#------------------------------------------------------------------------------
#$Date: 2016-03-23 15:49:35 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179349 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/46/4324614.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4324614
loop_
_publ_author_name
'Jessica M. Morrison'
'Laura J. Moore-Shay'
'Peter C. Burns'
_publ_section_title
;
 U(VI) Uranyl Cation-Cation Interactions in Framework Germanates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2272
_journal_page_last               2277
_journal_paper_doi               10.1021/ic1019444
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         'K+, (UO2)2+, (UO6)6-, (GeO4)4-, (OH)-'
_chemical_formula_sum            'Ge2 H K O38 U11'
_chemical_formula_weight         3410.61
_chemical_name_systematic        'Potassium uranyl germanmate hydroxide'
_space_group_IT_number           163
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-P 3 2c'
_symmetry_space_group_name_H-M   'P -3 1 c'
_atom_sites_solution_hydrogens   notdet
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            2
_cell_length_a                   10.226(4)
_cell_length_b                   10.226(4)
_cell_length_c                   17.150(9)
_cell_measurement_reflns_used    3196
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.35
_cell_measurement_theta_min      2.37
_cell_volume                     1553.1(12)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'CrystalMaker v.8.2.3'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0781
_diffrn_reflns_av_sigmaI/netI    0.0327
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            17590
_diffrn_reflns_theta_full        27.69
_diffrn_reflns_theta_max         27.69
_diffrn_reflns_theta_min         2.30
_exptl_absorpt_coefficient_mu    59.282
_exptl_absorpt_correction_T_max  0.7174
_exptl_absorpt_correction_T_min  0.2308
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red-orange
_exptl_crystal_density_diffrn    7.293
_exptl_crystal_description       platy
_exptl_crystal_F_000             2798
_exptl_crystal_size_max          0.035
_exptl_crystal_size_mid          0.017
_exptl_crystal_size_min          0.006
_refine_diff_density_max         1.446
_refine_diff_density_min         -2.943
_refine_diff_density_rms         0.360
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.006
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     83
_refine_ls_number_reflns         1229
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.006
_refine_ls_R_factor_all          0.0307
_refine_ls_R_factor_gt           0.0232
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0312P)²+14.9626P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0561
_refine_ls_wR_factor_ref         0.0593
_reflns_number_gt                1077
_reflns_number_total             1229
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic1019444_si_002_3.cif
_cod_data_source_block           final_k
_cod_database_code               4324614
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-y, -x, -z+1/2'
'-x+y, y, -z+1/2'
'x, x-y, -z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'y, x, z-1/2'
'x-y, -y, z-1/2'
'-x, -x+y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U1 U 0.6667 0.3333 0.60095(3) 0.00530(13) Uani 1 3 d S
U2 U 0.01996(4) 0.35909(4) 0.55938(2) 0.00666(11) Uani 1 1 d .
U3 U 0.85801(3) 0.14199(3) 0.7500 0.00928(13) Uani 1 2 d S
Ge1 Ge 0.0000 0.0000 0.1017(4) 0.0225(11) Uani 0.759(14) 3 d SP
Ge2 Ge 0.0000 0.0000 0.1375(11) 0.0225(11) Uani 0.241(14) 3 d SP
K1 K 0.3333 0.6667 0.7500 0.0342(15) Uani 1 6 d S
O1 O 0.8461(7) 0.8257(7) 0.6287(4) 0.0110(13) Uani 1 1 d .
O2 O 0.1391(7) 0.4914(7) 0.6291(4) 0.0141(14) Uani 1 1 d .
O3 O 0.8156(7) 0.2879(7) 0.6564(4) 0.0134(13) Uani 1 1 d .
O4 O 0.5955(7) 0.1382(7) 0.5336(4) 0.0094(13) Uani 1 1 d .
O5 O 0.9032(7) 0.2247(7) 0.4846(4) 0.0127(14) Uani 1 1 d .
