#------------------------------------------------------------------------------
#$Date: 2016-03-23 02:57:22 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179221 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/45/4314519.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4314519
loop_
_publ_author_name
'C. W. Liu'
'Hao-Wei Chang'
'Bijay Sarkar'
'Jean-Yves Saillard'
'Samia Kahlal'
'Ying-Yann Wu'
_publ_section_title
;
 Stable Silver(I) Hydride Complexes Supported by Diselenophosphate Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              468
_journal_page_last               475
_journal_paper_doi               10.1021/ic901408n
_journal_volume                  49
_journal_year                    2010
_chemical_formula_sum            'C24 H61 Ag8 F6 O12 P7 Se12'
_chemical_formula_weight         2683.00
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           167
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            12
_cell_length_a                   17.8467(9)
_cell_length_b                   17.8467(9)
_cell_length_c                   74.722(4)
_cell_measurement_reflns_used    3761
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      23.16
_cell_measurement_theta_min      2.28
_cell_volume                     20610.8(18)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0449
_diffrn_reflns_av_sigmaI/netI    0.0338
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       87
_diffrn_reflns_limit_l_min       -86
_diffrn_reflns_number            19353
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.43
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    8.808
_exptl_absorpt_correction_T_max  0.4945
_exptl_absorpt_correction_T_min  0.1412
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.594
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plane
_exptl_crystal_F_000             14928
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.352
_refine_diff_density_min         -1.530
_refine_diff_density_rms         0.185
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     235
_refine_ls_number_reflns         4030
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0917
_refine_ls_R_factor_gt           0.0631
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1187P)²+178.2488P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1870
_refine_ls_wR_factor_ref         0.2057
_reflns_number_gt                2801
_reflns_number_total             4030
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic901408n_si_001_2.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               4314519
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+5/6'
'x-y+2/3, -y+1/3, -z+5/6'
'-x+2/3, -x+y+1/3, -z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+7/6'
'x-y+1/3, -y+2/3, -z+7/6'
'-x+1/3, -x+y+2/3, -z+7/6'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-y+2/3, -x+1/3, z-1/6'
'-x+y+2/3, y+1/3, z-1/6'
'x+2/3, x-y+1/3, z-1/6'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-y+1/3, -x+2/3, z+1/6'
'-x+y+1/3, y+2/3, z+1/6'
'x+1/3, x-y+2/3, z+1/6'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.3333 0.6667 0.06089(4) 0.0609(6) Uani 0.75 3 d SP . .
Ag5 Ag 0.3333 0.6667 0.04937(15) 0.0736(19) Uani 0.25 3 d SP . .
Ag2 Ag 0.3333 0.6667 0.12946(3) 0.0774(6) Uani 0.75 3 d SP . .
Ag6 Ag 0.3333 0.6667 0.11508(19) 0.110(3) Uani 0.25 3 d SP . .
Ag3 Ag 0.35497(8) 0.77499(8) 0.096378(16) 0.0642(4) Uani 0.75 1 d P . .
Ag7 Ag 0.3528(4) 0.8338(5) 0.10275(8) 0.1239(18) Uani 0.25 1 d P . .
Ag4 Ag 0.52130(11) 0.81291(9) 0.075603(18) 0.0816(4) Uani 0.75 1 d P . .
Ag8 Ag 0.4473(5) 0.7636(4) 0.08071(7) 0.1091(16) Uani 0.25 1 d P . .
Se1 Se 0.49330(7) 0.72830(7) 0.046459(15) 0.0650(4) Uani 1 1 d . . .
Se2 Se 0.45667(9) 0.91673(7) 0.076349(17) 0.0750(4) Uani 1 1 d . . .
Se3 Se 0.39762(9) 0.56644(10) 0.12951(2) 0.0911(5) Uani 1 1 d . . .
Se4 Se 0.21525(12) 0.80012(11) 0.103537(19) 0.0982(5) Uani 1 1 d . . .
P1 P 0.49671(19) 0.6111(2) 0.05091(4) 0.0645(7) Uani 1 1 d . . .
P2 P 0.2927(3) 0.4382(3) 0.12443(5) 0.0889(10) Uani 1 1 d . . .
O1 O 0.5926(5) 0.6359(6) 0.04615(13) 0.091(3) Uani 1 1 d . . .
O2 O 0.4332(6) 0.5398(5) 0.03698(11) 0.082(2) Uani 1 1 d . . .
O3 O 0.3339(17) 0.3833(15) 0.1219(4) 0.265(13) Uani 1 1 d . . .
O4 O 0.2419(9) 0.3913(10) 0.14082(15) 0.149(5) Uani 1 1 d . . .
C1 C 0.6285(11) 0.5810(13) 0.0477(4) 0.165(10) Uani 1 1 d . . .
H1A H 0.6199 0.5595 0.0599 0.198 Uiso 1 1 calc R . .
H1B H 0.5965 0.5316 0.0399 0.198 Uiso 1 1 calc R . .
C2 C 0.7128(12) 0.6170(16) 0.0437(4) 0.199(13) Uani 1 1 d . . .
H2A H 0.7311 0.5753 0.0456 0.299 Uiso 1 1 calc R . .
H2B H 0.7456 0.6660 0.0514 0.299 Uiso 1 1 calc R . .
H2C H 0.7220 0.6353 0.0315 0.299 Uiso 1 1 calc R . .
C3 C 0.4338(11) 0.5599(11) 0.01844(18) 0.106(5) Uani 1 1 d . . .
H3A H 0.4926 0.5886 0.0139 0.127 Uiso 1 1 calc R . .
H3B H 0.4107 0.5985 0.0169 0.127 Uiso 1 1 calc R . .
C4 C 0.3812(13) 0.4801(13) 0.0088(2) 0.146(8) Uani 1 1 d . . .
H4A H 0.3819 0.4924 -0.0038 0.219 Uiso 1 1 calc R . .
