#------------------------------------------------------------------------------
#$Date: 2016-03-23 16:20:08 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179372 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/69/4326901.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4326901
loop_
_publ_author_name
'Miriam M. Gillett-Kunnath'
'Joseph I. Paik'
'Sara M. Jensen'
'Jacob D. Taylor'
'Slavi C. Sevov'
_publ_contact_author_address
;
University of Notre Dame
Department of Chemistry and Biochemistry
251 Nieuwland Science Hall
Notre Dame, Indiana 46556
;
_publ_contact_author_email       ssevov@nd.edu
_publ_contact_author_name        'Sevov, S. C.'
_publ_section_title
;
 Metal-Centered Deltahedral Zintl Ions: Synthesis of [Ni@Sn9]4- by direct
 Extraction from Intermetallic Precursors and of the Vertex-Fused Dimer
 [{Ni@Sn8(μ-Ge)1/2}2]4-
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11695
_journal_page_last               11701
_journal_paper_doi               10.1021/ic2016963
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         '(Ni Sn9), 3(C18 H36 K N2 O6), K'
_chemical_formula_sum            'C54 H108 K4 N6 Ni O18 Sn9'
_chemical_formula_weight         2412.78
_chemical_name_systematic
; 
 (K-crypt)3(KSn9) 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.7140(10)
_cell_angle_beta                 104.4690(10)
_cell_angle_gamma                118.3890(10)
_cell_formula_units_Z            2
_cell_length_a                   15.8028(8)
_cell_length_b                   16.2350(9)
_cell_length_c                   20.1760(12)
_cell_measurement_reflns_used    15561
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      25.57
_cell_measurement_theta_min      2.18
_cell_volume                     4181.5(4)
_computing_cell_refinement       'Bruker SAINT v7.60A'
_computing_data_collection       'Bruker APEX-II v2008-6'
_computing_data_reduction        'Bruker SAINT v7.60A'
_computing_molecular_graphics    SHELXL-XP
_computing_publication_material  SHELXTL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 83.33
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Bruker APEX-II'
_diffrn_measurement_method       'combination of ω/2θ-scans and φ-scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0701
_diffrn_reflns_av_sigmaI/netI    0.0508
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            94056
_diffrn_reflns_theta_full        25.57
_diffrn_reflns_theta_max         25.57
_diffrn_reflns_theta_min         1.10
_exptl_absorpt_coefficient_mu    3.116
_exptl_absorpt_correction_T_max  0.4652
_exptl_absorpt_correction_T_min  0.4085
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'Sheldrick, 2008'
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.916
_exptl_crystal_description       block
_exptl_crystal_F_000             2344
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.29
_refine_diff_density_max         1.796
_refine_diff_density_min         -0.940
_refine_diff_density_rms         0.146
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.036
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     832
_refine_ls_number_reflns         15561
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.036
_refine_ls_R_factor_all          0.0585
_refine_ls_R_factor_gt           0.0372
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0209P)²+13.4671P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0701
_refine_ls_wR_factor_ref         0.0782
_reflns_number_gt                11800
_reflns_number_total             15561
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic2016963_si_001_3.cif
_cod_data_source_block           compd1b
_cod_database_code               4326901
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ni1 Ni -0.00759(5) 0.07855(5) 0.25642(4) 0.01791(16) Uani 1 1 d .
Sn1 Sn 0.08114(3) 0.15776(3) 0.39738(2) 0.03086(11) Uani 1 1 d .
Sn2 Sn -0.04265(3) 0.21465(3) 0.29792(2) 0.02875(11) Uani 1 1 d .
Sn3 Sn -0.13500(3) -0.02907(3) 0.31120(2) 0.02844(10) Uani 1 1 d .
Sn4 Sn 0.12068(3) 0.06727(3) 0.19863(2) 0.02091(9) Uani 1 1 d .
Sn5 Sn -0.02062(3) 0.14267(3) 0.14719(2) 0.02306(10) Uani 1 1 d .
Sn6 Sn -0.10470(3) -0.09032(3) 0.15714(2) 0.02780(10) Uani 1 1 d .
Sn7 Sn 0.05503(3) -0.02950(3) 0.30910(2) 0.02812(10) Uani 1 1 d .
Sn8 Sn 0.16057(3) 0.25427(3) 0.29220(2) 0.02082(9) Uani 1 1 d .
Sn9 Sn -0.20614(3) 0.02288(3) 0.18161(2) 0.02853(11) Uani 1 1 d .
K1 K 0.75908(9) 0.33216(8) 0.86710(6) 0.0192(3) Uani 1 1 d .
N1 N 0.7843(3) 0.5089(3) 0.8340(2) 0.0210(11) Uani 1 1 d .
N2 N 0.7357(3) 0.1560(3) 0.9026(2) 0.0221(11) Uani 1 1 d .
O1 O 0.5797(3) 0.3247(3) 0.78236(19) 0.0203(8) Uani 1 1 d .
O2 O 0.5568(3) 0.1773(3) 0.84617(19) 0.0215(9) Uani 1 1 d .
O3 O 0.8412(3) 0.5077(3) 0.98196(19) 0.0233(9) Uani 1 1 d .
O4 O 0.8617(3) 0.3530(3) 1.0134(2) 0.0241(9) Uani 1 1 d .
O5 O 0.8836(3) 0.4088(3) 0.78465(19) 0.0246(9) Uani 1 1 d .
O6 O 0.8171(3) 0.2189(3) 0.7906(2) 0.0290(10) Uani 1 1 d .
C1 C 0.6919(4) 0.4807(4) 0.7720(3) 0.0223(13) Uani 1 1 d .
H1A H 0.6930 0.4457 0.7279 0.027 Uiso 1 1 calc R
H1B H 0.6959 0.5415 0.7654 0.027 Uiso 1 1 calc R
C2 C 0.5908(4) 0.4161(4) 0.7797(3) 0.0219(13) Uani 1 1 d .
H2A H 0.5893 0.4491 0.8245 0.026 Uiso 1 1 calc R
H2B H 0.5328 0.4044 0.7382 0.026 Uiso 1 1 calc R
C3 C 0.4846(4) 0.2601(4) 0.7889(3) 0.0245(13) Uani 1 1 d .
H3A H 0.4262 0.2498 0.7485 0.029 Uiso 1 1 calc R
H3B H 0.4827 0.2901 0.8347 0.029 Uiso 1 1 calc R
C4 C 0.4733(4) 0.1633(4) 0.7880(3) 0.0236(13) Uani 1 1 d .
H4A H 0.4068 0.1186 0.7923 0.028 Uiso 1 1 calc R
H4B H 0.4728 0.1323 0.7416 0.028 Uiso 1 1 calc R
C5 C 0.5451(5) 0.0844(4) 0.8455(3) 0.0301(15) Uani 1 1 d .
H5A H 0.5442 0.0528 0.7991 0.036 Uiso 1 1 calc R
H5B H 0.4786 0.0403 0.8501 0.036 Uiso 1 1 calc R
C6 C 0.6330(4) 0.0989(4) 0.9069(3) 0.0282(14) Uani 1 1 d .
