#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:57:32 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179163 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/24/4312482.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4312482
loop_
_publ_author_name
'Xian-He Bu'
'Ya-Bo Xie'
'Jian-Rong Li'
'Ruo-Hua Zhang'
_publ_section_title
;
 Adjusting the Frameworks of Silver(I) Complexes with New Pyridyl
 Thioethers by Varying the Chain Lengths of Ligand Spacers, Solvents, and
 Counteranions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              7422
_journal_page_last               7430
_journal_paper_doi               10.1021/ic034454j
_journal_volume                  42
_journal_year                    2003
_chemical_formula_sum            'C29 H33 Ag2 Cl5 N4 O8 S4'
_chemical_formula_weight         1086.82
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 107.389(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.285(10)
_cell_length_b                   10.782(5)
_cell_length_c                   18.036(8)
_cell_measurement_reflns_used    639
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      19.35
_cell_measurement_theta_min      2.28
_cell_volume                     4136(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      273(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0825
_diffrn_reflns_av_sigmaI/netI    0.1435
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            9536
_diffrn_reflns_theta_full        26.42
_diffrn_reflns_theta_max         26.42
_diffrn_reflns_theta_min         1.92
_exptl_absorpt_coefficient_mu    1.522
_exptl_absorpt_correction_T_max  1.000000
_exptl_absorpt_correction_T_min  0.771244
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_density_diffrn    1.746
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2168
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.760
_refine_diff_density_min         -0.536
_refine_diff_density_rms         0.098
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.964
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     249
_refine_ls_number_reflns         4243
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      0.982
_refine_ls_R_factor_all          0.1807
_refine_ls_R_factor_gt           0.0647
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0583P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1159
_refine_ls_wR_factor_ref         0.1490
_reflns_number_gt                1869
_reflns_number_total             4243
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic034454jsi20030429_113007.cif
_cod_data_source_block           021014c
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'MULTI-SCAN'
changed to 'multi-scan' according to the built-in table from CIF Core
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        4135(3)
_cod_database_code               4312482
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.19895(3) 0.32526(6) 1.03104(4) 0.0628(3) Uani 1 1 d . . .
S1 S 0.24417(11) 0.5562(2) 0.96974(14) 0.0750(7) Uani 1 1 d . . .
S2 S 0.29197(9) 0.7253(2) 0.64343(11) 0.0553(6) Uani 1 1 d . . .
N1 N 0.1507(3) 0.5192(6) 1.0222(4) 0.0591(18) Uani 1 1 d . . .
N2 N 0.3658(2) 0.6964(5) 0.5561(3) 0.0447(16) Uani 1 1 d . . .
C1 C 0.0962(4) 0.5452(9) 1.0357(6) 0.081(3) Uani 1 1 d . . .
H1 H 0.0842 0.4951 1.0708 0.098 Uiso 1 1 calc R . .
C2 C 0.0571(5) 0.6393(11) 1.0018(7) 0.105(4) Uani 1 1 d . . .
H2 H 0.0200 0.6543 1.0139 0.126 Uiso 1 1 calc R . .
C3 C 0.0742(5) 0.7109(10) 0.9495(8) 0.108(4) Uani 1 1 d . . .
H3 H 0.0473 0.7732 0.9232 0.130 Uiso 1 1 calc R . .
C4 C 0.1307(5) 0.6923(9) 0.9350(6) 0.088(3) Uani 1 1 d . . .
H4 H 0.1431 0.7424 0.9002 0.105 Uiso 1 1 calc R . .
C5 C 0.1689(4) 0.5951(8) 0.9744(5) 0.057(2) Uani 1 1 d . . .
C6 C 0.2488(5) 0.6361(10) 0.8832(6) 0.096(3) Uani 1 1 d . . .
H6A H 0.2139 0.6116 0.8389 0.115 Uiso 1 1 calc R . .
H6B H 0.2465 0.7250 0.8900 0.115 Uiso 1 1 calc R . .
C7 C 0.3085(5) 0.6039(11) 0.8693(6) 0.106(4) Uani 1 1 d . . .