H4B H 0.3229 0.4529 0.0131 0.219 Uiso 1 1 calc R . .
H4C H 0.4041 0.4420 0.0105 0.219 Uiso 1 1 calc R . .
C5 C 0.1814(19) 0.3990(19) 0.1496(3) 0.174(11) Uani 1 1 d . . .
H5A H 0.2112 0.4552 0.1553 0.208 Uiso 1 1 calc R . .
H5B H 0.1447 0.4027 0.1405 0.208 Uiso 1 1 calc R . .
C6 C 0.1287(16) 0.3452(15) 0.1617(3) 0.196(14) Uani 1 1 d . . .
H6A H 0.0911 0.3653 0.1659 0.294 Uiso 1 1 calc R . .
H6B H 0.1617 0.3420 0.1715 0.294 Uiso 1 1 calc R . .
H6C H 0.0948 0.2888 0.1565 0.294 Uiso 1 1 calc R . .
C7 C 0.386(2) 0.3672(17) 0.1177(4) 0.212(14) Uani 1 1 d . . .
H7A H 0.4257 0.4256 0.1137 0.254 Uiso 1 1 calc R . .
H7B H 0.3559 0.3384 0.1068 0.254 Uiso 1 1 calc R . .
C8 C 0.4376(16) 0.3439(18) 0.1165(5) 0.28(2) Uani 1 1 d . . .
H8A H 0.4478 0.3378 0.1041 0.417 Uiso 1 1 calc R . .
H8B H 0.4161 0.2893 0.1225 0.417 Uiso 1 1 calc R . .
H8C H 0.4908 0.3860 0.1220 0.417 Uiso 1 1 calc R . .
H0 H 0.3333 0.6667 0.084(2) 0.050 Uiso 1 3 d S . .
P3 P 0.3333 0.6667 -0.02374(16) 0.172(5) Uani 1 3 d S . .
F1 F 0.349(2) 0.6057(16) -0.0331(4) 0.325(14) Uani 1 1 d . . .
F2 F 0.411(2) 0.690(2) -0.0134(4) 0.39(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag5 Ag1 Ag8 127.93(18) . . ?
Ag5 Ag1 Ag8 127.93(18) . 3_565 ?
Ag8 Ag1 Ag8 86.2(3) . 3_565 ?
Ag5 Ag1 Ag8 127.93(18) . 2_665 ?
Ag8 Ag1 Ag8 86.2(3) . 2_665 ?
Ag8 Ag1 Ag8 86.2(3) 3_565 2_665 ?
Ag5 Ag1 Se1 66.63(6) . 2_665 ?
Ag8 Ag1 Se1 104.45(12) . 2_665 ?
Ag8 Ag1 Se1 150.23(14) 3_565 2_665 ?
Ag8 Ag1 Se1 67.30(16) 2_665 2_665 ?
Ag5 Ag1 Se1 66.63(6) . 3_565 ?
Ag8 Ag1 Se1 150.23(14) . 3_565 ?
Ag8 Ag1 Se1 67.30(16) 3_565 3_565 ?
Ag8 Ag1 Se1 104.45(12) 2_665 3_565 ?
Se1 Ag1 Se1 105.30(7) 2_665 3_565 ?
Ag5 Ag1 Se1 66.62(6) . . ?
Ag8 Ag1 Se1 67.30(16) . . ?
Ag8 Ag1 Se1 104.45(12) 3_565 . ?
Ag8 Ag1 Se1 150.23(14) 2_665 . ?
Se1 Ag1 Se1 105.30(7) 2_665 . ?
Se1 Ag1 Se1 105.30(7) 3_565 . ?
Ag5 Ag1 Ag3 146.25(4) . . ?
Ag8 Ag1 Ag3 41.49(16) . . ?
Ag8 Ag1 Ag3 85.78(19) 3_565 . ?
Ag8 Ag1 Ag3 44.70(15) 2_665 . ?
Se1 Ag1 Ag3 84.48(4) 2_665 . ?
Se1 Ag1 Ag3 141.77(8) 3_565 . ?
Se1 Ag1 Ag3 107.47(5) . . ?
Ag5 Ag1 Ag3 146.25(4) . 2_665 ?
Ag8 Ag1 Ag3 85.79(19) . 2_665 ?
Ag8 Ag1 Ag3 44.69(15) 3_565 2_665 ?
Ag8 Ag1 Ag3 41.49(16) 2_665 2_665 ?
Se1 Ag1 Ag3 107.47(5) 2_665 2_665 ?
Se1 Ag1 Ag3 84.48(4) 3_565 2_665 ?
Se1 Ag1 Ag3 141.78(8) . 2_665 ?
Ag3 Ag1 Ag3 57.52(6) . 2_665 ?
Ag5 Ag1 Ag3 146.25(4) . 3_565 ?
Ag8 Ag1 Ag3 44.70(15) . 3_565 ?
Ag8 Ag1 Ag3 41.49(16) 3_565 3_565 ?
Ag8 Ag1 Ag3 85.78(19) 2_665 3_565 ?
Se1 Ag1 Ag3 141.77(8) 2_665 3_565 ?
Se1 Ag1 Ag3 107.47(5) 3_565 3_565 ?
Se1 Ag1 Ag3 84.49(4) . 3_565 ?
Ag3 Ag1 Ag3 57.52(6) . 3_565 ?
Ag3 Ag1 Ag3 57.52(6) 2_665 3_565 ?
Ag5 Ag1 Ag4 109.82(6) . . ?
Ag8 Ag1 Ag4 18.47(16) . . ?
Ag8 Ag1 Ag4 96.57(16) 3_565 . ?
Ag8 Ag1 Ag4 102.05(16) 2_665 . ?
Se1 Ag1 Ag4 101.81(3) 2_665 . ?
Se1 Ag1 Ag4 147.66(4) 3_565 . ?
Se1 Ag1 Ag4 49.77(4) . . ?
Ag3 Ag1 Ag4 57.81(5) . . ?
