#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:14:52 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179237 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/57/4315737.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4315737
loop_
_publ_author_name
'Wan-Jung Chuang'
'I-Jung Lin'
'Hsing-Yin Chen'
'Yu-Lun Chang'
'Sodio C. N. Hsu'
_publ_section_title
;
 Characterization of A New Copper(I)-Nitrito Complex That Evolves Nitric
 Oxide
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5377
_journal_page_last               5384
_journal_paper_doi               10.1021/ic100083b
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C38 H34 Cl Cu O2 P2'
_chemical_formula_sum            'C38 H34 Cl Cu O2 P2'
_chemical_formula_weight         683.58
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 105.1710(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   22.2512(3)
_cell_length_b                   16.0416(2)
_cell_length_c                   19.2459(3)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      0
_cell_measurement_theta_min      0
_cell_volume                     6630.31(16)
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1986)'
_diffrn_ambient_temperature      200(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0274
_diffrn_reflns_av_sigmaI/netI    0.0272
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            20951
_diffrn_reflns_theta_full        25.03
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_min         1.58
_exptl_absorpt_coefficient_mu    0.869
_exptl_absorpt_correction_T_max  0.8318
_exptl_absorpt_correction_T_min  0.7226
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.370
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2832
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.22
_refine_diff_density_max         0.540
_refine_diff_density_min         -0.681
_refine_diff_density_rms         0.227
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.180
_refine_ls_hydrogen_treatment    fixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     397
_refine_ls_number_reflns         5834
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.180
_refine_ls_R_factor_all          0.0407
_refine_ls_R_factor_gt           0.0294
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0592P)²+1.9165P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0845
_refine_ls_wR_factor_ref         0.1034
_reflns_number_gt                5053
_reflns_number_total             5834
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic100083b_si_002_2.cif
_cod_data_source_block           2
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4315737
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.33450(10) 0.41056(14) 0.01861(12) 0.0281(5) Uani 1 1 d . . .
C2 C 0.33770(12) 0.32444(15) 0.02002(14) 0.0400(6) Uani 1 1 d . . .
H2 H 0.3457 0.2960 0.0648 0.048 Uiso 1 1 calc R . .
C3 C 0.32937(14) 0.27908(18) -0.04309(17) 0.0527(7) Uani 1 1 d . . .
H3 H 0.3319 0.2200 -0.0415 0.063 Uiso 1 1 calc R . .
C4 C 0.31750(13) 0.31986(19) -0.10776(15) 0.0486(7) Uani 1 1 d . . .
H4 H 0.3119 0.2886 -0.1509 0.058 Uiso 1 1 calc R . .
C5 C 0.31355(11) 0.40556(17) -0.11133(13) 0.0394(6) Uani 1 1 d . . .
H5 H 0.3049 0.4332 -0.1565 0.047 Uiso 1 1 calc R . .
C6 C 0.32243(11) 0.45094(15) -0.04820(13) 0.0318(5) Uani 1 1 d . . .
C7 C 0.30400(16) 0.5804(2) -0.11157(16) 0.0616(8) Uani 1 1 d . . .
H7A H 0.3040 0.6404 -0.1019 0.092 Uiso 1 1 calc R . .
H7B H 0.2624 0.5631 -0.1392 0.092 Uiso 1 1 calc R . .
H7C H 0.3342 0.5682 -0.1392 0.092 Uiso 1 1 calc R . .
C8 C 0.41669(10) 0.52346(14) 0.11215(12) 0.0281(5) Uani 1 1 d . . .
C9 C 0.42854(11) 0.59685(16) 0.15119(13) 0.0371(6) Uani 1 1 d . . .
H9 H 0.3973 0.6205 0.1706 0.044 Uiso 1 1 calc R . .
C10 C 0.48571(13) 0.63591(19) 0.16202(16) 0.0506(7) Uani 1 1 d . . .
H10 H 0.4930 0.6869 0.1880 0.061 Uiso 1 1 calc R . .