H6A H 0.6344 0.1328 0.9526 0.034 Uiso 1 1 calc R
H6B H 0.6193 0.0332 0.9086 0.034 Uiso 1 1 calc R
C7 C 0.7984(4) 0.5817(4) 0.8957(3) 0.0241(13) Uani 1 1 d .
H7A H 0.7306 0.5592 0.9005 0.029 Uiso 1 1 calc R
H7B H 0.8222 0.6454 0.8858 0.029 Uiso 1 1 calc R
C8 C 0.8751(5) 0.5985(4) 0.9666(3) 0.0301(15) Uani 1 1 d .
H8A H 0.9443 0.6244 0.9636 0.036 Uiso 1 1 calc R
H8B H 0.8807 0.6478 1.0058 0.036 Uiso 1 1 calc R
C9 C 0.9094(4) 0.5215(4) 1.0492(3) 0.0265(14) Uani 1 1 d .
H9A H 0.9171 0.5733 1.0875 0.032 Uiso 1 1 calc R
H9B H 0.9785 0.5430 1.0471 0.032 Uiso 1 1 calc R
C10 C 0.8664(4) 0.4259(4) 1.0658(3) 0.0234(13) Uani 1 1 d .
H10A H 0.9109 0.4359 1.1144 0.028 Uiso 1 1 calc R
H10B H 0.7961 0.4032 1.0658 0.028 Uiso 1 1 calc R
C11 C 0.8286(5) 0.2634(4) 1.0318(3) 0.0291(14) Uani 1 1 d .
H11A H 0.7617 0.2405 1.0381 0.035 Uiso 1 1 calc R
H11B H 0.8802 0.2758 1.0779 0.035 Uiso 1 1 calc R
C12 C 0.8167(4) 0.1852(4) 0.9728(3) 0.0271(14) Uani 1 1 d .
H12A H 0.8838 0.2098 0.9664 0.033 Uiso 1 1 calc R
H12B H 0.8001 0.1259 0.9882 0.033 Uiso 1 1 calc R
C13 C 0.8773(4) 0.5539(4) 0.8161(3) 0.0249(13) Uani 1 1 d .
H13A H 0.9387 0.5813 0.8606 0.030 Uiso 1 1 calc R
H13B H 0.8825 0.6098 0.7993 0.030 Uiso 1 1 calc R
C14 C 0.8808(5) 0.4851(5) 0.7593(3) 0.0315(15) Uani 1 1 d .
H14A H 0.8189 0.4556 0.7147 0.038 Uiso 1 1 calc R
H14B H 0.9430 0.5224 0.7477 0.038 Uiso 1 1 calc R
C15 C 0.8764(5) 0.3369(4) 0.7302(3) 0.0320(15) Uani 1 1 d .
H15A H 0.9287 0.3697 0.7089 0.038 Uiso 1 1 calc R
H15B H 0.8070 0.3008 0.6913 0.038 Uiso 1 1 calc R
C16 C 0.8936(5) 0.2664(4) 0.7610(3) 0.0301(15) Uani 1 1 d .
H16A H 0.8890 0.2166 0.7228 0.036 Uiso 1 1 calc R
H16B H 0.9635 0.3020 0.7992 0.036 Uiso 1 1 calc R
C17 C 0.8335(5) 0.1531(5) 0.8224(4) 0.0362(16) Uani 1 1 d .
H17A H 0.8994 0.1907 0.8647 0.043 Uiso 1 1 calc R
H17B H 0.8380 0.1073 0.7871 0.043 Uiso 1 1 calc R
C18 C 0.7453(5) 0.0957(4) 0.8456(3) 0.0336(15) Uani 1 1 d .
H18A H 0.6800 0.0602 0.8028 0.040 Uiso 1 1 calc R
H18B H 0.7539 0.0455 0.8633 0.040 Uiso 1 1 calc R
K2 K 0.61028(9) 0.39292(9) 0.17620(6) 0.0223(3) Uani 1 1 d .
N3 N 0.7658(4) 0.5535(4) 0.3204(3) 0.0310(12) Uani 1 1 d .
N4 N 0.4566(3) 0.2304(3) 0.0335(2) 0.0208(10) Uani 1 1 d .
O7 O 0.6462(3) 0.2452(3) 0.1172(2) 0.0234(9) Uani 1 1 d .
O8 O 0.7677(3) 0.3768(3) 0.2634(2) 0.0277(9) Uani 1 1 d .
O9 O 0.4016(3) 0.2737(3) 0.1569(2) 0.0257(9) Uani 1 1 d .
O10 O 0.5405(3) 0.4474(3) 0.2816(2) 0.0270(9) Uani 1 1 d .
O11 O 0.5729(3) 0.4432(3) 0.0506(2) 0.0250(9) Uani 1 1 d .
O12 O 0.7422(3) 0.5877(3) 0.1799(2) 0.0350(11) Uani 1 1 d .
C19 C 0.4981(5) 0.1721(4) 0.0089(3) 0.0283(14) Uani 1 1 d .
H19A H 0.5453 0.2078 -0.0150 0.034 Uiso 1 1 calc R
H19B H 0.4402 0.1080 -0.0270 0.034 Uiso 1 1 calc R
C20 C 0.5557(5) 0.1539(4) 0.0705(3) 0.0290(14) Uani 1 1 d .
H20A H 0.5109 0.1233 0.0973 0.035 Uiso 1 1 calc R
H20B H 0.5751 0.1081 0.0516 0.035 Uiso 1 1 calc R
C21 C 0.7098(5) 0.2295(5) 0.1715(3) 0.0314(15) Uani 1 1 d .
H21A H 0.7342 0.1912 0.1485 0.038 Uiso 1 1 calc R
H21B H 0.6691 0.1914 0.1981 0.038 Uiso 1 1 calc R
C22 C 0.7999(5) 0.3264(5) 0.2222(3) 0.0312(15) Uani 1 1 d .
H22A H 0.8495 0.3161 0.2551 0.037 Uiso 1 1 calc R
H22B H 0.8357 0.3672 0.1947 0.037 Uiso 1 1 calc R
C23 C 0.8546(5) 0.4611(5) 0.3186(3) 0.0360(16) Uani 1 1 d .
H23A H 0.9000 0.5057 0.2972 0.043 Uiso 1 1 calc R
H23B H 0.8948 0.4412 0.3507 0.043 Uiso 1 1 calc R
C24 C 0.8196(5) 0.5141(5) 0.3616(3) 0.0321(15) Uani 1 1 d .
H24A H 0.7728 0.4679 0.3814 0.039 Uiso 1 1 calc R
H24B H 0.8808 0.5693 0.4029 0.039 Uiso 1 1 calc R
C25 C 0.3592(4) 0.1644(4) 0.0429(3) 0.0270(14) Uani 1 1 d .