Ag3 Ag1 Ag4 103.92(9) 2_665 . ?
Ag3 Ag1 Ag4 56.39(5) 3_565 . ?
Ag5 Ag1 Ag4 109.82(6) . 2_665 ?
Ag8 Ag1 Ag4 96.57(16) . 2_665 ?
Ag8 Ag1 Ag4 102.04(16) 3_565 2_665 ?
Ag8 Ag1 Ag4 18.47(16) 2_665 2_665 ?
Se1 Ag1 Ag4 49.77(4) 2_665 2_665 ?
Se1 Ag1 Ag4 101.81(3) 3_565 2_665 ?
Se1 Ag1 Ag4 147.66(4) . 2_665 ?
Ag3 Ag1 Ag4 56.38(5) . 2_665 ?
Ag3 Ag1 Ag4 57.81(5) 2_665 2_665 ?
Ag3 Ag1 Ag4 103.92(9) 3_565 2_665 ?
Ag4 Ag1 Ag4 109.12(6) . 2_665 ?
Ag5 Ag1 H0 180.000(16) . . ?
Ag8 Ag1 H0 52.07(18) . . ?
Ag8 Ag1 H0 52.07(18) 3_565 . ?
Ag8 Ag1 H0 52.07(18) 2_665 . ?
Se1 Ag1 H0 113.37(6) 2_665 . ?
Se1 Ag1 H0 113.37(6) 3_565 . ?
Se1 Ag1 H0 113.38(6) . . ?
Ag3 Ag1 H0 33.75(4) . . ?
Ag3 Ag1 H0 33.75(4) 2_665 . ?
Ag3 Ag1 H0 33.75(4) 3_565 . ?
Ag4 Ag1 H0 70.18(6) . . ?
Ag4 Ag1 H0 70.18(6) 2_665 . ?
Ag1 Ag5 Se1 95.0(3) . 2_665 ?
Ag1 Ag5 Se1 95.0(3) . 3_565 ?
Se1 Ag5 Se1 119.25(8) 2_665 3_565 ?
Ag1 Ag5 Se1 95.0(3) . . ?
Se1 Ag5 Se1 119.25(8) 2_665 . ?
Se1 Ag5 Se1 119.25(8) 3_565 . ?
Ag1 Ag5 Ag8 39.1(2) . . ?
Se1 Ag5 Ag8 94.1(2) 2_665 . ?
Se1 Ag5 Ag8 127.5(4) 3_565 . ?
Se1 Ag5 Ag8 61.40(18) . . ?
Ag1 Ag5 Ag8 39.06(19) . 3_565 ?
Se1 Ag5 Ag8 127.5(4) 2_665 3_565 ?
Se1 Ag5 Ag8 61.40(18) 3_565 3_565 ?
Se1 Ag5 Ag8 94.2(2) . 3_565 ?
Ag8 Ag5 Ag8 66.2(3) . 3_565 ?
Ag1 Ag5 Ag8 39.06(19) . 2_665 ?
Se1 Ag5 Ag8 61.40(18) 2_665 2_665 ?
Se1 Ag5 Ag8 94.1(2) 3_565 2_665 ?
Se1 Ag5 Ag8 127.5(4) . 2_665 ?
Ag8 Ag5 Ag8 66.2(3) . 2_665 ?
Ag8 Ag5 Ag8 66.2(3) 3_565 2_665 ?
Ag6 Ag2 Se3 90.08(7) . 2_665 ?
Ag6 Ag2 Se3 90.08(7) . . ?
Se3 Ag2 Se3 120.000(1) 2_665 . ?
Ag6 Ag2 Se3 90.08(7) . 3_565 ?
Se3 Ag2 Se3 119.999(1) 2_665 3_565 ?
Se3 Ag2 Se3 120.001(1) . 3_565 ?
Ag6 Ag2 Ag3 35.63(4) . 2_665 ?
Se3 Ag2 Ag3 119.07(9) 2_665 2_665 ?
Se3 Ag2 Ag3 92.21(6) . 2_665 ?
Se3 Ag2 Ag3 58.59(5) 3_565 2_665 ?
Ag6 Ag2 Ag3 35.63(4) . 3_565 ?
Se3 Ag2 Ag3 92.22(6) 2_665 3_565 ?
Se3 Ag2 Ag3 58.59(5) . 3_565 ?
Se3 Ag2 Ag3 119.07(9) 3_565 3_565 ?
Ag3 Ag2 Ag3 60.60(6) 2_665 3_565 ?
Ag6 Ag2 Ag3 35.63(4) . . ?
Se3 Ag2 Ag3 58.59(5) 2_665 . ?
Se3 Ag2 Ag3 119.07(9) . . ?
Se3 Ag2 Ag3 92.21(6) 3_565 . ?
Ag3 Ag2 Ag3 60.60(6) 2_665 . ?
Ag3 Ag2 Ag3 60.60(6) 3_565 . ?
Ag2 Ag6 Ag3 128.3(3) . 2_665 ?
Ag2 Ag6 Ag3 128.3(3) . 3_565 ?
Ag3 Ag6 Ag3 85.7(4) 2_665 3_565 ?
Ag2 Ag6 Ag3 128.3(3) . . ?
Ag3 Ag6 Ag3 85.7(4) 2_665 . ?
Ag3 Ag6 Ag3 85.7(4) 3_565 . ?
Ag2 Ag6 Se3 67.2(3) . 2_665 ?
Ag3 Ag6 Se3 147.4(3) 2_665 2_665 ?
Ag3 Ag6 Se3 106.66(9) 3_565 2_665 ?
Ag3 Ag6 Se3 65.88(5) . 2_665 ?
Ag2 Ag6 Se3 67.2(3) . . ?
Ag3 Ag6 Se3 106.66(9) 2_665 . ?
Ag3 Ag6 Se3 65.88(5) 3_565 . ?
Ag3 Ag6 Se3 147.4(3) . . ?
