(3) 0.105(3) Uiso 1 1 d GDU . .
H53 H 0.2208 0.3084 -0.2852 0.126 Uiso 1 1 calc R . .
C68 C 0.2628(3) 0.24689(13) -0.2676(3) 0.105(3) Uiso 1 1 d GDU . .
H54 H 0.2157 0.2219 -0.2842 0.126 Uiso 1 1 calc R . .
C69 C 0.32706(9) 0.38851(3) -0.24865(3) 0.132(4) Uiso 1 1 d DU . .
H55 H 0.2655 0.3973 -0.2454 0.158 Uiso 1 1 calc R . .
C70 C 0.38237(16) 0.43267(5) -0.20583(4) 0.132(4) Uiso 1 1 d DU . .
H56 H 0.3626 0.4345 -0.1728 0.197 Uiso 1 1 calc R . .
H57 H 0.3767 0.4673 -0.2092 0.197 Uiso 1 1 calc R . .
H58 H 0.4428 0.4243 -0.2084 0.197 Uiso 1 1 calc R . .
C71 C 0.3562(2) 0.38787(7) -0.29959(5) 0.132(4) Uiso 1 1 d DU . .
H59 H 0.3206 0.3606 -0.3271 0.197 Uiso 1 1 calc R . .
H60 H 0.4166 0.3795 -0.3030 0.197 Uiso 1 1 calc R . .
H61 H 0.3501 0.4231 -0.3015 0.197 Uiso 1 1 calc R . .
C72 C 0.32726(15) 0.17667(3) -0.24134(10) 0.132(4) Uiso 1 1 d DU . .
H62 H 0.3558 0.1530 -0.2708 0.197 Uiso 1 1 calc R . .
H63 H 0.2675 0.1627 -0.2423 0.197 Uiso 1 1 calc R . .
H64 H 0.3575 0.1783 -0.2100 0.197 Uiso 1 1 calc R . .
C73 C 0.02129(5) 0.36953(4) -0.16384(3) 0.105(3) Uiso 1 1 d GDU . .
C74 C 0.02131(7) 0.38477(5) -0.11138(4) 0.105(3) Uiso 1 1 d GDU . .
H65 H -0.0169 0.3664 -0.0968 0.126 Uiso 1 1 calc R . .
C75 C 0.07730(10) 0.42693(5) -0.08023(3) 0.105(3) Uiso 1 1 d GDU . .
H66 H 0.0773 0.4373 -0.0444 0.126 Uiso 1 1 calc R . .
C76 C 0.13326(12) 0.45385(7) -0.10154(4) 0.105(3) Uiso 1 1 d GDU . .
C77 C 0.13324(11) 0.43861(7) -0.15401(5) 0.105(3) Uiso 1 1 d GDU . .
H67 H 0.1715 0.4570 -0.1686 0.126 Uiso 1 1 calc R . .
C78 C 0.07726(8) 0.39645(5) -0.18516(4) 0.105(3) Uiso 1 1 d GDU . .
H68 H 0.0772 0.3860 -0.2210 0.126 Uiso 1 1 calc R . .
C79 C 0.19976(8) 0.49940(3) -0.07401(4) 0.132(4) Uiso 1 1 d DU . .
H69 H 0.2541 0.4929 -0.0926 0.158 Uiso 1 1 calc R . .
C80 C 0.21861(14) 0.50217(5) -0.01931(5) 0.132(4) Uiso 1 1 d DU . .
H70 H 0.2360 0.4674 -0.0204 0.197 Uiso 1 1 calc R . .
H71 H 0.1667 0.5110 -0.0001 0.197 Uiso 1 1 calc R . .
H72 H 0.2651 0.5298 -0.0028 0.197 Uiso 1 1 calc R . .
C81 C 0.1696(2) 0.55296(5) -0.07143(9) 0.132(4) Uiso 1 1 d DU . .
H73 H 0.1600 0.5523 -0.1059 0.197 Uiso 1 1 calc R . .
H74 H 0.2137 0.5816 -0.0529 0.197 Uiso 1 1 calc R . .
H75 H 0.1158 0.5595 -0.0538 0.197 Uiso 1 1 calc R . .
C82 C -0.03993(12) 0.32355(9) -0.19658(6) 0.132(4) Uiso 1 1 d DU . .
H76 H -0.0942 0.3373 -0.2028 0.197 Uiso 1 1 calc R . .
H77 H -0.0511 0.2987 -0.1792 0.197 Uiso 1 1 calc R . .
H78 H -0.0144 0.3048 -0.2290 0.197 Uiso 1 1 calc R . .
Co1 Co 0.3678(3) 0.22115(17) 0.18263(15) 0.0658(15) Uani 1 1 d U . .
Co2 Co 0.3620(3) 0.12802(16) -0.09424(14) 0.0641(16) Uani 1 1 d U . .
Co3 Co 0.0412(3) 0.29346(18) 0.04272(15) 0.0655(16) Uani 1 1 d U . .
Co4 Co 0.4636(3) 0.40262(16) 0.05554(13) 0.0513(14) Uani 1 1 d U . .
Cs1 Cs 0.31038(12) 0.26061(8) 0.04999(7) 0.0464(6) Uani 1 1 d U . .
Ru1 Ru 0.25602(17) 0.39834(9) 0.19005(8) 0.0462(9) Uani 1 1 d U . .
Ru2 Ru 0.58353(16) 0.23011(11) 0.05137(9) 0.0622(10) Uani 1 1 d U . .
Ru3 Ru 0.1526(2) 0.11692(11) 0.03674(11) 0.0852(12) Uani 1 1 d U . .
Ru4 Ru 0.24582(16) 0.30400(10) -0.09098(9) 0.0517(9) Uani 1 1 d U . .
Ru5 Ru 0.27539(18) 0.30297(11) -0.18934(9) 0.0678(10) Uani 1 1 d U . .
Ru6 Ru 0.1520(2) 0.36408(13) -0.13471(11) 0.0967(11) Uani 1 1 d U . .
S1 S 0.2942(6) 0.3707(3) -0.1141(3) 0.067(2) Uani 1 1 d U . .
S2 S 0.1556(6) 0.2733(4) -0.1612(3) 0.077(2) Uani 1 1 d U . .
C83 C 0.8096(14) 0.2461(5) 0.3368(8) 0.025(7) Uiso 1 1 d DU . .
C84 C 0.7658(11) 0.3374(10) 0.3974(7) 0.043(8) Uiso 1 1 d DU . .
C85 C 0.9284(11) 0.3109(8) 0.3980(6) 0.015(7) Uiso 1 1 d DU . .
C86 C 0.8894(10) 0.1335(9) 0.4976(7) 0.021(7) Uiso 1 1 d DU B .
C87 C 0.8863(12) 0.1176(8) 0.3993(6) 0.020(7) Uiso 1 1 d DU B .
C88 C 1.0032(13) 0.1847(5) 0.4613(7) 0.010(7) Uiso 1 1 d DU B .
C89 C 0.8166(15) 0.2987(6) 0.6015(8) 0.041(8) Uiso 1 1 d DU . .
C90 C 0.7615(11) 0.3727(8) 0.5674(6) 0.010(7) Uiso 1 1 d DU . .
C91 C 0.9280(11) 0.3492(10) 0.5667(7) 0.039(8) Uiso 1 1 d DU . .
C92 C 0.6106(10) 0.1767(8) 0.4958(6) 0.007(6) Uiso 1 1 d DU . .
C93 C 0.6144(11) 0.1527(9) 0.3932(6) 0.025(7) Uiso 1 1 d DU . .
C94 C 0.5605(13) 0.2490(6) 0.4595(7) 0.016(7) Uiso 1 1 d DU . .
N83 N 0.7905(12) 0.1998(6) 0.3240(7) 0.040(6) Uiso 1 1 d DU . .
N84 N 0.7149(11) 0.3492(7) 0.4286(6) 0.021(6) Uiso 1 1 d DU . .
N85 N 0.9800(11) 0.3065(7) 0.4276(6) 0.021(6) Uiso 1 1 d DU . .
N86 N 0.8351(10) 0.1506(7) 0.5263(6) 0.015(6) Uiso 1 1 d DU . .
N87 N 0.8401(11) 0.1217(7) 0.3673(6) 0.026(6) Uiso 1 1 d DU . .
N88 N 1.0242(11) 0.2291(5) 0.4672(6) 0.016(5) Uiso 1 1 d DU . .
N89 N 0.7965(12) 0.2531(6) 0.5926(7) 0.032(6) Uiso 1 1 d DU . .
N90 N 0.7137(11) 0.3712(7) 0.5340(6) 0.018(6) Uiso 1 1 d DU . .
N91 N 0.9780(11) 0.3331(7) 0.5360(6) 0.032(6) Uiso 1 1 d DU . .
N92 N 0.6668(10) 0.1812(7) 0.5258(6) 0.019(6) Uiso 1 1 d DU . .
N93 N 0.6651(11) 0.1441(7) 0.3619(6) 0.023(6) Uiso 1 1 d DU . .
N94 N 0.5876(11) 0.2931(6) 0.4678(6) 0.024(6) Uiso 1 1 d DU . .
C95 C 0.8564(11) 0.3000(5) 0.2752(5) 0.053(2) Uiso 1 1 d GU . .
H79 H 0.8487 0.2655 0.2490 0.063 Uiso 1 1 calc R . .
C96 C 0.7910(9) 0.3357(7) 0.2945(6) 0.053(2) Uiso 1 1 d GU . .
H80 H 0.7319 0.3292 0.2835 0.063 Uiso 1 1 calc R . .
C97 C 0.8295(13) 0.3827(6) 0.3332(6) 0.053(2) Uiso 1 1 d GU . .
H81 H 0.8006 0.4132 0.3526 0.063 Uiso 1 1 calc R . .
C98 C 0.9186(12) 0.3761(6) 0.3378(6) 0.053(2) Uiso 1 1 d GU . .
H82 H 0.9599 0.4014 0.3608 0.063 Uiso 1 1 calc R . .
C99 C 0.9353(10) 0.3250(7) 0.3020(6) 0.053(2) Uiso 1 1 d GU . .
H83 H 0.9896 0.3102 0.2968 0.063 Uiso 1 1 calc R . .
C100 C 0.9713(16) 0.0334(10) 0.4449(10) 0.053(2) Uiso 0.64(3) 1 d PGU B 1
H197 H 0.9269 0.0116 0.4515 0.063 Uiso 0.64(3) 1 calc PR B 1
C101 C 1.0311(19) 0.0704(12) 0.4816(9) 0.053(2) Uiso 0.64(3) 1 d PGU B 1
H198 H 1.0337 0.0776 0.5170 0.063 Uiso 0.64(3) 1 calc PR B 1
C102 C 1.0864(18) 0.0947(12) 0.4560(13) 0.053(2) Uiso 0.64(3) 1 d PGU B 1
H199 H 1.1325 0.1210 0.4713 0.063 Uiso 0.64(3) 1 calc PR B 1
C103 C 1.061(2) 0.0727(15) 0.4035(12) 0.053(2) Uiso 0.64(3) 1 d PGU B 1
H200 H 1.0867 0.0817 0.3775 0.063 Uiso 0.64(3) 1 calc PR B 1
C104 C 0.990(2) 0.0348(13) 0.3966(9) 0.053(2) Uiso 0.64(3) 1 d PGU B 1
H201 H 0.9596 0.0141 0.3652 0.063 Uiso 0.64(3) 1 calc PR B 1
C195 C 1.003(4) 0.058(2) 0.4700(17) 0.053(2) Uiso 0.36(3) 1 d PGU B 2
H202 H 0.9793 0.0537 0.4987 0.063 Uiso 0.36(3) 1 calc PR B 2
C196 C 1.078(4) 0.091(2) 0.4707(19) 0.053(2) Uiso 0.36(3) 1 d PGU B 2
H203 H 1.1123 0.1132 0.5000 0.063 Uiso 0.36(3) 1 calc PR B 2
C197 C 1.092(4) 0.086(3) 0.420(2) 0.053(2) Uiso 0.36(3) 1 d PGU B 2
H204 H 1.1370 0.1044 0.4093 0.063 Uiso 0.36(3) 1 calc PR B 2
C198 C 1.026(4) 0.050(3) 0.3879(16) 0.053(2) Uiso 0.36(3) 1 d PGU B 2
H205 H 1.0192 0.0394 0.3520 0.063 Uiso 0.36(3) 1 calc PR B 2
C199 C 0.971(3) 0.033(2) 0.4188(19) 0.053(2) Uiso 0.36(3) 1 d PGU B 2
H206 H 0.9217 0.0081 0.4072 0.063 Uiso 0.36(3) 1 calc PR B 2
C105 C 0.9329(9) 0.4001(6) 0.6795(5) 0.053(2) Uiso 1 1 d GU . .
H84 H 0.9846 0.3851 0.6840 0.063 Uiso 1 1 calc R . .
C106 C 0.9249(11) 0.4399(6) 0.6584(6) 0.053(2) Uiso 1 1 d GU . .
H85 H 0.9704 0.4563 0.6464 0.063 Uiso 1 1 calc R . .
C107 C 0.8370(12) 0.4511(7) 0.6585(6) 0.053(2) Uiso 1 1 d GU . .
H86 H 0.8133 0.4762 0.6465 0.063 Uiso 1 1 calc R . .
C108 C 0.7906(9) 0.4181(8) 0.6796(6) 0.053(2) Uiso 1 1 d GU . .
H87 H 0.7305 0.4173 0.6843 0.063 Uiso 1 1 calc R . .
C109 C 0.8498(11) 0.3866(6) 0.6926(6) 0.053(2) Uiso 1 1 d GU . .
H88 H 0.8363 0.3609 0.7075 0.063 Uiso 1 1 calc R . .
C110 C 0.4016(9) 0.1933(5) 0.4467(6) 0.053(2) Uiso 1 1 d GU . .
H89 H 0.3802 0.2273 0.4530 0.063 Uiso 1 1 calc R . .
C111 C 0.4180(12) 0.1549(7) 0.3983(5) 0.053(2) Uiso 1 1 d GU . .
H90 H 0.4093 0.1588 0.3666 0.063 Uiso 1 1 calc R . .
C112 C 0.4494(12) 0.1098(6) 0.4056(7) 0.053(2) Uiso 1 1 d GU . .
H91 H 0.4656 0.0782 0.3797 0.063 Uiso 1 1 calc R . .
C113 C 0.4526(11) 0.1203(7) 0.4585(7) 0.053(2) Uiso 1 1 d GU . .
H92 H 0.4712 0.0969 0.4742 0.063 Uiso 1 1 calc R . .
C114 C 0.4230(12) 0.1719(7) 0.4839(5) 0.053(2) Uiso 1 1 d GU . .
H93 H 0.4184 0.1890 0.5195 0.063 Uiso 1 1 calc R . .
C115 C 1.2022(6) 0.2979(4) 0.5058(4) 0.069(2) Uiso 1 1 d GU . .
C116 C 1.1782(7) 0.3487(4) 0.5386(4) 0.069(2) Uiso 1 1 d GU . .
C117 C 1.1621(7) 0.3795(4) 0.5085(4) 0.069(2) Uiso 1 1 d GU . .
C118 C 1.1761(7) 0.3477(5) 0.4572(4) 0.069(2) Uiso 1 1 d GU . .
C119 C 1.2009(7) 0.2972(4) 0.4556(4) 0.069(2) Uiso 1 1 d GU . .
C120 C 1.2251(10) 0.2525(5) 0.5217(5) 0.081(2) Uiso 1 1 d GU . .
H94 H 1.2867 0.2564 0.5313 0.122 Uiso 1 1 calc R . .
H95 H 1.2115 0.2183 0.4934 0.122 Uiso 1 1 calc R . .
H96 H 1.1919 0.2533 0.5508 0.122 Uiso 1 1 calc R . .
C121 C 1.1711(11) 0.3669(6) 0.5953(4) 0.081(2) Uiso 1 1 d GU . .
H97 H 1.2264 0.3843 0.6125 0.122 Uiso 1 1 calc R . .
H98 H 1.1558 0.3358 0.6043 0.122 Uiso 1 1 calc R . .
H99 H 1.1265 0.3924 0.6060 0.122 Uiso 1 1 calc R . .
C122 C 1.1349(11) 0.4361(5) 0.5277(6) 0.081(2) Uiso 1 1 d GU . .
H100 H 1.1860 0.4614 0.5377 0.122 Uiso 1 1 calc R . .
H101 H 1.0997 0.4419 0.5571 0.122 Uiso 1 1 calc R . .
H102 H 1.1011 0.4418 0.5007 0.122 Uiso 1 1 calc R . .
C123 C 1.1664(11) 0.3645(6) 0.4123(5) 0.081(2) Uiso 1 1 d GU . .
H103 H 1.2208 0.3822 0.4081 0.122 Uiso 1 1 calc R . .
H104 H 1.1209 0.3894 0.4181 0.122 Uiso 1 1 calc R . .
H105 H 1.1511 0.3329 0.3815 0.122 Uiso 1 1 calc R . .
C124 C 1.2222(11) 0.2510(5) 0.4086(4) 0.081(2) Uiso 1 1 d GU . .
H106 H 1.2839 0.2538 0.4035 0.122 Uiso 1 1 calc R . .
H107 H 1.1896 0.2521 0.3790 0.122 Uiso 1 1 calc R . .
H108 H 1.2068 0.2172 0.4128 0.122 Uiso 1 1 calc R . .
C125 C 0.7481(7) 0.0318(4) 0.2686(3) 0.069(2) Uiso 1 1 d GU . .
C126 C 0.6682(7) 0.0494(4) 0.2582(4) 0.069(2) Uiso 1 1 d GU . .
C127 C 0.6847(8) 0.0847(4) 0.2321(4) 0.069(2) Uiso 1 1 d GU . .
C128 C 0.7748(8) 0.0888(4) 0.2264(4) 0.069(2) Uiso 1 1 d GU . .
C129 C 0.8139(7) 0.0561(4) 0.2489(4) 0.069(2) Uiso 1 1 d GU . .
C130 C 0.7607(9) -0.0061(5) 0.2957(5) 0.081(2) Uiso 1 1 d GU . .
H109 H 0.7559 -0.0431 0.2710 0.122 Uiso 1 1 calc R . .
H110 H 0.7166 -0.0019 0.3206 0.122 Uiso 1 1 calc R . .
H111 H 0.8178 0.0019 0.3132 0.122 Uiso 1 1 calc R . .
C131 C 0.5810(7) 0.0335(6) 0.2723(6) 0.081(2) Uiso 1 1 d GU . .
H112 H 0.5551 0.0019 0.2444 0.122 Uiso 1 1 calc R . .
H113 H 0.5438 0.0632 0.2788 0.122 Uiso 1 1 calc R . .
H114 H 0.5876 0.0252 0.3030 0.122 Uiso 1 1 calc R . .
C132 C 0.6182(9) 0.1128(6) 0.2137(6) 0.081(2) Uiso 1 1 d GU . .
H115 H 0.5972 0.0901 0.1791 0.122 Uiso 1 1 calc R . .
H116 H 0.6443 0.1469 0.2139 0.122 Uiso 1 1 calc R . .
H117 H 0.5700 0.1197 0.2362 0.122 Uiso 1 1 calc R . .
C133 C 0.8209(10) 0.1221(6) 0.2009(6) 0.081(2) Uiso 1 1 d GU . .
H118 H 0.8230 0.1009 0.1645 0.122 Uiso 1 1 calc R . .
H119 H 0.8796 0.1329 0.2160 0.122 Uiso 1 1 calc R . .
H120 H 0.7899 0.1541 0.2056 0.122 Uiso 1 1 calc R . .
C134 C 0.9089(7) 0.0486(6) 0.2516(6) 0.081(2) Uiso 1 1 d GU . .
H121 H 0.9231 0.0185 0.2213 0.122 Uiso 1 1 calc R . .
H122 H 0.9232 0.0410 0.2820 0.122 Uiso 1 1 calc R . .
H123 H 0.9420 0.0813 0.2532 0.122 Uiso 1 1 calc R . .
C135 C 0.5472(6) 0.4337(4) 0.5363(4) 0.069(2) Uiso 1 1 d GU . .
C136 C 0.6040(6) 0.4583(4) 0.5117(4) 0.069(2) Uiso 1 1 d GU . .
C137 C 0.5808(7) 0.4365(4) 0.4589(4) 0.069(2) Uiso 1 1 d GU . .
C138 C 0.5097(7) 0.3983(4) 0.4508(4) 0.069(2) Uiso 1 1 d GU . .
C139 C 0.4889(6) 0.3966(4) 0.4987(4) 0.069(2) Uiso 1 1 d GU . .
C140 C 0.5486(9) 0.4450(5) 0.5925(4) 0.081(2) Uiso 1 1 d GU . .
H124 H 0.5106 0.4734 0.6090 0.122 Uiso 1 1 calc R . .
H125 H 0.6075 0.4564 0.6072 0.122 Uiso 1 1 calc R . .
H126 H 0.5288 0.4124 0.5980 0.122 Uiso 1 1 calc R . .
C141 C 0.6763(8) 0.5004(5) 0.5373(5) 0.081(2) Uiso 1 1 d GU . .
H127 H 0.6549 0.5361 0.5467 0.122 Uiso 1 1 calc R . .
H128 H 0.7227 0.4968 0.5138 0.122 Uiso 1 1 calc R . .
H129 H 0.6984 0.4956 0.5678 0.122 Uiso 1 1 calc R . .
C142 C 0.6241(10) 0.4512(6) 0.4185(5) 0.081(2) Uiso 1 1 d GU . .
H130 H 0.5950 0.4801 0.4133 0.122 Uiso 1 1 calc R . .
H131 H 0.6209 0.4198 0.3866 0.122 Uiso 1 1 calc R . .
H132 H 0.6846 0.4631 0.4292 0.122 Uiso 1 1 calc R . .
C143 C 0.4641(10) 0.3653(6) 0.4003(4) 0.081(2) Uiso 1 1 d GU . .