C11 C 0.53175(13) 0.6023(2) 0.13587(16) 0.0539(8) Uani 1 1 d . . .
H11 H 0.5709 0.6293 0.1440 0.065 Uiso 1 1 calc R . .
C12 C 0.52099(13) 0.5292(2) 0.09787(17) 0.0549(8) Uani 1 1 d . . .
H12 H 0.5530 0.5052 0.0801 0.066 Uiso 1 1 calc R . .
C13 C 0.46352(12) 0.49000(17) 0.08524(16) 0.0447(7) Uani 1 1 d . . .
H13 H 0.4562 0.4399 0.0580 0.054 Uiso 1 1 calc R . .
C14 C 0.35240(10) 0.39693(13) 0.17010(12) 0.0267(5) Uani 1 1 d . . .
C15 C 0.41013(12) 0.37241(19) 0.21162(16) 0.0505(7) Uani 1 1 d . . .
H15 H 0.4467 0.3970 0.2040 0.061 Uiso 1 1 calc R . .
C16 C 0.41508(13) 0.3121(2) 0.26441(17) 0.0601(9) Uani 1 1 d . . .
H16 H 0.4551 0.2952 0.2922 0.072 Uiso 1 1 calc R . .
C17 C 0.36290(13) 0.27683(16) 0.27694(14) 0.0422(6) Uani 1 1 d . . .
H17 H 0.3666 0.2357 0.3133 0.051 Uiso 1 1 calc R . .
C18 C 0.30528(12) 0.30125(15) 0.23666(14) 0.0394(6) Uani 1 1 d . . .
H18 H 0.2689 0.2770 0.2451 0.047 Uiso 1 1 calc R . .
C19 C 0.30009(11) 0.36094(15) 0.18393(13) 0.0350(6) Uani 1 1 d . . .
H19 H 0.2599 0.3777 0.1566 0.042 Uiso 1 1 calc R . .
C20 C 0.12897(10) 0.45982(13) 0.11356(13) 0.0284(5) Uani 1 1 d . . .
C21 C 0.15346(13) 0.46454(18) 0.18765(14) 0.0436(7) Uani 1 1 d . . .
H21 H 0.1832 0.5064 0.2075 0.052 Uiso 1 1 calc R . .
C22 C 0.13486(13) 0.4089(2) 0.23280(15) 0.0534(7) Uani 1 1 d . . .
H22 H 0.1518 0.4127 0.2834 0.064 Uiso 1 1 calc R . .
C23 C 0.09182(13) 0.34800(18) 0.20454(16) 0.0502(7) Uani 1 1 d . . .
H23 H 0.0796 0.3091 0.2355 0.060 Uiso 1 1 calc R . .
C24 C 0.06657(13) 0.34366(16) 0.13144(16) 0.0475(7) Uani 1 1 d . . .
H24 H 0.0363 0.3023 0.1120 0.057 Uiso 1 1 calc R . .
C25 C 0.08494(11) 0.39912(15) 0.08614(14) 0.0369(6) Uani 1 1 d . . .
H25 H 0.0672 0.3956 0.0357 0.044 Uiso 1 1 calc R . .
C26 C 0.13095(10) 0.48938(14) -0.03344(13) 0.0303(5) Uani 1 1 d . . .
C27 C 0.16596(12) 0.42738(15) -0.05485(14) 0.0371(6) Uani 1 1 d . . .
H27 H 0.2037 0.4092 -0.0226 0.045 Uiso 1 1 calc R . .
C28 C 0.14659(13) 0.39179(17) -0.12245(15) 0.0466(7) Uani 1 1 d . . .
H28 H 0.1705 0.3486 -0.1359 0.056 Uiso 1 1 calc R . .
C29 C 0.09285(14) 0.41873(19) -0.17016(15) 0.0491(7) Uani 1 1 d . . .
H29 H 0.0798 0.3946 -0.2168 0.059 Uiso 1 1 calc R . .
C30 C 0.05789(13) 0.48078(19) -0.15026(14) 0.0479(7) Uani 1 1 d . . .