Se3 Ag6 Se3 105.9(3) 2_665 . ?
Ag2 Ag6 Se3 67.2(3) . 3_565 ?
Ag3 Ag6 Se3 65.88(5) 2_665 3_565 ?
Ag3 Ag6 Se3 147.4(3) 3_565 3_565 ?
Ag3 Ag6 Se3 106.66(9) . 3_565 ?
Se3 Ag6 Se3 105.9(3) 2_665 3_565 ?
Se3 Ag6 Se3 105.9(3) . 3_565 ?
Ag2 Ag6 Ag7 108.1(3) . 3_565 ?
Ag3 Ag6 Ag7 103.5(4) 2_665 3_565 ?
Ag3 Ag6 Ag7 20.63(13) 3_565 3_565 ?
Ag3 Ag6 Ag7 97.2(3) . 3_565 ?
Se3 Ag6 Ag7 95.94(13) 2_665 3_565 ?
Se3 Ag6 Ag7 50.93(12) . 3_565 ?
Se3 Ag6 Ag7 152.54(15) 3_565 3_565 ?
Ag2 Ag6 Ag7 108.1(3) . 2_665 ?
Ag3 Ag6 Ag7 20.63(13) 2_665 2_665 ?
Ag3 Ag6 Ag7 97.2(3) 3_565 2_665 ?
Ag3 Ag6 Ag7 103.5(4) . 2_665 ?
Se3 Ag6 Ag7 152.54(15) 2_665 2_665 ?
Se3 Ag6 Ag7 95.94(13) . 2_665 ?
Se3 Ag6 Ag7 50.93(12) 3_565 2_665 ?
Ag7 Ag6 Ag7 110.8(3) 3_565 2_665 ?
Ag2 Ag6 Ag7 108.1(3) . . ?
Ag3 Ag6 Ag7 97.2(3) 2_665 . ?
Ag3 Ag6 Ag7 103.5(4) 3_565 . ?
Ag3 Ag6 Ag7 20.62(13) . . ?
Se3 Ag6 Ag7 50.93(12) 2_665 . ?
Se3 Ag6 Ag7 152.54(15) . . ?
Se3 Ag6 Ag7 95.94(13) 3_565 . ?
Ag7 Ag6 Ag7 110.8(3) 3_565 . ?
Ag7 Ag6 Ag7 110.8(3) 2_665 . ?
Ag2 Ag6 Ag8 143.49(18) . 3_565 ?
Ag3 Ag6 Ag8 44.7(2) 2_665 3_565 ?
Ag3 Ag6 Ag8 41.3(2) 3_565 3_565 ?
Ag3 Ag6 Ag8 88.2(4) . 3_565 ?
Se3 Ag6 Ag8 142.2(4) 2_665 3_565 ?
Se3 Ag6 Ag8 80.83(17) . 3_565 ?
Se3 Ag6 Ag8 107.7(2) 3_565 3_565 ?
Ag7 Ag6 Ag8 59.0(2) 3_565 3_565 ?
Ag7 Ag6 Ag8 56.8(2) 2_665 3_565 ?
Ag7 Ag6 Ag8 108.4(4) . 3_565 ?
Ag2 Ag6 Ag8 143.49(18) . 2_665 ?
Ag3 Ag6 Ag8 41.3(2) 2_665 2_665 ?
Ag3 Ag6 Ag8 88.2(4) 3_565 2_665 ?
Ag3 Ag6 Ag8 44.7(2) . 2_665 ?
Se3 Ag6 Ag8 107.7(2) 2_665 2_665 ?
Se3 Ag6 Ag8 142.2(4) . 2_665 ?
Se3 Ag6 Ag8 80.83(17) 3_565 2_665 ?
Ag7 Ag6 Ag8 108.4(4) 3_565 2_665 ?
Ag7 Ag6 Ag8 59.0(2) 2_665 2_665 ?
Ag7 Ag6 Ag8 56.8(2) . 2_665 ?
Ag8 Ag6 Ag8 62.0(3) 3_565 2_665 ?
Ag7 Ag3 Ag8 133.6(4) . . ?
Ag7 Ag3 Ag8 114.8(4) . 2_665 ?
Ag8 Ag3 Ag8 98.0(3) . 2_665 ?
Ag7 Ag3 Ag6 116.6(4) . . ?
Ag8 Ag3 Ag6 93.9(2) . . ?
Ag8 Ag3 Ag6 90.3(2) 2_665 . ?
Ag7 Ag3 Se2 72.2(3) . . ?
Ag8 Ag3 Se2 66.00(17) . . ?
Ag8 Ag3 Se2 109.70(15) 2_665 . ?
Ag6 Ag3 Se2 152.83(6) . . ?
Ag7 Ag3 Se3 63.3(3) . 2_665 ?
Ag8 Ag3 Se3 104.57(16) . 2_665 ?
Ag8 Ag3 Se3 148.13(15) 2_665 2_665 ?
Ag6 Ag3 Se3 66.2(3) . 2_665 ?
Se2 Ag3 Se3 100.01(6) . 2_665 ?
Ag7 Ag3 Se4 49.2(3) . . ?
Ag8 Ag3 Se4 157.27(16) . . ?
Ag8 Ag3 Se4 67.91(17) 2_665 . ?
Ag6 Ag3 Se4 103.57(14) . . ?
Se2 Ag3 Se4 100.99(6) . . ?
Se3 Ag3 Se4 95.82(6) 2_665 . ?
Ag7 Ag3 Ag4 95.1(3) . 2_665 ?
Ag8 Ag3 Ag4 110.08(16) . 2_665 ?
Ag8 Ag3 Ag4 20.60(17) 2_665 2_665 ?
Ag6 Ag3 Ag4 105.56(14) . 2_665 ?
Se2 Ag3 Ag4 98.75(5) . 2_665 ?
Se3 Ag3 Ag4 144.93(6) 2_665 2_665 ?