H133 H 0.4167 0.3847 0.3938 0.122 Uiso 1 1 calc R . .
H134 H 0.4412 0.3310 0.4009 0.122 Uiso 1 1 calc R . .
H135 H 0.5048 0.3589 0.3733 0.122 Uiso 1 1 calc R . .
C144 C 0.4175(8) 0.3615(5) 0.5079(5) 0.081(2) Uiso 1 1 d GU . .
H136 H 0.3642 0.3801 0.5133 0.122 Uiso 1 1 calc R . .
H137 H 0.4330 0.3538 0.5380 0.122 Uiso 1 1 calc R . .
H138 H 0.4087 0.3279 0.4783 0.122 Uiso 1 1 calc R . .
C145 C 0.78512(5) 0.02227(5) 0.60420(4) 0.094(3) Uiso 1 1 d GDU . .
C146 C 0.85421(7) 0.04336(6) 0.58583(4) 0.094(3) Uiso 1 1 d GDU . .
H139 H 0.8614 0.0314 0.5503 0.112 Uiso 1 1 calc R . .
C147 C 0.91275(9) 0.08199(8) 0.61944(5) 0.094(3) Uiso 1 1 d GDU . .
H140 H 0.9600 0.0964 0.6069 0.112 Uiso 1 1 calc R . .
C148 C 0.90219(9) 0.09952(7) 0.67142(5) 0.094(3) Uiso 1 1 d GDU . .
C149 C 0.83309(8) 0.07843(6) 0.68979(4) 0.094(3) Uiso 1 1 d GDU . .
H141 H 0.8259 0.0904 0.7253 0.112 Uiso 1 1 calc R . .
C150 C 0.77456(6) 0.03981(6) 0.65618(4) 0.094(3) Uiso 1 1 d GDU . .
H142 H 0.7273 0.0254 0.6687 0.112 Uiso 1 1 calc R . .
C151 C 0.96456(6) 0.13583(4) 0.71361(5) 0.127(4) Uiso 1 1 d DU . .
H143 H 0.9343 0.1482 0.7462 0.152 Uiso 1 1 calc R . .
C152 C 1.04196(10) 0.10494(5) 0.71957(11) 0.127(4) Uiso 1 1 d DU . .
H144 H 1.0215 0.0743 0.7281 0.191 Uiso 1 1 calc R . .
H145 H 1.0821 0.1288 0.7468 0.191 Uiso 1 1 calc R . .
H146 H 1.0714 0.0921 0.6876 0.191 Uiso 1 1 calc R . .
C153 C 0.99800(14) 0.18458(6) 0.70293(11) 0.127(4) Uiso 1 1 d DU . .
H147 H 0.9497 0.2053 0.7005 0.191 Uiso 1 1 calc R . .
H148 H 1.0271 0.1729 0.6708 0.191 Uiso 1 1 calc R . .
H149 H 1.0387 0.2069 0.7306 0.191 Uiso 1 1 calc R . .
C154 C 0.72627(13) -0.02219(11) 0.56706(7) 0.127(4) Uiso 1 1 d DU . .
H150 H 0.7478 -0.0568 0.5633 0.191 Uiso 1 1 calc R . .
H151 H 0.7246 -0.0184 0.5340 0.191 Uiso 1 1 calc R . .
H152 H 0.6682 -0.0203 0.5797 0.191 Uiso 1 1 calc R . .
C155 C 0.5560(2) 0.13990(4) 0.70566(7) 0.094(3) Uiso 1 1 d GDU . .
C156 C 0.6000(4) 0.18748(7) 0.73735(15) 0.094(3) Uiso 1 1 d GDU . .
H153 H 0.6323 0.1886 0.7667 0.112 Uiso 1 1 calc R . .
C157 C 0.5967(3) 0.23339(6) 0.72617(14) 0.094(3) Uiso 1 1 d GDU . .
H154 H 0.6267 0.2659 0.7478 0.112 Uiso 1 1 calc R . .
C158 C 0.5494(3) 0.23171(5) 0.68330(9) 0.094(3) Uiso 1 1 d GDU . .
C159 C 0.5055(5) 0.18413(8) 0.65161(18) 0.094(3) Uiso 1 1 d GDU . .
H155 H 0.4731 0.1830 0.6223 0.112 Uiso 1 1 calc R . .
C160 C 0.5088(4) 0.13822(7) 0.66279(16) 0.094(3) Uiso 1 1 d GDU . .
H156 H 0.4787 0.1057 0.6411 0.112 Uiso 1 1 calc R . .
C161 C 0.53012(13) 0.27855(5) 0.66848(6) 0.127(4) Uiso 1 1 d DU . .
H157 H 0.4824 0.2975 0.6890 0.152 Uiso 1 1 calc R . .
C162 C 0.61064(16) 0.31821(10) 0.67948(13) 0.127(4) Uiso 1 1 d DU . .
H158 H 0.6284 0.3308 0.7156 0.191 Uiso 1 1 calc R . .
H159 H 0.5971 0.3488 0.6706 0.191 Uiso 1 1 calc R . .
H160 H 0.6575 0.3002 0.6591 0.191 Uiso 1 1 calc R . .
C163 C 0.5028(3) 0.26017(11) 0.61241(9) 0.127(4) Uiso 1 1 d DU . .
H161 H 0.4515 0.2352 0.6050 0.191 Uiso 1 1 calc R . .
H162 H 0.5496 0.2422 0.5919 0.191 Uiso 1 1 calc R . .
H163 H 0.4898 0.2913 0.6042 0.191 Uiso 1 1 calc R . .
C164 C 0.5646(4) 0.09019(7) 0.71734(16) 0.127(4) Uiso 1 1 d DU . .
H164 H 0.5194 0.0874 0.7397 0.191 Uiso 1 1 calc R . .
H165 H 0.6211 0.0923 0.7342 0.191 Uiso 1 1 calc R . .
H166 H 0.5589 0.0586 0.6857 0.191 Uiso 1 1 calc R . .
Co5 Co 0.8473(2) 0.31542(14) 0.35077(13) 0.0383(13) Uani 1 1 d U . .
Co6 Co 0.9646(2) 0.11224(13) 0.44588(12) 0.0303(12) Uani 1 1 d U . .
Co7 Co 0.8483(2) 0.37025(14) 0.61491(13) 0.0391(13) Uani 1 1 d U . .
Co8 Co 0.5317(2) 0.17615(15) 0.44454(14) 0.0435(13) Uani 1 1 d U . .
Cs2 Cs 0.79783(12) 0.24605(7) 0.46218(6) 0.0372(6) Uani 1 1 d U . .
Ru7 Ru 1.07362(14) 0.30678(9) 0.48184(8) 0.0351(8) Uani 1 1 d U . .
Ru8 Ru 0.75279(16) 0.11664(9) 0.30808(8) 0.0409(9) Uani 1 1 d U . .
Ru9 Ru 0.61908(15) 0.37458(9) 0.48463(9) 0.0404(9) Uani 1 1 d U . .
Ru10 Ru 0.74673(15) 0.17642(9) 0.58210(8) 0.0368(8) Uani 1 1 d U . .
Ru11 Ru 0.78123(17) 0.10769(10) 0.63035(9) 0.0501(9) Uani 1 1 d U . .
Ru12 Ru 0.63886(17) 0.16655(11) 0.65666(9) 0.0656(9) Uani 1 1 d U . .
S3 S 0.6649(5) 0.1046(3) 0.5810(3) 0.052(2) Uani 1 1 d U . .
S4 S 0.7781(5) 0.1970(3) 0.6641(3) 0.055(2) Uani 1 1 d U . .
P1 P 1.2375(5) 0.0760(3) 0.2867(3) 0.100(4) Uiso 1 1 d GDU . .
F1 F 1.3351(6) 0.0950(6) 0.2858(5) 0.145(8) Uiso 1 1 d GDU . .
F2 F 1.1399(6) 0.0570(6) 0.2876(6) 0.238(13) Uiso 1 1 d GDU . .
F3 F 1.2514(10) 0.0844(6) 0.3446(3) 0.165(9) Uiso 1 1 d GDU . .
F4 F 1.2236(9) 0.0676(6) 0.2288(3) 0.157(9) Uiso 1 1 d GDU . .
F5 F 1.2625(10) 0.0162(3) 0.2709(5) 0.191(11) Uiso 1 1 d GDU . .
F6 F 1.2126(10) 0.1358(4) 0.3026(5) 0.222(12) Uiso 1 1 d GDU . .
P2 P 1.2442(8) 0.1201(5) 0.5886(4) 0.101(4) Uiso 0.568(12) 1 d PGU C 1
F7 F 1.2635(14) 0.1031(8) 0.6352(6) 0.106(4) Uiso 0.568(12) 1 d PGU C 1
F8 F 1.2249(14) 0.1371(9) 0.5420(6) 0.129(7) Uiso 0.568(12) 1 d PGU C 1
F9 F 1.2990(13) 0.1750(6) 0.6166(8) 0.127(7) Uiso 0.568(12) 1 d PGU C 1
F10 F 1.1893(13) 0.0652(6) 0.5606(7) 0.104(6) Uiso 0.568(12) 1 d PGU C 1
F11 F 1.1607(11) 0.1465(8) 0.6140(8) 0.112(5) Uiso 0.568(12) 1 d PGU C 1
F12 F 1.3276(11) 0.0937(8) 0.5632(7) 0.116(7) Uiso 0.568(12) 1 d PGU C 1
P5 P 1.2170(11) 0.1025(7) 0.5894(6) 0.093(5) Uiso 0.432(12) 1 d PGU C 2
F25 F 1.1928(19) 0.0474(8) 0.5440(8) 0.107(8) Uiso 0.432(12) 1 d PGU C 2
F26 F 1.2412(19) 0.1576(8) 0.6347(8) 0.115(5) Uiso 0.432(12) 1 d PGU C 2
F27 F 1.3135(12) 0.0877(11) 0.5898(11) 0.113(5) Uiso 0.432(12) 1 d PGU C 2
F28 F 1.1204(12) 0.1173(12) 0.5889(11) 0.115(8) Uiso 0.432(12) 1 d PGU C 2
F29 F 1.1962(19) 0.0752(11) 0.6287(9) 0.110(8) Uiso 0.432(12) 1 d PGU C 2
F30 F 1.2378(19) 0.1299(11) 0.5500(9) 0.120(6) Uiso 0.432(12) 1 d PGU C 2
P3 P 0.6399(6) 0.3780(3) -0.1362(3) 0.144(5) Uiso 1 1 d GU . .
F13 F 0.6040(11) 0.3176(4) -0.1635(6) 0.215(12) Uiso 1 1 d GU . .
F14 F 0.6757(11) 0.4383(4) -0.1088(6) 0.234(13) Uiso 1 1 d GU . .
F15 F 0.5997(11) 0.3916(7) -0.1813(5) 0.237(13) Uiso 1 1 d GU . .
F16 F 0.6800(10) 0.3643(7) -0.0911(5) 0.168(10) Uiso 1 1 d GU . .
F17 F 0.7262(8) 0.3647(7) -0.1648(6) 0.225(12) Uiso 1 1 d GU . .
F18 F 0.5536(8) 0.3912(7) -0.1075(6) 0.218(12) Uiso 1 1 d GU . .
P4 P 0.8042(14) 0.4637(8) 0.2369(8) 0.212(5) Uiso 0.50(2) 1 d PGU D 1
F19 F 0.823(3) 0.4027(9) 0.2192(14) 0.216(6) Uiso 0.50(2) 1 d PGU D 1
F20 F 0.786(3) 0.5248(9) 0.2546(13) 0.216(5) Uiso 0.50(2) 1 d PGU D 1
F21 F 0.8848(19) 0.4744(17) 0.2085(14) 0.215(5) Uiso 0.50(2) 1 d PGU D 1
F22 F 0.7235(18) 0.4530(17) 0.2653(14) 0.222(6) Uiso 0.50(2) 1 d PGU D 1
F23 F 0.863(2) 0.4765(14) 0.2867(10) 0.198(6) Uiso 0.50(2) 1 d PGU D 1
F24 F 0.745(2) 0.4509(14) 0.1871(10) 0.213(9) Uiso 0.50(2) 1 d PGU D 1
P6 P 0.8100(14) 0.4668(9) 0.2397(8) 0.208(5) Uiso 0.50(2) 1 d PGU D 2
F31 F 0.867(2) 0.4381(16) 0.1936(11) 0.213(5) Uiso 0.50(2) 1 d PGU D 2
F32 F 0.753(2) 0.4955(17) 0.2859(11) 0.219(7) Uiso 0.50(2) 1 d PGU D 2
F33 F 0.855(3) 0.5229(11) 0.2451(15) 0.216(7) Uiso 0.50(2) 1 d PGU D 2
F34 F 0.765(3) 0.4107(12) 0.2344(15) 0.218(6) Uiso 0.50(2) 1 d PGU D 2
F35 F 0.881(2) 0.4613(16) 0.2777(12) 0.195(9) Uiso 0.50(2) 1 d PGU D 2
F36 F 0.739(2) 0.4723(16) 0.2017(12) 0.214(7) Uiso 0.50(2) 1 d PGU D 2
C165 C 0.7064(17) 0.0447(9) 0.4333(8) 0.126(8) Uiso 1 1 d GU . .
H207 H 0.7434 0.0153 0.4290 0.189 Uiso 1 1 d G . .
H208 H 0.7095 0.0690 0.4690 0.189 Uiso 1 1 d G . .
H209 H 0.7258 0.0645 0.4122 0.189 Uiso 1 1 d G . .
C166 C 0.6201(17) 0.0235(8) 0.4182(7) 0.140(7) Uiso 1 1 d GU . .
N166 N 0.5508(17) 0.0065(11) 0.4061(9) 0.153(8) Uiso 1 1 d GU . .
C167 C 0.5149(15) 0.2801(9) 0.9205(8) 0.099(8) Uiso 1 1 d GU . .
H210 H 0.5547 0.3110 0.9241 0.148 Uiso 1 1 d G . .
H211 H 0.5174 0.2731 0.9520 0.148 Uiso 1 1 d G . .
H212 H 0.4562 0.2878 0.9136 0.148 Uiso 1 1 d G . .
C168 C 0.5388(12) 0.2345(9) 0.8796(7) 0.107(7) Uiso 1 1 d GU . .
N168 N 0.5579(17) 0.1979(10) 0.8468(8) 0.126(8) Uiso 1 1 d GU . .
C169 C 0.0839(14) 0.2315(9) 0.2830(8) 0.091(7) Uiso 1 1 d GU . .
H213 H 0.0624 0.2160 0.2474 0.136 Uiso 1 1 d G . .
H214 H 0.1467 0.2309 0.2848 0.136 Uiso 1 1 d G . .
H215 H 0.0681 0.2685 0.2982 0.136 Uiso 1 1 d G . .
C170 C 0.0470(12) 0.2010(8) 0.3099(7) 0.107(7) Uiso 1 1 d GU . .
N170 N 0.0174(16) 0.1766(10) 0.3314(9) 0.120(8) Uiso 1 1 d GU . .
C171 C 0.5456(16) 0.3738(9) 0.1932(9) 0.112(8) Uiso 1 1 d GU . .
H216 H 0.5700 0.3479 0.1633 0.168 Uiso 1 1 d G . .
H217 H 0.5741 0.4094 0.2007 0.168 Uiso 1 1 d G . .
H218 H 0.4838 0.3745 0.1863 0.168 Uiso 1 1 d G . .
C172 C 0.5583(12) 0.3584(7) 0.2355(8) 0.119(7) Uiso 1 1 d GU . .
N172 N 0.5686(18) 0.3461(10) 0.2694(9) 0.133(8) Uiso 1 1 d GU . .
C173 C 0.0241(13) 0.2313(7) 0.5940(7) 0.057(7) Uiso 1 1 d GU . .
H219 H 0.0772 0.2159 0.5794 0.086 Uiso 1 1 d G . .
H220 H -0.0027 0.2476 0.5722 0.086 Uiso 1 1 d G . .
H221 H -0.0158 0.2031 0.5966 0.086 Uiso 1 1 d G . .
C174 C 0.0437(10) 0.2711(7) 0.6432(7) 0.067(6) Uiso 1 1 d GU . .
N174 N 0.0594(14) 0.3030(8) 0.6826(7) 0.077(7) Uiso 1 1 d GU . .
C175 C 0.8963(14) 0.4358(8) 0.4976(7) 0.084(7) Uiso 1 1 d GU . .
H222 H 0.8333 0.4304 0.4949 0.126 Uiso 1 1 d G . .
H223 H 0.9209 0.4031 0.4973 0.126 Uiso 1 1 d G . .
H224 H 0.9164 0.4442 0.4688 0.126 Uiso 1 1 d G . .
C176 C 0.9227(10) 0.4788(7) 0.5437(7) 0.078(6) Uiso 1 1 d GU . .
N176 N 0.9439(14) 0.5134(8) 0.5807(7) 0.081(7) Uiso 1 1 d GU . .
C177 C 0.0698(19) 0.1757(11) 0.9043(10) 0.172(9) Uiso 1 1 d GU . .
H225 H 0.0722 0.1685 0.9357 0.259 Uiso 1 1 d G . .
H226 H 0.0107 0.1824 0.8969 0.259 Uiso 1 1 d G . .
H227 H 0.1083 0.2073 0.9084 0.259 Uiso 1 1 d G . .
C178 C 0.0960(15) 0.1308(10) 0.8636(9) 0.177(7) Uiso 1 1 d GU . .
N178 N 0.117(2) 0.0947(12) 0.8309(10) 0.184(9) Uiso 1 1 d GU . .
C179 C 0.211(2) 0.4426(12) 0.0601(11) 0.213(9) Uiso 1 1 d GU . .
H228 H 0.2354 0.4673 0.0933 0.319 Uiso 1 1 d G . .
H229 H 0.2416 0.4497 0.0332 0.319 Uiso 1 1 d G . .
H230 H 0.2178 0.4057 0.0570 0.319 Uiso 1 1 d G . .
C180 C 0.122(2) 0.4503(9) 0.0554(8) 0.217(8) Uiso 1 1 d GU . .
N180 N 0.051(2) 0.4564(14) 0.0516(13) 0.223(9) Uiso 1 1 d GU . .
C181 C 0.1022(16) 0.2505(9) 0.1736(8) 0.110(8) Uiso 1 1 d GU . .
H231 H 0.1263 0.2280 0.1418 0.165 Uiso 1 1 d G . .
H232 H 0.1219 0.2396 0.2012 0.165 Uiso 1 1 d G . .
H233 H 0.1216 0.2881 0.1815 0.165 Uiso 1 1 d G . .
C182 C 0.0110(16) 0.2442(7) 0.1683(6) 0.122(7) Uiso 1 1 d GU . .
N182 N -0.0623(16) 0.2393(10) 0.1640(9) 0.128(8) Uiso 1 1 d GU . .
C183 C 0.4318(19) 0.0868(11) 0.0329(10) 0.173(9) Uiso 1 1 d GU . .
H234 H 0.3689 0.0824 0.0283 0.260 Uiso 1 1 d G . .
H235 H 0.4570 0.0778 -0.0002 0.260 Uiso 1 1 d G . .
H236 H 0.4497 0.1240 0.0544 0.260 Uiso 1 1 d G . .
C184 C 0.4605(15) 0.0522(10) 0.0566(8) 0.184(8) Uiso 1 1 d GU . .
N184 N 0.483(2) 0.0244(12) 0.0756(11) 0.198(9) Uiso 1 1 d GU . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
0.00 -1.00 1.00 0.0100
0.00 1.00 -1.00 0.0100
0.00 1.00 1.00 0.0350
0.00 -1.00 -1.00 0.0350
-1.00 0.00 0.00 0.1200
1.00 0.00 0.00 0.1200
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 C1 Co1 169.8(19) . . ?
N1 C1 Cs1 74.0(15) . . ?
Co1 C1 Cs1 97.5(7) . . ?
N2 C2 Co1 178(2) . . ?
N2 C2 Cs1 79.1(14) . . ?
Co1 C2 Cs1 101.1(7) . . ?
N3 C3 Co1 177(3) . . ?
N3 C3 Cs1 74.6(17) . . ?
Co1 C3 Cs1 102.7(11) . . ?
N4 C4 Co2 178(2) . . ?
N4 C4 Cs1 76.8(15) . . ?
Co2 C4 Cs1 103.7(8) . . ?
N5 C5 Co2 178(2) . . ?
N5 C5 Cs1 84.6(14) . . ?
Co2 C5 Cs1 97.4(8) . . ?
N6 C6 Co2 175(2) . . ?
N6 C6 Cs1 81.3(15) . . ?
Co2 C6 Cs1 103.4(8) . . ?
N7 C7 Co3 176.1(18) . . ?
N7 C7 Cs1 83.2(13) . . ?
Co3 C7 Cs1 100.7(7) . . ?
N8 C8 Co3 180(3) . . ?
N8 C8 Cs1 84.9(15) . . ?
Co3 C8 Cs1 95.1(8) . . ?
N9 C9 Co3 172(3) . . ?
N9 C9 Cs1 82.1(19) . . ?
Co3 C9 Cs1 102.0(9) . . ?
N10 C10 Co4 174(2) . . ?
N10 C10 Cs1 73.4(14) . . ?
Co4 C10 Cs1 101.6(8) . . ?
N11 C11 Co4 178(2) . . ?
N11 C11 Cs1 80.2(16) . . ?
Co4 C11 Cs1 99.3(8) . . ?
N12 C12 Co4 177(2) . . ?
N12 C12 Cs1 77.4(16) . . ?
Co4 C12 Cs1 99.7(9) . . ?
C1 N1 Ru2 170.3(19) . . ?
C1 N1 Cs1 87.4(15) . . ?
Ru2 N1 Cs1 99.2(7) . . ?
C2 N2 Ru1 176.4(19) . . ?
C2 N2 Cs1 82.1(14) . . ?