H25A H 0.3686 0.1193 0.0675 0.032 Uiso 1 1 calc R
H25B H 0.3036 0.1235 -0.0052 0.032 Uiso 1 1 calc R
C26 C 0.3261(4) 0.2186(5) 0.0855(3) 0.0301(15) Uani 1 1 d .
H26A H 0.3165 0.2640 0.0614 0.036 Uiso 1 1 calc R
H26B H 0.2589 0.1710 0.0878 0.036 Uiso 1 1 calc R
C27 C 0.3700(4) 0.3259(4) 0.1968(3) 0.0243(13) Uani 1 1 d .
H27A H 0.2982 0.2803 0.1930 0.029 Uiso 1 1 calc R
H27B H 0.3714 0.3785 0.1769 0.029 Uiso 1 1 calc R
C28 C 0.4413(4) 0.3706(4) 0.2742(3) 0.0273(14) Uani 1 1 d .
H28A H 0.4128 0.3972 0.3036 0.033 Uiso 1 1 calc R
H28B H 0.4470 0.3192 0.2920 0.033 Uiso 1 1 calc R
C29 C 0.6121(5) 0.4892(5) 0.3544(3) 0.0345(16) Uani 1 1 d .
H29A H 0.6258 0.4398 0.3689 0.041 Uiso 1 1 calc R
H29B H 0.5822 0.5083 0.3869 0.041 Uiso 1 1 calc R
C30 C 0.7107(5) 0.5778(4) 0.3610(3) 0.0390(17) Uani 1 1 d .
H30A H 0.6954 0.6246 0.3432 0.047 Uiso 1 1 calc R
H30B H 0.7565 0.6111 0.4126 0.047 Uiso 1 1 calc R
C31 C 0.4361(4) 0.2773(4) -0.0208(3) 0.0273(14) Uani 1 1 d .
H31A H 0.3865 0.2952 -0.0140 0.033 Uiso 1 1 calc R
H31B H 0.4038 0.2291 -0.0697 0.033 Uiso 1 1 calc R
C32 C 0.5330(4) 0.3683(4) -0.0159(3) 0.0279(14) Uani 1 1 d .
H32A H 0.5854 0.3524 -0.0188 0.033 Uiso 1 1 calc R
H32B H 0.5171 0.3923 -0.0568 0.033 Uiso 1 1 calc R
C33 C 0.6560(5) 0.5337(4) 0.0527(3) 0.0332(15) Uani 1 1 d .
H33A H 0.6322 0.5543 0.0118 0.040 Uiso 1 1 calc R
H33B H 0.7124 0.5253 0.0479 0.040 Uiso 1 1 calc R
C34 C 0.6952(5) 0.6111(4) 0.1221(3) 0.0371(16) Uani 1 1 d .
H34A H 0.7465 0.6762 0.1208 0.045 Uiso 1 1 calc R
H34B H 0.6372 0.6146 0.1295 0.045 Uiso 1 1 calc R
C35 C 0.7866(6) 0.6655(4) 0.2465(4) 0.051(2) Uani 1 1 d .
H35A H 0.7318 0.6723 0.2568 0.061 Uiso 1 1 calc R
H35B H 0.8378 0.7289 0.2429 0.061 Uiso 1 1 calc R
C36 C 0.8385(5) 0.6407(5) 0.3060(4) 0.047(2) Uani 1 1 d .
H36A H 0.8892 0.6290 0.2931 0.057 Uiso 1 1 calc R
H36B H 0.8772 0.6980 0.3507 0.057 Uiso 1 1 calc R
K3 K 0.62971(9) 0.24044(9) 0.49154(6) 0.0207(3) Uani 1 1 d .
N5 N 0.4708(3) 0.2769(3) 0.5162(2) 0.0226(11) Uani 1 1 d .
N6 N 0.7896(3) 0.2030(3) 0.4700(2) 0.0211(10) Uani 1 1 d .
O13 O 0.4701(3) 0.2096(3) 0.37183(19) 0.0231(9) Uani 1 1 d .
O14 O 0.5943(3) 0.1355(3) 0.3489(2) 0.0244(9) Uani 1 1 d .
O15 O 0.5114(3) 0.1368(3) 0.57256(19) 0.0245(9) Uani 1 1 d .
O16 O 0.6902(3) 0.1362(3) 0.5732(2) 0.0233(9) Uani 1 1 d .
O17 O 0.6892(3) 0.4348(3) 0.5619(2) 0.0273(9) Uani 1 1 d .
O18 O 0.8284(3) 0.4042(3) 0.51182(19) 0.0242(9) Uani 1 1 d .
C37 C 0.4085(5) 0.2756(4) 0.4480(3) 0.0273(14) Uani 1 1 d .
H37A H 0.4481 0.3395 0.4399 0.033 Uiso 1 1 calc R
H37B H 0.3446 0.2690 0.4522 0.033 Uiso 1 1 calc R
C38 C 0.3787(4) 0.1936(4) 0.3834(3) 0.0239(13) Uani 1 1 d .
H38A H 0.3429 0.1293 0.3919 0.029 Uiso 1 1 calc R
H38B H 0.3309 0.1923 0.3403 0.029 Uiso 1 1 calc R
C39 C 0.4441(4) 0.1418(4) 0.3054(3) 0.0229(13) Uani 1 1 d .
H39A H 0.4018 0.1504 0.2650 0.027 Uiso 1 1 calc R
H39B H 0.4029 0.0733 0.3059 0.027 Uiso 1 1 calc R
C40 C 0.5421(4) 0.1607(4) 0.2954(3) 0.0234(13) Uani 1 1 d .
H40A H 0.5256 0.1202 0.2466 0.028 Uiso 1 1 calc R
H40B H 0.5869 0.2311 0.3002 0.028 Uiso 1 1 calc R
C41 C 0.6840(4) 0.1432(4) 0.3385(3) 0.0264(14) Uani 1 1 d .
H41A H 0.7291 0.2098 0.3360 0.032 Uiso 1 1 calc R
H41B H 0.6625 0.0940 0.2924 0.032 Uiso 1 1 calc R
C42 C 0.7428(4) 0.1257(4) 0.3999(3) 0.0258(14) Uani 1 1 d .
H42A H 0.6952 0.0613 0.4042 0.031 Uiso 1 1 calc R
H42B H 0.7983 0.1217 0.3884 0.031 Uiso 1 1 calc R
C43 C 0.4021(4) 0.1995(4) 0.5411(3) 0.0263(14) Uani 1 1 d .
H43A H 0.3530 0.1388 0.4992 0.032 Uiso 1 1 calc R
H43B H 0.3612 0.2212 0.5595 0.032 Uiso 1 1 calc R
C44 C 0.4575(5) 0.1750(4) 0.5988(3) 0.0275(14) Uani 1 1 d .
H44A H 0.5072 0.2351 0.6411 0.033 Uiso 1 1 calc R
H44B H 0.4069 0.1255 0.6146 0.033 Uiso 1 1 calc R
C45 C 0.5674(5) 0.1160(4) 0.6285(3) 0.0271(14) Uani 1 1 d .