Se4 Ag3 Ag4 51.45(5) . 2_665 ?
Ag7 Ag3 Ag2 100.9(3) . . ?
Ag8 Ag3 Ag2 104.26(16) . . ?
Ag8 Ag3 Ag2 100.87(15) 2_665 . ?
Ag6 Ag3 Ag2 16.1(3) . . ?
Se2 Ag3 Ag2 148.79(5) . . ?
Se3 Ag3 Ag2 52.05(5) 2_665 . ?
Se4 Ag3 Ag2 96.11(5) . . ?
Ag4 Ag3 Ag2 112.30(5) 2_665 . ?
Ag7 Ag3 Ag3 132.2(3) . 2_665 ?
Ag8 Ag3 Ag3 94.27(18) . 2_665 ?
Ag8 Ag3 Ag3 43.51(17) 2_665 2_665 ?
Ag6 Ag3 Ag3 47.2(2) . 2_665 ?
Se2 Ag3 Ag3 146.34(4) . 2_665 ?
Se3 Ag3 Ag3 111.64(4) 2_665 2_665 ?
Se4 Ag3 Ag3 87.31(6) . 2_665 ?
Ag4 Ag3 Ag3 61.20(5) 2_665 2_665 ?
Ag2 Ag3 Ag3 59.70(3) . 2_665 ?
Ag7 Ag3 Ag3 150.8(3) . 3_565 ?
Ag8 Ag3 Ag3 47.09(16) . 3_565 ?
Ag8 Ag3 Ag3 91.57(18) 2_665 3_565 ?
Ag6 Ag3 Ag3 47.2(2) . 3_565 ?
Se2 Ag3 Ag3 112.06(6) . 3_565 ?
Se3 Ag3 Ag3 87.67(5) 2_665 3_565 ?
Se4 Ag3 Ag3 145.64(6) . 3_565 ?
Ag4 Ag3 Ag3 112.08(5) 2_665 3_565 ?
Ag2 Ag3 Ag3 59.70(3) . 3_565 ?
Ag3 Ag3 Ag3 60.0 2_665 3_565 ?
Ag7 Ag3 Ag4 117.6(3) . . ?
Ag8 Ag3 Ag4 15.98(18) . . ?
Ag8 Ag3 Ag4 110.37(15) 2_665 . ?
Ag6 Ag3 Ag4 103.38(14) . . ?
Se2 Ag3 Ag4 53.14(4) . . ?
Se3 Ag3 Ag4 96.42(5) 2_665 . ?
Se4 Ag3 Ag4 153.01(6) . . ?
Ag4 Ag3 Ag4 118.51(6) 2_665 . ?
Ag2 Ag3 Ag4 110.37(5) . . ?
Ag3 Ag3 Ag4 110.17(5) 2_665 . ?
Ag3 Ag3 Ag4 58.93(5) 3_565 . ?
Ag7 Ag3 H0 168.1(11) . . ?
Ag8 Ag3 H0 55.6(17) . . ?
Ag8 Ag3 H0 53.3(14) 2_665 . ?
Ag6 Ag3 H0 66(4) . . ?
Se2 Ag3 H0 111(4) . . ?
Se3 Ag3 H0 125(4) 2_665 . ?
Se4 Ag3 H0 119.15(18) . . ?
Ag4 Ag3 H0 73.2(18) 2_665 . ?
Ag2 Ag3 H0 82(4) . . ?
Ag3 Ag3 H0 40(3) 2_665 . ?
Ag3 Ag3 H0 40(3) 3_565 . ?
Ag4 Ag3 H0 71.5(17) . . ?
Ag3 Ag7 Se4 107.3(4) . . ?
Ag3 Ag7 Se3 91.7(4) . 2_665 ?
Se4 Ag7 Se3 123.3(3) . 2_665 ?
Ag3 Ag7 Se2 82.4(3) . . ?
Se4 Ag7 Se2 123.5(3) . . ?
Se3 Ag7 Se2 111.5(2) 2_665 . ?
Ag3 Ag7 Ag8 44.0(3) . 2_665 ?
Se4 Ag7 Ag8 65.5(2) . 2_665 ?
Se3 Ag7 Ag8 126.0(3) 2_665 2_665 ?
Se2 Ag7 Ag8 94.1(2) . 2_665 ?
Ag3 Ag7 Ag6 42.7(4) . . ?
Se4 Ag7 Ag6 99.3(2) . . ?
Se3 Ag7 Ag6 60.5(3) 2_665 . ?
Se2 Ag7 Ag6 119.9(3) . . ?
Ag8 Ag7 Ag6 65.4(3) 2_665 . ?
Ag3 Ag7 Ag8 30.2(3) . . ?
Se4 Ag7 Ag8 132.1(3) . . ?
Se3 Ag7 Ag8 88.9(2) 2_665 . ?
Se2 Ag7 Ag8 55.90(18) . . ?
Ag8 Ag7 Ag8 66.8(3) 2_665 . ?
Ag6 Ag7 Ag8 64.2(3) . . ?
Ag3 Ag7 Ag4 64.5(3) . 2_665 ?
Se4 Ag7 Ag4 49.30(13) . 2_665 ?
Se3 Ag7 Ag4 143.3(3) 2_665 2_665 ?
Se2 Ag7 Ag4 93.50(18) . 2_665 ?
Ag8 Ag7 Ag4 21.15(15) 2_665 2_665 ?
Ag6 Ag7 Ag4 84.0(3) . 2_665 ?
Ag8 Ag7 Ag4 83.3(2) . 2_665 ?
Ag8 Ag4 Se4 91.7(3) . 3_565 ?
Ag8 Ag4 Se1 91.1(2) . . ?
Se4 Ag4 Se1 123.92(8) 3_565 . ?
Ag8 Ag4 Se2 78.8(3) . . ?
Se4 Ag4 Se2 121.23(7) 3_565 . ?
Se1 Ag4 Se2 114.21(6) . . ?
