#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:01:37 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179227 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/47/4314724.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4314724
loop_
_publ_author_name
'Jamie S. Ritch'
'Tristram Chivers'
'Kibriya Ahmad'
'Mohammad Afzaal'
'Paul O'Brien'
_publ_contact_author_address
;
Department of Chemistry
University of Calgary
2500 University Drive NW
Calgary AB  T2N 1N4
Canada
;
_publ_contact_author_name        'Prof. Tristram Chivers'
_publ_section_title
;
 Synthesis, Structures, and Multinuclear NMR Spectra of Tin(II) and
 Lead(II) Complexes of Tellurium-Containing Imidodiphosphinate Ligands:
 Preparation of Two Morphologies of Phase-Pure PbTe from a Single-Source
 Precursor
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1198
_journal_page_last               1205
_journal_paper_doi               10.1021/ic9021728
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C24 H56 N2 P4 Pb Se2 Te2'
_chemical_formula_sum            'C24 H56 N2 P4 Pb Se2 Te2'
_chemical_formula_weight         1116.90
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 120.15(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   34.625(7)
_cell_length_b                   9.7284(19)
_cell_length_c                   25.834(5)
_cell_measurement_reflns_used    35222
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.03
_cell_measurement_theta_min      2.63
_cell_volume                     7525(3)
_computing_cell_refinement       'Nonius DENZO'
_computing_data_collection       'Nonius COLLECT'
_computing_data_reduction        'Nonius DENZO'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'phiω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0329
_diffrn_reflns_av_sigmaI/netI    0.0529
_diffrn_reflns_limit_h_max       41
_diffrn_reflns_limit_h_min       -41
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            35222
_diffrn_reflns_theta_full        25.03
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_min         2.63
_exptl_absorpt_coefficient_mu    8.126
_exptl_absorpt_correction_T_max  0.6001
_exptl_absorpt_correction_T_min  0.4422
_exptl_absorpt_correction_type   integration
_exptl_absorpt_process_details   'HKL Scalepack (Otwinowski & Minor 1997)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.972
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4224
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.07
_refine_diff_density_max         2.515
_refine_diff_density_min         -4.222
_refine_diff_density_rms         0.309
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.085
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     345
_refine_ls_number_reflns         6613
_refine_ls_number_restraints     8
_refine_ls_restrained_S_all      1.103
_refine_ls_R_factor_all          0.0620
_refine_ls_R_factor_gt           0.0595
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1046P)²+101.5145P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1606
_refine_ls_wR_factor_ref         0.1638
_reflns_number_gt                6243
_reflns_number_total             6613
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic9021728_si_002_6.cif
_cod_data_source_block           Compound8
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        7524(3)
_cod_database_code               4314724
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pb1 Pb 0.069920(10) 0.85455(3) 0.352304(14) 0.02806(15) Uani 1 1 d . . .
Te1 Te 0.04534(6) 0.76177(15) 0.21855(9) 0.0247(4) Uani 0.644(4) 1 d PD A 1
Se1 Se 0.15332(13) 0.9929(5) 0.37200(16) 0.0298(7) Uani 0.644(4) 1 d PD A 1
Se1A Se 0.0462(2) 0.7913(7) 0.2152(3) 0.0298(7) Uani 0.356(4) 1 d PD A 2
Te1A Te 0.15716(15) 0.9791(7) 0.38027(18) 0.0247(4) Uani 0.356(4) 1 d PD A 2
P1 P 0.09654(7) 0.8740(2) 0.19517(10) 0.0224(4) Uani 1 1 d D . .
C1 C 0.0316(4) 1.0259(11) 0.0991(4) 0.042(2) Uani 1 1 d . . .
H1A H 0.0159 1.0439 0.0560 0.063 Uiso 1 1 calc R A .
H1B H 0.0463 1.1104 0.1208 0.063 Uiso 1 1 calc R . .
H1C H 0.0103 0.9950 0.1110 0.063 Uiso 1 1 calc R . .
C2 C 0.0670(3) 0.9138(9) 0.1143(4) 0.0317(19) Uani 1 1 d . A .
H2A H 0.0895 0.9511 0.1046 0.038 Uiso 1 1 calc R . .