O6 O 0.0000 0.0000 0.0000 0.018(4) Uani 1 6 d S
O7 O 0.6945(7) -0.0186(8) 0.7170(5) 0.0177(15) Uani 1 1 d .
O8 O 0.0000 0.0000 0.7500 0.018(4) Uani 1 6 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O3 U1 O3 99.9(2) . 3_665
O3 U1 O3 99.9(2) . 2_655
O3 U1 O3 99.9(2) 3_665 2_655
O3 U1 O4 78.5(3) . 2_655
O3 U1 O4 171.0(2) 3_665 2_655
O3 U1 O4 89.1(3) 2_655 2_655
O3 U1 O4 171.0(3) . 3_665
O3 U1 O4 89.1(3) 3_665 3_665
O3 U1 O4 78.5(2) 2_655 3_665
O4 U1 O4 92.6(2) 2_655 3_665
O3 U1 O4 89.1(3) . .
O3 U1 O4 78.5(3) 3_665 .
O3 U1 O4 171.0(2) 2_655 .
O4 U1 O4 92.6(2) 2_655 .
O4 U1 O4 92.6(2) 3_665 .
O3 U1 U2 42.58(19) . 1_655
O3 U1 U2 136.34(19) 3_665 1_655
O3 U1 U2 107.06(19) 2_655 1_655
O4 U1 U2 38.81(16) 2_655 1_655
O4 U1 U2 129.17(17) 3_665 1_655
O4 U1 U2 79.44(16) . 1_655
O3 U1 U2 107.07(19) . 3
O3 U1 U2 42.59(19) 3_665 3
O3 U1 U2 136.34(19) 2_655 3
O4 U1 U2 129.17(17) 2_655 3
O4 U1 U2 79.45(16) 3_665 3
O4 U1 U2 38.81(16) . 3
U2 U1 U2 116.096(8) 1_655 3
O3 U1 U2 136.34(19) . 2_665
O3 U1 U2 107.06(18) 3_665 2_665
O3 U1 U2 42.59(18) 2_655 2_665
O4 U1 U2 79.45(16) 2_655 2_665
O4 U1 U2 38.81(16) 3_665 2_665
O4 U1 U2 129.17(17) . 2_665
U2 U1 U2 116.096(8) 1_655 2_665
U2 U1 U2 116.096(9) 3 2_665
O2 U2 O5 177.7(3) . 1_455
O2 U2 O1 95.2(3) . 3_565
O5 U2 O1 85.6(3) 1_455 3_565
O2 U2 O4 88.0(3) . 8_566
O5 U2 O4 90.4(3) 1_455 8_566
O1 U2 O4 154.3(2) 3_565 8_566
O2 U2 O4 99.2(3) . 2
O5 U2 O4 81.8(2) 1_455 2
O1 U2 O4 130.9(2) 3_565 2
O4 U2 O4 73.2(2) 8_566 2
O2 U2 O5 90.7(3) . 8_566
O5 U2 O5 87.3(3) 1_455 8_566
O1 U2 O5 77.8(2) 3_565 8_566
O4 U2 O5 76.7(2) 8_566 8_566
O4 U2 O5 147.9(2) 2 8_566
O2 U2 O3 85.8(3) . 1_455
O5 U2 O3 96.5(3) 1_455 1_455
O1 U2 O3 68.8(2) 3_565 1_455
O4 U2 O3 136.8(2) 8_566 1_455
O4 U2 O3 65.8(2) 2 1_455
O5 U2 O3 145.9(2) 8_566 1_455
O2 U2 U1 102.0(2) . 1_455
O5 U2 U1 80.0(2) 1_455 1_455
O1 U2 U1 96.81(16) 3_565 1_455
O4 U2 U1 107.44(15) 8_566 1_455
O4 U2 U1 34.26(15) 2 1_455
O5 U2 U1 166.66(15) 8_566 1_455
O3 U2 U1 33.77(14) 1_455 1_455
O2 U2 U2 94.5(2) . 7_566
O5 U2 U2 85.1(2) 1_455 7_566
O1 U2 U2 165.39(16) 3_565 7_566
O4 U2 U2 36.96(15) 8_566 7_566
O4 U2 U2 36.25(15) 2 7_566
O5 U2 U2 112.97(15) 8_566 7_566
O3 U2 U2 101.09(14) 1_455 7_566
U1 U2 U2 70.493(17) 1_455 7_566
O2 U2 U3 78.4(2) . 1_455
O5 U2 U3 103.5(2) 1_455 1_455
O1 U2 U3 35.81(16) 3_565 1_455
O4 U2 U3 164.97(15) 8_566 1_455
O4 U2 U3 102.64(15) 2 1_455
O5 U2 U3 109.27(15) 8_566 1_455
O3 U2 U3 36.91(14) 1_455 1_455
U1 U2 U3 69.985(12) 1_455 1_455
U2 U2 U3 137.225(18) 7_566 1_455
O2 U2 K1 5.3(2) . .