H7A H 0.3084 0.5160 0.8577 0.127 Uiso 1 1 calc R . .
H7B H 0.3426 0.6189 0.9165 0.127 Uiso 1 1 calc R . .
C8 C 0.3210(5) 0.6772(10) 0.8027(5) 0.091(3) Uani 1 1 d . . .
H8A H 0.3127 0.7644 0.8086 0.109 Uiso 1 1 calc R . .
H8B H 0.3650 0.6688 0.8055 0.109 Uiso 1 1 calc R . .
C9 C 0.2806(4) 0.6329(9) 0.7242(5) 0.071(3) Uani 1 1 d . . .
H9A H 0.2367 0.6370 0.7226 0.085 Uiso 1 1 calc R . .
H9B H 0.2905 0.5468 0.7174 0.085 Uiso 1 1 calc R . .
C10 C 0.3574(3) 0.6542(7) 0.6226(4) 0.0432(18) Uani 1 1 d . . .
C11 C 0.3968(3) 0.5703(8) 0.6701(4) 0.058(2) Uani 1 1 d . . .
H11 H 0.3900 0.5445 0.7161 0.070 Uiso 1 1 calc R . .
C12 C 0.4462(4) 0.5256(8) 0.6482(5) 0.065(2) Uani 1 1 d . . .
H12 H 0.4725 0.4660 0.6784 0.078 Uiso 1 1 calc R . .
C13 C 0.4572(4) 0.5683(8) 0.5816(5) 0.064(2) Uani 1 1 d . . .
H13 H 0.4918 0.5409 0.5676 0.077 Uiso 1 1 calc R . .
C14 C 0.4166(4) 0.6510(8) 0.5371(4) 0.058(2) Uani 1 1 d . . .
H14 H 0.4235 0.6782 0.4914 0.069 Uiso 1 1 calc R . .
Cl1 Cl 0.10750(10) 0.2091(2) 0.18958(13) 0.0617(6) Uani 1 1 d . . .
O1 O 0.1205(4) 0.2923(7) 0.1380(4) 0.114(3) Uani 1 1 d . . .
O2 O 0.1641(4) 0.1754(7) 0.2463(4) 0.125(3) Uani 1 1 d . . .
O3 O 0.0785(3) 0.1012(7) 0.1498(4) 0.112(2) Uani 1 1 d . . .
O4 O 0.0695(5) 0.2565(10) 0.2293(6) 0.180(4) Uani 1 1 d . . .
C15 C 1.0000 0.5204(10) 0.2500 0.089(4) Uani 1 2 d SD . .
Cl2 Cl 0.9644(5) 0.5741(9) 0.1589(4) 0.159(4) Uani 0.50 1 d PD . .
Cl3 Cl 0.9179(3) 0.5675(7) 0.2315(7) 0.161(3) Uani 0.50 1 d PD . .
Cl4 Cl 1.0226(7) 0.6079(10) 0.1811(7) 0.210(5) Uani 0.50 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 Ag1 N1 108.5(2) 4_546 . ?
N2 Ag1 S2 129.33(15) 4_546 6_566 ?
N1 Ag1 S2 120.43(17) . 6_566 ?
N2 Ag1 Ag1 79.71(14) 4_546 7_557 ?
N1 Ag1 Ag1 141.13(16) . 7_557 ?
S2 Ag1 Ag1 70.91(6) 6_566 7_557 ?
C5 S1 C6 103.2(4) . . ?
C10 S2 C9 104.4(4) . . ?
C10 S2 Ag1 105.6(2) . 6_565 ?
C9 S2 Ag1 104.3(3) . 6_565 ?
C1 N1 C5 117.1(7) . . ?
C1 N1 Ag1 126.9(6) . . ?
C5 N1 Ag1 111.7(5) . . ?
C10 N2 C14 116.5(6) . . ?
C10 N2 Ag1 126.6(4) . 4_556 ?
C14 N2 Ag1 116.7(5) . 4_556 ?
N1 C1 C2 124.7(9) . . ?
N1 C1 H1 117.6 . . ?