C3 C 0.0462(4) 0.7875(12) 0.0755(5) 0.055(3) Uani 1 1 d . . .
H3A H 0.0288 0.8152 0.0334 0.082 Uiso 1 1 calc R A .
H3B H 0.0265 0.7421 0.0873 0.082 Uiso 1 1 calc R . .
H3C H 0.0698 0.7238 0.0808 0.082 Uiso 1 1 calc R . .
C4 C 0.1669(3) 0.7020(12) 0.2712(5) 0.042(2) Uani 1 1 d . . .
H4A H 0.1855 0.6228 0.2745 0.063 Uiso 1 1 calc R A .
H4B H 0.1479 0.6782 0.2880 0.063 Uiso 1 1 calc R . .
H4C H 0.1861 0.7798 0.2933 0.063 Uiso 1 1 calc R . .
C5 C 0.1374(3) 0.7414(9) 0.2049(5) 0.032(2) Uani 1 1 d . A .
H5A H 0.1206 0.6576 0.1825 0.039 Uiso 1 1 calc R . .
C6 C 0.1665(4) 0.7886(12) 0.1791(5) 0.046(3) Uani 1 1 d . . .
H6A H 0.1867 0.7139 0.1825 0.069 Uiso 1 1 calc R A .
H6B H 0.1841 0.8689 0.2014 0.069 Uiso 1 1 calc R . .
H6C H 0.1474 0.8131 0.1368 0.069 Uiso 1 1 calc R . .
N1 N 0.1216(3) 1.0138(8) 0.2281(3) 0.0273(15) Uani 1 1 d . A .
P2 P 0.13775(7) 1.0967(2) 0.28809(9) 0.0216(4) Uani 1 1 d D . .
C7 C 0.0522(3) 1.1803(11) 0.2563(5) 0.038(2) Uani 1 1 d . . .
H7A H 0.0324 1.2567 0.2522 0.057 Uiso 1 1 calc R A .
H7B H 0.0539 1.1154 0.2864 0.057 Uiso 1 1 calc R . .
H7C H 0.0403 1.1332 0.2177 0.057 Uiso 1 1 calc R . .
C8 C 0.0986(3) 1.2354(9) 0.2757(4) 0.0281(18) Uani 1 1 d . A .
H8A H 0.1095 1.2846 0.3146 0.034 Uiso 1 1 calc R . .
C9 C 0.0965(4) 1.3403(10) 0.2299(5) 0.038(2) Uani 1 1 d . . .
H9A H 0.0749 1.4124 0.2239 0.057 Uiso 1 1 calc R A .
H9B H 0.0873 1.2939 0.1918 0.057 Uiso 1 1 calc R . .
H9C H 0.1261 1.3815 0.2449 0.057 Uiso 1 1 calc R . .
C10 C 0.2059(4) 1.2872(12) 0.3527(6) 0.050(3) Uani 1 1 d . . .
H10A H 0.2330 1.3313 0.3578 0.075 Uiso 1 1 calc R A .
H10B H 0.2124 1.2423 0.3902 0.075 Uiso 1 1 calc R . .
H10C H 0.1826 1.3569 0.3421 0.075 Uiso 1 1 calc R . .
C11 C 0.1897(3) 1.1805(10) 0.3030(4) 0.0321(19) Uani 1 1 d . A .
H11A H 0.1831 1.2307 0.2657 0.039 Uiso 1 1 calc R . .
C12 C 0.2261(3) 1.0763(12) 0.3153(6) 0.048(3) Uani 1 1 d . . .
H12A H 0.2520 1.1238 0.3182 0.071 Uiso 1 1 calc R A .
H12B H 0.2147 1.0094 0.2825 0.071 Uiso 1 1 calc R . .
H12C H 0.2348 1.0285 0.3530 0.071 Uiso 1 1 calc R . .
Te2 Te 0.09946(3) 0.57626(12) 0.35742(4) 0.0252(3) Uani 0.70 1 d PD A 1
Se2 Se 0.09203(10) 0.8735(2) 0.48597(12) 0.0346(5) Uani 0.70 1 d PD A 1
Se2A Se 0.11153(18) 0.5692(6) 0.3716(2) 0.0346(5) Uani 0.30 1 d PD A 2
Te2A Te 0.09100(16) 0.8953(4) 0.4789(2) 0.0252(3) Uani 0.30 1 d PD A 2
P3 P 0.12013(7) 0.4798(2) 0.45555(9) 0.0217(4) Uani 1 1 d D . .