Ru1 N2 Cs1 99.4(6) . . ?
C3 N3 Ru3 177(2) . . ?
C3 N3 Cs1 86.6(18) . . ?
Ru3 N3 Cs1 96.8(7) . . ?
C4 N4 Ru2 176(2) . . ?
C4 N4 Cs1 84.4(15) . . ?
Ru2 N4 Cs1 97.8(6) . . ?
C5 N5 Ru4 174.9(17) . . ?
C6 N6 Ru3 174.8(19) . . ?
C6 N6 Cs1 80.2(15) . . ?
Ru3 N6 Cs1 97.1(6) . . ?
C7 N7 Ru1 176.0(17) . . ?
C7 N7 Cs1 78.1(13) . . ?
Ru1 N7 Cs1 98.5(6) . . ?
C8 N8 Ru4 176.5(19) . . ?
C9 N9 Ru3 171(2) . . ?
C9 N9 Cs1 78.9(19) . . ?
Ru3 N9 Cs1 97.8(8) . . ?
C10 N10 Ru2 167.3(19) . . ?
C10 N10 Cs1 87.3(15) . . ?
Ru2 N10 Cs1 103.7(6) . . ?
C11 N11 Ru1 179(2) . . ?
C11 N11 Cs1 81.3(16) . . ?
Ru1 N11 Cs1 98.2(7) . . ?
C12 N12 Ru4 169(2) . . ?
C12 N12 Cs1 83.9(17) . . ?
Ru4 N12 Cs1 106.8(7) . . ?
C14 C13 C17 108.0 . . ?
C14 C13 Co1 70.8(7) . . ?
C17 C13 Co1 69.4(7) . . ?
C14 C13 H1 126.0 . . ?
C17 C13 H1 126.0 . . ?
Co1 C13 H1 125.4 . . ?
C15 C14 C13 108.0 . . ?
C15 C14 Co1 70.1(6) . . ?
C13 C14 Co1 69.3(7) . . ?
C15 C14 H2 126.0 . . ?
C13 C14 H2 126.0 . . ?
Co1 C14 H2 126.2 . . ?
C16 C15 C14 108.0 . . ?
C16 C15 Co1 69.3(7) . . ?
C14 C15 Co1 70.1(6) . . ?
C16 C15 H3 126.0 . . ?
C14 C15 H3 126.0 . . ?
Co1 C15 H3 126.2 . . ?
C17 C16 C15 108.0 . . ?
C17 C16 Co1 69.4(6) . . ?
C15 C16 Co1 70.8(7) . . ?
C17 C16 H4 126.0 . . ?
C15 C16 H4 126.0 . . ?
Co1 C16 H4 125.4 . . ?
C16 C17 C13 108.0 . . ?
C16 C17 Co1 70.3(6) . . ?
C13 C17 Co1 70.3(6) . . ?
C16 C17 H5 126.0 . . ?
C13 C17 H5 126.0 . . ?
Co1 C17 H5 125.0 . . ?
C19 C18 C22 108.0 . . ?
C19 C18 Co2 71.5(7) . . ?
C22 C18 Co2 70.2(7) . . ?
C19 C18 H6 126.0 . . ?
C22 C18 H6 126.0 . . ?
Co2 C18 H6 123.9 . . ?
C20 C19 C18 108.0 . . ?
C20 C19 Co2 71.7(6) . . ?
C18 C19 Co2 68.4(7) . . ?
C20 C19 H7 126.0 . . ?
C18 C19 H7 126.0 . . ?
Co2 C19 H7 125.5 . . ?
C21 C20 C19 108.0 . . ?
C21 C20 Co2 69.7(7) . . ?
C19 C20 Co2 68.9(6) . . ?
C21 C20 H8 126.0 . . ?
C19 C20 H8 126.0 . . ?
Co2 C20 H8 126.9 . . ?
C20 C21 C22 108.0 . . ?
C20 C21 Co2 71.1(7) . . ?
C22 C21 Co2 68.2(6) . . ?
C20 C21 H9 126.0 . . ?
C22 C21 H9 126.0 . . ?
Co2 C21 H9 126.2 . . ?
C21 C22 C18 108.0 . . ?
C21 C22 Co2 71.9(6) . . ?
C18 C22 Co2 69.3(7) . . ?
C21 C22 H10 126.0 . . ?
C18 C22 H10 126.0 . . ?
Co2 C22 H10 124.4 . . ?
C27 C23 C24 108.0 . . ?
C27 C23 Co3 70.1(7) . . ?
C24 C23 Co3 69.7(7) . . ?
C27 C23 H11 126.0 . . ?
C24 C23 H11 126.0 . . ?
Co3 C23 H11 125.8 . . ?
C23 C24 C25 108.0 . . ?
C23 C24 Co3 71.1(6) . . ?
C25 C24 Co3 69.4(7) . . ?
C23 C24 H12 126.0 . . ?
C25 C24 H12 126.0 . . ?
Co3 C24 H12 125.1 . . ?
C26 C25 C24 108.0 . . ?
C26 C25 Co3 70.3(7) . . ?
C24 C25 Co3 71.0(7) . . ?
C26 C25 H13 126.0 . . ?
C24 C25 H13 126.0 . . ?
Co3 C25 H13 124.3 . . ?
C25 C26 C27 108.0 . . ?
C25 C26 Co3 69.9(7) . . ?
C27 C26 Co3 71.2(6) . . ?
C25 C26 H14 126.0 . . ?
C27 C26 H14 126.0 . . ?
Co3 C26 H14 124.5 . . ?
C26 C27 C23 108.0 . . ?
C26 C27 Co3 69.3(7) . . ?
C23 C27 Co3 70.8(7) . . ?
C26 C27 H15 126.0 . . ?
C23 C27 H15 126.0 . . ?
Co3 C27 H15 125.5 . . ?
C29 C28 C32 108.0 . . ?
C29 C28 Co4 69.7(8) . . ?
C32 C28 Co4 71.3(7) . . ?
C29 C28 H16 126.0 . . ?
C32 C28 H16 126.0 . . ?
Co4 C28 H16 124.6 . . ?
C28 C29 C30 108.0 . . ?
C28 C29 Co4 69.8(7) . . ?
C30 C29 Co4 71.2(6) . . ?
C28 C29 H17 126.0 . . ?
C30 C29 H17 126.0 . . ?
Co4 C29 H17 124.6 . . ?
C31 C30 C29 108.0 . . ?
C31 C30 Co4 71.0(7) . . ?
C29 C30 Co4 68.6(6) . . ?
C31 C30 H18 126.0 . . ?
C29 C30 H18 126.0 . . ?
Co4 C30 H18 125.9 . . ?
C32 C31 C30 108.0 . . ?
C32 C31 Co4 69.4(7) . . ?
C30 C31 Co4 69.4(8) . . ?
C32 C31 H19 126.0 . . ?
C30 C31 H19 126.0 . . ?
Co4 C31 H19 126.8 . . ?
C31 C32 C28 108.0 . . ?
C31 C32 Co4 71.0(7) . . ?
C28 C32 Co4 68.6(6) . . ?
C31 C32 H20 126.0 . . ?
C28 C32 H20 126.0 . . ?
Co4 C32 H20 126.0 . . ?
C34 C33 C37 108.0 . . ?
C34 C33 C38 126.0 . . ?
C37 C33 C38 126.0 . . ?
C34 C33 Ru1 70.9(7) . . ?
C37 C33 Ru1 72.8(7) . . ?
C38 C33 Ru1 122.1(7) . . ?
C33 C34 C35 108.0 . . ?
C33 C34 C39 126.0 . . ?
C35 C34 C39 126.0 . . ?
C33 C34 Ru1 70.8(7) . . ?
C35 C34 Ru1 72.8(7) . . ?
C39 C34 Ru1 122.1(7) . . ?
C36 C35 C34 108.0 . . ?
C36 C35 C40 126.0 . . ?
C34 C35 C40 126.0 . . ?
C36 C35 Ru1 72.4(7) . . ?
C34 C35 Ru1 69.3(6) . . ?
C40 C35 Ru1 123.9(6) . . ?
C37 C36 C35 108.0 . . ?
C37 C36 C41 126.0 . . ?
C35 C36 C41 126.0 . . ?
C37 C36 Ru1 70.3(7) . . ?
C35 C36 Ru1 70.4(7) . . ?
C41 C36 Ru1 125.0(6) . . ?
C36 C37 C33 108.0 . . ?
C36 C37 C42 126.0 . . ?
C33 C37 C42 126.0 . . ?
C36 C37 Ru1 72.5(7) . . ?
C33 C37 Ru1 69.3(6) . . ?
C42 C37 Ru1 123.8(7) . . ?
C33 C38 H167 109.5 . . ?
C33 C38 H168 109.5 . . ?
H167 C38 H168 109.5 . . ?
C33 C38 H169 109.5 . . ?
H167 C38 H169 109.5 . . ?
H168 C38 H169 109.5 . . ?
C34 C39 H170 109.5 . . ?
C34 C39 H171 109.5 . . ?
H170 C39 H171 109.5 . . ?
C34 C39 H172 109.5 . . ?
H170 C39 H172 109.5 . . ?
H171 C39 H172 109.5 . . ?
C35 C40 H173 109.5 . . ?
C35 C40 H174 109.5 . . ?
H173 C40 H174 109.5 . . ?
C35 C40 H175 109.5 . . ?
H173 C40 H175 109.5 . . ?
H174 C40 H175 109.5 . . ?
C36 C41 H176 109.5 . . ?
C36 C41 H177 109.5 . . ?
H176 C41 H177 109.5 . . ?
C36 C41 H178 109.5 . . ?
H176 C41 H178 109.5 . . ?
H177 C41 H178 109.5 . . ?
C37 C42 H179 109.5 . . ?
C37 C42 H180 109.5 . . ?
H179 C42 H180 109.5 . . ?
C37 C42 H181 109.5 . . ?
H179 C42 H181 109.5 . . ?
H180 C42 H181 109.5 . . ?
C186 C185 C189 108.0 . . ?
C186 C185 C190 126.0 . . ?
C189 C185 C190 126.0 . . ?
C186 C185 Ru1 72.0(14) . . ?
C189 C185 Ru1 70.0(15) . . ?
C190 C185 Ru1 123.7(13) . . ?
C185 C186 C187 108.0 . . ?
C185 C186 C191 126.0 . . ?
C187 C186 C191 126.0 . . ?
C185 C186 Ru1 69.3(13) . . ?
C187 C186 Ru1 71.3(13) . . ?
C191 C186 Ru1 125.1(13) . . ?
C188 C187 C186 108.0 . . ?
C188 C187 C192 126.0 . . ?
C186 C187 C192 126.0 . . ?
C188 C187 Ru1 69.7(14) . . ?
C186 C187 Ru1 70.4(13) . . ?
C192 C187 Ru1 125.5(12) . . ?
C189 C188 C187 108.0 . . ?
C189 C188 C193 126.0 . . ?
C187 C188 C193 126.0 . . ?
C189 C188 Ru1 69.4(13) . . ?
C187 C188 Ru1 71.8(14) . . ?
C193 C188 Ru1 124.4(12) . . ?
C188 C189 C185 108.0 . . ?
C188 C189 C194 126.0 . . ?
C185 C189 C194 126.0 . . ?
C188 C189 Ru1 71.6(14) . . ?
C185 C189 Ru1 70.8(14) . . ?
C194 C189 Ru1 123.3(14) . . ?
C185 C190 H182 109.5 . . ?
C185 C190 H183 109.5 . . ?
H182 C190 H183 109.5 . . ?
C185 C190 H184 109.5 . . ?
H182 C190 H184 109.5 . . ?
H183 C190 H184 109.5 . . ?
C186 C191 H185 109.5 . . ?
C186 C191 H186 109.5 . . ?
H185 C191 H186 109.5 . . ?
C186 C191 H187 109.5 . . ?
H185 C191 H187 109.5 . . ?
H186 C191 H187 109.5 . . ?
C187 C192 H188 109.5 . . ?
C187 C192 H189 109.5 . . ?
H188 C192 H189 109.5 . . ?
C187 C192 H190 109.5 . . ?
H188 C192 H190 109.5 . . ?
H189 C192 H190 109.5 . . ?
C188 C193 H191 109.5 . . ?
C188 C193 H192 109.5 . . ?
H191 C193 H192 109.5 . . ?
C188 C193 H193 109.5 . . ?
H191 C193 H193 109.5 . . ?
H192 C193 H193 109.5 . . ?
C189 C194 H194 109.5 . . ?
C189 C194 H195 109.5 . . ?
H194 C194 H195 109.5 . . ?
C189 C194 H196 109.5 . . ?
H194 C194 H196 109.5 . . ?
H195 C194 H196 109.5 . . ?
C44 C43 C47 108.0 . . ?
C44 C43 C48 126.0 . . ?
C47 C43 C48 126.0 . . ?
C44 C43 Ru2 69.8(4) . . ?
C47 C43 Ru2 72.5(5) . . ?
C48 C43 Ru2 123.3(4) . . ?
C45 C44 C43 108.0 . . ?
C45 C44 C49 126.0 . . ?
C43 C44 C49 126.0 . . ?
C45 C44 Ru2 72.0(5) . . ?
C43 C44 Ru2 70.9(4) . . ?
C49 C44 Ru2 122.8(4) . . ?
C44 C45 C46 108.0 . . ?
C44 C45 C50 126.0 . . ?
C46 C45 C50 126.0 . . ?
C44 C45 Ru2 69.0(5) . . ?
C46 C45 Ru2 72.3(4) . . ?
C50 C45 Ru2 124.3(4) . . ?
C47 C46 C45 108.0 . . ?
C47 C46 C51 126.0 . . ?
C45 C46 C51 126.0 . . ?
C47 C46 Ru2 70.4(4) . . ?
C45 C46 Ru2 69.4(4) . . ?
C51 C46 Ru2 125.7(4) . . ?
C46 C47 C43 108.0 . . ?
C46 C47 C52 126.0 . . ?
C43 C47 C52 126.0 . . ?
C46 C47 Ru2 71.5(4) . . ?
C43 C47 Ru2 68.9(5) . . ?
C52 C47 Ru2 125.2(4) . . ?
C43 C48 H21 109.5 . . ?
C43 C48 H22 109.5 . . ?
H21 C48 H22 109.5 . . ?
C43 C48 H23 109.5 . . ?
H21 C48 H23 109.5 . . ?
H22 C48 H23 109.5 . . ?
C44 C49 H24 109.5 . . ?
C44 C49 H25 109.5 . . ?
H24 C49 H25 109.5 . . ?
C44 C49 H26 109.5 . . ?
H24 C49 H26 109.5 . . ?
H25 C49 H26 109.5 . . ?
C45 C50 H27 109.5 . . ?
C45 C50 H28 109.5 . . ?
H27 C50 H28 109.5 . . ?
C45 C50 H29 109.5 . . ?
H27 C50 H29 109.5 . . ?
H28 C50 H29 109.5 . . ?
C46 C51 H30 109.5 . . ?
C46 C51 H31 109.5 . . ?
H30 C51 H31 109.5 . . ?
C46 C51 H32 109.5 . . ?
H30 C51 H32 109.5 . . ?
H31 C51 H32 109.5 . . ?
C47 C52 H33 109.5 . . ?
C47 C52 H34 109.5 . . ?
H33 C52 H34 109.5 . . ?
C47 C52 H35 109.5 . . ?
H33 C52 H35 109.5 . . ?
H34 C52 H35 109.5 . . ?
C54 C53 C57 108.0 . . ?
C54 C53 C58 126.0 . . ?
C57 C53 C58 126.0 . . ?
C54 C53 Ru3 73.2(5) . . ?
C57 C53 Ru3 67.2(5) . . ?
C58 C53 Ru3 125.1(4) . . ?
C55 C54 C53 108.0 . . ?
C55 C54 C59 126.0 . . ?
C53 C54 C59 126.0 . . ?
C55 C54 Ru3 69.0(4) . . ?
C53 C54 Ru3 69.5(5) . . ?
C59 C54 Ru3 127.1(4) . . ?
C56 C55 C54 108.0 . . ?
C56 C55 C60 126.0 . . ?
C54 C55 C60 126.0 . . ?
C56 C55 Ru3 67.3(5) . . ?
C54 C55 Ru3 73.5(4) . . ?
C60 C55 Ru3 124.7(4) . . ?
C55 C56 C57 108.0 . . ?
C55 C56 C61 126.0 . . ?
C57 C56 C61 126.0 . . ?
C55 C56 Ru3 74.0(5) . . ?
C57 C56 Ru3 70.5(5) . . ?
C61 C56 Ru3 121.3(4) . . ?
C56 C57 C53 108.0 . . ?
C56 C57 C62 126.0 . . ?
C53 C57 C62 126.0 . . ?
C56 C57 Ru3 69.9(5) . . ?
C53 C57 Ru3 74.2(5) . . ?
C62 C57 Ru3 121.6(5) . . ?
C53 C58 H36 109.5 . . ?
C53 C58 H37 109.5 . . ?
H36 C58 H37 109.5 . . ?
C53 C58 H38 109.5 . . ?
H36 C58 H38 109.5 . . ?
H37 C58 H38 109.5 . . ?
C54 C59 H39 109.5 . . ?
C54 C59 H40 109.5 . . ?
H39 C59 H40 109.5 . . ?
C54 C59 H41 109.5 . . ?
H39 C59 H41 109.5 . . ?
H40 C59 H41 109.5 . . ?
C55 C60 H42 109.5 . . ?
C55 C60 H43 109.5 . . ?
H42 C60 H43 109.5 . . ?
C55 C60 H44 109.5 . . ?
H42 C60 H44 109.5 . . ?
H43 C60 H44 109.5 . . ?
C56 C61 H45 109.5 . . ?
C56 C61 H46 109.5 . . ?
H45 C61 H46 109.5 . . ?
C56 C61 H47 109.5 . . ?
H45 C61 H47 109.5 . . ?
H46 C61 H47 109.5 . . ?
C57 C62 H48 109.5 . . ?
C57 C62 H49 109.5 . . ?
H48 C62 H49 109.5 . . ?
C57 C62 H50 109.5 . . ?
H48 C62 H50 109.5 . . ?
H49 C62 H50 109.5 . . ?
C64 C63 C68 120.0 . . ?
C64 C63 C72 118.73(8) . . ?
C68 C63 C72 121.27(8) . . ?
C64 C63 Ru5 72.9(4) . . ?
C68 C63 Ru5 71.0(4) . . ?
C72 C63 Ru5 128.27(14) . . ?
C63 C64 C65 120.0 . . ?
C63 C64 Ru5 70.2(3) . . ?
C65 C64 Ru5 72.76(10) . . ?
C63 C64 H51 120.0 . . ?
C65 C64 H51 120.0 . . ?
Ru5 C64 H51 129.4 . . ?
C66 C65 C64 120.0 . . ?
C66 C65 Ru5 71.5(3) . . ?
C64 C65 Ru5 70.85(11) . . ?
C66 C65 H52 120.0 . . ?
C64 C65 H52 120.0 . . ?
Ru5 C65 H52 130.2 . . ?
C65 C66 C67 120.0 . . ?
C65 C66 C69 127.47(7) . . ?
C67 C66 C69 112.53(7) . . ?
C65 C66 Ru5 72.2(4) . . ?
C67 C66 Ru5 70.4(4) . . ?
C69 C66 Ru5 129.34(11) . . ?
C68 C67 C66 120.0 . . ?
C68 C67 Ru5 70.46(10) . . ?
C66 C67 Ru5 73.0(3) . . ?
C68 C67 H53 120.0 . . ?
C66 C67 H53 120.0 . . ?
Ru5 C67 H53 128.8 . . ?
C67 C68 C63 120.0 . . ?
C67 C68 Ru5 72.40(11) . . ?
C63 C68 Ru5 71.7(3) . . ?
C67 C68 H54 120.0 . . ?
C63 C68 H54 120.0 . . ?
Ru5 C68 H54 128.0 . . ?
C66 C69 C71 111.56(9) . . ?
C66 C69 C70 110.17(9) . . ?
C71 C69 C70 108.68(10) . . ?
C66 C69 H55 108.8 . . ?
C71 C69 H55 108.8 . . ?
C70 C69 H55 108.8 . . ?
C69 C70 H56 109.5 . . ?
C69 C70 H57 109.5 . . ?
H56 C70 H57 109.5 . . ?
C69 C70 H58 109.5 . . ?
H56 C70 H58 109.5 . . ?
H57 C70 H58 109.5 . . ?
C69 C71 H59 109.5 . . ?
C69 C71 H60 109.5 . . ?
H59 C71 H60 109.5 . . ?
C69 C71 H61 109.5 . . ?
H59 C71 H61 109.5 . . ?
H60 C71 H61 109.5 . . ?
C63 C72 H62 109.5 . . ?
C63 C72 H63 109.5 . . ?
H62 C72 H63 109.5 . . ?
C63 C72 H64 109.5 . . ?
H62 C72 H64 109.5 . . ?
H63 C72 H64 109.5 . . ?
C74 C73 C78 120.0 . . ?
C74 C73 C82 118.73(8) . . ?
C78 C73 C82 121.27(8) . . ?
C74 C73 Ru6 71.09(8) . . ?
C78 C73 Ru6 73.96(10) . . ?
C82 C73 Ru6 126.66(15) . . ?
C75 C74 C73 120.0 . . ?
C75 C74 Ru6 73.27(9) . . ?
C73 C74 Ru6 72.16(8) . . ?
C75 C74 H65 120.0 . . ?
C73 C74 H65 120.0 . . ?
Ru6 C74 H65 126.5 . . ?
C74 C75 C76 120.0 . . ?
C74 C75 Ru6 70.21(9) . . ?
C76 C75 Ru6 74.15(10) . . ?
C74 C75 H66 120.0 . . ?
C76 C75 H66 120.0 . . ?
Ru6 C75 H66 127.7 . . ?
C75 C76 C77 120.0 . . ?
C75 C76 C79 127.46(7) . . ?