Ag8 Ag4 Ag3 40.2(2) . 3_565 ?
Se4 Ag4 Ag3 59.35(5) 3_565 3_565 ?
Se1 Ag4 Ag3 90.49(5) . 3_565 ?
Se2 Ag4 Ag3 115.46(7) . 3_565 ?
Ag8 Ag4 Ag3 28.3(2) . . ?
Se4 Ag4 Ag3 91.08(6) 3_565 . ?
Se1 Ag4 Ag3 114.44(6) . . ?
Se2 Ag4 Ag3 55.60(5) . . ?
Ag3 Ag4 Ag3 59.87(5) 3_565 . ?
Ag8 Ag4 Ag1 38.6(2) . . ?
Se4 Ag4 Ag1 120.22(8) 3_565 . ?
Se1 Ag4 Ag1 54.34(5) . . ?
Se2 Ag4 Ag1 86.13(5) . . ?
Ag3 Ag4 Ag1 60.91(6) 3_565 . ?
Ag3 Ag4 Ag1 60.23(6) . . ?
Ag8 Ag4 Ag7 60.0(3) . 3_565 ?
Se4 Ag4 Ag7 41.36(14) 3_565 3_565 ?
Se1 Ag4 Ag7 95.86(11) . 3_565 ?
Se2 Ag4 Ag7 129.26(13) . 3_565 ?
Ag3 Ag4 Ag7 20.36(13) 3_565 3_565 ?
Ag3 Ag4 Ag7 75.28(13) . 3_565 ?
Ag1 Ag4 Ag7 79.41(14) . 3_565 ?
Ag4 Ag8 Ag3 135.7(4) . . ?
Ag4 Ag8 Ag3 119.2(4) . 3_565 ?
Ag3 Ag8 Ag3 89.4(3) . 3_565 ?
Ag4 Ag8 Ag1 123.0(4) . . ?
Ag3 Ag8 Ag1 89.4(3) . . ?
Ag3 Ag8 Ag1 86.4(2) 3_565 . ?
Ag4 Ag8 Se2 74.5(3) . . ?
Ag3 Ag8 Se2 67.78(14) . . ?
Ag3 Ag8 Se2 154.0(3) 3_565 . ?
Ag1 Ag8 Se2 104.92(19) . . ?
Ag4 Ag8 Se1 63.5(2) . . ?
Ag3 Ag8 Se1 147.4(3) . . ?
Ag3 Ag8 Se1 102.16(18) 3_565 . ?
Ag1 Ag8 Se1 61.50(13) . . ?
Se2 Ag8 Se1 103.8(2) . . ?
Ag4 Ag8 Se4 62.9(2) . 3_565 ?
Ag3 Ag8 Se4 108.5(2) . 3_565 ?
Ag3 Ag8 Se4 65.22(14) 3_565 3_565 ?
Ag1 Ag8 Se4 145.5(2) . 3_565 ?
Se2 Ag8 Se4 109.1(2) . 3_565 ?
Se1 Ag8 Se4 104.0(2) . 3_565 ?
Ag4 Ag8 Ag7 98.9(3) . 3_565 ?
Ag3 Ag8 Ag7 101.7(3) . 3_565 ?
Ag3 Ag8 Ag7 21.22(15) 3_565 3_565 ?
Ag1 Ag8 Ag7 103.6(2) . 3_565 ?
Se2 Ag8 Ag7 149.4(2) . 3_565 ?
Se1 Ag8 Ag7 99.43(19) . 3_565 ?
Se4 Ag8 Ag7 44.95(17) 3_565 3_565 ?
Ag4 Ag8 Ag5 110.2(3) . . ?
Ag3 Ag8 Ag5 98.6(3) . . ?
Ag3 Ag8 Ag5 95.6(2) 3_565 . ?
Ag1 Ag8 Ag5 13.00(11) . . ?
Se2 Ag8 Ag5 99.84(17) . . ?
Se1 Ag8 Ag5 50.41(14) . . ?
Se4 Ag8 Ag5 145.97(19) 3_565 . ?
Ag7 Ag8 Ag5 110.3(2) 3_565 . ?
Ag4 Ag8 Ag7 119.5(3) . . ?
Ag3 Ag8 Ag7 16.21(13) . . ?
Ag3 Ag8 Ag7 101.7(3) 3_565 . ?
Ag1 Ag8 Ag7 100.7(3) . . ?
Se2 Ag8 Ag7 53.72(15) . . ?
Se1 Ag8 Ag7 149.0(2) . . ?
Se4 Ag8 Ag7 103.86(19) 3_565 . ?
Ag7 Ag8 Ag7 109.9(3) 3_565 . ?
Ag5 Ag8 Ag7 107.6(2) . . ?
Ag4 Ag8 Ag6 143.6(4) . . ?
Ag3 Ag8 Ag6 44.80(14) . . ?
Ag3 Ag8 Ag6 44.93(13) 3_565 . ?
Ag1 Ag8 Ag6 91.4(3) . . ?
Se2 Ag8 Ag6 110.40(19) . . ?
Se1 Ag8 Ag6 141.0(2) . . ?
Se4 Ag8 Ag6 82.18(19) 3_565 . ?
Ag7 Ag8 Ag6 57.79(18) 3_565 . ?
Ag5 Ag8 Ag6 104.4(3) . . ?
Ag7 Ag8 Ag6 56.87(17) . . ?
Ag4 Ag8 Ag8 154.0(3) . 2_665 ?
Ag3 Ag8 Ag8 42.55(19) . 2_665 ?
Ag3 Ag8 Ag8 85.96(16) 3_565 2_665 ?
Ag1 Ag8 Ag8 46.92(13) . 2_665 ?
Se2 Ag8 Ag8 85.2(3) . 2_665 ?
Se1 Ag8 Ag8 107.30(13) . 2_665 ?
Se4 Ag8 Ag8 141.13(15) 3_565 2_665 ?