C2 C1 H1 117.6 . . ?
C3 C2 C1 117.6(9) . . ?
C3 C2 H2 121.2 . . ?
C1 C2 H2 121.2 . . ?
C2 C3 C4 120.8(10) . . ?
C2 C3 H3 119.6 . . ?
C4 C3 H3 119.6 . . ?
C3 C4 C5 117.7(9) . . ?
C3 C4 H4 121.2 . . ?
C5 C4 H4 121.2 . . ?
N1 C5 C4 121.9(7) . . ?
N1 C5 S1 111.3(7) . . ?
C4 C5 S1 126.8(7) . . ?
C7 C6 S1 108.8(7) . . ?
C7 C6 H6A 109.9 . . ?
S1 C6 H6A 109.9 . . ?
C7 C6 H6B 109.9 . . ?
S1 C6 H6B 109.9 . . ?
H6A C6 H6B 108.3 . . ?
C6 C7 C8 113.5(8) . . ?
C6 C7 H7A 108.9 . . ?
C8 C7 H7A 108.9 . . ?
C6 C7 H7B 108.9 . . ?
C8 C7 H7B 108.9 . . ?
H7A C7 H7B 107.7 . . ?
C9 C8 C7 112.0(9) . . ?
C9 C8 H8A 109.2 . . ?
C7 C8 H8A 109.2 . . ?
C9 C8 H8B 109.2 . . ?
C7 C8 H8B 109.2 . . ?
H8A C8 H8B 107.9 . . ?
C8 C9 S2 112.6(6) . . ?
C8 C9 H9A 109.1 . . ?
S2 C9 H9A 109.1 . . ?
C8 C9 H9B 109.1 . . ?
S2 C9 H9B 109.1 . . ?
H9A C9 H9B 107.8 . . ?
N2 C10 C11 123.2(6) . . ?
N2 C10 S2 112.5(5) . . ?
C11 C10 S2 124.3(5) . . ?
C12 C11 C10 118.3(7) . . ?
C12 C11 H11 120.9 . . ?
C10 C11 H11 120.9 . . ?
C11 C12 C13 120.3(8) . . ?
C11 C12 H12 119.8 . . ?
C13 C12 H12 119.8 . . ?
C14 C13 C12 118.5(7) . . ?
C14 C13 H13 120.8 . . ?
C12 C13 H13 120.8 . . ?
C13 C14 N2 123.1(7) . . ?
C13 C14 H14 118.5 . . ?
N2 C14 H14 118.5 . . ?
O4 Cl1 O1 113.5(6) . . ?
O4 Cl1 O2 106.0(6) . . ?
O1 Cl1 O2 109.4(5) . . ?
O4 Cl1 O3 108.2(6) . . ?
O1 Cl1 O3 110.3(4) . . ?
O2 Cl1 O3 109.2(5) . . ?
Cl2 C15 Cl2 140.1(10) 2_755 . ?
Cl2 C15 Cl4 43.8(4) 2_755 2_755 ?
Cl2 C15 Cl4 110.7(7) . 2_755 ?
Cl2 C15 Cl4 110.7(7) 2_755 . ?
Cl2 C15 Cl4 43.8(4) . . ?
Cl4 C15 Cl4 114.7(9) 2_755 . ?
Cl2 C15 Cl3 65.0(5) 2_755 2_755 ?
Cl2 C15 Cl3 103.5(5) . 2_755 ?
Cl4 C15 Cl3 101.8(6) 2_755 2_755 ?
Cl4 C15 Cl3 59.7(5) . 2_755 ?
Cl2 C15 Cl3 103.5(5) 2_755 . ?
Cl2 C15 Cl3 65.0(5) . . ?
Cl4 C15 Cl3 59.7(5) 2_755 . ?
Cl4 C15 Cl3 101.8(6) . . ?
Cl3 C15 Cl3 147.8(8) 2_755 . ?
Cl4 Cl2 C15 70.2(4) . . ?
Cl4 Cl2 Cl3 120.1(7) . . ?
C15 Cl2 Cl3 60.8(3) . . ?