O5 U2 K1 174.36(19) 1_455 .
O1 U2 K1 90.15(17) 3_565 .
O4 U2 K1 91.89(16) 8_566 .
O4 U2 K1 103.78(15) 2 .
O5 U2 K1 88.15(16) 8_566 .
O3 U2 K1 85.39(16) 1_455 .
U1 U2 K1 104.169(19) 1_455 .
U2 U2 K1 99.79(3) 7_566 .
U3 U2 K1 74.87(4) 1_455 .
O7 U3 O7 178.3(5) 4_666 .
O7 U3 O3 89.0(3) 4_666 4_666
O7 U3 O3 89.8(3) . 4_666
O7 U3 O3 89.8(3) 4_666 .
O7 U3 O3 89.0(3) . .
O3 U3 O3 90.7(3) 4_666 .
O7 U3 O1 89.7(3) 4_666 6_556
O7 U3 O1 91.0(3) . 6_556
O3 U3 O1 68.6(2) 4_666 6_556
O3 U3 O1 159.3(2) . 6_556
O7 U3 O1 91.0(3) 4_666 3_665
O7 U3 O1 89.7(3) . 3_665
O3 U3 O1 159.3(2) 4_666 3_665
O3 U3 O1 68.6(2) . 3_665
O1 U3 O1 132.1(3) 6_556 3_665
O7 U3 O8 90.8(2) 4_666 1_655
O7 U3 O8 90.8(2) . 1_655
O3 U3 O8 134.63(16) 4_666 1_655
O3 U3 O8 134.63(16) . 1_655
O1 U3 O8 66.07(15) 6_556 1_655
O1 U3 O8 66.07(15) 3_665 1_655
O7 U3 Ge2 102.0(3) 4_666 10_656
O7 U3 Ge2 79.3(3) . 10_656
O3 U3 Ge2 165.6(2) 4_666 10_656
O3 U3 Ge2 98.4(3) . 10_656
O1 U3 Ge2 101.9(3) 6_556 10_656
O1 U3 Ge2 31.7(3) 3_665 10_656
O8 U3 Ge2 37.5(3) 1_655 10_656
O7 U3 Ge2 79.3(3) 4_666 7_656
O7 U3 Ge2 102.0(3) . 7_656
O3 U3 Ge2 98.4(3) 4_666 7_656
O3 U3 Ge2 165.6(2) . 7_656
O1 U3 Ge2 31.7(3) 6_556 7_656
O1 U3 Ge2 101.9(3) 3_665 7_656
O8 U3 Ge2 37.5(3) 1_655 7_656
Ge2 U3 Ge2 75.0(6) 10_656 7_656
O7 U3 U2 78.2(3) 4_666 1_655
O7 U3 U2 101.6(3) . 1_655
O3 U3 U2 126.85(16) 4_666 1_655
O3 U3 U2 38.84(16) . 1_655
O1 U3 U2 159.52(15) 6_556 1_655
O1 U3 U2 33.55(15) 3_665 1_655
O8 U3 U2 97.322(9) 1_655 1_655
Ge2 U3 U2 65.3(2) 10_656 1_655
Ge2 U3 U2 128.3(2) 7_656 1_655
O7 U3 U2 101.6(3) 4_666 4_656
O7 U3 U2 78.2(3) . 4_656
O3 U3 U2 38.84(16) 4_666 4_656
O3 U3 U2 126.85(16) . 4_656
O1 U3 U2 33.55(15) 6_556 4_656
O1 U3 U2 159.52(15) 3_665 4_656
O8 U3 U2 97.322(9) 1_655 4_656
Ge2 U3 U2 128.3(2) 10_656 4_656
Ge2 U3 U2 65.3(2) 7_656 4_656
U2 U3 U2 165.356(18) 1_655 4_656
Ge2 Ge1 O6 180.000(2) . .