H45A H 0.5194 0.0711 0.6482 0.032 Uiso 1 1 calc R
H45B H 0.6211 0.1781 0.6682 0.032 Uiso 1 1 calc R
C46 C 0.6171(4) 0.0690(4) 0.5982(3) 0.0271(14) Uani 1 1 d .
H46A H 0.6527 0.0515 0.6360 0.032 Uiso 1 1 calc R
H46B H 0.5636 0.0077 0.5578 0.032 Uiso 1 1 calc R
C47 C 0.7415(4) 0.0939(4) 0.5470(3) 0.0243(13) Uani 1 1 d .
H47A H 0.6910 0.0354 0.5038 0.029 Uiso 1 1 calc R
H47B H 0.7715 0.0722 0.5844 0.029 Uiso 1 1 calc R
C48 C 0.8253(4) 0.1683(4) 0.5282(3) 0.0258(14) Uani 1 1 d .
H48A H 0.8749 0.2261 0.5720 0.031 Uiso 1 1 calc R
H48B H 0.8631 0.1392 0.5135 0.031 Uiso 1 1 calc R
C49 C 0.5241(5) 0.3737(4) 0.5714(3) 0.0308(15) Uani 1 1 d .
H49A H 0.5514 0.3678 0.6191 0.037 Uiso 1 1 calc R
H49B H 0.4727 0.3917 0.5730 0.037 Uiso 1 1 calc R
C50 C 0.6116(5) 0.4559(4) 0.5597(4) 0.0349(16) Uani 1 1 d .
H50A H 0.5857 0.4631 0.5123 0.042 Uiso 1 1 calc R
H50B H 0.6410 0.5188 0.5977 0.042 Uiso 1 1 calc R
C51 C 0.7715(5) 0.5099(4) 0.5485(3) 0.0286(14) Uani 1 1 d .
H51A H 0.7950 0.5753 0.5804 0.034 Uiso 1 1 calc R
H51B H 0.7467 0.5082 0.4978 0.034 Uiso 1 1 calc R
C52 C 0.8602(4) 0.4950(4) 0.5618(3) 0.0260(14) Uani 1 1 d .
H52A H 0.9192 0.5504 0.5561 0.031 Uiso 1 1 calc R
H52B H 0.8831 0.4936 0.6118 0.031 Uiso 1 1 calc R
C53 C 0.9086(4) 0.3842(4) 0.5278(3) 0.0245(13) Uani 1 1 d .
H53A H 0.9205 0.3734 0.5754 0.029 Uiso 1 1 calc R
H53B H 0.9737 0.4415 0.5300 0.029 Uiso 1 1 calc R
C54 C 0.8781(4) 0.2937(4) 0.4702(3) 0.0226(13) Uani 1 1 d .
H54A H 0.8605 0.3030 0.4225 0.027 Uiso 1 1 calc R
H54B H 0.9381 0.2861 0.4779 0.027 Uiso 1 1 calc R
K4 K 0.0000 0.0000 0.0000 0.0399(5) Uani 1 2 d S
K5 K 0.0000 0.0000 0.5000 0.0565(7) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Sn5 Ni1 Sn3 136.34(3) . .
Sn5 Ni1 Sn6 82.94(2) . .
Sn3 Ni1 Sn6 80.43(2) . .
Sn5 Ni1 Sn2 77.89(2) . .
Sn3 Ni1 Sn2 87.76(3) . .
Sn6 Ni1 Sn2 137.37(3) . .
Sn5 Ni1 Sn7 140.07(3) . .
Sn3 Ni1 Sn7 70.82(2) . .
Sn6 Ni1 Sn7 72.99(2) . .
Sn2 Ni1 Sn7 140.26(3) . .
Sn5 Ni1 Sn1 136.18(3) . .
Sn3 Ni1 Sn1 72.41(2) . .
Sn6 Ni1 Sn1 140.60(3) . .
Sn2 Ni1 Sn1 70.28(2) . .
Sn7 Ni1 Sn1 71.43(2) . .
Sn5 Ni1 Sn8 71.68(2) . .
Sn3 Ni1 Sn8 140.57(3) . .
Sn6 Ni1 Sn8 137.63(3) . .
Sn2 Ni1 Sn8 69.99(2) . .
Sn7 Ni1 Sn8 105.85(3) . .
Sn1 Ni1 Sn8 69.59(2) . .
Sn5 Ni1 Sn4 71.87(2) . .
Sn3 Ni1 Sn4 136.70(3) . .
Sn6 Ni1 Sn4 70.64(2) . .
Sn2 Ni1 Sn4 135.14(3) . .
Sn7 Ni1 Sn4 70.30(2) . .
Sn1 Ni1 Sn4 111.60(3) . .
Sn8 Ni1 Sn4 69.47(2) . .
Sn5 Ni1 Sn9 68.12(2) . .
Sn3 Ni1 Sn9 68.26(2) . .
Sn6 Ni1 Sn9 69.12(2) . .
Sn2 Ni1 Sn9 68.44(2) . .
Sn7 Ni1 Sn9 127.54(3) . .
Sn1 Ni1 Sn9 122.86(3) . .
Sn8 Ni1 Sn9 126.61(3) . .
Sn4 Ni1 Sn9 125.50(3) . .
Ni1 Sn1 Sn8 55.316(18) . .
Ni1 Sn1 Sn2 54.360(19) . .
Sn8 Sn1 Sn2 59.894(14) . .
Ni1 Sn1 Sn7 54.236(19) . .
Sn8 Sn1 Sn7 87.471(16) . .
Sn2 Sn1 Sn7 107.881(17) . .
Ni1 Sn1 Sn3 53.180(18) . .
Sn8 Sn1 Sn3 107.803(16) . .
Sn2 Sn1 Sn3 72.324(15) . .
Sn7 Sn1 Sn3 58.854(14) . .
Ni1 Sn1 K5 116.95(2) . .
Sn8 Sn1 K5 165.249(18) . .
Sn2 Sn1 K5 128.299(17) . .
Sn7 Sn1 K5 78.307(13) . .
Sn3 Sn1 K5 68.099(12) . .
Ni1 Sn2 Sn9 57.966(19) . .
Ni1 Sn2 Sn8 55.615(18) . .
Sn9 Sn2 Sn8 106.170(16) . .
Ni1 Sn2 Sn1 55.358(19) . .
Sn9 Sn2 Sn1 103.264(17) . .
Sn8 Sn2 Sn1 59.991(14) . .
Ni1 Sn2 Sn5 50.865(18) . .
Sn9 Sn2 Sn5 56.730(13) . .
Sn8 Sn2 Sn5 58.302(13) . .
Sn1 Sn2 Sn5 100.981(16) . .
Ni1 Sn2 Sn3 46.018(18) . .
Sn9 Sn2 Sn3 52.980(13) . .
Sn8 Sn2 Sn3 96.015(15) . .
Sn1 Sn2 Sn3 54.788(13) . .
Sn5 Sn2 Sn3 88.836(14) . .
Ni1 Sn3 Sn9 58.212(19) . .