C77 C76 C79 112.52(7) . . ?
C75 C76 Ru6 70.10(9) . . ?
C77 C76 Ru6 72.89(8) . . ?
C79 C76 Ru6 127.94(15) . . ?
C78 C77 C76 120.0 . . ?
C78 C77 Ru6 70.79(8) . . ?
C76 C77 Ru6 71.86(8) . . ?
C78 C77 H67 120.0 . . ?
C76 C77 H67 120.0 . . ?
Ru6 C77 H67 129.8 . . ?
C77 C78 C73 120.0 . . ?
C77 C78 Ru6 73.77(10) . . ?
C73 C78 Ru6 69.87(10) . . ?
C77 C78 H68 120.0 . . ?
C73 C78 H68 120.0 . . ?
Ru6 C78 H68 128.6 . . ?
C76 C79 C81 111.56(10) . . ?
C76 C79 C80 110.17(8) . . ?
C81 C79 C80 108.68(9) . . ?
C76 C79 H69 108.8 . . ?
C81 C79 H69 108.8 . . ?
C80 C79 H69 108.8 . . ?
C79 C80 H70 109.5 . . ?
C79 C80 H71 109.5 . . ?
H70 C80 H71 109.5 . . ?
C79 C80 H72 109.5 . . ?
H70 C80 H72 109.5 . . ?
H71 C80 H72 109.5 . . ?
C79 C81 H73 109.5 . . ?
C79 C81 H74 109.5 . . ?
H73 C81 H74 109.5 . . ?
C79 C81 H75 109.5 . . ?
H73 C81 H75 109.5 . . ?
H74 C81 H75 109.5 . . ?
C73 C82 H76 109.5 . . ?
C73 C82 H77 109.5 . . ?
H76 C82 H77 109.5 . . ?
C73 C82 H78 109.5 . . ?
H76 C82 H78 109.5 . . ?
H77 C82 H78 109.5 . . ?
C3 Co1 C2 91.2(11) . . ?
C3 Co1 C1 90.8(10) . . ?
C2 Co1 C1 90.8(10) . . ?
C3 Co1 C17 143.3(11) . . ?
C2 Co1 C17 125.5(9) . . ?
C1 Co1 C17 90.3(8) . . ?
C3 Co1 C16 152.6(11) . . ?
C2 Co1 C16 92.8(8) . . ?
C1 Co1 C16 116.2(9) . . ?
C17 Co1 C16 40.3(3) . . ?
C3 Co1 C13 104.0(11) . . ?
C2 Co1 C13 159.7(8) . . ?
C1 Co1 C13 102.3(9) . . ?
C17 Co1 C13 40.3(3) . . ?
C16 Co1 C13 67.5(4) . . ?
C3 Co1 C15 112.6(11) . . ?
C2 Co1 C15 94.7(9) . . ?
C1 Co1 C15 155.7(9) . . ?
C17 Co1 C15 67.4(4) . . ?
C16 Co1 C15 40.0(3) . . ?
C13 Co1 C15 67.2(4) . . ?
C3 Co1 C14 89.4(10) . . ?
C2 Co1 C14 128.8(10) . . ?
C1 Co1 C14 140.5(9) . . ?
C17 Co1 C14 67.4(4) . . ?
C16 Co1 C14 67.2(4) . . ?
C13 Co1 C14 40.0(3) . . ?
C15 Co1 C14 39.8(3) . . ?
C3 Co1 Cs1 54.6(9) . . ?
C2 Co1 Cs1 54.7(7) . . ?
C1 Co1 Cs1 56.9(6) . . ?
C17 Co1 Cs1 146.1(5) . . ?
C16 Co1 Cs1 144.1(5) . . ?
C13 Co1 Cs1 145.6(4) . . ?
C15 Co1 Cs1 142.5(5) . . ?
C14 Co1 Cs1 143.3(5) . . ?
C4 Co2 C5 91.1(10) . . ?
C4 Co2 C6 86.4(9) . . ?
C5 Co2 C6 90.8(10) . . ?
C4 Co2 C18 108.5(9) . . ?
C5 Co2 C18 158.7(8) . . ?
C6 Co2 C18 98.4(9) . . ?
C4 Co2 C22 148.5(10) . . ?
C5 Co2 C22 120.4(9) . . ?
C6 Co2 C22 93.0(8) . . ?
C18 Co2 C22 40.5(3) . . ?
C4 Co2 C19 91.1(8) . . ?
C5 Co2 C19 134.6(10) . . ?
C6 Co2 C19 134.6(10) . . ?
C18 Co2 C19 40.1(3) . . ?
C22 Co2 C19 67.3(4) . . ?
C4 Co2 C21 150.3(10) . . ?
C5 Co2 C21 91.8(8) . . ?
C6 Co2 C21 123.1(9) . . ?
C18 Co2 C21 67.1(4) . . ?
C22 Co2 C21 39.8(3) . . ?
C19 Co2 C21 66.4(4) . . ?
C4 Co2 C20 111.2(9) . . ?
C5 Co2 C20 98.9(9) . . ?
C6 Co2 C20 159.5(9) . . ?
C18 Co2 C20 66.8(4) . . ?
C22 Co2 C20 66.6(4) . . ?
C19 Co2 C20 39.4(3) . . ?
C21 Co2 C20 39.2(3) . . ?
C8 Co3 C7 94.0(9) . . ?
C8 Co3 C9 91.1(11) . . ?
C7 Co3 C9 89.3(10) . . ?
C8 Co3 C25 102.5(9) . . ?
C7 Co3 C25 157.9(8) . . ?
C9 Co3 C25 104.8(9) . . ?
C8 Co3 C26 141.1(9) . . ?
C7 Co3 C26 124.8(9) . . ?
C9 Co3 C26 91.5(10) . . ?
C25 Co3 C26 39.8(3) . . ?
C8 Co3 C24 89.3(9) . . ?
C7 Co3 C24 127.5(9) . . ?
C9 Co3 C24 143.1(9) . . ?
C25 Co3 C24 39.6(3) . . ?
C26 Co3 C24 66.4(4) . . ?
C8 Co3 C27 152.7(10) . . ?
C7 Co3 C27 92.4(8) . . ?
C9 Co3 C27 115.5(10) . . ?
C25 Co3 C27 66.3(4) . . ?
C26 Co3 C27 39.5(3) . . ?
C24 Co3 C27 66.0(4) . . ?
C8 Co3 C23 113.9(10) . . ?
C7 Co3 C23 93.9(8) . . ?
C9 Co3 C23 154.5(10) . . ?
C25 Co3 C23 66.2(4) . . ?
C26 Co3 C23 66.1(4) . . ?
C24 Co3 C23 39.2(3) . . ?
C27 Co3 C23 39.1(3) . . ?
C8 Co3 Cs1 60.0(7) . . ?
C7 Co3 Cs1 54.6(6) . . ?
C9 Co3 Cs1 52.8(8) . . ?
C25 Co3 Cs1 147.3(5) . . ?
C26 Co3 Cs1 142.8(5) . . ?
C24 Co3 Cs1 148.4(5) . . ?
C27 Co3 Cs1 141.3(5) . . ?
C23 Co3 Cs1 144.5(5) . . ?
C12 Co4 C11 92.9(10) . . ?
C12 Co4 C10 90.3(10) . . ?
C11 Co4 C10 89.3(11) . . ?
C12 Co4 C29 154.5(9) . . ?
C11 Co4 C29 111.2(9) . . ?
C10 Co4 C29 98.0(8) . . ?
C12 Co4 C28 135.5(9) . . ?
C11 Co4 C28 90.7(9) . . ?
C10 Co4 C28 134.1(8) . . ?
C29 Co4 C28 40.5(3) . . ?
C12 Co4 C30 115.7(9) . . ?
C11 Co4 C30 151.3(9) . . ?
C10 Co4 C30 93.0(9) . . ?
C29 Co4 C30 40.2(4) . . ?
C28 Co4 C30 67.5(5) . . ?
C12 Co4 C32 97.6(9) . . ?
C11 Co4 C32 108.7(10) . . ?
C10 Co4 C32 159.9(9) . . ?
C29 Co4 C32 67.5(4) . . ?
C28 Co4 C32 40.1(3) . . ?
C30 Co4 C32 66.9(5) . . ?
C12 Co4 C31 88.2(9) . . ?
C11 Co4 C31 147.8(10) . . ?
C10 Co4 C31 122.9(9) . . ?
C29 Co4 C31 67.1(5) . . ?
C28 Co4 C31 67.1(5) . . ?
C30 Co4 C31 39.6(3) . . ?
C32 Co4 C31 39.6(3) . . ?
C12 Co4 Cs1 56.1(8) . . ?
C11 Co4 Cs1 56.2(8) . . ?
C10 Co4 Cs1 53.5(7) . . ?
C29 Co4 Cs1 145.4(5) . . ?
C28 Co4 Cs1 146.9(5) . . ?
C30 Co4 Cs1 142.5(5) . . ?
C32 Co4 Cs1 144.8(5) . . ?
C31 Co4 Cs1 142.2(5) . . ?
N10 Cs1 N3 118.0(4) . . ?
N10 Cs1 N1 47.3(4) . . ?
N3 Cs1 N1 70.8(4) . . ?
N10 Cs1 C9 176.0(5) . . ?
N3 Cs1 C9 65.9(5) . . ?
N1 Cs1 C9 136.7(5) . . ?
N10 Cs1 C10 19.3(2) . . ?
N3 Cs1 C10 135.2(4) . . ?
N1 Cs1 C10 64.9(4) . . ?
C9 Cs1 C10 157.1(4) . . ?
N10 Cs1 N4 48.1(4) . . ?
N3 Cs1 N4 90.9(5) . . ?
N1 Cs1 N4 47.6(4) . . ?
C9 Cs1 N4 133.5(4) . . ?
C10 Cs1 N4 63.9(4) . . ?
N10 Cs1 N9 164.5(4) . . ?
N3 Cs1 N9 48.7(4) . . ?
N1 Cs1 N9 119.1(5) . . ?
C9 Cs1 N9 19.0(2) . . ?
C10 Cs1 N9 176.0(4) . . ?
N4 Cs1 N9 118.7(5) . . ?
N10 Cs1 N12 73.9(4) . . ?
N3 Cs1 N12 164.2(4) . . ?
N1 Cs1 N12 120.8(4) . . ?
C9 Cs1 N12 102.1(5) . . ?
C10 Cs1 N12 58.6(4) . . ?
N4 Cs1 N12 90.6(5) . . ?
N9 Cs1 N12 117.7(4) . . ?
N10 Cs1 N2 90.3(4) . . ?
N3 Cs1 N2 72.3(4) . . ?
N1 Cs1 N2 73.5(4) . . ?
C9 Cs1 N2 91.1(5) . . ?
C10 Cs1 N2 89.1(4) . . ?
N4 Cs1 N2 120.8(4) . . ?
N9 Cs1 N2 91.8(5) . . ?
N12 Cs1 N2 119.9(4) . . ?
N10 Cs1 C6 105.5(4) . . ?
N3 Cs1 C6 65.5(4) . . ?
N1 Cs1 C6 88.7(5) . . ?
C9 Cs1 C6 75.8(4) . . ?
C10 Cs1 C6 118.1(4) . . ?
N4 Cs1 C6 57.7(4) . . ?
N9 Cs1 C6 63.4(4) . . ?
N12 Cs1 C6 102.4(4) . . ?
N2 Cs1 C6 137.6(4) . . ?
N10 Cs1 C7 134.8(4) . . ?
N3 Cs1 C7 90.5(5) . . ?
N1 Cs1 C7 137.4(4) . . ?
C9 Cs1 C7 43.2(4) . . ?
C10 Cs1 C7 118.0(4) . . ?
N4 Cs1 C7 174.9(4) . . ?
N9 Cs1 C7 59.1(4) . . ?
N12 Cs1 C7 86.8(5) . . ?
N2 Cs1 C7 64.3(4) . . ?
C6 Cs1 C7 118.6(4) . . ?
N10 Cs1 N6 120.2(4) . . ?
N3 Cs1 N6 50.0(4) . . ?
N1 Cs1 N6 91.9(5) . . ?
C9 Cs1 N6 61.9(4) . . ?
C10 Cs1 N6 135.3(4) . . ?
N4 Cs1 N6 72.2(4) . . ?
N9 Cs1 N6 46.8(4) . . ?
N12 Cs1 N6 115.9(4) . . ?
N2 Cs1 N6 121.8(4) . . ?
C6 Cs1 N6 18.5(2) . . ?
C7 Cs1 N6 105.0(4) . . ?
N7 Ru1 N11 88.6(7) . . ?
N7 Ru1 C189 139.3(13) . . ?
N11 Ru1 C189 93.3(13) . . ?
N7 Ru1 C185 155.2(13) . . ?
N11 Ru1 C185 115.3(13) . . ?
C189 Ru1 C185 39.2(7) . . ?
N7 Ru1 N2 88.9(7) . . ?
N11 Ru1 N2 87.8(8) . . ?
C189 Ru1 N2 131.8(13) . . ?
C185 Ru1 N2 98.1(12) . . ?
N7 Ru1 C188 102.3(13) . . ?
N11 Ru1 C188 108.2(15) . . ?
C189 Ru1 C188 39.0(7) . . ?
C185 Ru1 C188 65.3(10) . . ?
N2 Ru1 C188 160.5(13) . . ?
N7 Ru1 C186 117.0(13) . . ?
N11 Ru1 C186 154.1(13) . . ?
C189 Ru1 C186 65.2(10) . . ?
C185 Ru1 C186 38.8(7) . . ?
N2 Ru1 C186 96.1(13) . . ?
C188 Ru1 C186 64.7(10) . . ?
N7 Ru1 C33 155.0(8) . . ?
N11 Ru1 C33 98.3(8) . . ?
C189 Ru1 C33 17.2(13) . . ?
C185 Ru1 C33 23.7(13) . . ?
N2 Ru1 C33 115.2(7) . . ?
C188 Ru1 C33 52.7(12) . . ?
C186 Ru1 C33 56.9(12) . . ?
N7 Ru1 C34 138.7(8) . . ?
N11 Ru1 C34 132.5(8) . . ?
C189 Ru1 C34 50.7(12) . . ?
C185 Ru1 C34 17.3(13) . . ?
N2 Ru1 C34 95.7(7) . . ?
C188 Ru1 C34 65.4(11) . . ?
C186 Ru1 C34 21.6(12) . . ?
C33 Ru1 C34 38.3(3) . . ?
N7 Ru1 C187 91.9(12) . . ?
N11 Ru1 C187 145.8(15) . . ?
C189 Ru1 C187 64.9(11) . . ?
C185 Ru1 C187 64.8(10) . . ?
N2 Ru1 C187 126.5(15) . . ?
C188 Ru1 C187 38.5(7) . . ?
C186 Ru1 C187 38.3(7) . . ?
C33 Ru1 C187 69.0(12) . . ?
C34 Ru1 C187 53.0(12) . . ?
N7 Ru1 C37 117.9(8) . . ?
N11 Ru1 C37 94.5(8) . . ?
C189 Ru1 C37 21.4(13) . . ?
C185 Ru1 C37 56.8(12) . . ?
N2 Ru1 C37 153.1(7) . . ?
C188 Ru1 C37 20.4(14) . . ?
C186 Ru1 C37 70.9(12) . . ?
C33 Ru1 C37 37.9(3) . . ?
C34 Ru1 C37 63.4(5) . . ?
C187 Ru1 C37 55.5(13) . . ?
N7 Ru1 C35 102.8(8) . . ?
N11 Ru1 C35 157.1(8) . . ?
C189 Ru1 C35 65.1(12) . . ?
C185 Ru1 C35 52.5(12) . . ?
N2 Ru1 C35 111.9(8) . . ?
C188 Ru1 C35 50.4(13) . . ?
C186 Ru1 C35 20.6(12) . . ?
C33 Ru1 C35 63.4(5) . . ?
C34 Ru1 C35 37.9(4) . . ?
C187 Ru1 C35 17.9(13) . . ?
C37 Ru1 C35 62.7(5) . . ?
N10 Ru2 N1 85.0(8) . . ?
N10 Ru2 C44 94.3(6) . . ?
N1 Ru2 C44 129.1(6) . . ?
N10 Ru2 N4 86.5(7) . . ?
N1 Ru2 N4 86.5(8) . . ?
C44 Ru2 N4 144.4(7) . . ?
N10 Ru2 C43 104.7(6) . . ?
N1 Ru2 C43 164.2(7) . . ?
C44 Ru2 C43 39.2(2) . . ?
N4 Ru2 C43 106.2(7) . . ?
N10 Ru2 C45 120.0(6) . . ?
N1 Ru2 C45 99.2(7) . . ?
C44 Ru2 C45 39.0(2) . . ?
N4 Ru2 C45 153.1(7) . . ?
C43 Ru2 C45 65.1(3) . . ?
N10 Ru2 C47 141.2(7) . . ?
N1 Ru2 C47 133.7(7) . . ?
C44 Ru2 C47 65.0(3) . . ?
N4 Ru2 C47 92.7(6) . . ?
C43 Ru2 C47 38.6(2) . . ?
C45 Ru2 C47 64.3(3) . . ?
N10 Ru2 C46 157.7(6) . . ?
N1 Ru2 C46 101.9(7) . . ?
C44 Ru2 C46 64.7(3) . . ?
N4 Ru2 C46 114.8(7) . . ?
C43 Ru2 C46 64.5(3) . . ?
C45 Ru2 C46 38.3(2) . . ?
C47 Ru2 C46 38.1(2) . . ?
N10 Ru2 Cs1 49.2(5) . . ?
N1 Ru2 Cs1 52.9(6) . . ?
C44 Ru2 Cs1 143.0(4) . . ?
N4 Ru2 Cs1 53.8(5) . . ?
C43 Ru2 Cs1 142.6(4) . . ?
C45 Ru2 Cs1 147.1(4) . . ?
C47 Ru2 Cs1 146.4(3) . . ?
C46 Ru2 Cs1 149.3(4) . . ?
N6 Ru3 N9 89.5(9) . . ?
N6 Ru3 C56 96.8(7) . . ?
N9 Ru3 C56 113.1(8) . . ?
N6 Ru3 C57 133.6(7) . . ?
N9 Ru3 C57 95.0(8) . . ?
C56 Ru3 C57 39.6(2) . . ?
N6 Ru3 N3 91.8(8) . . ?
N9 Ru3 N3 87.6(8) . . ?
C56 Ru3 N3 157.5(7) . . ?
C57 Ru3 N3 134.5(7) . . ?
N6 Ru3 C55 90.9(7) . . ?
N9 Ru3 C55 151.6(8) . . ?
C56 Ru3 C55 38.7(2) . . ?
C57 Ru3 C55 64.9(3) . . ?
N3 Ru3 C55 120.7(7) . . ?
N6 Ru3 C53 154.2(7) . . ?
N9 Ru3 C53 113.9(8) . . ?
C56 Ru3 C53 64.8(3) . . ?
C57 Ru3 C53 38.6(2) . . ?
N3 Ru3 C53 99.6(7) . . ?
C55 Ru3 C53 63.4(3) . . ?
N6 Ru3 C54 119.4(7) . . ?
N9 Ru3 C54 151.0(8) . . ?
C56 Ru3 C54 63.9(3) . . ?
C57 Ru3 C54 63.8(3) . . ?
N3 Ru3 C54 93.7(7) . . ?
C55 Ru3 C54 37.4(2) . . ?
C53 Ru3 C54 37.4(2) . . ?
N6 Ru3 Cs1 55.5(6) . . ?
N9 Ru3 Cs1 54.5(7) . . ?
C56 Ru3 Cs1 146.3(4) . . ?
C57 Ru3 Cs1 149.6(4) . . ?
N3 Ru3 Cs1 53.4(6) . . ?
C55 Ru3 Cs1 142.7(4) . . ?
C53 Ru3 Cs1 147.5(3) . . ?
C54 Ru3 Cs1 143.5(4) . . ?
N8 Ru4 N12 84.6(7) . . ?
N8 Ru4 N5 91.0(7) . . ?
N12 Ru4 N5 85.8(7) . . ?
N8 Ru4 S1 132.5(6) . . ?
N12 Ru4 S1 85.2(6) . . ?
N5 Ru4 S1 134.2(6) . . ?
N8 Ru4 S2 98.6(5) . . ?
N12 Ru4 S2 174.1(6) . . ?
N5 Ru4 S2 99.0(5) . . ?
S1 Ru4 S2 89.0(3) . . ?
N8 Ru4 Ru6 98.5(5) . . ?
N12 Ru4 Ru6 122.9(6) . . ?
N5 Ru4 Ru6 150.3(5) . . ?
S1 Ru4 Ru6 51.4(2) . . ?
S2 Ru4 Ru6 51.9(2) . . ?
N8 Ru4 Ru5 148.7(5) . . ?
N12 Ru4 Ru5 124.4(6) . . ?
N5 Ru4 Ru5 101.4(5) . . ?
S1 Ru4 Ru5 50.7(2) . . ?
S2 Ru4 Ru5 51.4(2) . . ?
Ru6 Ru4 Ru5 57.75(9) . . ?
C68 Ru5 C63 37.28(8) . . ?
C68 Ru5 C67 37.13(15) . . ?
C63 Ru5 C67 66.79(16) . . ?
C68 Ru5 C64 66.62(8) . . ?
C63 Ru5 C64 36.88(9) . . ?
C67 Ru5 C64 78.19(9) . . ?
C68 Ru5 C66 66.36(16) . . ?
C63 Ru5 C66 78.19(10) . . ?
C67 Ru5 C66 36.62(8) . . ?
C64 Ru5 C66 65.64(15) . . ?
C68 Ru5 S1 170.6(3) . . ?
C63 Ru5 S1 146.0(3) . . ?
C67 Ru5 S1 133.8(3) . . ?
C64 Ru5 S1 112.6(3) . . ?
C66 Ru5 S1 104.6(3) . . ?