C13 C 0.0309(3) 0.4797(13) 0.4248(5) 0.048(3) Uani 1 1 d . . .
H13A H 0.0064 0.4283 0.4243 0.072 Uiso 1 1 calc R A .
H13B H 0.0213 0.5147 0.3846 0.072 Uiso 1 1 calc R . .
H13C H 0.0392 0.5569 0.4528 0.072 Uiso 1 1 calc R . .
C14 C 0.0712(3) 0.3846(10) 0.4448(4) 0.0302(19) Uani 1 1 d . A .
H14A H 0.0786 0.3453 0.4845 0.036 Uiso 1 1 calc R . .
C15 C 0.0589(4) 0.2631(11) 0.4006(5) 0.046(3) Uani 1 1 d . . .
H15A H 0.0350 0.2087 0.4005 0.069 Uiso 1 1 calc R A .
H15B H 0.0852 0.2048 0.4130 0.069 Uiso 1 1 calc R . .
H15C H 0.0486 0.2986 0.3602 0.069 Uiso 1 1 calc R . .
C16 C 0.2077(3) 0.4262(11) 0.4866(5) 0.038(2) Uani 1 1 d . . .
H16A H 0.2301 0.3587 0.4909 0.057 Uiso 1 1 calc R A .
H16B H 0.2188 0.4776 0.5240 0.057 Uiso 1 1 calc R . .
H16C H 0.2018 0.4900 0.4540 0.057 Uiso 1 1 calc R . .
C17 C 0.1641(3) 0.3513(8) 0.4720(4) 0.0273(19) Uani 1 1 d . A .
H17A H 0.1545 0.2937 0.4355 0.033 Uiso 1 1 calc R . .
C18 C 0.1712(4) 0.2562(10) 0.5239(5) 0.040(2) Uani 1 1 d . . .
H18A H 0.1970 0.1963 0.5349 0.059 Uiso 1 1 calc R A .
H18B H 0.1445 0.1998 0.5112 0.059 Uiso 1 1 calc R . .
H18C H 0.1767 0.3120 0.5585 0.059 Uiso 1 1 calc R . .
N2 N 0.1390(2) 0.5735(7) 0.5134(3) 0.0265(15) Uani 1 1 d . A .
P4 P 0.13968(7) 0.7185(2) 0.54115(9) 0.0215(4) Uani 1 1 d D . .
C19 C 0.2086(4) 0.8199(13) 0.5283(6) 0.047(3) Uani 1 1 d . . .
H19A H 0.2407 0.8388 0.5475 0.071 Uiso 1 1 calc R A .
H19B H 0.1918 0.9012 0.5059 0.071 Uiso 1 1 calc R . .
H19C H 0.2011 0.7421 0.5007 0.071 Uiso 1 1 calc R . .
C20 C 0.1966(3) 0.7851(9) 0.5754(4) 0.032(2) Uani 1 1 d . A .
H20A H 0.2170 0.7096 0.6004 0.039 Uiso 1 1 calc R . .
C21 C 0.2044(4) 0.9064(11) 0.6173(5) 0.044(3) Uani 1 1 d . . .
H21A H 0.2339 0.9462 0.6306 0.067 Uiso 1 1 calc R A .
H21B H 0.2028 0.8743 0.6522 0.067 Uiso 1 1 calc R . .
H21C H 0.1814 0.9764 0.5960 0.067 Uiso 1 1 calc R . .
C22 C 0.0829(4) 0.6204(12) 0.5777(5) 0.040(2) Uani 1 1 d . . .
H22A H 0.0777 0.5988 0.6107 0.060 Uiso 1 1 calc R A .
H22B H 0.0818 0.5356 0.5565 0.060 Uiso 1 1 calc R . .
H22C H 0.0598 0.6839 0.5499 0.060 Uiso 1 1 calc R . .