H30 H 0.0208 0.4996 -0.1833 0.058 Uiso 1 1 calc R . .
C31 C 0.07660(12) 0.51567(17) -0.08257(13) 0.0383(6) Uani 1 1 d . . .
H31 H 0.0521 0.5582 -0.0693 0.046 Uiso 1 1 calc R . .
C32 C 0.10782(10) 0.62339(14) 0.05294(12) 0.0298(5) Uani 1 1 d . . .
C33 C 0.05694(10) 0.62520(15) 0.08199(13) 0.0335(5) Uani 1 1 d . . .
H33 H 0.0481 0.5782 0.1077 0.040 Uiso 1 1 calc R . .
C34 C 0.01888(11) 0.69473(16) 0.07388(14) 0.0410(6) Uani 1 1 d . . .
H34 H -0.0160 0.6954 0.0937 0.049 Uiso 1 1 calc R . .
C35 C 0.03201(13) 0.76290(17) 0.03684(15) 0.0477(7) Uani 1 1 d . . .
H35 H 0.0057 0.8105 0.0309 0.057 Uiso 1 1 calc R . .
C36 C 0.08284(13) 0.76306(16) 0.00812(15) 0.0450(7) Uani 1 1 d . . .
H36 H 0.0919 0.8106 -0.0168 0.054 Uiso 1 1 calc R . .
C37 C 0.12038(11) 0.69302(15) 0.01611(14) 0.0372(6) Uani 1 1 d . . .
C38 C 0.17829(15) 0.74526(19) -0.06353(18) 0.0620(9) Uani 1 1 d . . .
H38A H 0.2159 0.7323 -0.0788 0.093 Uiso 1 1 calc R . .
H38B H 0.1821 0.8010 -0.0420 0.093 Uiso 1 1 calc R . .
H38C H 0.1420 0.7436 -0.1053 0.093 Uiso 1 1 calc R . .
Cl1 Cl 0.27972(3) 0.64511(4) 0.19547(4) 0.04631(18) Uani 1 1 d . . .
Cu1 Cu 0.259983(12) 0.552814(16) 0.106123(14) 0.02567(11) Uani 1 1 d . . .
O1 O 0.32065(9) 0.53610(11) -0.04516(9) 0.0414(4) Uani 1 1 d . . .
O2 O 0.17066(9) 0.68504(11) -0.01145(11) 0.0503(5) Uani 1 1 d . . .
P1 P 0.34084(3) 0.47418(3) 0.09862(3) 0.02378(14) Uani 1 1 d . . .
P2 P 0.15812(3) 0.53270(4) 0.05713(3) 0.02724(15) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 C6 118.4(2) . . ?
C2 C1 P1 123.42(19) . . ?
C6 C1 P1 118.06(17) . . ?
C1 C2 C3 120.9(3) . . ?
C1 C2 H2 119.6 . . ?
C3 C2 H2 119.6 . . ?
C4 C3 C2 119.7(3) . . ?
C4 C3 H3 120.1 . . ?
C2 C3 H3 120.1 . . ?
C3 C4 C5 121.1(2) . . ?
C3 C4 H4 119.4 . . ?
C5 C4 H4 119.4 . . ?
C4 C5 C6 119.2(2) . . ?
C4 C5 H5 120.4 . . ?
C6 C5 H5 120.4 . . ?
O1 C6 C5 124.3(2) . . ?
O1 C6 C1 115.0(2) . . ?
C5 C6 C1 120.7(2) . . ?
O1 C7 H7A 109.5 . . ?
O1 C7 H7B 109.5 . . ?
H7A C7 H7B 109.5 . . ?
O1 C7 H7C 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C13 C8 C9 118.5(2) . . ?
C13 C8 P1 122.52(19) . . ?
C9 C8 P1 119.01(17) . . ?
C10 C9 C8 120.3(2) . . ?
C10 C9 H9 119.9 . . ?
C8 C9 H9 119.9 . . ?
C11 C10 C9 120.9(3) . . ?