Cl4 Cl3 C15 57.9(3) 2_755 . ?
Cl4 Cl3 Cl2 100.7(4) 2_755 . ?
C15 Cl3 Cl2 54.2(3) . . ?
Cl2 Cl4 C15 66.0(4) . . ?
Cl2 Cl4 Cl3 128.2(6) . 2_755 ?
C15 Cl4 Cl3 62.4(4) . 2_755 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N2 2.264(6) 4_546 ?
Ag1 N1 2.335(7) . ?
Ag1 S2 2.488(2) 6_566 ?
Ag1 Ag1 3.2537(15) 7_557 ?
S1 C5 1.755(8) . ?
S1 C6 1.813(9) . ?
S2 C10 1.785(7) . ?
S2 C9 1.844(8) . ?
S2 Ag1 2.488(2) 6_565 ?
N1 C1 1.337(10) . ?
N1 C5 1.338(9) . ?
N2 C10 1.347(8) . ?
N2 C14 1.367(9) . ?
N2 Ag1 2.264(6) 4_556 ?
C1 C2 1.358(12) . ?
C1 H1 0.9300 . ?
C2 C3 1.357(14) . ?
C2 H2 0.9300 . ?
C3 C4 1.376(13) . ?
C3 H3 0.9300 . ?
C4 C5 1.402(12) . ?
C4 H4 0.9300 . ?
C6 C7 1.468(12) . ?
C6 H6A 0.9700 . ?
C6 H6B 0.9700 . ?
C7 C8 1.532(12) . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C8 C9 1.511(12) . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C9 H9A 0.9700 . ?
C9 H9B 0.9700 . ?
C10 C11 1.369(9) . ?
C11 C12 1.363(9) . ?
C11 H11 0.9300 . ?
C12 C13 1.375(10) . ?
C12 H12 0.9300 . ?
C13 C14 1.351(10) . ?
C13 H13 0.9300 . ?
C14 H14 0.9300 . ?
Cl1 O4 1.361(7) . ?
Cl1 O1 1.383(6) . ?
Cl1 O2 1.413(7) . ?
Cl1 O3 1.417(7) . ?
C15 Cl2 1.699(6) 2_755 ?
C15 Cl2 1.699(6) . ?
C15 Cl4 1.750(8) 2_755 ?
C15 Cl4 1.750(8) . ?
C15 Cl3 1.830(6) 2_755 ?
C15 Cl3 1.830(6) . ?
Cl2 Cl4 1.289(12) . ?
Cl2 Cl3 1.900(12) . ?
Cl3 Cl4 1.784(14) 2_755 ?
Cl4 Cl3 1.784(14) 2_755 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 Ag1 N1 C1 61.6(8) 4_546 . . . ?
S2 Ag1 N1 C1 -104.7(7) 6_566 . . . ?
Ag1 Ag1 N1 C1 158.2(6) 7_557 . . . ?
N2 Ag1 N1 C5 -94.2(5) 4_546 . . . ?
S2 Ag1 N1 C5 99.5(5) 6_566 . . . ?
Ag1 Ag1 N1 C5 2.4(7) 7_557 . . . ?
C5 N1 C1 C2 3.0(15) . . . . ?
Ag1 N1 C1 C2 -151.6(9) . . . . ?
N1 C1 C2 C3 1.2(18) . . . . ?
C1 C2 C3 C4 -3.5(19) . . . . ?
C2 C3 C4 C5 1.7(17) . . . . ?
C1 N1 C5 C4 -4.8(12) . . . . ?
Ag1 N1 C5 C4 153.5(7) . . . . ?
C1 N1 C5 S1 174.8(6) . . . . ?
Ag1 N1 C5 S1 -26.8(7) . . . . ?
C3 C4 C5 N1 2.6(14) . . . . ?
C3 C4 C5 S1 -177.0(8) . . . . ?
C6 S1 C5 N1 163.5(6) . . . . ?
C6 S1 C5 C4 -16.8(9) . . . . ?
C5 S1 C6 C7 -176.1(8) . . . . ?