Ge2 Ge1 O1 74.7(3) . 11_565
O6 Ge1 O1 105.3(3) . 11_565
Ge2 Ge1 O1 74.7(3) . 10_445
O6 Ge1 O1 105.3(3) . 10_445
O1 Ge1 O1 113.3(3) 11_565 10_445
Ge2 Ge1 O1 74.7(3) . 12_655
O6 Ge1 O1 105.3(3) . 12_655
O1 Ge1 O1 113.3(3) 11_565 12_655
O1 Ge1 O1 113.3(3) 10_445 12_655
Ge1 Ge2 O1 84.9(7) . 10_445
Ge1 Ge2 O1 84.9(7) . 11_565
O1 Ge2 O1 119.2(2) 10_445 11_565
Ge1 Ge2 O1 84.9(7) . 12_655
O1 Ge2 O1 119.2(2) 10_445 12_655
O1 Ge2 O1 119.2(2) 11_565 12_655
Ge1 Ge2 O8 180.0 . 7_556
O1 Ge2 O8 95.1(7) 10_445 7_556
O1 Ge2 O8 95.1(7) 11_565 7_556
O1 Ge2 O8 95.1(7) 12_655 7_556
O1 Ge2 O6 84.9(7) 10_445 .
O1 Ge2 O6 84.9(7) 11_565 .
O1 Ge2 O6 84.9(7) 12_655 .
O8 Ge2 O6 180.0 7_556 .
Ge1 Ge2 U3 127.5(3) . 7_656
O1 Ge2 U3 98.0(5) 10_445 7_656
O1 Ge2 U3 133.8(7) 11_565 7_656
O1 Ge2 U3 48.1(4) 12_655 7_656
O8 Ge2 U3 52.5(3) 7_556 7_656
O6 Ge2 U3 127.5(3) . 7_656
Ge1 Ge2 U3 127.5(3) . 8_566
O1 Ge2 U3 133.8(7) 10_445 8_566
O1 Ge2 U3 48.1(4) 11_565 8_566
O1 Ge2 U3 98.0(5) 12_655 8_566
O8 Ge2 U3 52.5(3) 7_556 8_566
O6 Ge2 U3 127.5(3) . 8_566
U3 Ge2 U3 86.8(4) 7_656 8_566
Ge1 Ge2 U3 127.5(3) . 9_446
O1 Ge2 U3 48.1(4) 10_445 9_446
O1 Ge2 U3 98.0(5) 11_565 9_446
O1 Ge2 U3 133.8(7) 12_655 9_446
O8 Ge2 U3 52.5(3) 7_556 9_446
O6 Ge2 U3 127.5(3) . 9_446
U3 Ge2 U3 86.8(4) 7_656 9_446
U3 Ge2 U3 86.8(4) 8_566 9_446
O2 K1 O2 71.5(2) 4_666 6_566
O2 K1 O2 104.5(3) 4_666 3_565
O2 K1 O2 112.9(3) 6_566 3_565
O2 K1 O2 71.5(2) 4_666 5_556
O2 K1 O2 71.5(2) 6_566 5_556
O2 K1 O2 173.1(3) 3_565 5_556
O2 K1 O2 112.9(3) 4_666 2_665
O2 K1 O2 173.1(3) 6_566 2_665
O2 K1 O2 71.5(2) 3_565 2_665
O2 K1 O2 104.5(3) 5_556 2_665
O2 K1 O2 173.1(3) 4_666 .