C23 C 0.1282(3) 0.6864(10) 0.6022(4) 0.0293(18) Uani 1 1 d . A .
H23A H 0.1282 0.7761 0.6211 0.035 Uiso 1 1 calc R . .
C24 C 0.1647(3) 0.5938(10) 0.6498(4) 0.035(2) Uani 1 1 d . . .
H24A H 0.1584 0.5771 0.6822 0.052 Uiso 1 1 calc R A .
H24B H 0.1938 0.6392 0.6659 0.052 Uiso 1 1 calc R . .
H24C H 0.1653 0.5060 0.6315 0.052 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Te2 Pb1 Te1A 94.45(12) . . ?
Te2 Pb1 Se1 97.19(10) . . ?
Te1A Pb1 Se1 4.40(13) . . ?
Te2 Pb1 Te2A 100.86(7) . . ?
Te1A Pb1 Te2A 91.15(13) . . ?
Se1 Pb1 Te2A 94.00(12) . . ?
Te2 Pb1 Se2A 6.94(11) . . ?
Te1A Pb1 Se2A 89.57(16) . . ?
Se1 Pb1 Se2A 92.60(14) . . ?
Te2A Pb1 Se2A 96.06(12) . . ?
Te2 Pb1 Se2 96.90(5) . . ?
Te1A Pb1 Se2 92.97(10) . . ?
Se1 Pb1 Se2 96.04(9) . . ?
Te2A Pb1 Se2 4.24(10) . . ?
Se2A Pb1 Se2 92.25(9) . . ?
Te2 Pb1 Te1 71.56(4) . . ?
Te1A Pb1 Te1 93.60(10) . . ?
Se1 Pb1 Te1 91.19(8) . . ?
Te2A Pb1 Te1 171.34(8) . . ?
Se2A Pb1 Te1 76.75(9) . . ?
Se2 Pb1 Te1 167.13(5) . . ?
Te2 Pb1 Se1A 76.26(13) . . ?
Te1A Pb1 Se1A 90.65(13) . . ?
Se1 Pb1 Se1A 87.96(11) . . ?
Te2A Pb1 Se1A 176.72(13) . . ?
Se2A Pb1 Se1A 81.21(16) . . ?
Se2 Pb1 Se1A 172.50(12) . . ?
Te1 Pb1 Se1A 5.38(12) . . ?
Te2 Pb1 Te1 93.77(3) . 2 ?
Te1A Pb1 Te1 163.84(7) . 2 ?
Se1 Pb1 Te1 159.47(7) . 2 ?
Te2A Pb1 Te1 100.93(10) . 2 ?
Se2A Pb1 Te1 99.68(11) . 2 ?
Se2 Pb1 Te1 99.82(7) . 2 ?
Te1 Pb1 Te1 75.88(5) . 2 ?
Se1A Pb1 Te1 77.83(11) . 2 ?
P1 Te1 Pb1 108.01(8) . . ?
P2 Se1 Pb1 107.55(15) . . ?
P1 Se1A Pb1 112.8(2) . . ?
P2 Te1A Pb1 101.95(15) . . ?
N1 P1 C5 110.4(4) . . ?
N1 P1 C2 105.5(4) . . ?
C5 P1 C2 104.6(4) . . ?
N1 P1 Se1A 117.7(3) . . ?
C5 P1 Se1A 110.9(4) . . ?
C2 P1 Se1A 106.7(4) . . ?
N1 P1 Te1 121.4(3) . . ?
C5 P1 Te1 105.1(3) . . ?
C2 P1 Te1 108.7(3) . . ?
C3 C2 C1 110.7(9) . . ?
C3 C2 P1 112.8(7) . . ?
C1 C2 P1 110.7(6) . . ?
C6 C5 C4 110.1(9) . . ?
C6 C5 P1 111.1(7) . . ?
C4 C5 P1 111.3(6) . . ?
P2 N1 P1 141.5(5) . . ?
N1 P2 C8 109.9(4) . . ?
N1 P2 C11 105.2(4) . . ?
C8 P2 C11 105.8(4) . . ?
N1 P2 Se1 121.5(3) . . ?
C8 P2 Se1 107.8(3) . . ?
C11 P2 Se1 105.6(3) . . ?