Ni1 Sn3 Sn7 55.171(19) . .
Sn9 Sn3 Sn7 106.288(17) . .
Ni1 Sn3 Sn1 54.406(19) . .
Sn9 Sn3 Sn1 101.790(16) . .
Sn7 Sn3 Sn1 60.337(15) . .
Ni1 Sn3 Sn6 49.793(18) . .
Sn9 Sn3 Sn6 56.705(14) . .
Sn7 Sn3 Sn6 58.070(13) . .
Sn1 Sn3 Sn6 99.671(16) . .
Ni1 Sn3 Sn2 46.221(18) . .
Sn9 Sn3 Sn2 53.284(12) . .
Sn7 Sn3 Sn2 95.495(15) . .
Sn1 Sn3 Sn2 52.888(12) . .
Sn6 Sn3 Sn2 88.210(14) . .
Ni1 Sn3 K5 111.90(2) . .
Sn9 Sn3 K5 160.122(16) . .
Sn7 Sn3 K5 75.772(12) . .
Sn1 Sn3 K5 61.464(11) . .
Sn6 Sn3 K5 132.730(15) . .
Sn2 Sn3 K5 107.018(13) . .
Ni1 Sn4 Sn8 55.143(18) . .
Ni1 Sn4 Sn6 53.828(18) . .
Sn8 Sn4 Sn6 107.680(16) . .
Ni1 Sn4 Sn7 54.575(18) . .
Sn8 Sn4 Sn7 88.020(16) . .
Sn6 Sn4 Sn7 61.573(14) . .
Ni1 Sn4 Sn5 53.147(18) . .
Sn8 Sn4 Sn5 60.383(13) . .
Sn6 Sn4 Sn5 68.393(14) . .
Sn7 Sn4 Sn5 106.718(16) . .
Ni1 Sn4 K4 108.225(19) . .
Sn8 Sn4 K4 118.491(14) . .
Sn6 Sn4 K4 73.865(11) . .
Sn7 Sn4 K4 133.681(15) . .
Sn5 Sn4 K4 64.620(10) . .
Ni1 Sn5 Sn9 58.368(19) . .
Ni1 Sn5 Sn8 54.964(18) . .
Sn9 Sn5 Sn8 105.285(16) . .
Ni1 Sn5 Sn4 54.979(19) . .
Sn9 Sn5 Sn4 104.467(16) . .
Sn8 Sn5 Sn4 58.843(13) . .
Ni1 Sn5 Sn2 51.242(19) . .
Sn9 Sn5 Sn2 57.318(13) . .
Sn8 Sn5 Sn2 56.674(13) . .
Sn4 Sn5 Sn2 99.946(15) . .
Ni1 Sn5 Sn6 48.598(17) . .
Sn9 Sn5 Sn6 55.793(13) . .
Sn8 Sn5 Sn6 97.303(14) . .
Sn4 Sn5 Sn6 55.212(12) . .
Sn2 Sn5 Sn6 92.581(15) . .
Ni1 Sn5 K4 111.09(2) . .
Sn9 Sn5 K4 113.250(14) . .
Sn8 Sn5 K4 118.607(14) . .
Sn4 Sn5 K4 66.267(11) . .
Sn2 Sn5 K4 162.073(15) . .
Sn6 Sn5 K4 70.300(11) . .
Ni1 Sn6 Sn9 57.732(19) . .
Ni1 Sn6 Sn4 55.534(19) . .
Sn9 Sn6 Sn4 104.507(16) . .
Ni1 Sn6 Sn7 54.061(19) . .
Sn9 Sn6 Sn7 103.497(17) . .
Sn4 Sn6 Sn7 59.348(13) . .
Ni1 Sn6 Sn3 49.782(19) . .
Sn9 Sn6 Sn3 55.749(13) . .
Sn4 Sn6 Sn3 99.461(15) . .
Sn7 Sn6 Sn3 55.776(13) . .
Ni1 Sn6 Sn5 48.463(18) . .
Sn9 Sn6 Sn5 54.652(13) . .
Sn4 Sn6 Sn5 56.396(12) . .
Sn7 Sn6 Sn5 97.096(14) . .
Sn3 Sn6 Sn5 90.363(14) . .
Ni1 Sn6 K4 99.59(2) . .
Sn9 Sn6 K4 101.952(14) . .
Sn4 Sn6 K4 60.820(11) . .
Sn7 Sn6 K4 118.889(15) . .
Sn3 Sn6 K4 147.688(14) . .
Sn5 Sn6 K4 57.622(9) . .
Ni1 Sn7 Sn3 54.004(19) . .
Ni1 Sn7 Sn4 55.128(19) . .
Sn3 Sn7 Sn4 106.850(16) . .
Ni1 Sn7 Sn1 54.331(19) . .
Sn3 Sn7 Sn1 60.809(14) . .
Sn4 Sn7 Sn1 91.247(16) . .
Ni1 Sn7 Sn6 52.953(18) . .
Sn3 Sn7 Sn6 66.153(15) . .
Sn4 Sn7 Sn6 59.079(14) . .
Sn1 Sn7 Sn6 105.551(16) . .
Ni1 Sn7 K5 98.785(19) . .
Sn3 Sn7 K5 59.596(11) . .
Sn4 Sn7 K5 146.836(15) . .
Sn1 Sn7 K5 55.588(11) . .
Sn6 Sn7 K5 124.799(15) . .
Ni1 Sn8 Sn2 54.392(19) . .
Ni1 Sn8 Sn1 55.095(18) . .
Sn2 Sn8 Sn1 60.115(14) . .
Ni1 Sn8 Sn4 55.384(19) . .
Sn2 Sn8 Sn4 107.423(15) . .
Sn1 Sn8 Sn4 92.987(16) . .
Ni1 Sn8 Sn5 53.357(18) . .
Sn2 Sn8 Sn5 65.024(14) . .
Sn1 Sn8 Sn5 105.852(16) . .
Sn4 Sn8 Sn5 60.774(13) . .
Ni1 Sn9 Sn5 53.516(18) . .
Ni1 Sn9 Sn3 53.533(18) . .
Sn5 Sn9 Sn3 107.034(16) . .
Ni1 Sn9 Sn2 53.590(18) . .
Sn5 Sn9 Sn2 65.952(14) . .
Sn3 Sn9 Sn2 73.736(16) . .
Ni1 Sn9 Sn6 53.143(18) . .
Sn5 Sn9 Sn6 69.555(15) . .
Sn3 Sn9 Sn6 67.545(15) . .
Sn2 Sn9 Sn6 106.631(16) . .
O6 K1 O2 98.53(11) . .
O6 K1 O5 58.50(11) . .
O2 K1 O5 139.38(11) . .
O6 K1 O3 142.78(12) . .
O2 K1 O3 114.41(11) . .
O5 K1 O3 100.68(11) . .
O6 K1 O1 114.57(12) . .
O2 K1 O1 58.91(10) . .
O5 K1 O1 98.06(11) . .
O3 K1 O1 97.70(11) . .
O6 K1 O4 101.11(12) . .