Ag7 Ag8 Ag8 106.7(2) 3_565 2_665 ?
Ag5 Ag8 Ag8 56.93(15) . 2_665 ?
Ag7 Ag8 Ag8 55.1(2) . 2_665 ?
Ag6 Ag8 Ag8 58.98(15) . 2_665 ?
Ag4 Ag8 H0 165(3) . . ?
Ag3 Ag8 H0 59(3) . . ?
Ag3 Ag8 H0 57(3) 3_565 . ?
Ag1 Ag8 H0 46(5) . . ?
Se2 Ag8 H0 115.7(4) . . ?
Se1 Ag8 H0 102(4) . . ?
Se4 Ag8 H0 120(4) 3_565 . ?
Ag7 Ag8 H0 78(3) 3_565 . ?
Ag5 Ag8 H0 59(5) . . ?
Ag7 Ag8 H0 75(3) . . ?
Ag6 Ag8 H0 46(5) . . ?
Ag8 Ag8 H0 30.9(11) 2_665 . ?
P1 Se1 Ag5 98.05(10) . . ?
P1 Se1 Ag4 110.57(10) . . ?
Ag5 Se1 Ag4 91.6(2) . . ?
P1 Se1 Ag1 94.59(9) . . ?
Ag5 Se1 Ag1 18.4(2) . . ?
Ag4 Se1 Ag1 75.89(7) . . ?
P1 Se1 Ag8 103.13(14) . . ?
Ag5 Se1 Ag8 68.2(3) . . ?
Ag4 Se1 Ag8 25.43(13) . . ?
Ag1 Se1 Ag8 51.20(15) . . ?
P1 Se2 Ag7 111.76(17) 2_665 . ?
P1 Se2 Ag4 100.72(10) 2_665 . ?
Ag7 Se2 Ag4 93.12(18) . . ?
P1 Se2 Ag8 95.93(14) 2_665 . ?
Ag7 Se2 Ag8 70.4(2) . . ?
Ag4 Se2 Ag8 26.70(15) . . ?
P1 Se2 Ag3 102.56(9) 2_665 . ?
Ag7 Se2 Ag3 25.37(17) . . ?
Ag4 Se2 Ag3 71.26(5) . . ?
Ag8 Se2 Ag3 46.22(16) . . ?
P2 Se3 Ag7 115.32(19) . 3_565 ?
P2 Se3 Ag2 106.73(12) . . ?
Ag7 Se3 Ag2 86.63(17) 3_565 . ?
P2 Se3 Ag3 102.11(12) . 3_565 ?
Ag7 Se3 Ag3 24.97(18) 3_565 3_565 ?
Ag2 Se3 Ag3 69.36(7) . 3_565 ?
P2 Se3 Ag6 101.36(13) . . ?
Ag7 Se3 Ag6 68.5(3) 3_565 . ?
Ag2 Se3 Ag6 22.7(3) . . ?
Ag3 Se3 Ag6 47.9(3) 3_565 . ?
P2 Se4 Ag7 111.3(2) 3_565 . ?
P2 Se4 Ag4 104.27(12) 3_565 2_665 ?
Ag7 Se4 Ag4 89.3(2) . 2_665 ?
P2 Se4 Ag3 103.49(12) 3_565 . ?
Ag7 Se4 Ag3 23.6(2) . . ?
Ag4 Se4 Ag3 69.20(5) 2_665 . ?
P2 Se4 Ag8 96.24(15) 3_565 2_665 ?
Ag7 Se4 Ag8 69.5(2) . 2_665 ?
Ag4 Se4 Ag8 25.40(14) 2_665 2_665 ?
Ag3 Se4 Ag8 46.86(14) . 2_665 ?
O1 P1 O2 108.3(5) . . ?
O1 P1 Se1 104.3(4) . . ?
O2 P1 Se1 108.7(3) . . ?
O1 P1 Se2 109.6(4) . 3_565 ?
O2 P1 Se2 103.4(3) . 3_565 ?
Se1 P1 Se2 122.03(14) . 3_565 ?
O3 P2 O4 95.5(14) . . ?
O3 P2 Se3 105.5(10) . . ?
O4 P2 Se3 114.3(6) . . ?
O3 P2 Se4 111.3(10) . 2_665 ?
O4 P2 Se4 106.9(5) . 2_665 ?
Se3 P2 Se4 120.55(17) . 2_665 ?
C1 O1 P1 126.1(10) . . ?
C3 O2 P1 121.2(9) . . ?
C7 O3 P2 157(3) . . ?
C5 O4 P2 129.8(15) . . ?
C2 C1 O1 116.0(18) . . ?
C2 C1 H1A 108.3 . . ?
O1 C1 H1A 108.3 . . ?
C2 C1 H1B 108.3 . . ?
O1 C1 H1B 108.3 . . ?
H1A C1 H1B 107.4 . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
O2 C3 C4 108.5(14) . . ?
O2 C3 H3A 110.0 . . ?
C4 C3 H3A 110.0 . . ?
O2 C3 H3B 110.0 . . ?
C4 C3 H3B 110.0 . . ?
H3A C3 H3B 108.4 . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C6 C5 O4 126(3) . . ?
C6 C5 H5A 105.8 . . ?
O4 C5 H5A 105.8 . . ?
C6 C5 H5B 105.8 . . ?
O4 C5 H5B 105.8 . . ?
H5A C5 H5B 106.2 . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
O3 C7 C8 167(4) . . ?
O3 C7 H7A 93.9 . . ?
C8 C7 H7A 93.9 . . ?
O3 C7 H7B 93.9 . . ?
C8 C7 H7B 93.9 . . ?
H7A C7 H7B 103.1 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
F1 P3 F1 98.1(16) 2_665 . ?
F1 P3 F1 98.1(16) 2_665 3_565 ?
F1 P3 F1 98.1(16) . 3_565 ?
F1 P3 F2 80.3(18) 2_665 . ?
F1 P3 F2 87.4(18) . . ?