C68 Ru5 C65 78.19(9) . . ?
C63 Ru5 C65 66.04(16) . . ?
C67 Ru5 C65 65.79(9) . . ?
C64 Ru5 C65 36.39(14) . . ?
C66 Ru5 C65 36.26(8) . . ?
S1 Ru5 C65 95.8(3) . . ?
C68 Ru5 S2 98.1(3) . . ?
C63 Ru5 S2 106.2(3) . . ?
C67 Ru5 S2 115.8(3) . . ?
C64 Ru5 S2 134.9(3) . . ?
C66 Ru5 S2 148.9(2) . . ?
S1 Ru5 S2 88.8(3) . . ?
C65 Ru5 S2 171.3(3) . . ?
C68 Ru5 Ru6 127.29(19) . . ?
C63 Ru5 Ru6 157.14(15) . . ?
C67 Ru5 Ru6 110.1(2) . . ?
C64 Ru5 Ru6 165.39(18) . . ?
C66 Ru5 Ru6 113.49(14) . . ?
S1 Ru5 Ru6 52.9(2) . . ?
C65 Ru5 Ru6 134.98(18) . . ?
S2 Ru5 Ru6 53.4(2) . . ?
C68 Ru5 Ru4 138.72(19) . . ?
C63 Ru5 Ru4 117.06(13) . . ?
C67 Ru5 Ru4 166.7(2) . . ?
C64 Ru5 Ru4 112.8(2) . . ?
C66 Ru5 Ru4 153.92(13) . . ?
S1 Ru5 Ru4 50.6(2) . . ?
C65 Ru5 Ru4 127.51(18) . . ?
S2 Ru5 Ru4 51.3(2) . . ?
Ru6 Ru5 Ru4 60.98(10) . . ?
C74 Ru6 C73 36.75(5) . . ?
C74 Ru6 C75 36.52(5) . . ?
C73 Ru6 C75 65.53(9) . . ?
C74 Ru6 S1 149.0(2) . . ?
C73 Ru6 S1 167.2(3) . . ?
C75 Ru6 S1 114.9(2) . . ?
C74 Ru6 C78 65.30(9) . . ?
C73 Ru6 C78 36.17(5) . . ?
C75 Ru6 C78 76.30(10) . . ?
S1 Ru6 C78 131.0(3) . . ?
C74 Ru6 S2 108.1(3) . . ?
C73 Ru6 S2 100.2(2) . . ?
C75 Ru6 S2 136.4(3) . . ?
S1 Ru6 S2 87.9(3) . . ?
C78 Ru6 S2 117.3(2) . . ?
C74 Ru6 C76 64.87(9) . . ?
C73 Ru6 C76 76.29(10) . . ?
C75 Ru6 C76 35.75(5) . . ?
S1 Ru6 C76 96.8(2) . . ?
C78 Ru6 C76 63.86(10) . . ?
S2 Ru6 C76 172.1(3) . . ?
C74 Ru6 C77 76.28(10) . . ?
C73 Ru6 C77 64.45(9) . . ?
C75 Ru6 C77 64.06(9) . . ?
S1 Ru6 C77 103.7(3) . . ?
C78 Ru6 C77 35.44(5) . . ?
S2 Ru6 C77 149.2(2) . . ?
C76 Ru6 C77 35.25(6) . . ?
C74 Ru6 Ru5 156.82(16) . . ?
C73 Ru6 Ru5 126.06(13) . . ?
C75 Ru6 Ru5 166.65(16) . . ?
S1 Ru6 Ru5 52.2(2) . . ?
C78 Ru6 Ru5 109.05(13) . . ?
S2 Ru6 Ru5 52.9(2) . . ?
C76 Ru6 Ru5 134.84(16) . . ?
C77 Ru6 Ru5 112.88(14) . . ?
C74 Ru6 Ru4 120.18(14) . . ?
C73 Ru6 Ru4 141.89(16) . . ?
C75 Ru6 Ru4 114.89(13) . . ?
S1 Ru6 Ru4 50.6(2) . . ?
C78 Ru6 Ru4 167.70(14) . . ?
S2 Ru6 Ru4 51.3(2) . . ?
C76 Ru6 Ru4 128.13(13) . . ?
C77 Ru6 Ru4 152.86(16) . . ?
Ru5 Ru6 Ru4 61.27(10) . . ?
Ru4 S1 Ru5 78.7(3) . . ?
Ru4 S1 Ru6 78.0(3) . . ?
Ru5 S1 Ru6 74.9(3) . . ?
Ru4 S2 Ru5 77.3(3) . . ?
Ru4 S2 Ru6 76.8(3) . . ?
Ru5 S2 Ru6 73.7(3) . . ?
N83 C83 Co5 174(2) . . ?
N83 C83 Cs2 84.3(15) . . ?
Co5 C83 Cs2 100.6(7) . . ?
N84 C84 Co5 176(2) . . ?
N84 C84 Cs2 77.1(16) . . ?
Co5 C84 Cs2 98.6(9) . . ?
N85 C85 Co5 178.2(19) . . ?
N85 C85 Cs2 79.1(14) . . ?
Co5 C85 Cs2 100.1(7) . . ?
N86 C86 Co6 170(2) . . ?
N86 C86 Cs2 74.3(14) . . ?
Co6 C86 Cs2 96.4(8) . . ?
N87 C87 Co6 175.4(19) . . ?
N87 C87 Cs2 76.5(12) . . ?
Co6 C87 Cs2 104.8(7) . . ?
N88 C88 Co6 174.7(19) . . ?
N88 C88 Cs2 76.2(13) . . ?
Co6 C88 Cs2 101.4(7) . . ?
N89 C89 Co7 180(2) . . ?
N89 C89 Cs2 79.1(15) . . ?
Co7 C89 Cs2 100.4(9) . . ?
N90 C90 Co7 172.8(16) . . ?
N90 C90 Cs2 75.3(12) . . ?
Co7 C90 Cs2 98.5(7) . . ?
N91 C91 Co7 176(2) . . ?
N91 C91 Cs2 77.5(14) . . ?
Co7 C91 Cs2 100.6(7) . . ?
N92 C92 Co8 171.4(19) . . ?
N92 C92 Cs2 73.1(13) . . ?
Co8 C92 Cs2 98.4(7) . . ?
N93 C93 Co8 173(2) . . ?
N93 C93 Cs2 78.2(13) . . ?
Co8 C93 Cs2 98.3(7) . . ?
N94 C94 Co8 173(2) . . ?
N94 C94 Cs2 74.2(14) . . ?
Co8 C94 Cs2 98.5(7) . . ?
C83 N83 Ru8 174.5(19) . . ?
C83 N83 Cs2 77.0(15) . . ?
Ru8 N83 Cs2 97.6(6) . . ?
C84 N84 Ru9 177(2) . . ?
C84 N84 Cs2 84.1(16) . . ?
Ru9 N84 Cs2 99.3(6) . . ?
C85 N85 Ru7 174.4(17) . . ?
C85 N85 Cs2 81.6(14) . . ?
Ru7 N85 Cs2 101.7(6) . . ?
C86 N86 Ru10 173.2(18) . . ?
C86 N86 Cs2 87.9(15) . . ?
Ru10 N86 Cs2 98.5(6) . . ?
C87 N87 Ru8 171.2(18) . . ?
C87 N87 Cs2 84.5(13) . . ?
Ru8 N87 Cs2 101.9(6) . . ?
C88 N88 Ru7 173.7(18) . . ?
C88 N88 Cs2 85.3(14) . . ?
Ru7 N88 Cs2 100.2(5) . . ?
C89 N89 Ru10 172(2) . . ?
C89 N89 Cs2 82.3(15) . . ?
Ru10 N89 Cs2 101.1(6) . . ?
C90 N90 Ru9 171.4(16) . . ?
C90 N90 Cs2 86.2(12) . . ?
Ru9 N90 Cs2 101.1(5) . . ?
C91 N91 Ru7 177(2) . . ?
C91 N91 Cs2 84.2(14) . . ?
Ru7 N91 Cs2 98.4(5) . . ?
C92 N92 Ru10 166.6(18) . . ?
C92 N92 Cs2 88.4(14) . . ?
Ru10 N92 Cs2 104.6(6) . . ?
C93 N93 Ru8 170(2) . . ?
C93 N93 Cs2 83.4(13) . . ?
Ru8 N93 Cs2 100.7(6) . . ?
C94 N94 Ru9 172.3(18) . . ?
C94 N94 Cs2 87.3(14) . . ?
Ru9 N94 Cs2 100.3(6) . . ?
C99 C95 C96 108.0 . . ?
C99 C95 Co5 70.0(6) . . ?
C96 C95 Co5 70.5(6) . . ?
C99 C95 H79 126.0 . . ?
C96 C95 H79 126.0 . . ?
Co5 C95 H79 125.1 . . ?
C97 C96 C95 108.0 . . ?
C97 C96 Co5 70.8(5) . . ?
C95 C96 Co5 68.9(6) . . ?
C97 C96 H80 126.0 . . ?
C95 C96 H80 126.0 . . ?
Co5 C96 H80 125.9 . . ?
C96 C97 C98 108.0 . . ?
C96 C97 Co5 69.1(5) . . ?
C98 C97 Co5 69.7(6) . . ?
C96 C97 H81 126.0 . . ?
C98 C97 H81 126.0 . . ?
Co5 C97 H81 126.7 . . ?
C99 C98 C97 108.0 . . ?
C99 C98 Co5 68.8(5) . . ?
C97 C98 Co5 70.3(6) . . ?
C99 C98 H82 126.0 . . ?
C97 C98 H82 126.0 . . ?
Co5 C98 H82 126.4 . . ?
C98 C99 C95 108.0 . . ?
C98 C99 Co5 70.9(5) . . ?
C95 C99 Co5 69.3(6) . . ?
C98 C99 H83 126.0 . . ?
C95 C99 H83 126.0 . . ?
Co5 C99 H83 125.4 . . ?
C104 C100 C101 108.0 . . ?
C104 C100 Co6 69.6(11) . . ?
C101 C100 Co6 68.4(10) . . ?
C104 C100 H197 126.0 . . ?
C101 C100 H197 126.0 . . ?
Co6 C100 H197 127.6 . . ?
C102 C101 C100 108.0 . . ?
C102 C101 Co6 67.8(10) . . ?
C100 C101 Co6 72.1(9) . . ?
C102 C101 H198 126.0 . . ?
C100 C101 H198 126.0 . . ?
Co6 C101 H198 125.7 . . ?
C101 C102 C103 108.0 . . ?
C101 C102 Co6 71.7(10) . . ?
C103 C102 Co6 70.3(11) . . ?
C101 C102 H199 126.0 . . ?
C103 C102 H199 126.0 . . ?
Co6 C102 H199 123.7 . . ?
C102 C103 C104 108.0 . . ?
C102 C103 Co6 68.8(11) . . ?
C104 C103 Co6 72.3(9) . . ?
C102 C103 H200 126.0 . . ?
C104 C103 H200 126.0 . . ?
Co6 C103 H200 124.4 . . ?
C100 C104 C103 108.0 . . ?
C100 C104 Co6 71.1(10) . . ?
C103 C104 Co6 67.6(9) . . ?
C100 C104 H201 126.0 . . ?
C103 C104 H201 126.0 . . ?
Co6 C104 H201 126.8 . . ?
C196 C195 C199 108.0 . . ?
C196 C195 Co6 74(2) . . ?
C199 C195 Co6 71(2) . . ?
C196 C195 H202 126.0 . . ?
C199 C195 H202 126.0 . . ?
Co6 C195 H202 120.6 . . ?
C195 C196 C197 108.0 . . ?
C195 C196 Co6 64.7(19) . . ?
C197 C196 Co6 75(2) . . ?
C195 C196 H203 126.0 . . ?
C197 C196 H203 126.0 . . ?
Co6 C196 H203 125.3 . . ?
C198 C197 C196 108.0 . . ?
C198 C197 Co6 69.6(18) . . ?
C196 C197 Co6 65.8(18) . . ?
C198 C197 H204 126.0 . . ?
C196 C197 H204 126.0 . . ?
Co6 C197 H204 130.2 . . ?
C199 C198 C197 108.0 . . ?
C199 C198 Co6 64.4(19) . . ?
C197 C198 Co6 72(2) . . ?
C199 C198 H205 126.0 . . ?
C197 C198 H205 126.0 . . ?
Co6 C198 H205 128.8 . . ?
C198 C199 C195 108.0 . . ?
C198 C199 Co6 76(2) . . ?
C195 C199 Co6 67(2) . . ?
C198 C199 H206 126.0 . . ?
C195 C199 H206 126.0 . . ?
Co6 C199 H206 122.9 . . ?
C109 C105 C106 108.0 . . ?
C109 C105 Co7 69.6(6) . . ?
C106 C105 Co7 70.4(6) . . ?
C109 C105 H84 126.0 . . ?
C106 C105 H84 126.0 . . ?
Co7 C105 H84 125.6 . . ?
C107 C106 C105 108.0 . . ?
C107 C106 Co7 69.7(6) . . ?
C105 C106 Co7 70.0(6) . . ?
C107 C106 H85 126.0 . . ?
C105 C106 H85 126.0 . . ?
Co7 C106 H85 125.8 . . ?
C106 C107 C108 108.0 . . ?
C106 C107 Co7 70.7(5) . . ?
C108 C107 Co7 69.6(6) . . ?
C106 C107 H86 126.0 . . ?
C108 C107 H86 126.0 . . ?
Co7 C107 H86 125.3 . . ?
C109 C108 C107 108.0 . . ?
C109 C108 Co7 70.2(6) . . ?
C107 C108 Co7 70.6(6) . . ?
C109 C108 H87 126.0 . . ?
C107 C108 H87 126.0 . . ?
Co7 C108 H87 124.8 . . ?
C108 C109 C105 108.0 . . ?
C108 C109 Co7 69.9(6) . . ?
C105 C109 Co7 70.7(6) . . ?
C108 C109 H88 126.0 . . ?
C105 C109 H88 126.0 . . ?
Co7 C109 H88 125.0 . . ?
C111 C110 C114 108.0 . . ?
C111 C110 Co8 69.9(6) . . ?
C114 C110 Co8 69.1(6) . . ?
C111 C110 H89 126.0 . . ?
C114 C110 H89 126.0 . . ?
Co8 C110 H89 126.6 . . ?
C110 C111 C112 108.0 . . ?
C110 C111 Co8 70.5(6) . . ?
C112 C111 Co8 68.8(6) . . ?
C110 C111 H90 126.0 . . ?
C112 C111 H90 126.0 . . ?
Co8 C111 H90 126.3 . . ?
C111 C112 C113 108.0 . . ?
C111 C112 Co8 71.3(6) . . ?
C113 C112 Co8 69.3(7) . . ?
C111 C112 H91 126.0 . . ?
C113 C112 H91 126.0 . . ?
Co8 C112 H91 125.0 . . ?
C114 C113 C112 108.0 . . ?
C114 C113 Co8 70.8(6) . . ?
C112 C113 Co8 70.3(7) . . ?
C114 C113 H92 126.0 . . ?
C112 C113 H92 126.0 . . ?
Co8 C113 H92 124.5 . . ?
C113 C114 C110 108.0 . . ?
C113 C114 Co8 68.9(6) . . ?
C110 C114 Co8 71.2(6) . . ?
C113 C114 H93 126.0 . . ?
C110 C114 H93 126.0 . . ?
Co8 C114 H93 125.5 . . ?
C116 C115 C119 108.0 . . ?
C116 C115 C120 126.0 . . ?
C119 C115 C120 126.0 . . ?
C116 C115 Ru7 72.5(4) . . ?
C119 C115 Ru7 69.9(4) . . ?
C120 C115 Ru7 123.2(4) . . ?
C115 C116 C117 108.0 . . ?
C115 C116 C121 126.0 . . ?
C117 C116 C121 126.0 . . ?
C115 C116 Ru7 69.4(4) . . ?
C117 C116 Ru7 71.4(4) . . ?
C121 C116 Ru7 124.8(3) . . ?
C116 C117 C118 108.0 . . ?
C116 C117 C122 126.0 . . ?
C118 C117 C122 126.0 . . ?
C116 C117 Ru7 71.0(4) . . ?
C118 C117 Ru7 69.6(4) . . ?
C122 C117 Ru7 125.1(3) . . ?
C119 C118 C117 108.0 . . ?
C119 C118 C123 126.0 . . ?
C117 C118 C123 126.0 . . ?
C119 C118 Ru7 69.6(4) . . ?
C117 C118 Ru7 72.5(4) . . ?
C123 C118 Ru7 123.6(3) . . ?
C118 C119 C115 108.0 . . ?
C118 C119 C124 126.0 . . ?
C115 C119 C124 126.0 . . ?
C118 C119 Ru7 71.8(4) . . ?
C115 C119 Ru7 71.4(4) . . ?
C124 C119 Ru7 122.4(3) . . ?
C115 C120 H94 109.5 . . ?
C115 C120 H95 109.5 . . ?
H94 C120 H95 109.5 . . ?
C115 C120 H96 109.5 . . ?
H94 C120 H96 109.5 . . ?
H95 C120 H96 109.5 . . ?
C116 C121 H97 109.5 . . ?
C116 C121 H98 109.5 . . ?
H97 C121 H98 109.5 . . ?
C116 C121 H99 109.5 . . ?
H97 C121 H99 109.5 . . ?
H98 C121 H99 109.5 . . ?
C117 C122 H100 109.5 . . ?
C117 C122 H101 109.5 . . ?
H100 C122 H101 109.5 . . ?
C117 C122 H102 109.5 . . ?
H100 C122 H102 109.5 . . ?
H101 C122 H102 109.5 . . ?
C118 C123 H103 109.5 . . ?
C118 C123 H104 109.5 . . ?
H103 C123 H104 109.5 . . ?
C118 C123 H105 109.5 . . ?
H103 C123 H105 109.5 . . ?
H104 C123 H105 109.5 . . ?
C119 C124 H106 109.5 . . ?
C119 C124 H107 109.5 . . ?
H106 C124 H107 109.5 . . ?
C119 C124 H108 109.5 . . ?
H106 C124 H108 109.5 . . ?
H107 C124 H108 109.5 . . ?
C126 C125 C129 108.0 . . ?
C126 C125 C130 126.0 . . ?
C129 C125 C130 126.0 . . ?
C126 C125 Ru8 72.3(4) . . ?
C129 C125 Ru8 71.2(4) . . ?
C130 C125 Ru8 122.2(3) . . ?
C125 C126 C127 108.0 . . ?
C125 C126 C131 126.0 . . ?
C127 C126 C131 126.0 . . ?
C125 C126 Ru8 69.2(3) . . ?
C127 C126 Ru8 72.6(4) . . ?
C131 C126 Ru8 123.8(3) . . ?
C128 C127 C126 108.0 . . ?
C128 C127 C132 126.0 . . ?
C126 C127 C132 126.0 . . ?
C128 C127 Ru8 70.6(4) . . ?
C126 C127 Ru8 69.7(3) . . ?
C132 C127 Ru8 125.3(3) . . ?
C127 C128 C129 108.0 . . ?
C127 C128 C133 126.0 . . ?
C129 C128 C133 126.0 . . ?
C127 C128 Ru8 71.9(4) . . ?
C129 C128 Ru8 69.1(3) . . ?
C133 C128 Ru8 124.6(3) . . ?
C128 C129 C125 108.0 . . ?
C128 C129 C134 126.0 . . ?
C125 C129 C134 126.0 . . ?
C128 C129 Ru8 72.8(4) . . ?
C125 C129 Ru8 70.2(4) . . ?
C134 C129 Ru8 122.7(3) . . ?
C125 C130 H109 109.5 . . ?
C125 C130 H110 109.5 . . ?
H109 C130 H110 109.5 . . ?
C125 C130 H111 109.5 . . ?
H109 C130 H111 109.5 . . ?
H110 C130 H111 109.5 . . ?
C126 C131 H112 109.5 . . ?
C126 C131 H113 109.5 . . ?
H112 C131 H113 109.5 . . ?
C126 C131 H114 109.5 . . ?
H112 C131 H114 109.5 . . ?
H113 C131 H114 109.5 . . ?
C127 C132 H115 109.5 . . ?
C127 C132 H116 109.5 . . ?
H115 C132 H116 109.5 . . ?
C127 C132 H117 109.5 . . ?
H115 C132 H117 109.5 . . ?
H116 C132 H117 109.5 . . ?
C128 C133 H118 109.5 . . ?
C128 C133 H119 109.5 . . ?
H118 C133 H119 109.5 . . ?
C128 C133 H120 109.5 . . ?
H118 C133 H120 109.5 . . ?
H119 C133 H120 109.5 . . ?
C129 C134 H121 109.5 . . ?
C129 C134 H122 109.5 . . ?
H121 C134 H122 109.5 . . ?
C129 C134 H123 109.5 . . ?
H121 C134 H123 109.5 . . ?
H122 C134 H123 109.5 . . ?
C136 C135 C139 108.0 . . ?
C136 C135 C140 126.0 . . ?
C139 C135 C140 126.0 . . ?
C136 C135 Ru9 70.7(4) . . ?
C139 C135 Ru9 71.7(4) . . ?
C140 C135 Ru9 123.3(3) . . ?
C137 C136 C135 108.0 . . ?
C137 C136 C141 126.0 . . ?
C135 C136 C141 126.0 . . ?
C137 C136 Ru9 71.9(3) . . ?
C135 C136 Ru9 70.3(4) . . ?
C141 C136 Ru9 123.4(3) . . ?
C136 C137 C138 108.0 . . ?
C136 C137 C142 126.0 . . ?
C138 C137 C142 126.0 . . ?
C136 C137 Ru9 69.4(3) . . ?
C138 C137 Ru9 71.5(4) . . ?
C142 C137 Ru9 124.7(3) . . ?
C137 C138 C139 108.0 . . ?
C137 C138 C143 126.0 . . ?
C139 C138 C143 126.0 . . ?