C11 C10 H10 119.5 . . ?
C9 C10 H10 119.5 . . ?
C10 C11 C12 119.5(2) . . ?
C10 C11 H11 120.3 . . ?
C12 C11 H11 120.3 . . ?
C11 C12 C13 120.4(3) . . ?
C11 C12 H12 119.8 . . ?
C13 C12 H12 119.8 . . ?
C8 C13 C12 120.5(3) . . ?
C8 C13 H13 119.8 . . ?
C12 C13 H13 119.8 . . ?
C15 C14 C19 118.1(2) . . ?
C15 C14 P1 123.91(18) . . ?
C19 C14 P1 117.99(17) . . ?
C14 C15 C16 120.4(2) . . ?
C14 C15 H15 119.8 . . ?
C16 C15 H15 119.8 . . ?
C17 C16 C15 120.6(3) . . ?
C17 C16 H16 119.7 . . ?
C15 C16 H16 119.7 . . ?
C18 C17 C16 119.6(2) . . ?
C18 C17 H17 120.2 . . ?
C16 C17 H17 120.2 . . ?
C17 C18 C19 120.1(2) . . ?
C17 C18 H18 120.0 . . ?
C19 C18 H18 120.0 . . ?
C18 C19 C14 121.2(2) . . ?
C18 C19 H19 119.4 . . ?
C14 C19 H19 119.4 . . ?
C25 C20 C21 118.6(2) . . ?
C25 C20 P2 123.35(19) . . ?
C21 C20 P2 118.07(18) . . ?
C22 C21 C20 120.6(2) . . ?
C22 C21 H21 119.7 . . ?
C20 C21 H21 119.7 . . ?
C23 C22 C21 120.1(3) . . ?
C23 C22 H22 119.9 . . ?
C21 C22 H22 119.9 . . ?
C24 C23 C22 119.8(3) . . ?
C24 C23 H23 120.1 . . ?
C22 C23 H23 120.1 . . ?
C23 C24 C25 120.3(3) . . ?
C23 C24 H24 119.8 . . ?
C25 C24 H24 119.8 . . ?
C20 C25 C24 120.6(2) . . ?
C20 C25 H25 119.7 . . ?
C24 C25 H25 119.7 . . ?
C27 C26 C31 118.0(2) . . ?
C27 C26 P2 118.94(19) . . ?
C31 C26 P2 123.02(18) . . ?
C28 C27 C26 120.9(2) . . ?
C28 C27 H27 119.6 . . ?
C26 C27 H27 119.6 . . ?
C29 C28 C27 120.1(3) . . ?
C29 C28 H28 119.9 . . ?
C27 C28 H28 119.9 . . ?
C28 C29 C30 119.9(3) . . ?
C28 C29 H29 120.1 . . ?
C30 C29 H29 120.1 . . ?
C29 C30 C31 120.2(3) . . ?
C29 C30 H30 119.9 . . ?
C31 C30 H30 119.9 . . ?
C30 C31 C26 120.9(2) . . ?
C30 C31 H31 119.6 . . ?
C26 C31 H31 119.6 . . ?
C33 C32 C37 118.9(2) . . ?
C33 C32 P2 123.68(19) . . ?
C37 C32 P2 117.42(18) . . ?
C32 C33 C34 120.7(2) . . ?
C32 C33 H33 119.6 . . ?
C34 C33 H33 119.6 . . ?
C35 C34 C33 119.5(2) . . ?
C35 C34 H34 120.3 . . ?
C33 C34 H34 120.3 . . ?
C34 C35 C36 121.0(2) . . ?
C34 C35 H35 119.5 . . ?
C36 C35 H35 119.5 . . ?
C35 C36 C37 119.1(3) . . ?
C35 C36 H36 120.4 . . ?
C37 C36 H36 120.4 . . ?
O2 C37 C36 124.4(2) . . ?
O2 C37 C32 114.7(2) . . ?
C36 C37 C32 120.9(2) . . ?
O2 C38 H38A 109.5 . . ?