F1 P3 F2 174.4(18) 3_565 . ?
F1 P3 F2 87.4(18) 2_665 2_665 ?
F1 P3 F2 174.4(18) . 2_665 ?
F1 P3 F2 80.3(18) 3_565 2_665 ?
F2 P3 F2 94(2) . 2_665 ?
F1 P3 F2 174.4(18) 2_665 3_565 ?
F1 P3 F2 80.3(18) . 3_565 ?
F1 P3 F2 87.4(18) 3_565 3_565 ?
F2 P3 F2 94(2) . 3_565 ?
F2 P3 F2 94(2) 2_665 3_565 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag5 0.860(9) . ?
Ag1 Ag8 2.410(6) . ?
Ag1 Ag8 2.410(6) 3_565 ?
Ag1 Ag8 2.410(6) 2_665 ?
Ag1 Se1 2.7168(16) 2_665 ?
Ag1 Se1 2.7168(16) 3_565 ?
Ag1 Se1 2.7170(16) . ?
Ag1 Ag3 3.189(3) . ?
Ag1 Ag3 3.190(3) 2_665 ?
Ag1 Ag3 3.190(3) 3_565 ?
Ag1 Ag4 3.2433(18) . ?
Ag1 Ag4 3.2434(18) 2_665 ?
Ag1 H0 1.74(16) . ?
Ag5 Se1 2.5034(15) 2_665 ?
Ag5 Se1 2.5034(15) 3_565 ?
Ag5 Se1 2.5034(15) . ?
Ag5 Ag8 3.016(10) . ?
Ag5 Ag8 3.016(10) 3_565 ?
Ag5 Ag8 3.016(10) 2_665 ?
Ag2 Ag6 1.075(13) . ?
Ag2 Se3 2.5629(16) 2_665 ?
Ag2 Se3 2.5630(16) . ?
Ag2 Se3 2.5630(16) 3_565 ?
Ag2 Ag3 3.041(2) 2_665 ?
Ag2 Ag3 3.041(2) 3_565 ?
Ag2 Ag3 3.041(2) . ?
Ag6 Ag3 2.256(9) 2_665 ?
Ag6 Ag3 2.257(9) 3_565 ?
Ag6 Ag3 2.257(9) . ?
Ag6 Se3 2.781(6) 2_665 ?
Ag6 Se3 2.781(6) . ?
Ag6 Se3 2.781(6) 3_565 ?
Ag6 Ag7 2.972(8) 3_565 ?
Ag6 Ag7 2.972(8) 2_665 ?
Ag6 Ag7 2.972(8) . ?
Ag6 Ag8 3.195(14) 3_565 ?
Ag6 Ag8 3.195(14) 2_665 ?
Ag3 Ag7 1.171(8) . ?
Ag3 Ag8 2.113(7) . ?
Ag3 Ag8 2.248(6) 2_665 ?
Ag3 Se2 2.7096(16) . ?
Ag3 Se3 2.7740(18) 2_665 ?
Ag3 Se4 2.7971(19) . ?
Ag3 Ag4 3.0393(19) 2_665 ?
Ag3 Ag3 3.069(2) 2_665 ?
Ag3 Ag3 3.069(2) 3_565 ?
Ag3 Ag4 3.110(2) . ?
Ag3 H0 1.99(7) . ?
Ag7 Se4 2.216(7) . ?
Ag7 Se3 2.480(6) 2_665 ?
Ag7 Se2 2.603(6) . ?
Ag7 Ag8 2.938(9) 2_665 ?
Ag7 Ag8 3.041(9) . ?
Ag7 Ag4 3.354(6) 2_665 ?
Ag4 Ag8 1.225(7) . ?
Ag4 Se4 2.5432(19) 3_565 ?
Ag4 Se1 2.5530(18) . ?
Ag4 Se2 2.627(2) . ?
Ag4 Ag3 3.0395(19) 3_565 ?
Ag4 Ag7 3.354(6) 3_565 ?
Ag8 Ag3 2.248(6) 3_565 ?
Ag8 Se2 2.674(5) . ?
Ag8 Se1 2.852(6) . ?
Ag8 Se4 2.855(6) 3_565 ?
Ag8 Ag7 2.939(9) 3_565 ?
Ag8 Ag8 3.292(13) 2_665 ?
Ag8 H0 1.92(2) . ?
Se1 P1 2.149(3) . ?
Se2 P1 2.171(3) 2_665 ?
Se3 P2 2.145(5) . ?
Se3 Ag7 2.480(6) 3_565 ?
Se3 Ag3 2.7739(18) 3_565 ?
Se4 P2 2.161(4) 3_565 ?
Se4 Ag4 2.5427(19) 2_665 ?
Se4 Ag8 2.854(6) 2_665 ?
P1 O1 1.579(8) . ?
P1 O2 1.596(9) . ?
P1 Se2 2.171(3) 3_565 ?
P2 O3 1.503(16) . ?
P2 O4 1.505(11) . ?
P2 Se4 2.161(4) 2_665 ?
O1 C1 1.418(18) . ?
O2 C3 1.430(17) . ?
O3 C7 1.14(3) . ?
O4 C5 1.33(3) . ?
C1 C2 1.34(2) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C2 H2A 0.9600 . ?
C2 H2B 0.9600 . ?
C2 H2C 0.9600 . ?
C3 C4 1.45(2) . ?
C3 H3A 0.9700 . ?
C3 H3B 0.9700 . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C4 H4C 0.9600 . ?
C5 C6 1.31(3) . ?
C5 H5A 0.9700 . ?
C5 H5B 0.9700 . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C7 C8 1.19(3) . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
P3 F1 1.44(2) 2_665 ?
P3 F1 1.44(2) . ?
P3 F1 1.44(2) 3_565 ?
P3 F2 1.45(2) . ?
P3 F2 1.45(2) 2_665 ?
P3 F2 1.45(2) 3_565 ?