O2 K1 O2 104.5(3) 6_566 .
O2 K1 O2 71.5(2) 3_565 .
O2 K1 O2 112.9(3) 5_556 .
O2 K1 O2 71.5(2) 2_665 .
O2 K1 U2 175.53(13) 4_666 .
O2 K1 U2 104.64(14) 6_566 .
O2 K1 U2 74.63(14) 3_565 .
O2 K1 U2 109.76(14) 5_556 .
O2 K1 U2 71.08(14) 2_665 .
O2 K1 U2 3.33(13) . .
O2 K1 U2 3.33(13) 4_666 4_666
O2 K1 U2 74.63(14) 6_566 4_666
O2 K1 U2 104.64(14) 3_565 4_666
O2 K1 U2 71.08(14) 5_556 4_666
O2 K1 U2 109.76(14) 2_665 4_666
O2 K1 U2 175.53(13) . 4_666
U2 K1 U2 178.710(8) . 4_666
O2 K1 U2 71.08(14) 4_666 6_566
O2 K1 U2 3.33(13) 6_566 6_566
O2 K1 U2 109.76(14) 3_565 6_566
O2 K1 U2 74.63(14) 5_556 6_566
O2 K1 U2 175.53(13) 2_665 6_566
O2 K1 U2 104.64(14) . 6_566
U2 K1 U2 104.97(3) . 6_566
U2 K1 U2 74.23(3) 4_666 6_566
O2 K1 U2 104.64(14) 4_666 3_565
O2 K1 U2 109.76(14) 6_566 3_565
O2 K1 U2 3.33(13) 3_565 3_565
O2 K1 U2 175.53(14) 5_556 3_565
O2 K1 U2 74.63(14) 2_665 3_565
O2 K1 U2 71.08(14) . 3_565
U2 K1 U2 74.23(3) . 3_565
U2 K1 U2 104.97(3) 4_666 3_565
U2 K1 U2 106.59(3) 6_566 3_565
O2 K1 U2 74.63(14) 4_666 5_556
O2 K1 U2 71.08(14) 6_566 5_556
O2 K1 U2 175.53(13) 3_565 5_556
O2 K1 U2 3.33(14) 5_556 5_556
O2 K1 U2 104.64(14) 2_665 5_556
O2 K1 U2 109.76(14) . 5_556
U2 K1 U2 106.59(3) . 5_556
U2 K1 U2 74.23(3) 4_666 5_556
U2 K1 U2 74.23(3) 6_566 5_556
U2 K1 U2 178.710(8) 3_565 5_556
O2 K1 U2 109.76(14) 4_666 2_665
O2 K1 U2 175.53(13) 6_566 2_665
O2 K1 U2 71.08(14) 3_565 2_665
O2 K1 U2 104.64(14) 5_556 2_665
O2 K1 U2 3.33(13) 2_665 2_665
O2 K1 U2 74.63(14) . 2_665
U2 K1 U2 74.23(3) . 2_665
U2 K1 U2 106.59(3) 4_666 2_665
U2 K1 U2 178.710(8) 6_566 2_665
U2 K1 U2 74.23(3) 3_565 2_665
U2 K1 U2 104.97(3) 5_556 2_665
Ge2 O1 U2 149.1(7) 10_666 2_665
Ge1 O1 U2 130.3(4) 10_666 2_665
Ge2 O1 U3 100.2(6) 10_666 2_655
Ge1 O1 U3 118.4(4) 10_666 2_655
U2 O1 U3 110.6(3) 2_665 2_655
U2 O2 K1 171.4(3) . .