C137 C138 Ru9 70.3(4) . . ?
C139 C138 Ru9 70.0(3) . . ?
C143 C138 Ru9 125.3(3) . . ?
C138 C139 C135 108.0 . . ?
C138 C139 C144 126.0 . . ?
C135 C139 C144 126.0 . . ?
C138 C139 Ru9 71.7(3) . . ?
C135 C139 Ru9 69.5(3) . . ?
C144 C139 Ru9 124.4(3) . . ?
C135 C140 H124 109.5 . . ?
C135 C140 H125 109.5 . . ?
H124 C140 H125 109.5 . . ?
C135 C140 H126 109.5 . . ?
H124 C140 H126 109.5 . . ?
H125 C140 H126 109.5 . . ?
C136 C141 H127 109.5 . . ?
C136 C141 H128 109.5 . . ?
H127 C141 H128 109.5 . . ?
C136 C141 H129 109.5 . . ?
H127 C141 H129 109.5 . . ?
H128 C141 H129 109.5 . . ?
C137 C142 H130 109.5 . . ?
C137 C142 H131 109.5 . . ?
H130 C142 H131 109.5 . . ?
C137 C142 H132 109.5 . . ?
H130 C142 H132 109.5 . . ?
H131 C142 H132 109.5 . . ?
C138 C143 H133 109.5 . . ?
C138 C143 H134 109.5 . . ?
H133 C143 H134 109.5 . . ?
C138 C143 H135 109.5 . . ?
H133 C143 H135 109.5 . . ?
H134 C143 H135 109.5 . . ?
C139 C144 H136 109.5 . . ?
C139 C144 H137 109.5 . . ?
H136 C144 H137 109.5 . . ?
C139 C144 H138 109.5 . . ?
H136 C144 H138 109.5 . . ?
H137 C144 H138 109.5 . . ?
C146 C145 C150 120.0 . . ?
C146 C145 C154 118.67(8) . . ?
C150 C145 C154 121.21(8) . . ?
C146 C145 Ru11 70.85(9) . . ?
C150 C145 Ru11 73.75(8) . . ?
C154 C145 Ru11 130.96(16) . . ?
C147 C146 C145 120.0 . . ?
C147 C146 Ru11 73.45(8) . . ?
C145 C146 Ru11 71.32(9) . . ?
C147 C146 H139 120.0 . . ?
C145 C146 H139 120.0 . . ?
Ru11 C146 H139 127.2 . . ?
C146 C147 C148 120.0 . . ?
C146 C147 Ru11 69.19(7) . . ?
C148 C147 Ru11 74.12(7) . . ?
C146 C147 H140 120.0 . . ?
C148 C147 H140 120.0 . . ?
Ru11 C147 H140 129.0 . . ?
C149 C148 C147 120.0 . . ?
C149 C148 C151 112.35(7) . . ?
C147 C148 C151 127.22(7) . . ?
C149 C148 Ru11 72.29(9) . . ?
C147 C148 Ru11 69.50(7) . . ?
C151 C148 Ru11 137.10(14) . . ?
C148 C149 C150 120.0 . . ?
C148 C149 Ru11 71.84(9) . . ?
C150 C149 Ru11 69.81(8) . . ?
C148 C149 H141 120.0 . . ?
C150 C149 H141 120.0 . . ?
Ru11 C149 H141 131.1 . . ?
C149 C150 C145 120.0 . . ?
C149 C150 Ru11 73.96(8) . . ?
C145 C150 Ru11 69.04(7) . . ?
C149 C150 H142 120.0 . . ?
C145 C150 H142 120.0 . . ?
Ru11 C150 H142 129.3 . . ?
C148 C151 C153 111.47(10) . . ?
C148 C151 C152 110.07(9) . . ?
C153 C151 C152 108.67(10) . . ?
C148 C151 H143 108.9 . . ?
C153 C151 H143 108.9 . . ?
C152 C151 H143 108.9 . . ?
C151 C152 H144 109.5 . . ?
C151 C152 H145 109.5 . . ?
H144 C152 H145 109.5 . . ?
C151 C152 H146 109.5 . . ?
H144 C152 H146 109.5 . . ?
H145 C152 H146 109.5 . . ?
C151 C153 H147 109.5 . . ?
C151 C153 H148 109.5 . . ?
H147 C153 H148 109.5 . . ?
C151 C153 H149 109.5 . . ?
H147 C153 H149 109.5 . . ?
H148 C153 H149 109.5 . . ?
C145 C154 H150 109.5 . . ?
C145 C154 H151 109.5 . . ?
H150 C154 H151 109.5 . . ?
C145 C154 H152 109.5 . . ?
H150 C154 H152 109.5 . . ?
H151 C154 H152 109.5 . . ?
C156 C155 C160 120.0 . . ?
C156 C155 C164 118.69(9) . . ?
C160 C155 C164 121.24(8) . . ?
C156 C155 Ru12 74.0(2) . . ?
C160 C155 Ru12 69.8(3) . . ?
C164 C155 Ru12 125.8(3) . . ?
C157 C156 C155 120.0 . . ?
C157 C156 Ru12 72.62(9) . . ?
C155 C156 Ru12 69.70(18) . . ?
C157 C156 H153 120.0 . . ?
C155 C156 H153 120.0 . . ?
Ru12 C156 H153 130.2 . . ?
C156 C157 C158 120.0 . . ?
C156 C157 Ru12 71.59(12) . . ?
C158 C157 Ru12 70.4(2) . . ?
C156 C157 H154 120.0 . . ?
C158 C157 H154 120.0 . . ?
Ru12 C157 H154 130.6 . . ?
C159 C158 C157 120.0 . . ?
C159 C158 C161 112.38(8) . . ?
C157 C158 C161 127.25(7) . . ?
C159 C158 Ru12 69.4(2) . . ?
C157 C158 Ru12 73.6(3) . . ?
C161 C158 Ru12 134.5(2) . . ?
C158 C159 C160 120.0 . . ?
C158 C159 Ru12 73.76(18) . . ?
C160 C159 Ru12 70.75(9) . . ?
C158 C159 H155 120.0 . . ?
C160 C159 H155 120.0 . . ?
Ru12 C159 H155 127.5 . . ?
C159 C160 C155 120.0 . . ?
C159 C160 Ru12 71.81(14) . . ?
C155 C160 Ru12 73.1(2) . . ?
C159 C160 H156 120.0 . . ?
C155 C160 H156 120.0 . . ?
Ru12 C160 H156 127.1 . . ?
C158 C161 C163 111.49(10) . . ?
C158 C161 C162 110.09(10) . . ?
C163 C161 C162 108.68(11) . . ?
C158 C161 H157 108.8 . . ?
C163 C161 H157 108.8 . . ?
C162 C161 H157 108.8 . . ?
C161 C162 H158 109.5 . . ?
C161 C162 H159 109.5 . . ?
H158 C162 H159 109.5 . . ?
C161 C162 H160 109.5 . . ?
H158 C162 H160 109.5 . . ?
H159 C162 H160 109.5 . . ?
C161 C163 H161 109.5 . . ?
C161 C163 H162 109.5 . . ?
H161 C163 H162 109.5 . . ?
C161 C163 H163 109.5 . . ?
H161 C163 H163 109.5 . . ?
H162 C163 H163 109.5 . . ?
C155 C164 H164 109.5 . . ?
C155 C164 H165 109.5 . . ?
H164 C164 H165 109.5 . . ?
C155 C164 H166 109.5 . . ?
H164 C164 H166 109.5 . . ?
H165 C164 H166 109.5 . . ?
C83 Co5 C84 89.9(11) . . ?
C83 Co5 C85 89.4(10) . . ?
C84 Co5 C85 93.3(9) . . ?
C83 Co5 C95 90.5(8) . . ?
C84 Co5 C95 136.8(8) . . ?
C85 Co5 C95 130.0(8) . . ?
C83 Co5 C99 113.9(9) . . ?
C84 Co5 C99 154.7(10) . . ?
C85 Co5 C99 95.3(7) . . ?
C95 Co5 C99 40.7(3) . . ?
C83 Co5 C96 105.6(9) . . ?
C84 Co5 C96 98.3(8) . . ?
C85 Co5 C96 160.9(8) . . ?
C95 Co5 C96 40.5(3) . . ?
C99 Co5 C96 68.0(3) . . ?
C83 Co5 C98 154.1(9) . . ?
C84 Co5 C98 115.4(10) . . ?
C85 Co5 C98 93.8(8) . . ?
C95 Co5 C98 67.9(4) . . ?
C99 Co5 C98 40.3(3) . . ?
C96 Co5 C98 67.5(4) . . ?
C83 Co5 C97 144.6(9) . . ?
C84 Co5 C97 88.1(9) . . ?
C85 Co5 C97 126.0(9) . . ?
C95 Co5 C97 67.8(4) . . ?
C99 Co5 C97 67.6(4) . . ?
C96 Co5 C97 40.1(3) . . ?
C98 Co5 C97 40.0(3) . . ?
C83 Co5 Cs2 54.8(7) . . ?
C84 Co5 Cs2 56.6(8) . . ?
C85 Co5 Cs2 54.7(6) . . ?
C95 Co5 Cs2 145.0(4) . . ?
C99 Co5 Cs2 144.6(4) . . ?
C96 Co5 Cs2 144.1(5) . . ?
C98 Co5 Cs2 143.5(4) . . ?
C97 Co5 Cs2 143.2(4) . . ?
C87 Co6 C86 92.8(8) . . ?
C87 Co6 C88 88.8(9) . . ?
C86 Co6 C88 89.8(9) . . ?
C87 Co6 C195 138.8(17) . . ?
C86 Co6 C195 90.3(15) . . ?
C88 Co6 C195 132.4(17) . . ?
C87 Co6 C199 99.5(16) . . ?
C86 Co6 C199 111.1(18) . . ?
C88 Co6 C199 156.9(17) . . ?
C195 Co6 C199 42.1(11) . . ?
C87 Co6 C102 144.0(11) . . ?
C86 Co6 C102 123.2(11) . . ?
C88 Co6 C102 90.2(10) . . ?
C195 Co6 C102 51.5(18) . . ?
C199 Co6 C102 70.3(16) . . ?
C87 Co6 C103 104.4(11) . . ?
C86 Co6 C103 159.2(11) . . ?
C88 Co6 C103 101.9(11) . . ?
C195 Co6 C103 69.1(16) . . ?
C199 Co6 C103 55.2(18) . . ?
C102 Co6 C103 40.9(6) . . ?
C87 Co6 C101 153.7(10) . . ?
C86 Co6 C101 91.5(10) . . ?
C88 Co6 C101 117.2(10) . . ?
C195 Co6 C101 15.2(18) . . ?
C199 Co6 C101 54.9(16) . . ?
C102 Co6 C101 40.5(6) . . ?
C103 Co6 C101 67.9(9) . . ?
C87 Co6 C196 156.1(16) . . ?
C86 Co6 C196 110.7(17) . . ?
C88 Co6 C196 95.3(16) . . ?
C195 Co6 C196 41.3(11) . . ?
C199 Co6 C196 68.7(16) . . ?
C102 Co6 C196 13(2) . . ?
C103 Co6 C196 51.7(18) . . ?
C101 Co6 C196 28.5(19) . . ?
C87 Co6 C104 90.9(10) . . ?
C86 Co6 C104 130.0(11) . . ?
C88 Co6 C104 140.2(11) . . ?
C195 Co6 C104 57.1(15) . . ?
C199 Co6 C104 20.0(18) . . ?
C102 Co6 C104 67.7(9) . . ?
C103 Co6 C104 40.0(6) . . ?
C101 Co6 C104 66.7(8) . . ?
C196 Co6 C104 71.0(16) . . ?
C87 Co6 C100 114.2(10) . . ?
C86 Co6 C100 95.6(10) . . ?
C88 Co6 C100 156.0(9) . . ?
C195 Co6 C100 24.8(17) . . ?
C199 Co6 C100 20.2(17) . . ?
C102 Co6 C100 67.3(8) . . ?
C103 Co6 C100 66.9(8) . . ?
C101 Co6 C100 39.5(5) . . ?
C196 Co6 C100 61.0(16) . . ?
C104 Co6 C100 39.3(5) . . ?
C87 Co6 C198 91.6(16) . . ?
C86 Co6 C198 150.7(19) . . ?
C88 Co6 C198 119.2(19) . . ?
C195 Co6 C198 67.9(16) . . ?
C199 Co6 C198 39.7(11) . . ?
C102 Co6 C198 58.0(18) . . ?
C103 Co6 C198 21(2) . . ?
C101 Co6 C198 72.6(16) . . ?
C196 Co6 C198 65.9(16) . . ?
C104 Co6 C198 21.0(19) . . ?
C100 Co6 C198 56.5(17) . . ?
C91 Co7 C89 89.0(11) . . ?
C91 Co7 C90 92.9(8) . . ?
C89 Co7 C90 91.3(10) . . ?
C91 Co7 C108 158.9(9) . . ?
C89 Co7 C108 109.7(9) . . ?
C90 Co7 C108 96.4(7) . . ?
C91 Co7 C109 134.3(8) . . ?
C89 Co7 C109 90.2(9) . . ?
C90 Co7 C109 132.9(7) . . ?
C108 Co7 C109 39.9(3) . . ?
C91 Co7 C107 121.5(10) . . ?
C89 Co7 C107 149.4(9) . . ?
C90 Co7 C107 90.3(7) . . ?
C108 Co7 C107 39.8(3) . . ?
C109 Co7 C107 66.8(4) . . ?
C91 Co7 C105 98.4(7) . . ?
C89 Co7 C105 109.0(9) . . ?
C90 Co7 C105 156.8(7) . . ?
C108 Co7 C105 66.8(3) . . ?
C109 Co7 C105 39.7(2) . . ?
C107 Co7 C105 66.6(4) . . ?
C91 Co7 C106 92.3(8) . . ?
C89 Co7 C106 148.3(9) . . ?
C90 Co7 C106 120.2(8) . . ?
C108 Co7 C106 66.7(4) . . ?
C109 Co7 C106 66.6(3) . . ?
C107 Co7 C106 39.6(3) . . ?
C105 Co7 C106 39.5(2) . . ?
C94 Co8 C92 90.6(9) . . ?
C94 Co8 C93 94.0(9) . . ?
C92 Co8 C93 92.4(8) . . ?
C94 Co8 C113 146.6(8) . . ?
C92 Co8 C113 90.1(8) . . ?
C93 Co8 C113 119.3(9) . . ?
C94 Co8 C112 147.3(8) . . ?
C92 Co8 C112 121.5(8) . . ?
C93 Co8 C112 90.9(8) . . ?
C113 Co8 C112 40.4(3) . . ?
C94 Co8 C114 106.5(8) . . ?
C92 Co8 C114 95.4(7) . . ?
C93 Co8 C114 157.9(8) . . ?
C113 Co8 C114 40.3(3) . . ?
C112 Co8 C114 67.5(4) . . ?
C94 Co8 C111 107.5(8) . . ?
C92 Co8 C111 157.4(8) . . ?
C93 Co8 C111 99.6(7) . . ?
C113 Co8 C111 67.3(4) . . ?
C112 Co8 C111 39.9(3) . . ?
C114 Co8 C111 66.9(4) . . ?
C94 Co8 C110 87.8(7) . . ?
C92 Co8 C110 131.3(7) . . ?
C93 Co8 C110 136.3(7) . . ?
C113 Co8 C110 67.2(4) . . ?
C112 Co8 C110 67.0(4) . . ?
C114 Co8 C110 39.7(3) . . ?
C111 Co8 C110 39.5(3) . . ?
C94 Co8 Cs2 56.5(6) . . ?
C92 Co8 Cs2 56.7(6) . . ?
C93 Co8 Cs2 56.0(6) . . ?
C113 Co8 Cs2 144.0(5) . . ?
C112 Co8 Cs2 145.0(4) . . ?
C114 Co8 Cs2 143.5(4) . . ?
C111 Co8 Cs2 145.3(5) . . ?
C110 Co8 Cs2 144.4(4) . . ?
N85 Cs2 N87 89.2(4) . . ?
N85 Cs2 N92 160.9(4) . . ?
N87 Cs2 N92 91.7(4) . . ?
N85 Cs2 N84 75.8(4) . . ?
N87 Cs2 N84 120.8(4) . . ?
N92 Cs2 N84 119.4(4) . . ?
N85 Cs2 C85 19.3(2) . . ?
N87 Cs2 C85 88.2(4) . . ?
N92 Cs2 C85 179.8(4) . . ?
N84 Cs2 C85 60.4(4) . . ?
N85 Cs2 N94 123.9(4) . . ?
N87 Cs2 N94 119.9(4) . . ?
N92 Cs2 N94 71.6(4) . . ?
N84 Cs2 N94 48.2(4) . . ?
C85 Cs2 N94 108.3(4) . . ?
N85 Cs2 C83 59.4(4) . . ?
N87 Cs2 C83 64.8(4) . . ?
N92 Cs2 C83 137.2(4) . . ?
N84 Cs2 C83 58.3(4) . . ?
C85 Cs2 C83 42.6(4) . . ?
N94 Cs2 C83 89.2(4) . . ?
N85 Cs2 N90 93.9(4) . . ?
N87 Cs2 N90 165.2(4) . . ?
N92 Cs2 N90 90.1(4) . . ?
N84 Cs2 N90 46.7(4) . . ?
C85 Cs2 N90 89.9(4) . . ?
N94 Cs2 N90 47.3(3) . . ?
C83 Cs2 N90 104.6(4) . . ?
N85 Cs2 N88 46.7(4) . . ?
N87 Cs2 N88 71.0(4) . . ?
N92 Cs2 N88 116.1(4) . . ?
N84 Cs2 N88 122.2(4) . . ?
C85 Cs2 N88 64.1(4) . . ?
N94 Cs2 N88 167.6(3) . . ?
C83 Cs2 N88 90.6(4) . . ?
N90 Cs2 N88 121.1(3) . . ?
N85 Cs2 N91 47.7(4) . . ?
N87 Cs2 N91 118.4(4) . . ?
N92 Cs2 N91 116.4(4) . . ?
N84 Cs2 N91 92.6(4) . . ?
C85 Cs2 N91 63.8(4) . . ?
N94 Cs2 N91 120.8(4) . . ?
C83 Cs2 N91 106.3(4) . . ?
N90 Cs2 N91 73.6(4) . . ?
N88 Cs2 N91 47.6(3) . . ?
N85 Cs2 C84 61.2(4) . . ?
N87 Cs2 C84 106.5(4) . . ?
N92 Cs2 C84 136.1(4) . . ?
N84 Cs2 C84 18.8(2) . . ?
C85 Cs2 C84 43.7(4) . . ?
N94 Cs2 C84 64.7(4) . . ?
C83 Cs2 C84 41.9(4) . . ?
N90 Cs2 C84 63.0(4) . . ?
N88 Cs2 C84 107.6(4) . . ?
N91 Cs2 C84 89.9(4) . . ?
N85 Cs2 N93 118.1(4) . . ?
N87 Cs2 N93 46.6(4) . . ?
N92 Cs2 N93 75.2(4) . . ?
N84 Cs2 N93 91.4(4) . . ?
C85 Cs2 N93 104.6(4) . . ?
N94 Cs2 N93 73.3(4) . . ?
C83 Cs2 N93 62.6(4) . . ?
N90 Cs2 N93 120.1(4) . . ?
N88 Cs2 N93 117.4(3) . . ?
N91 Cs2 N93 163.3(4) . . ?
C84 Cs2 N93 88.7(4) . . ?
N88 Ru7 N85 85.3(7) . . ?
N88 Ru7 N91 87.5(7) . . ?
N85 Ru7 N91 86.5(7) . . ?
N88 Ru7 C119 103.8(6) . . ?
N85 Ru7 C119 114.7(6) . . ?
N91 Ru7 C119 156.3(5) . . ?
N88 Ru7 C115 97.2(6) . . ?
N85 Ru7 C115 153.1(5) . . ?
N91 Ru7 C115 120.3(6) . . ?
C119 Ru7 C115 38.66(18) . . ?
N88 Ru7 C118 138.7(6) . . ?
N85 Ru7 C118 96.4(6) . . ?
N91 Ru7 C118 133.7(6) . . ?
C119 Ru7 C118 38.58(19) . . ?
C115 Ru7 C118 64.3(3) . . ?
N88 Ru7 C116 124.3(6) . . ?
N85 Ru7 C116 150.3(6) . . ?
N91 Ru7 C116 92.3(5) . . ?
C119 Ru7 C116 64.1(3) . . ?
C115 Ru7 C116 38.08(17) . . ?
C118 Ru7 C116 63.6(3) . . ?
N88 Ru7 C117 160.5(6) . . ?
N85 Ru7 C117 113.2(6) . . ?
N91 Ru7 C117 99.0(6) . . ?
C119 Ru7 C117 64.0(3) . . ?
C115 Ru7 C117 63.7(3) . . ?
C118 Ru7 C117 38.0(2) . . ?
C116 Ru7 C117 37.68(18) . . ?
N88 Ru7 Cs2 52.5(5) . . ?
N85 Ru7 Cs2 50.9(5) . . ?
N91 Ru7 Cs2 53.4(5) . . ?
C119 Ru7 Cs2 148.8(3) . . ?
C115 Ru7 Cs2 146.5(3) . . ?
C118 Ru7 Cs2 147.2(3) . . ?
C116 Ru7 Cs2 143.8(3) . . ?
C117 Ru7 Cs2 144.3(3) . . ?
N93 Ru8 N87 86.9(7) . . ?
N93 Ru8 C125 116.2(6) . . ?
N87 Ru8 C125 97.6(6) . . ?
N93 Ru8 C129 154.8(6) . . ?
N87 Ru8 C129 96.4(5) . . ?
C125 Ru8 C129 38.68(16) . . ?
N93 Ru8 N83 86.1(7) . . ?
N87 Ru8 N83 87.2(7) . . ?
C125 Ru8 N83 157.3(6) . . ?