N1 P2 Te1A 120.8(3) . . ?
C8 P2 Te1A 109.8(3) . . ?
C11 P2 Te1A 104.2(3) . . ?
C7 C8 P2 111.5(6) . . ?
C9 C8 P2 111.7(6) . . ?
C10 C11 C12 111.4(9) . . ?
C10 C11 P2 112.9(7) . . ?
C12 C11 P2 111.7(7) . . ?
P3 Te2 Pb1 108.72(6) . . ?
P4 Se2 Pb1 111.57(13) . . ?
P3 Se2A Pb1 109.8(2) . . ?
P4 Te2A Pb1 110.07(15) . . ?
N2 P3 C14 110.3(4) . . ?
N2 P3 C17 105.7(4) . . ?
C14 P3 C17 106.7(4) . . ?
N2 P3 Se2A 119.1(3) . . ?
C14 P3 Se2A 113.1(3) . . ?
C17 P3 Se2A 100.4(3) . . ?
N2 P3 Te2 121.5(3) . . ?
C14 P3 Te2 105.7(3) . . ?
C17 P3 Te2 106.0(3) . . ?
C13 C14 C15 110.2(8) . . ?
C13 C14 P3 111.3(7) . . ?
C15 C14 P3 112.9(7) . . ?
C16 C17 C18 111.2(8) . . ?
C16 C17 P3 109.2(6) . . ?
C18 C17 P3 111.1(6) . . ?
P4 N2 P3 148.0(5) . . ?
N2 P4 C20 107.6(4) . . ?
N2 P4 C23 106.2(4) . . ?
C20 P4 C23 106.9(4) . . ?
N2 P4 Se2 119.5(3) . . ?
C20 P4 Se2 110.6(3) . . ?
C23 P4 Se2 105.2(3) . . ?
N2 P4 Te2A 119.7(3) . . ?
C20 P4 Te2A 107.2(3) . . ?
C23 P4 Te2A 108.5(3) . . ?
C19 C20 C21 112.1(8) . . ?
C19 C20 P4 110.9(7) . . ?
C21 C20 P4 112.3(7) . . ?
C22 C23 C24 110.6(8) . . ?
C22 C23 P4 109.9(6) . . ?
C24 C23 P4 109.9(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pb1 Te2 2.8737(13) . ?
Pb1 Te1A 2.987(5) . ?
Pb1 Se1 2.988(4) . ?
Pb1 Te2A 2.998(4) . ?
Pb1 Se2A 3.051(6) . ?
Pb1 Se2 3.145(3) . ?
Pb1 Te1 3.244(2) . ?
Pb1 Se1A 3.268(6) . ?
Pb1 Te1 3.571(2) 2 ?
Te1 P1 2.404(2) . ?
Se1 P2 2.199(4) . ?
Se1A P1 2.204(4) . ?
Te1A P2 2.413(4) . ?
P1 N1 1.607(7) . ?
P1 C5 1.835(9) . ?
P1 C2 1.849(9) . ?
C1 C2 1.537(14) . ?
C2 C3 1.518(14) . ?
C4 C5 1.539(14) . ?
C5 C6 1.533(13) . ?
N1 P2 1.579(7) . ?
P2 C8 1.824(9) . ?
P2 C11 1.831(9) . ?
C7 C8 1.521(14) . ?
C8 C9 1.537(13) . ?
C10 C11 1.521(15) . ?
C11 C12 1.521(14) . ?
Te2 P3 2.449(2) . ?
Se2 P4 2.160(3) . ?
Se2A P3 2.213(4) . ?
Te2A P4 2.380(4) . ?
P3 N2 1.585(7) . ?
P3 C14 1.826(9) . ?
P3 C17 1.847(9) . ?
C13 C14 1.531(14) . ?
C14 C15 1.548(13) . ?
C16 C17 1.542(12) . ?
C17 C18 1.543(14) . ?
N2 P4 1.577(7) . ?
P4 C20 1.826(9) . ?
P4 C23 1.837(8) . ?
C19 C20 1.508(14) . ?
C20 C21 1.532(14) . ?
C22 C23 1.508(13) . ?
C23 C24 1.536(13) . ?