U1 O3 U3 148.4(3) . .
U1 O3 U2 103.6(3) . 1_655
U3 O3 U2 104.2(2) . 1_655
U1 O4 U2 146.2(3) . 9_656
U1 O4 U2 106.9(2) . 3
U2 O4 U2 106.8(2) 9_656 3
U2 O5 U2 150.4(4) 1_655 9_656
Ge1 O6 Ge1 180.0 7 .
Ge1 O6 Ge2 180.0 7 .
Ge1 O6 Ge2 180.0 . 7
Ge2 O6 Ge2 180.0 . 7
Ge2 O8 Ge2 180.000(4) 10_556 7_556
Ge2 O8 U3 90.0 10_556 1_455
Ge2 O8 U3 90.0 7_556 1_455
Ge2 O8 U3 90.000(3) 10_556 3_665
Ge2 O8 U3 90.000(3) 7_556 3_665
U3 O8 U3 120.0 1_455 3_665
Ge2 O8 U3 90.000(3) 10_556 2_545
Ge2 O8 U3 90.000(3) 7_556 2_545
U3 O8 U3 120.0 1_455 2_545
U3 O8 U3 120.0 3_665 2_545
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 O3 2.037(6) .
U1 O3 2.037(6) 3_665
U1 O3 2.037(6) 2_655
U1 O4 2.095(6) 2_655
U1 O4 2.095(6) 3_665
U1 O4 2.095(6) .
U2 O2 1.760(7) .
U2 O5 1.822(7) 1_455
U2 O1 2.263(6) 3_565
U2 O4 2.294(6) 8_566
U2 O4 2.333(6) 2
U2 O5 2.430(6) 8_566
U2 O3 2.479(7) 1_455
U3 O7 1.751(7) 4_666
U3 O7 1.751(7) .
U3 O3 2.374(6) 4_666
U3 O3 2.374(6) .
U3 O1 2.396(6) 6_556
U3 O1 2.396(6) 3_665
U3 O8 2.5150(11) 1_655
U3 Ge2 3.170(12) 10_656
U3 Ge2 3.170(12) 7_656
Ge1 Ge2 0.614(14) .
Ge1 O6 1.744(7) .
Ge1 O1 1.750(7) 11_565
Ge1 O1 1.750(7) 10_445
Ge1 O1 1.750(7) 12_655
Ge2 O1 1.694(6) 10_445
Ge2 O1 1.694(6) 11_565
Ge2 O1 1.694(6) 12_655
Ge2 O8 1.93(2) 7_556
Ge2 O6 2.36(2) .
Ge2 U3 3.170(12) 7_656
Ge2 U3 3.170(12) 8_566
Ge2 U3 3.170(12) 9_446
K1 O2 2.809(7) 4_666
K1 O2 2.809(7) 6_566
K1 O2 2.809(7) 3_565
K1 O2 2.809(7) 5_556
K1 O2 2.809(7) 2_665
K1 O2 2.809(7) .
O1 Ge2 1.694(7) 10_666
O1 Ge1 1.750(7) 10_666
O1 U2 2.263(6) 2_665
O1 U3 2.396(6) 2_655
O3 U2 2.479(7) 1_655
O4 U2 2.294(6) 9_656
O4 U2 2.333(6) 3
O5 U2 1.822(7) 1_655
O5 U2 2.430(6) 9_656
O6 Ge1 1.744(7) 7
O6 Ge2 2.36(2) 7
O8 Ge2 1.93(2) 10_556
O8 Ge2 1.93(2) 7_556
O8 U3 2.5149(11) 1_455
O8 U3 2.5150(11) 3_665
O8 U3 2.5150(11) 2_545