S1 C6 C7 C8 -173.6(8) . . . . ?
C6 C7 C8 C9 -74.2(12) . . . . ?
C7 C8 C9 S2 177.0(6) . . . . ?
C10 S2 C9 C8 86.2(7) . . . . ?
Ag1 S2 C9 C8 -163.2(6) 6_565 . . . ?
C14 N2 C10 C11 0.0(11) . . . . ?
Ag1 N2 C10 C11 175.9(6) 4_556 . . . ?
C14 N2 C10 S2 177.3(5) . . . . ?
Ag1 N2 C10 S2 -6.9(7) 4_556 . . . ?
C9 S2 C10 N2 169.2(5) . . . . ?
Ag1 S2 C10 N2 59.6(5) 6_565 . . . ?
C9 S2 C10 C11 -13.5(8) . . . . ?
Ag1 S2 C10 C11 -123.2(6) 6_565 . . . ?
N2 C10 C11 C12 -1.3(12) . . . . ?
S2 C10 C11 C12 -178.2(6) . . . . ?
C10 C11 C12 C13 2.7(13) . . . . ?
C11 C12 C13 C14 -2.8(13) . . . . ?
C12 C13 C14 N2 1.6(13) . . . . ?
C10 N2 C14 C13 -0.2(11) . . . . ?
Ag1 N2 C14 C13 -176.5(7) 4_556 . . . ?
Cl2 C15 Cl2 Cl4 63.2(7) 2_755 . . . ?
Cl4 C15 Cl2 Cl4 104.6(11) 2_755 . . . ?
Cl3 C15 Cl2 Cl4 -3.8(9) 2_755 . . . ?
Cl3 C15 Cl2 Cl4 144.2(9) . . . . ?
Cl2 C15 Cl2 Cl3 -81.0(4) 2_755 . . . ?
Cl4 C15 Cl2 Cl3 -39.6(5) 2_755 . . . ?
Cl4 C15 Cl2 Cl3 -144.2(9) . . . . ?
Cl3 C15 Cl2 Cl3 -148.0(8) 2_755 . . . ?
Cl2 C15 Cl3 Cl4 3.0(7) 2_755 . . 2_755 ?
Cl2 C15 Cl3 Cl4 -136.4(7) . . . 2_755 ?
Cl4 C15 Cl3 Cl4 -111.9(10) . . . 2_755 ?
Cl3 C15 Cl3 Cl4 -61.2(5) 2_755 . . 2_755 ?
Cl2 C15 Cl3 Cl2 139.4(9) 2_755 . . . ?
Cl4 C15 Cl3 Cl2 136.4(7) 2_755 . . . ?
Cl4 C15 Cl3 Cl2 24.4(6) . . . . ?
Cl3 C15 Cl3 Cl2 75.1(5) 2_755 . . . ?
Cl4 Cl2 Cl3 Cl4 -3.0(9) . . . 2_755 ?
C15 Cl2 Cl3 Cl4 36.5(6) . . . 2_755 ?
Cl4 Cl2 Cl3 C15 -39.5(9) . . . . ?
Cl3 Cl2 Cl4 C15 36.2(8) . . . . ?
C15 Cl2 Cl4 Cl3 4.8(11) . . . 2_755 ?
Cl3 Cl2 Cl4 Cl3 41.0(16) . . . 2_755 ?
Cl2 C15 Cl4 Cl2 -142.3(9) 2_755 . . . ?
Cl4 C15 Cl4 Cl2 -94.7(8) 2_755 . . . ?
Cl3 C15 Cl4 Cl2 175.8(10) 2_755 . . . ?
Cl3 C15 Cl4 Cl2 -32.8(8) . . . . ?
Cl2 C15 Cl4 Cl3 42.0(6) 2_755 . . 2_755 ?
Cl2 C15 Cl4 Cl3 -175.8(10) . . . 2_755 ?
Cl4 C15 Cl4 Cl3 89.5(5) 2_755 . . 2_755 ?
Cl3 C15 Cl4 Cl3 151.5(7) . . . 2_755 ?