O2 K1 O4 98.13(11) . .
O5 K1 O4 117.85(12) . .
O3 K1 O4 59.05(10) . .
O1 K1 O4 139.20(11) . .
O6 K1 N1 118.92(13) . .
O2 K1 N1 118.38(12) . .
O5 K1 N1 62.03(12) . .
O3 K1 N1 60.41(12) . .
O1 K1 N1 61.37(11) . .
O4 K1 N1 117.85(12) . .
O6 K1 N2 61.50(12) . .
O2 K1 N2 62.03(12) . .
O5 K1 N2 118.20(12) . .
O3 K1 N2 118.80(12) . .
O1 K1 N2 119.21(12) . .
O4 K1 N2 61.33(12) . .
N1 K1 N2 179.18(14) . .
C13 N1 C7 108.2(4) . .
C13 N1 C1 110.6(4) . .
C7 N1 C1 109.4(4) . .
C13 N1 K1 107.6(3) . .
C7 N1 K1 112.1(3) . .
C1 N1 K1 108.9(3) . .
C6 N2 C12 109.4(4) . .
C6 N2 C18 110.0(4) . .
C12 N2 C18 109.5(5) . .
C6 N2 K1 108.7(3) . .
C12 N2 K1 110.0(3) . .
C18 N2 K1 109.3(3) . .
C2 O1 C3 111.6(4) . .
C2 O1 K1 117.0(3) . .
C3 O1 K1 117.0(3) . .
C4 O2 C5 109.9(4) . .
C4 O2 K1 116.7(3) . .
C5 O2 K1 115.4(3) . .
C9 O3 C8 110.8(4) . .
C9 O3 K1 117.3(3) . .
C8 O3 K1 118.6(3) . .
C10 O4 C11 110.8(4) . .
C10 O4 K1 113.9(3) . .
C11 O4 K1 116.3(3) . .
C15 O5 C14 111.7(4) . .
C15 O5 K1 115.1(3) . .
C14 O5 K1 116.5(3) . .
C17 O6 C16 110.4(4) . .
C17 O6 K1 116.4(3) . .
C16 O6 K1 118.8(3) . .
N1 C1 C2 114.2(5) . .
N1 C1 H1A 108.7 . .
C2 C1 H1A 108.7 . .
N1 C1 H1B 108.7 . .
C2 C1 H1B 108.7 . .
H1A C1 H1B 107.6 . .
O1 C2 C1 109.3(4) . .
O1 C2 H2A 109.8 . .
C1 C2 H2A 109.8 . .
O1 C2 H2B 109.8 . .
C1 C2 H2B 109.8 . .
H2A C2 H2B 108.3 . .
O1 C3 C4 110.1(5) . .
O1 C3 H3A 109.6 . .
C4 C3 H3A 109.6 . .
O1 C3 H3B 109.6 . .
C4 C3 H3B 109.6 . .
H3A C3 H3B 108.2 . .
O2 C4 C3 110.1(4) . .
O2 C4 H4A 109.6 . .
C3 C4 H4A 109.6 . .
O2 C4 H4B 109.6 . .
C3 C4 H4B 109.6 . .
H4A C4 H4B 108.2 . .
O2 C5 C6 110.1(4) . .
O2 C5 H5A 109.6 . .
C6 C5 H5A 109.6 . .
O2 C5 H5B 109.6 . .
C6 C5 H5B 109.6 . .
H5A C5 H5B 108.2 . .
N2 C6 C5 114.8(5) . .
N2 C6 H6A 108.6 . .
C5 C6 H6A 108.6 . .
N2 C6 H6B 108.6 . .
C5 C6 H6B 108.6 . .
H6A C6 H6B 107.5 . .
N1 C7 C8 113.8(5) . .
N1 C7 H7A 108.8 . .
C8 C7 H7A 108.8 . .
N1 C7 H7B 108.8 . .
C8 C7 H7B 108.8 . .
H7A C7 H7B 107.7 . .
O3 C8 C7 109.4(5) . .
O3 C8 H8A 109.8 . .
C7 C8 H8A 109.8 . .
O3 C8 H8B 109.8 . .
C7 C8 H8B 109.8 . .
H8A C8 H8B 108.2 . .
O3 C9 C10 108.9(4) . .
O3 C9 H9A 109.9 . .
C10 C9 H9A 109.9 . .
O3 C9 H9B 109.9 . .
C10 C9 H9B 109.9 . .
H9A C9 H9B 108.3 . .
O4 C10 C9 110.1(4) . .
O4 C10 H10A 109.6 . .
C9 C10 H10A 109.6 . .
O4 C10 H10B 109.6 . .
C9 C10 H10B 109.6 . .
H10A C10 H10B 108.2 . .
O4 C11 C12 109.7(5) . .
O4 C11 H11A 109.7 . .
C12 C11 H11A 109.7 . .
O4 C11 H11B 109.7 . .
C12 C11 H11B 109.7 . .
H11A C11 H11B 108.2 . .
N2 C12 C11 114.0(5) . .
N2 C12 H12A 108.8 . .
C11 C12 H12A 108.8 . .
N2 C12 H12B 108.8 . .
C11 C12 H12B 108.8 . .
H12A C12 H12B 107.6 . .
N1 C13 C14 115.0(5) . .
N1 C13 H13A 108.5 . .
C14 C13 H13A 108.5 . .
N1 C13 H13B 108.5 . .
C14 C13 H13B 108.5 . .
H13A C13 H13B 107.5 . .
O5 C14 C13 110.0(5) . .
O5 C14 H14A 109.7 . .
C13 C14 H14A 109.7 . .
O5 C14 H14B 109.7 . .
C13 C14 H14B 109.7 . .
H14A C14 H14B 108.2 . .
O5 C15 C16 110.1(5) . .
O5 C15 H15A 109.6 . .
C16 C15 H15A 109.6 . .
O5 C15 H15B 109.6 . .
C16 C15 H15B 109.6 . .
H15A C15 H15B 108.1 . .
O6 C16 C15 109.1(5) . .
O6 C16 H16A 109.9 . .
C15 C16 H16A 109.9 . .
O6 C16 H16B 109.9 . .
C15 C16 H16B 109.9 . .
H16A C16 H16B 108.3 . .
O6 C17 C18 109.2(5) . .
O6 C17 H17A 109.8 . .
C18 C17 H17A 109.8 . .
O6 C17 H17B 109.8 . .
C18 C17 H17B 109.8 . .
H17A C17 H17B 108.3 . .
N2 C18 C17 114.7(5) . .
N2 C18 H18A 108.6 . .
C17 C18 H18A 108.6 . .
N2 C18 H18B 108.6 . .
C17 C18 H18B 108.6 . .
H18A C18 H18B 107.6 . .
O11 K2 O9 95.49(12) . .
O11 K2 O8 136.19(12) . .
O9 K2 O8 123.19(12) . .
O11 K2 O12 61.27(11) . .
O9 K2 O12 136.07(13) . .
O8 K2 O12 95.73(12) . .