O2 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
O2 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
Cl1 Cu1 P1 115.26(3) . . ?
Cl1 Cu1 P2 113.26(3) . . ?
P1 Cu1 P2 129.46(2) . . ?
C6 O1 C7 117.6(2) . . ?
C37 O2 C38 117.9(2) . . ?
C8 P1 C1 103.19(10) . . ?
C8 P1 C14 104.21(10) . . ?
C1 P1 C14 102.82(10) . . ?
C8 P1 Cu1 118.57(8) . . ?
C1 P1 Cu1 119.06(7) . . ?
C14 P1 Cu1 107.03(7) . . ?
C32 P2 C26 102.43(11) . . ?
C32 P2 C20 103.15(10) . . ?
C26 P2 C20 104.10(10) . . ?
C32 P2 Cu1 116.45(8) . . ?
C26 P2 Cu1 120.17(7) . . ?
C20 P2 Cu1 108.65(8) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.383(3) . ?
C1 C6 1.402(3) . ?
C1 P1 1.822(2) . ?
C2 C3 1.386(4) . ?
C2 H2 0.9500 . ?
C3 C4 1.369(4) . ?
C3 H3 0.9500 . ?
C4 C5 1.378(4) . ?
C4 H4 0.9500 . ?
C5 C6 1.386(3) . ?
C5 H5 0.9500 . ?
C6 O1 1.368(3) . ?
C7 O1 1.424(3) . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7C 0.9800 . ?
C8 C13 1.387(3) . ?
C8 C9 1.384(3) . ?
C8 P1 1.820(2) . ?
C9 C10 1.384(3) . ?
C9 H9 0.9500 . ?
C10 C11 1.365(4) . ?
C10 H10 0.9500 . ?
C11 C12 1.369(4) . ?
C11 H11 0.9500 . ?
C12 C13 1.388(4) . ?
C12 H12 0.9500 . ?
C13 H13 0.9500 . ?
C14 C15 1.381(3) . ?
C14 C19 1.386(3) . ?
C14 P1 1.819(2) . ?
C15 C16 1.386(4) . ?
C15 H15 0.9500 . ?
C16 C17 1.369(4) . ?
C16 H16 0.9500 . ?
C17 C18 1.370(4) . ?
C17 H17 0.9500 . ?
C18 C19 1.378(3) . ?
C18 H18 0.9500 . ?
C19 H19 0.9500 . ?
C20 C25 1.384(3) . ?
C20 C21 1.389(3) . ?
C20 P2 1.826(2) . ?
C21 C22 1.383(4) . ?
C21 H21 0.9500 . ?
C22 C23 1.376(4) . ?
C22 H22 0.9500 . ?
C23 C24 1.373(4) . ?
C23 H23 0.9500 . ?
C24 C25 1.380(3) . ?
C24 H24 0.9500 . ?
C25 H25 0.9500 . ?
C26 C27 1.390(3) . ?
C26 C31 1.392(3) . ?
C26 P2 1.826(2) . ?
C27 C28 1.382(4) . ?
C27 H27 0.9500 . ?
C28 C29 1.373(4) . ?
C28 H28 0.9500 . ?
C29 C30 1.378(4) . ?
C29 H29 0.9500 . ?
C30 C31 1.378(4) . ?
C30 H30 0.9500 . ?
C31 H31 0.9500 . ?
C32 C33 1.388(3) . ?
C32 C37 1.390(3) . ?
C32 P2 1.824(2) . ?
C33 C34 1.384(3) . ?
C33 H33 0.9500 . ?
C34 C35 1.378(4) . ?
C34 H34 0.9500 . ?
C35 C36 1.383(4) . ?
C35 H35 0.9500 . ?
C36 C37 1.384(3) . ?
C36 H36 0.9500 . ?
C37 O2 1.364(3) . ?
C38 O2 1.434(3) . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
Cl1 Cu1 2.2240(7) . ?
Cu1 P1 2.2326(6) . ?
Cu1 P2 2.2387(6) . ?