C129 Ru8 N83 118.9(6) . . ?
N93 Ru8 C126 94.8(6) . . ?
N87 Ru8 C126 130.5(6) . . ?
C125 Ru8 C126 38.41(16) . . ?
C129 Ru8 C126 64.1(2) . . ?
N83 Ru8 C126 142.3(6) . . ?
N93 Ru8 C128 145.3(6) . . ?
N87 Ru8 C128 127.8(6) . . ?
C125 Ru8 C128 64.0(2) . . ?
C129 Ru8 C128 38.09(17) . . ?
N83 Ru8 C128 95.6(6) . . ?
C126 Ru8 C128 63.3(2) . . ?
N93 Ru8 C127 108.9(6) . . ?
N87 Ru8 C127 159.2(5) . . ?
C125 Ru8 C127 63.7(2) . . ?
C129 Ru8 C127 63.5(2) . . ?
N83 Ru8 C127 106.7(6) . . ?
C126 Ru8 C127 37.70(17) . . ?
C128 Ru8 C127 37.52(17) . . ?
N93 Ru8 Cs2 52.8(5) . . ?
N87 Ru8 Cs2 50.8(5) . . ?
C125 Ru8 Cs2 143.0(3) . . ?
C129 Ru8 Cs2 143.7(3) . . ?
N83 Ru8 Cs2 53.8(5) . . ?
C126 Ru8 Cs2 146.7(3) . . ?
C128 Ru8 Cs2 147.9(3) . . ?
C127 Ru8 Cs2 149.9(3) . . ?
N90 Ru9 N94 87.9(7) . . ?
N90 Ru9 C135 99.1(5) . . ?
N94 Ru9 C135 120.7(6) . . ?
N90 Ru9 C136 101.2(6) . . ?
N94 Ru9 C136 158.6(6) . . ?
C135 Ru9 C136 39.02(15) . . ?
N90 Ru9 C139 129.4(5) . . ?
N94 Ru9 C139 94.3(6) . . ?
C135 Ru9 C139 38.78(16) . . ?
C136 Ru9 C139 64.9(2) . . ?
N90 Ru9 N84 84.6(6) . . ?
N94 Ru9 N84 86.3(7) . . ?
C135 Ru9 N84 152.7(6) . . ?
C136 Ru9 N84 113.6(6) . . ?
C139 Ru9 N84 146.0(5) . . ?
N90 Ru9 C137 133.8(6) . . ?
N94 Ru9 C137 138.2(6) . . ?
C135 Ru9 C137 64.9(2) . . ?
C136 Ru9 C137 38.67(18) . . ?
C139 Ru9 C137 64.4(2) . . ?
N84 Ru9 C137 93.0(6) . . ?
N90 Ru9 C138 163.4(5) . . ?
N94 Ru9 C138 102.9(6) . . ?
C135 Ru9 C138 64.6(2) . . ?
C136 Ru9 C138 64.5(2) . . ?
C139 Ru9 C138 38.30(17) . . ?
N84 Ru9 C138 108.4(5) . . ?
C137 Ru9 C138 38.24(17) . . ?
N90 Ru9 Cs2 52.2(4) . . ?
N94 Ru9 Cs2 52.2(5) . . ?
C135 Ru9 Cs2 147.2(3) . . ?
C136 Ru9 Cs2 146.9(3) . . ?
C139 Ru9 Cs2 145.5(3) . . ?
N84 Ru9 Cs2 52.1(5) . . ?
C137 Ru9 Cs2 145.0(3) . . ?
C138 Ru9 Cs2 144.2(3) . . ?
N92 Ru10 N86 85.5(6) . . ?
N92 Ru10 N89 87.0(7) . . ?
N86 Ru10 N89 85.6(7) . . ?
N92 Ru10 S4 149.4(5) . . ?
N86 Ru10 S4 123.9(5) . . ?
N89 Ru10 S4 87.0(5) . . ?
N92 Ru10 S3 89.3(6) . . ?
N86 Ru10 S3 108.1(5) . . ?
N89 Ru10 S3 165.4(6) . . ?
S4 Ru10 S3 89.1(3) . . ?
N92 Ru10 Ru11 140.4(5) . . ?
N86 Ru10 Ru11 97.3(5) . . ?
N89 Ru10 Ru11 132.6(5) . . ?
S4 Ru10 Ru11 52.3(2) . . ?
S3 Ru10 Ru11 52.1(2) . . ?
N92 Ru10 Ru12 106.0(5) . . ?
N86 Ru10 Ru12 154.9(5) . . ?
N89 Ru10 Ru12 116.7(5) . . ?
S4 Ru10 Ru12 51.5(2) . . ?
S3 Ru10 Ru12 51.14(19) . . ?
Ru11 Ru10 Ru12 59.49(9) . . ?
C146 Ru11 C145 37.8 . . ?
C146 Ru11 C147 37.4 . . ?
C145 Ru11 C147 67.34(8) . . ?
C146 Ru11 C150 67.23(8) . . ?
C145 Ru11 C150 37.2 . . ?
C147 Ru11 C150 78.32(10) . . ?
C146 Ru11 S3 105.5(2) . . ?
C145 Ru11 S3 94.5(2) . . ?
C147 Ru11 S3 137.0(2) . . ?
C150 Ru11 S3 111.1(2) . . ?
C146 Ru11 S4 144.3(3) . . ?
C145 Ru11 S4 175.4(2) . . ?
C147 Ru11 S4 112.6(2) . . ?
C150 Ru11 S4 138.3(2) . . ?
S3 Ru11 S4 88.6(3) . . ?
C146 Ru11 C148 66.37(9) . . ?
C145 Ru11 C148 78.30(10) . . ?
C147 Ru11 C148 36.4 . . ?
C150 Ru11 C148 65.31(8) . . ?
S3 Ru11 C148 171.8(2) . . ?
S4 Ru11 C148 98.9(2) . . ?
C146 Ru11 C149 78.30(10) . . ?
C145 Ru11 C149 66.17(8) . . ?
C147 Ru11 C149 65.40(8) . . ?
C150 Ru11 C149 36.2 . . ?
S3 Ru11 C149 143.9(2) . . ?
S4 Ru11 C149 109.4(2) . . ?
C148 Ru11 C149 35.9 . . ?
C146 Ru11 Ru10 112.61(11) . . ?
C145 Ru11 Ru10 133.06(11) . . ?
C147 Ru11 Ru10 112.15(12) . . ?
C150 Ru11 Ru10 163.25(13) . . ?
S3 Ru11 Ru10 52.3(2) . . ?
S4 Ru11 Ru10 51.5(2) . . ?
C148 Ru11 Ru10 130.88(13) . . ?
C149 Ru11 Ru10 159.60(12) . . ?
C146 Ru11 Ru12 156.64(13) . . ?
C145 Ru11 Ru12 127.64(13) . . ?
C147 Ru11 Ru12 164.68(13) . . ?
C150 Ru11 Ru12 111.50(12) . . ?
S3 Ru11 Ru12 52.1(2) . . ?
S4 Ru11 Ru12 52.2(2) . . ?
C148 Ru11 Ru12 135.76(12) . . ?
C149 Ru11 Ru12 115.16(11) . . ?
Ru10 Ru11 Ru12 61.47(9) . . ?
C160 Ru12 C159 37.44(13) . . ?
C160 Ru12 C155 37.17(8) . . ?
C159 Ru12 C155 66.81(16) . . ?
C160 Ru12 C158 66.57(18) . . ?
C159 Ru12 C158 36.81(10) . . ?
C155 Ru12 C158 77.78(13) . . ?
C160 Ru12 S3 98.5(3) . . ?
C159 Ru12 S3 106.3(3) . . ?
C155 Ru12 S3 116.7(2) . . ?
C158 Ru12 S3 134.8(2) . . ?
C160 Ru12 S4 170.2(2) . . ?
C159 Ru12 S4 146.7(2) . . ?
C155 Ru12 S4 133.1(2) . . ?
C158 Ru12 S4 113.3(2) . . ?
S3 Ru12 S4 88.2(3) . . ?
C160 Ru12 C156 66.07(11) . . ?
C159 Ru12 C156 77.77(13) . . ?
C155 Ru12 C156 36.33(8) . . ?
C158 Ru12 C156 64.97(11) . . ?
S3 Ru12 C156 149.8(2) . . ?
S4 Ru12 C156 104.6(2) . . ?
C160 Ru12 C157 77.76(13) . . ?
C159 Ru12 C157 65.62(12) . . ?
C155 Ru12 C157 65.17(12) . . ?
C158 Ru12 C157 36.01(6) . . ?
S3 Ru12 C157 170.8(2) . . ?
S4 Ru12 C157 96.6(2) . . ?
C156 Ru12 C157 35.79(9) . . ?
C160 Ru12 Ru11 127.96(16) . . ?
C159 Ru12 Ru11 156.51(15) . . ?
C155 Ru12 Ru11 112.02(13) . . ?
C158 Ru12 Ru11 165.24(16) . . ?
S3 Ru12 Ru11 51.9(2) . . ?
S4 Ru12 Ru11 51.9(2) . . ?
C156 Ru12 Ru11 115.95(16) . . ?
C157 Ru12 Ru11 136.72(15) . . ?
C160 Ru12 Ru10 139.35(15) . . ?
C159 Ru12 Ru10 117.32(19) . . ?
C155 Ru12 Ru10 167.42(13) . . ?
C158 Ru12 Ru10 112.89(14) . . ?
S3 Ru12 Ru10 51.2(2) . . ?
S4 Ru12 Ru10 50.4(2) . . ?
C156 Ru12 Ru10 153.44(16) . . ?
C157 Ru12 Ru10 127.37(15) . . ?
Ru11 Ru12 Ru10 59.04(9) . . ?
Ru11 S3 Ru12 76.0(2) . . ?
Ru11 S3 Ru10 75.6(3) . . ?
Ru12 S3 Ru10 77.7(2) . . ?
Ru10 S4 Ru11 76.2(2) . . ?
Ru10 S4 Ru12 78.2(3) . . ?
Ru11 S4 Ru12 75.9(3) . . ?
F4 P1 F1 90.0 . . ?
F4 P1 F2 90.0 . . ?
F1 P1 F2 180.0 . . ?
F4 P1 F5 90.0 . . ?
F1 P1 F5 90.0 . . ?
F2 P1 F5 90.0 . . ?
F4 P1 F6 90.0 . . ?
F1 P1 F6 90.0 . . ?
F2 P1 F6 90.0 . . ?
F5 P1 F6 180.0 . . ?
F4 P1 F3 180.0 . . ?
F1 P1 F3 90.0 . . ?
F2 P1 F3 90.0 . . ?
F5 P1 F3 90.0 . . ?
F6 P1 F3 90.0 . . ?
F8 P2 F12 90.0 . . ?
F8 P2 F11 90.0 . . ?
F12 P2 F11 180.0 . . ?
F8 P2 F7 180.0 . . ?
F12 P2 F7 90.0 . . ?
F11 P2 F7 90.0 . . ?
F8 P2 F10 90.0 . . ?
F12 P2 F10 90.0 . . ?
F11 P2 F10 90.0 . . ?
F7 P2 F10 90.0 . . ?
F8 P2 F9 90.0 . . ?
F12 P2 F9 90.0 . . ?
F11 P2 F9 90.0 . . ?
F7 P2 F9 90.0 . . ?
F10 P2 F9 180.0 . . ?
F30 P5 F26 90.0 . . ?
F30 P5 F28 90.0 . . ?
F26 P5 F28 90.0 . . ?
F30 P5 F29 180.0 . . ?
F26 P5 F29 90.0 . . ?
F28 P5 F29 90.0 . . ?
F30 P5 F27 90.0 . . ?
F26 P5 F27 90.0 . . ?
F28 P5 F27 180.0 . . ?
F29 P5 F27 90.0 . . ?
F30 P5 F25 90.0 . . ?
F26 P5 F25 180.0(13) . . ?
F28 P5 F25 90.0 . . ?
F29 P5 F25 90.0 . . ?
F27 P5 F25 90.0 . . ?
F13 P3 F16 90.0 . . ?
F13 P3 F18 90.0 . . ?
F16 P3 F18 90.0 . . ?
F13 P3 F14 180.0 . . ?
F16 P3 F14 90.0 . . ?
F18 P3 F14 90.0 . . ?
F13 P3 F17 90.0 . . ?
F16 P3 F17 90.0 . . ?
F18 P3 F17 180.0 . . ?
F14 P3 F17 90.0 . . ?
F13 P3 F15 90.0 . . ?
F16 P3 F15 180.0 . . ?
F18 P3 F15 90.0 . . ?
F14 P3 F15 90.0 . . ?
F17 P3 F15 90.0 . . ?
F21 P4 F19 90.0 . . ?
F21 P4 F20 90.0 . . ?
F19 P4 F20 180.0(6) . . ?
F21 P4 F24 90.0 . . ?
F19 P4 F24 90.0 . . ?
F20 P4 F24 90.0 . . ?
F21 P4 F23 90.0 . . ?
F19 P4 F23 90.0 . . ?
F20 P4 F23 90.0 . . ?
F24 P4 F23 180.0 . . ?
F21 P4 F22 180.0 . . ?
F19 P4 F22 90.0 . . ?
F20 P4 F22 90.0 . . ?
F24 P4 F22 90.0 . . ?
F23 P4 F22 90.0 . . ?
F34 P6 F35 90.0 . . ?
F34 P6 F32 90.0 . . ?
F35 P6 F32 90.0 . . ?
F34 P6 F31 90.0 . . ?
F35 P6 F31 90.0 . . ?
F32 P6 F31 179.98(5) . . ?
F34 P6 F36 90.0 . . ?
F35 P6 F36 180.0 . . ?
F32 P6 F36 90.0 . . ?
F31 P6 F36 90.0 . . ?
F34 P6 F33 179.99(6) . . ?
F35 P6 F33 90.0 . . ?
F32 P6 F33 90.0 . . ?
F31 P6 F33 90.0 . . ?
F36 P6 F33 90.0 . . ?
C166 C165 H207 109.5 . . ?
C166 C165 H208 109.5 . . ?
H207 C165 H208 109.5 . . ?
C166 C165 H209 109.5 . . ?
H207 C165 H209 109.5 . . ?
H208 C165 H209 109.5 . . ?
N166 C166 C165 180.0 . . ?
C168 C167 H210 109.5 . . ?
C168 C167 H211 109.5 . . ?
H210 C167 H211 109.5 . . ?
C168 C167 H212 109.5 . . ?
H210 C167 H212 109.5 . . ?
H211 C167 H212 109.5 . . ?
N168 C168 C167 180.0 . . ?
C170 C169 H213 109.5 . . ?
C170 C169 H214 109.5 . . ?
H213 C169 H214 109.5 . . ?
C170 C169 H215 109.5 . . ?
H213 C169 H215 109.5 . . ?
H214 C169 H215 109.5 . . ?
N170 C170 C169 180.0 . . ?
C172 C171 H216 109.5 . . ?
C172 C171 H217 109.5 . . ?
H216 C171 H217 109.5 . . ?
C172 C171 H218 109.5 . . ?
H216 C171 H218 109.5 . . ?
H217 C171 H218 109.5 . . ?
N172 C172 C171 180.0 . . ?
C174 C173 H219 109.5 . . ?
C174 C173 H220 109.5 . . ?
H219 C173 H220 109.5 . . ?
C174 C173 H221 109.5 . . ?
H219 C173 H221 109.5 . . ?
H220 C173 H221 109.5 . . ?
N174 C174 C173 180(4) . . ?
C176 C175 H222 109.5 . . ?
C176 C175 H223 109.5 . . ?
H222 C175 H223 109.5 . . ?
C176 C175 H224 109.5 . . ?
H222 C175 H224 109.5 . . ?
H223 C175 H224 109.5 . . ?
N176 C176 C175 180.0 . . ?
C178 C177 H225 109.5 . . ?
C178 C177 H226 109.5 . . ?
H225 C177 H226 109.5 . . ?
C178 C177 H227 109.5 . . ?
H225 C177 H227 109.5 . . ?
H226 C177 H227 109.5 . . ?
N178 C178 C177 180.0 . . ?
C180 C179 H228 109.5 . . ?
C180 C179 H229 109.5 . . ?
H228 C179 H229 109.5 . . ?
C180 C179 H230 109.5 . . ?
H228 C179 H230 109.5 . . ?
H229 C179 H230 109.5 . . ?
N180 C180 C179 180.0 . . ?
C182 C181 H231 109.5 . . ?
C182 C181 H232 109.5 . . ?
H231 C181 H232 109.5 . . ?
C182 C181 H233 109.5 . . ?
H231 C181 H233 109.5 . . ?
H232 C181 H233 109.5 . . ?
N182 C182 C181 180.0 . . ?
C184 C183 H234 109.5 . . ?
C184 C183 H235 109.5 . . ?
H234 C183 H235 109.5 . . ?
C184 C183 H236 109.5 . . ?
H234 C183 H236 109.5 . . ?
H235 C183 H236 109.5 . . ?
N184 C184 C183 180.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 N1 1.179(13) . ?
C1 Co1 1.900(18) . ?
C1 Cs1 3.68(2) . ?
C2 N2 1.178(13) . ?
C2 Co1 1.816(17) . ?
C2 Cs1 3.63(2) . ?
C3 N3 1.179(13) . ?
C3 Co1 1.724(18) . ?
C3 Cs1 3.64(3) . ?
C4 N4 1.183(13) . ?
C4 Co2 1.835(18) . ?
C4 Cs1 3.65(2) . ?
C5 N5 1.181(13) . ?
C5 Co2 1.843(17) . ?
C5 Cs1 3.83(2) . ?
C6 N6 1.163(13) . ?
C6 Co2 1.916(19) . ?
C6 Cs1 3.60(2) . ?
C7 N7 1.186(13) . ?
C7 Co3 1.854(16) . ?
C7 Cs1 3.609(18) . ?
C8 N8 1.166(13) . ?
C8 Co3 1.846(18) . ?
C8 Cs1 3.78(2) . ?
C9 N9 1.178(13) . ?
C9 Co3 1.897(19) . ?
C9 Cs1 3.54(3) . ?
C10 N10 1.177(13) . ?
C10 Co4 1.864(16) . ?
C10 Cs1 3.56(2) . ?
C11 N11 1.172(13) . ?
C11 Co4 1.822(19) . ?
C11 Cs1 3.66(2) . ?
C12 N12 1.176(13) . ?
C12 Co4 1.805(17) . ?
C12 Cs1 3.66(2) . ?
N1 Ru2 2.081(18) . ?
N1 Cs1 3.54(2) . ?
N2 Ru1 2.122(16) . ?
N2 Cs1 3.596(16) . ?
N3 Ru3 2.180(17) . ?
N3 Cs1 3.52(2) . ?
N4 Ru2 2.109(17) . ?
N4 Cs1 3.57(2) . ?
N5 Ru4 2.126(17) . ?
N6 Ru3 2.017(18) . ?
N6 Cs1 3.62(2) . ?
N7 Ru1 2.068(16) . ?
N7 Cs1 3.663(18) . ?
N8 Ru4 2.088(17) . ?
N9 Ru3 2.041(19) . ?
N9 Cs1 3.58(2) . ?
N10 Ru2 2.053(16) . ?
N10 Cs1 3.419(18) . ?
N11 Ru1 2.105(18) . ?
N11 Cs1 3.645(19) . ?
N12 Ru4 2.122(17) . ?
N12 Cs1 3.59(2) . ?
C13 C14 1.4200 . ?
C13 C17 1.4200 . ?
C13 Co1 2.067(16) . ?
C13 H1 0.9500 . ?
C14 C15 1.4200 . ?
C14 Co1 2.087(18) . ?
C14 H2 0.9500 . ?
C15 C16 1.4200 . ?
C15 Co1 2.087(17) . ?
C15 H3 0.9500 . ?
C16 C17 1.4200 . ?
C16 Co1 2.067(16) . ?
C16 H4 0.9500 . ?
C17 Co1 2.055(18) . ?
C17 H5 0.9500 . ?
C18 C19 1.4200 . ?
C18 C22 1.4200 . ?
C18 Co2 2.047(15) . ?
C18 H6 0.9500 . ?
C19 C20 1.4200 . ?
C19 Co2 2.089(18) . ?
C19 H7 0.9500 . ?
C20 C21 1.4200 . ?
C20 Co2 2.126(18) . ?
C20 H8 0.9500 . ?
C21 C22 1.4200 . ?
C21 Co2 2.108(18) . ?
C21 H9 0.9500 . ?
C22 Co2 2.060(18) . ?
C22 H10 0.9500 . ?
C23 C27 1.4200 . ?
C23 C24 1.4200 . ?
C23 Co3 2.124(16) . ?
C23 H11 0.9500 . ?
C24 C25 1.4200 . ?
C24 Co3 2.105(18) . ?
C24 H12 0.9500 . ?
C25 C26 1.4200 . ?
C25 Co3 2.084(19) . ?
C25 H13 0.9500 . ?
C26 C27 1.4200 . ?
C26 Co3 2.090(19) . ?
C26 H14 0.9500 . ?
C27 Co3 2.115(18) . ?
C27 H15 0.9500 . ?
C28 C29 1.4200 . ?
C28 C32 1.4200 . ?
C28 Co4 2.051(16) . ?
C28 H16 0.9500 . ?
C29 C30 1.4200 . ?
C29 Co4 2.050(19) . ?
C29 H17 0.9500 . ?
C30 C31 1.4200 . ?
C30 Co4 2.09(2) . ?
C30 H18 0.9500 . ?
C31 C32 1.4200 . ?
C31 Co4 2.107(19) . ?
C31 H19 0.9500 . ?
C32 Co4 2.09(2) . ?
C32 H20 0.9500 . ?
C33 C34 1.4200 . ?
C33 C37 1.4200 . ?
C33 C38 1.5095 . ?
C33 Ru1 2.162(18) . ?
C34 C35 1.4200 . ?