O11 K2 O10 117.44(12) . .
O9 K2 O10 61.52(11) . .
O8 K2 O10 100.14(12) . .
O12 K2 O10 94.88(13) . .
O11 K2 O7 95.47(11) . .
O9 K2 O7 100.15(11) . .
O8 K2 O7 60.87(11) . .
O12 K2 O7 117.67(13) . .
O10 K2 O7 142.52(12) . .
O11 K2 N4 60.67(11) . .
O9 K2 N4 59.98(12) . .
O8 K2 N4 118.98(12) . .
O12 K2 N4 120.91(13) . .
O10 K2 N4 120.68(12) . .
O7 K2 N4 59.17(11) . .
O11 K2 N3 120.24(13) . .
O9 K2 N3 120.13(13) . .
O8 K2 N3 59.98(12) . .
O12 K2 N3 59.87(13) . .
O10 K2 N3 59.63(13) . .
O7 K2 N3 119.89(13) . .
N4 K2 N3 178.92(14) . .
C24 N3 C36 111.2(5) . .
C24 N3 C30 108.9(5) . .
C36 N3 C30 110.8(5) . .
C24 N3 K2 107.7(3) . .
C36 N3 K2 108.5(4) . .
C30 N3 K2 109.8(3) . .
C19 N4 C25 109.3(4) . .
C19 N4 C31 109.5(4) . .
C25 N4 C31 109.8(4) . .
C19 N4 K2 111.1(3) . .
C25 N4 K2 109.0(3) . .
C31 N4 K2 108.1(3) . .
C20 O7 C21 110.8(4) . .
C20 O7 K2 115.1(3) . .
C21 O7 K2 112.7(3) . .
C23 O8 C22 110.1(4) . .
C23 O8 K2 119.5(3) . .
C22 O8 K2 112.5(3) . .
C27 O9 C26 110.1(4) . .
C27 O9 K2 111.6(3) . .
C26 O9 K2 119.3(3) . .
C28 O10 C29 111.9(4) . .
C28 O10 K2 112.4(3) . .
C29 O10 K2 115.6(3) . .
C33 O11 C32 110.8(4) . .
C33 O11 K2 114.2(3) . .
C32 O11 K2 116.7(3) . .
C34 O12 C35 109.7(5) . .
C34 O12 K2 111.7(3) . .
C35 O12 K2 117.7(4) . .
N4 C19 C20 111.9(5) . .
N4 C19 H19A 109.2 . .
C20 C19 H19A 109.2 . .
N4 C19 H19B 109.2 . .
C20 C19 H19B 109.2 . .
H19A C19 H19B 107.9 . .
O7 C20 C19 109.1(5) . .
O7 C20 H20A 109.9 . .
C19 C20 H20A 109.9 . .
O7 C20 H20B 109.9 . .
C19 C20 H20B 109.9 . .
H20A C20 H20B 108.3 . .
O7 C21 C22 109.4(5) . .
O7 C21 H21A 109.8 . .
C22 C21 H21A 109.8 . .
O7 C21 H21B 109.8 . .
C22 C21 H21B 109.8 . .
H21A C21 H21B 108.2 . .
O8 C22 C21 110.8(5) . .
O8 C22 H22A 109.5 . .
C21 C22 H22A 109.5 . .
O8 C22 H22B 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 108.1 . .
O8 C23 C24 109.7(5) . .
O8 C23 H23A 109.7 . .
C24 C23 H23A 109.7 . .
O8 C23 H23B 109.7 . .
C24 C23 H23B 109.7 . .
H23A C23 H23B 108.2 . .
N3 C24 C23 114.4(5) . .
N3 C24 H24A 108.7 . .
C23 C24 H24A 108.7 . .
N3 C24 H24B 108.7 . .
C23 C24 H24B 108.7 . .
H24A C24 H24B 107.6 . .
N4 C25 C26 113.3(5) . .
N4 C25 H25A 108.9 . .
C26 C25 H25A 108.9 . .
N4 C25 H25B 108.9 . .
C26 C25 H25B 108.9 . .
H25A C25 H25B 107.7 . .
O9 C26 C25 110.5(5) . .
O9 C26 H26A 109.5 . .
C25 C26 H26A 109.5 . .
O9 C26 H26B 109.5 . .
C25 C26 H26B 109.5 . .
H26A C26 H26B 108.1 . .
O9 C27 C28 109.4(4) . .
O9 C27 H27A 109.8 . .
C28 C27 H27A 109.8 . .
O9 C27 H27B 109.8 . .
C28 C27 H27B 109.8 . .
H27A C27 H27B 108.2 . .
O10 C28 C27 110.2(5) . .
O10 C28 H28A 109.6 . .
C27 C28 H28A 109.6 . .
O10 C28 H28B 109.6 . .
C27 C28 H28B 109.6 . .
H28A C28 H28B 108.1 . .
O10 C29 C30 109.6(5) . .
O10 C29 H29A 109.7 . .
C30 C29 H29A 109.7 . .
O10 C29 H29B 109.7 . .
C30 C29 H29B 109.7 . .
H29A C29 H29B 108.2 . .
N3 C30 C29 112.9(5) . .
N3 C30 H30A 109.0 . .
C29 C30 H30A 109.0 . .
N3 C30 H30B 109.0 . .
C29 C30 H30B 109.0 . .
H30A C30 H30B 107.8 . .
N4 C31 C32 112.6(4) . .
N4 C31 H31A 109.1 . .
C32 C31 H31A 109.1 . .
N4 C31 H31B 109.1 . .
C32 C31 H31B 109.1 . .
H31A C31 H31B 107.8 . .
O11 C32 C31 109.6(5) . .
O11 C32 H32A 109.8 . .
C31 C32 H32A 109.8 . .
O11 C32 H32B 109.8 . .
C31 C32 H32B 109.8 . .
H32A C32 H32B 108.2 . .
O11 C33 C34 109.8(5) . .
O11 C33 H33A 109.7 . .
C34 C33 H33A 109.7 . .
O11 C33 H33B 109.7 . .
C34 C33 H33B 109.7 . .
H33A C33 H33B 108.2 . .
O12 C34 C33 109.4(5) . .
O12 C34 H34A 109.8 . .
C33 C34 H34A 109.8 . .
O12 C34 H34B 109.8 . .
C33 C34 H34B 109.8 . .
H34A C34 H34B 108.2 . .
O12 C35 C36 108.7(5) . .
O12 C35 H35A 110.0 . .
C36 C35 H35A 110.0 . .
O12 C35 H35B 110.0 . .
C36 C35 H35B 110.0 . .
H35A C35 H35B 108.3 . .
N3 C36 C35 113.3(5) . .
N3 C36 H36A 108.9 . .
C35 C36 H36A 108.9 . .
N3 C36 H36B 108.9 . .
C35 C36 H36B 108.9 . .
H36A C36 H36B 107.7 . .
O13 K3 O17 94.71(11) . .
O13 K3 O16 141.42(12) . .
O17 K3 O16 119.23(12) . .