C34 C39 1.5095 . ?
C34 Ru1 2.16(2) . ?
C35 C36 1.4200 . ?
C35 C40 1.5095 . ?
C35 Ru1 2.21(2) . ?
C36 C37 1.4200 . ?
C36 C41 1.5095 . ?
C36 Ru1 2.24(2) . ?
C37 C42 1.5095 . ?
C37 Ru1 2.21(2) . ?
C38 H167 0.9800 . ?
C38 H168 0.9800 . ?
C38 H169 0.9800 . ?
C39 H170 0.9800 . ?
C39 H171 0.9800 . ?
C39 H172 0.9800 . ?
C40 H173 0.9800 . ?
C40 H174 0.9800 . ?
C40 H175 0.9800 . ?
C41 H176 0.9800 . ?
C41 H177 0.9800 . ?
C41 H178 0.9800 . ?
C42 H179 0.9800 . ?
C42 H180 0.9800 . ?
C42 H181 0.9800 . ?
C185 C186 1.4200 . ?
C185 C189 1.4200 . ?
C185 C190 1.5095 . ?
C185 Ru1 2.12(4) . ?
C186 C187 1.4200 . ?
C186 C191 1.5095 . ?
C186 Ru1 2.16(4) . ?
C187 C188 1.4200 . ?
C187 C192 1.5095 . ?
C187 Ru1 2.17(4) . ?
C188 C189 1.4200 . ?
C188 C193 1.5095 . ?
C188 Ru1 2.14(4) . ?
C189 C194 1.5095 . ?
C189 Ru1 2.11(4) . ?
C190 H182 0.9800 . ?
C190 H183 0.9800 . ?
C190 H184 0.9800 . ?
C191 H185 0.9800 . ?
C191 H186 0.9800 . ?
C191 H187 0.9800 . ?
C192 H188 0.9800 . ?
C192 H189 0.9800 . ?
C192 H190 0.9800 . ?
C193 H191 0.9800 . ?
C193 H192 0.9800 . ?
C193 H193 0.9800 . ?
C194 H194 0.9800 . ?
C194 H195 0.9800 . ?
C194 H196 0.9800 . ?
C43 C44 1.4200 . ?
C43 C47 1.4200 . ?
C43 C48 1.5095 . ?
C43 Ru2 2.122(13) . ?
C44 C45 1.4200 . ?
C44 C49 1.5095 . ?
C44 Ru2 2.107(13) . ?
C45 C46 1.4200 . ?
C45 C50 1.5095 . ?
C45 Ru2 2.146(13) . ?
C46 C47 1.4200 . ?
C46 C51 1.5095 . ?
C46 Ru2 2.183(14) . ?
C47 C52 1.5095 . ?
C47 Ru2 2.169(12) . ?
C48 H21 0.9800 . ?
C48 H22 0.9800 . ?
C48 H23 0.9800 . ?
C49 H24 0.9800 . ?
C49 H25 0.9800 . ?
C49 H26 0.9800 . ?
C50 H27 0.9800 . ?
C50 H28 0.9800 . ?
C50 H29 0.9800 . ?
C51 H30 0.9800 . ?
C51 H31 0.9800 . ?
C51 H32 0.9800 . ?
C52 H33 0.9800 . ?
C52 H34 0.9800 . ?
C52 H35 0.9800 . ?
C53 C54 1.4200 . ?
C53 C57 1.4200 . ?
C53 C58 1.5095 . ?
C53 Ru3 2.192(13) . ?
C54 C55 1.4200 . ?
C54 C59 1.5095 . ?
C54 Ru3 2.240(14) . ?
C55 C56 1.4200 . ?
C55 C60 1.5095 . ?
C55 Ru3 2.181(14) . ?
C56 C57 1.4200 . ?
C56 C61 1.5095 . ?
C56 Ru3 2.093(13) . ?
C57 C62 1.5095 . ?
C57 Ru3 2.100(14) . ?
C58 H36 0.9800 . ?
C58 H37 0.9800 . ?
C58 H38 0.9800 . ?
C59 H39 0.9800 . ?
C59 H40 0.9800 . ?
C59 H41 0.9800 . ?
C60 H42 0.9800 . ?
C60 H43 0.9800 . ?
C60 H44 0.9800 . ?
C61 H45 0.9800 . ?
C61 H46 0.9800 . ?
C61 H47 0.9800 . ?
C62 H48 0.9800 . ?
C62 H49 0.9800 . ?
C62 H50 0.9800 . ?
C63 C64 1.3900 . ?
C63 C68 1.3900 . ?
C63 C72 1.5065(13) . ?
C63 Ru5 2.179(3) . ?
C64 C65 1.3900 . ?
C64 Ru5 2.213(9) . ?
C64 H51 0.9500 . ?
C65 C66 1.3900 . ?
C65 Ru5 2.238(8) . ?
C65 H52 0.9500 . ?
C66 C67 1.3900 . ?
C66 C69 1.5126 . ?
C66 Ru5 2.229(3) . ?
C67 C68 1.3900 . ?
C67 Ru5 2.195(9) . ?
C67 H53 0.9500 . ?
C68 Ru5 2.170(9) . ?
C68 H54 0.9500 . ?
C69 C71 1.5210(15) . ?
C69 C70 1.5455(14) . ?
C69 H55 1.0000 . ?
C70 H56 0.9800 . ?
C70 H57 0.9800 . ?
C70 H58 0.9800 . ?
C71 H59 0.9800 . ?
C71 H60 0.9800 . ?
C71 H61 0.9800 . ?
C72 H62 0.9800 . ?
C72 H63 0.9800 . ?
C72 H64 0.9800 . ?
C73 C74 1.3900 . ?
C73 C78 1.3900 . ?
C73 C82 1.5065(13) . ?
C73 Ru6 2.211(3) . ?
C74 C75 1.3900 . ?
C74 Ru6 2.198(3) . ?
C74 H65 0.9500 . ?
C75 C76 1.3900 . ?
C75 Ru6 2.237(3) . ?
C75 H66 0.9500 . ?
C76 C77 1.3900 . ?
C76 C79 1.5127 . ?
C76 Ru6 2.288(4) . ?
C77 C78 1.3900 . ?
C77 Ru6 2.301(4) . ?
C77 H67 0.9500 . ?
C78 Ru6 2.264(3) . ?
C78 H68 0.9500 . ?
C79 C81 1.5209(15) . ?
C79 C80 1.5456(14) . ?
C79 H69 1.0000 . ?
C80 H70 0.9800 . ?
C80 H71 0.9800 . ?
C80 H72 0.9800 . ?
C81 H73 0.9800 . ?
C81 H74 0.9800 . ?
C81 H75 0.9800 . ?
C82 H76 0.9800 . ?
C82 H77 0.9800 . ?
C82 H78 0.9800 . ?
Co1 Cs1 4.359(5) . ?
Co3 Cs1 4.353(5) . ?
Co4 Cs1 4.340(5) . ?
Ru4 S1 2.231(9) . ?
Ru4 S2 2.263(8) . ?
Ru4 Ru6 2.823(4) . ?
Ru4 Ru5 2.831(4) . ?
Ru5 S1 2.234(8) . ?
Ru5 S2 2.268(9) . ?
Ru5 Ru6 2.731(4) . ?
Ru6 S1 2.257(9) . ?
Ru6 S2 2.283(10) . ?
C83 N83 1.179(13) . ?
C83 Co5 1.818(15) . ?
C83 Cs2 3.57(2) . ?
C84 N84 1.174(13) . ?
C84 Co5 1.819(17) . ?
C84 Cs2 3.63(3) . ?
C85 N85 1.189(13) . ?
C85 Co5 1.860(17) . ?
C85 Cs2 3.56(2) . ?
C86 N86 1.183(12) . ?
C86 Co6 1.845(16) . ?
C86 Cs2 3.86(2) . ?
C87 N87 1.187(13) . ?
C87 Co6 1.825(17) . ?
C87 Cs2 3.631(19) . ?
C88 N88 1.170(12) . ?
C88 Co6 1.892(14) . ?
C88 Cs2 3.69(2) . ?
C89 N89 1.181(13) . ?
C89 Co7 1.855(15) . ?
C89 Cs2 3.67(2) . ?
C90 N90 1.175(12) . ?
C90 Co7 1.905(16) . ?
C90 Cs2 3.694(18) . ?
C91 N91 1.161(13) . ?
C91 Co7 1.827(17) . ?
C91 Cs2 3.68(2) . ?
C92 N92 1.174(12) . ?
C92 Co8 1.875(16) . ?
C92 Cs2 3.707(19) . ?
C93 N93 1.170(13) . ?
C93 Co8 1.924(16) . ?
C93 Cs2 3.680(19) . ?
C94 N94 1.173(13) . ?
C94 Co8 1.872(15) . ?
C94 Cs2 3.70(2) . ?
N83 Ru8 2.158(15) . ?
N83 Cs2 3.645(18) . ?
N84 Ru9 2.160(15) . ?
N84 Cs2 3.553(18) . ?
N85 Ru7 2.090(16) . ?
N85 Cs2 3.531(18) . ?
N86 Ru10 2.074(15) . ?
N86 Cs2 3.723(18) . ?
N87 Ru8 2.092(16) . ?
N87 Cs2 3.547(16) . ?
N88 Ru7 2.074(14) . ?
N88 Cs2 3.591(17) . ?
N89 Ru10 2.075(15) . ?
N89 Cs2 3.636(18) . ?
N90 Ru9 2.037(15) . ?
N90 Cs2 3.580(16) . ?
N91 Ru7 2.128(16) . ?
N91 Cs2 3.613(18) . ?
N92 Ru10 2.046(15) . ?
N92 Cs2 3.549(18) . ?
N93 Ru8 2.036(15) . ?
N93 Cs2 3.627(16) . ?
N94 Ru9 2.092(15) . ?
N94 Cs2 3.568(18) . ?
C95 C99 1.4200 . ?
C95 C96 1.4200 . ?
C95 Co5 2.038(13) . ?
C95 H79 0.9500 . ?
C96 C97 1.4200 . ?
C96 Co5 2.060(16) . ?
C96 H80 0.9500 . ?
C97 C98 1.4200 . ?
C97 Co5 2.082(16) . ?
C97 H81 0.9500 . ?
C98 C99 1.4200 . ?
C98 Co5 2.074(16) . ?
C98 H82 0.9500 . ?
C99 Co5 2.047(16) . ?
C99 H83 0.9500 . ?
C100 C104 1.4200 . ?
C100 C101 1.4200 . ?
C100 Co6 2.12(3) . ?
C100 H197 0.9500 . ?
C101 C102 1.4200 . ?
C101 Co6 2.07(3) . ?
C101 H198 0.9500 . ?
C102 C103 1.4200 . ?
C102 Co6 2.02(3) . ?
C102 H199 0.9500 . ?
C103 C104 1.4200 . ?
C103 Co6 2.04(3) . ?
C103 H200 0.9500 . ?
C104 Co6 2.10(3) . ?
C104 H201 0.9500 . ?
C195 C196 1.4200 . ?
C195 C199 1.4200 . ?
C195 Co6 1.94(6) . ?
C195 H202 0.9500 . ?
C196 C197 1.4200 . ?
C196 Co6 2.07(6) . ?
C196 H203 0.9500 . ?
C197 C198 1.4200 . ?
C197 Co6 2.19(6) . ?
C197 H204 0.9500 . ?
C198 C199 1.4200 . ?
C198 Co6 2.16(6) . ?
C198 H205 0.9500 . ?
C199 Co6 2.00(6) . ?
C199 H206 0.9500 . ?
C105 C109 1.4200 . ?
C105 C106 1.4200 . ?
C105 Co7 2.097(14) . ?
C105 H84 0.9500 . ?
C106 C107 1.4200 . ?
C106 Co7 2.102(16) . ?
C106 H85 0.9500 . ?
C107 C108 1.4200 . ?
C107 Co7 2.090(17) . ?
C107 H86 0.9500 . ?
C108 C109 1.4200 . ?
C108 Co7 2.077(16) . ?
C108 H87 0.9500 . ?
C109 Co7 2.082(16) . ?
C109 H88 0.9500 . ?
C110 C111 1.4200 . ?
C110 C114 1.4200 . ?
C110 Co8 2.103(15) . ?
C110 H89 0.9500 . ?
C111 C112 1.4200 . ?
C111 Co8 2.095(17) . ?
C111 H90 0.9500 . ?
C112 C113 1.4200 . ?
C112 Co8 2.062(17) . ?
C112 H91 0.9500 . ?
C113 C114 1.4200 . ?
C113 Co8 2.049(18) . ?
C113 H92 0.9500 . ?
C114 Co8 2.074(17) . ?
C114 H93 0.9500 . ?
C115 C116 1.4200 . ?
C115 C119 1.4200 . ?
C115 C120 1.5095 . ?
C115 Ru7 2.155(10) . ?
C116 C117 1.4200 . ?
C116 C121 1.5095 . ?
C116 Ru7 2.196(11) . ?
C117 C118 1.4200 . ?
C117 C122 1.5095 . ?
C117 Ru7 2.201(12) . ?
C118 C119 1.4200 . ?
C118 C123 1.5095 . ?
C118 Ru7 2.163(12) . ?
C119 C124 1.5095 . ?
C119 Ru7 2.134(11) . ?
C120 H94 0.9800 . ?
C120 H95 0.9800 . ?
C120 H96 0.9800 . ?
C121 H97 0.9800 . ?
C121 H98 0.9800 . ?
C121 H99 0.9800 . ?
C122 H100 0.9800 . ?
C122 H101 0.9800 . ?
C122 H102 0.9800 . ?
C123 H103 0.9800 . ?
C123 H104 0.9800 . ?
C123 H105 0.9800 . ?
C124 H106 0.9800 . ?
C124 H107 0.9800 . ?
C124 H108 0.9800 . ?
C125 C126 1.4200 . ?
C125 C129 1.4200 . ?
C125 C130 1.5095 . ?
C125 Ru8 2.137(9) . ?
C126 C127 1.4200 . ?
C126 C131 1.5095 . ?
C126 Ru8 2.178(10) . ?
C127 C128 1.4200 . ?
C127 C132 1.5095 . ?
C127 Ru8 2.216(11) . ?
C128 C129 1.4200 . ?
C128 C133 1.5095 . ?
C128 Ru8 2.199(11) . ?
C129 C134 1.5095 . ?
C129 Ru8 2.151(10) . ?
C130 H109 0.9800 . ?
C130 H110 0.9800 . ?
C130 H111 0.9800 . ?
C131 H112 0.9800 . ?
C131 H113 0.9800 . ?
C131 H114 0.9800 . ?
C132 H115 0.9800 . ?
C132 H116 0.9800 . ?
C132 H117 0.9800 . ?
C133 H118 0.9800 . ?
C133 H119 0.9800 . ?
C133 H120 0.9800 . ?
C134 H121 0.9800 . ?
C134 H122 0.9800 . ?
C134 H123 0.9800 . ?
C135 C136 1.4200 . ?
C135 C139 1.4200 . ?
C135 C140 1.5095 . ?
C135 Ru9 2.124(9) . ?
C136 C137 1.4200 . ?
C136 C141 1.5095 . ?
C136 Ru9 2.128(10) . ?
C137 C138 1.4200 . ?
C137 C142 1.5095 . ?
C137 Ru9 2.160(11) . ?
C138 C139 1.4200 . ?
C138 C143 1.5095 . ?
C138 Ru9 2.175(10) . ?
C139 C144 1.5095 . ?
C139 Ru9 2.153(10) . ?
C140 H124 0.9800 . ?
C140 H125 0.9800 . ?
C140 H126 0.9800 . ?
C141 H127 0.9800 . ?
C141 H128 0.9800 . ?
C141 H129 0.9800 . ?
C142 H130 0.9800 . ?
C142 H131 0.9800 . ?
C142 H132 0.9800 . ?
C143 H133 0.9800 . ?
C143 H134 0.9800 . ?
C143 H135 0.9800 . ?
C144 H136 0.9800 . ?
C144 H137 0.9800 . ?
C144 H138 0.9800 . ?
C145 C146 1.3900 . ?
C145 C150 1.3900 . ?
C145 C154 1.5071(13) . ?
C145 Ru11 2.147(3) . ?
C146 C147 1.3900 . ?
C146 Ru11 2.141(3) . ?
C146 H139 0.9500 . ?
C147 C148 1.3900 . ?
C147 Ru11 2.195(3) . ?
C147 H140 0.9500 . ?
C148 C149 1.3900 . ?
C148 C151 1.5144 . ?
C148 Ru11 2.254(3) . ?
C149 C150 1.3900 . ?
C149 Ru11 2.260(3) . ?
C149 H141 0.9500 . ?
C150 Ru11 2.207(3) . ?
C150 H142 0.9500 . ?
C151 C153 1.5208(16) . ?
C151 C152 1.5456(13) . ?
C151 H143 1.0000 . ?
C152 H144 0.9800 . ?
C152 H145 0.9800 . ?
C152 H146 0.9800 . ?
C153 H147 0.9800 . ?
C153 H148 0.9800 . ?
C153 H149 0.9800 . ?
C154 H150 0.9800 . ?
C154 H151 0.9800 . ?
C154 H152 0.9800 . ?
C155 C156 1.3900 . ?
C155 C160 1.3900 . ?
C155 C164 1.5068(14) . ?
C155 Ru12 2.201(4) . ?
C156 C157 1.3900 . ?
C156 Ru12 2.255(6) . ?
C156 H153 0.9500 . ?
C157 C158 1.3900 . ?
C157 Ru12 2.268(5) . ?
C157 H154 0.9500 . ?
C158 C159 1.3900 . ?
C158 C161 1.5142 . ?
C158 Ru12 2.227(4) . ?
C159 C160 1.3900 . ?
C159 Ru12 2.172(8) . ?
C159 H155 0.9500 . ?
C160 Ru12 2.158(7) . ?
C160 H156 0.9500 . ?
C161 C163 1.5208(16) . ?
C161 C162 1.5455(15) . ?
C161 H157 1.0000 . ?
C162 H158 0.9800 . ?
C162 H159 0.9800 . ?
C162 H160 0.9800 . ?
C163 H161 0.9800 . ?
C163 H162 0.9800 . ?
C163 H163 0.9800 . ?
C164 H164 0.9800 . ?
C164 H165 0.9800 . ?
C164 H166 0.9800 . ?
Co5 Cs2 4.293(4) . ?
Co8 Cs2 4.391(4) . ?
Ru10 S4 2.216(8) . ?
Ru10 S3 2.245(8) . ?
Ru10 Ru11 2.748(4) . ?
Ru10 Ru12 2.816(4) . ?
Ru11 S3 2.241(8) . ?
Ru11 S4 2.241(8) . ?
Ru11 Ru12 2.761(4) . ?
Ru12 S3 2.244(7) . ?
Ru12 S4 2.251(9) . ?
P1 F4 1.5798 . ?
P1 F1 1.5799 . ?
P1 F2 1.5800 . ?
P1 F5 1.5801 . ?
P1 F6 1.5801 . ?
P1 F3 1.5801 . ?
P2 F8 1.5798 . ?
P2 F12 1.5798 . ?
P2 F11 1.5800 . ?
P2 F7 1.5800 . ?
P2 F10 1.5800 . ?
P2 F9 1.5801 . ?
P5 F30 1.5799 . ?
P5 F26 1.5799 . ?
P5 F28 1.5800 . ?
P5 F29 1.5800 . ?
P5 F27 1.5800 . ?
P5 F25 1.5802 . ?
P3 F13 1.5798 . ?
P3 F16 1.5799 . ?
P3 F18 1.5800 . ?
P3 F14 1.5801 . ?
P3 F17 1.5801 . ?
P3 F15 1.5802 . ?
P4 F21 1.5799 . ?
P4 F19 1.5799 . ?
P4 F20 1.5799 . ?
P4 F24 1.5800 . ?
P4 F23 1.5802 . ?
P4 F22 1.5802 . ?
P6 F34 1.5796 . ?
P6 F35 1.5799 . ?
P6 F32 1.5799 . ?
P6 F31 1.5800 . ?
P6 F36 1.5802 . ?
P6 F33 1.5804 . ?
C165 C166 1.4200 . ?
C165 H207 0.9802 . ?
C165 H208 0.9800 . ?
C165 H209 0.9799 . ?
C166 N166 1.1400 . ?
C167 C168 1.4200 . ?
C167 H210 0.9800 . ?
C167 H211 0.9801 . ?
C167 H212 0.9800 . ?
C168 N168 1.1397 . ?
C169 C170 1.4203 . ?
C169 H213 0.9800 . ?
C169 H214 0.9799 . ?
C169 H215 0.9801 . ?
C170 N170 1.1399 . ?
C171 C172 1.4201 . ?
C171 H216 0.9800 . ?
C171 H217 0.9799 . ?
C171 H218 0.9800 . ?
C172 N172 1.1398 . ?
C173 C174 1.4201 . ?
C173 H219 0.9800 . ?
C173 H220 0.9799 . ?
C173 H221 0.9800 . ?
C174 N174 1.1400 . ?
C175 C176 1.4200 . ?
C175 H222 0.9801 . ?
C175 H223 0.9801 . ?
C175 H224 0.9799 . ?
C176 N176 1.1400 . ?
C177 C178 1.4203 . ?
C177 H225 0.9800 . ?
C177 H226 0.9800 . ?
C177 H227 0.9799 . ?
C178 N178 1.1398 . ?
C179 C180 1.4201 . ?
C179 H228 0.9800 . ?
C179 H229 0.9800 . ?
C179 H230 0.9800 . ?
C180 N180 1.1399 . ?
C181 C182 1.4200 . ?
C181 H231 0.9800 . ?
C181 H232 0.9799 . ?
C181 H233 0.9801 . ?
C182 N182 1.1400 . ?
C183 C184 1.4200 . ?
C183 H234 0.9799 . ?
C183 H235 0.9800 . ?
C183 H236 0.9801 . ?
C184 N184 1.1400 . ?