O13 K3 O18 113.15(12) . .
O17 K3 O18 60.04(11) . .
O16 K3 O18 100.28(11) . .
O13 K3 O14 59.86(11) . .
O17 K3 O14 135.03(12) . .
O16 K3 O14 100.29(11) . .
O18 K3 O14 94.40(11) . .
O13 K3 O15 100.28(11) . .
O17 K3 O15 99.36(11) . .
O16 K3 O15 59.04(11) . .
O18 K3 O15 141.15(11) . .
O14 K3 O15 120.11(11) . .
O13 K3 N5 61.33(12) . .
O17 K3 N5 60.67(12) . .
O16 K3 N5 118.03(13) . .
O18 K3 N5 119.48(12) . .
O14 K3 N5 119.83(12) . .
O15 K3 N5 60.28(12) . .
O13 K3 N6 119.83(12) . .
O17 K3 N6 119.37(12) . .
O16 K3 N6 60.74(12) . .
O18 K3 N6 60.85(12) . .
O14 K3 N6 61.17(11) . .
O15 K3 N6 118.61(12) . .
N5 K3 N6 178.71(13) . .
C37 N5 C49 110.5(4) . .
C37 N5 C43 108.9(4) . .
C49 N5 C43 109.6(4) . .
C37 N5 K3 108.8(3) . .
C49 N5 K3 108.5(3) . .
C43 N5 K3 110.5(3) . .
C54 N6 C42 109.5(4) . .
C54 N6 C48 109.5(4) . .
C42 N6 C48 109.1(4) . .
C54 N6 K3 110.3(3) . .
C42 N6 K3 108.6(3) . .
C48 N6 K3 109.7(3) . .
C39 O13 C38 110.5(4) . .
C39 O13 K3 117.1(3) . .
C38 O13 K3 116.0(3) . .
C40 O14 C41 111.4(4) . .
C40 O14 K3 111.0(3) . .
C41 O14 K3 115.3(3) . .
C44 O15 C45 110.5(4) . .
C44 O15 K3 116.9(3) . .
C45 O15 K3 114.2(3) . .
C46 O16 C47 110.0(4) . .
C46 O16 K3 117.9(3) . .
C47 O16 K3 117.3(3) . .
C50 O17 C51 110.8(4) . .
C50 O17 K3 119.1(3) . .
C51 O17 K3 114.3(3) . .
C53 O18 C52 110.4(4) . .
C53 O18 K3 113.7(3) . .
C52 O18 K3 115.1(3) . .
N5 C37 C38 113.8(5) . .
N5 C37 H37A 108.8 . .
C38 C37 H37A 108.8 . .
N5 C37 H37B 108.8 . .
C38 C37 H37B 108.8 . .
H37A C37 H37B 107.7 . .
O13 C38 C37 109.0(4) . .
O13 C38 H38A 109.9 . .
C37 C38 H38A 109.9 . .
O13 C38 H38B 109.9 . .
C37 C38 H38B 109.9 . .
H38A C38 H38B 108.3 . .
O13 C39 C40 108.9(4) . .
O13 C39 H39A 109.9 . .
C40 C39 H39A 109.9 . .
O13 C39 H39B 109.9 . .
C40 C39 H39B 109.9 . .
H39A C39 H39B 108.3 . .
O14 C40 C39 108.4(4) . .
O14 C40 H40A 110.0 . .
C39 C40 H40A 110.0 . .
O14 C40 H40B 110.0 . .
C39 C40 H40B 110.0 . .
H40A C40 H40B 108.4 . .
O14 C41 C42 110.0(5) . .
O14 C41 H41A 109.7 . .
C42 C41 H41A 109.7 . .
O14 C41 H41B 109.7 . .
C42 C41 H41B 109.7 . .
H41A C41 H41B 108.2 . .
N6 C42 C41 113.8(5) . .
N6 C42 H42A 108.8 . .
C41 C42 H42A 108.8 . .
N6 C42 H42B 108.8 . .
C41 C42 H42B 108.8 . .
H42A C42 H42B 107.7 . .
N5 C43 C44 114.3(5) . .
N5 C43 H43A 108.7 . .
C44 C43 H43A 108.7 . .
N5 C43 H43B 108.7 . .
C44 C43 H43B 108.7 . .
H43A C43 H43B 107.6 . .
O15 C44 C43 110.3(5) . .
O15 C44 H44A 109.6 . .
C43 C44 H44A 109.6 . .
O15 C44 H44B 109.6 . .
C43 C44 H44B 109.6 . .
H44A C44 H44B 108.1 . .
O15 C45 C46 109.6(4) . .
O15 C45 H45A 109.7 . .
C46 C45 H45A 109.7 . .
O15 C45 H45B 109.7 . .
C46 C45 H45B 109.7 . .
H45A C45 H45B 108.2 . .
O16 C46 C45 109.5(5) . .
O16 C46 H46A 109.8 . .
C45 C46 H46A 109.8 . .
O16 C46 H46B 109.8 . .
C45 C46 H46B 109.8 . .
H46A C46 H46B 108.2 . .
O16 C47 C48 109.7(4) . .
O16 C47 H47A 109.7 . .
C48 C47 H47A 109.7 . .
O16 C47 H47B 109.7 . .
C48 C47 H47B 109.7 . .
H47A C47 H47B 108.2 . .
N6 C48 C47 115.0(5) . .
N6 C48 H48A 108.5 . .
C47 C48 H48A 108.5 . .
N6 C48 H48B 108.5 . .
C47 C48 H48B 108.5 . .
H48A C48 H48B 107.5 . .
N5 C49 C50 114.8(5) . .
N5 C49 H49A 108.6 . .
C50 C49 H49A 108.6 . .
N5 C49 H49B 108.6 . .
C50 C49 H49B 108.6 . .
H49A C49 H49B 107.5 . .
O17 C50 C49 109.6(5) . .
O17 C50 H50A 109.8 . .
C49 C50 H50A 109.8 . .
O17 C50 H50B 109.8 . .
C49 C50 H50B 109.8 . .
H50A C50 H50B 108.2 . .
O17 C51 C52 110.3(5) . .
O17 C51 H51A 109.6 . .
C52 C51 H51A 109.6 . .
O17 C51 H51B 109.6 . .
C52 C51 H51B 109.6 . .
H51A C51 H51B 108.1 . .
O18 C52 C51 109.6(4) . .
O18 C52 H52A 109.8 . .
C51 C52 H52A 109.8 . .
O18 C52 H52B 109.8 . .
C51 C52 H52B 109.8 . .
H52A C52 H52B 108.2 . .
O18 C53 C54 109.7(4) . .
O18 C53 H53A 109.7 . .
C54 C53 H53A 109.7 . .
O18 C53 H53B 109.7 . .
C54 C53 H53B 109.7 . .
H53A C53 H53B 108.2 . .
N6 C54 C53 112.9(4) . .
N6 C54 H54A 109.0 . .
C53 C54 H54A 109.0 . .
N6 C54 H54B 109.0 . .
C53 C54 H54B 109.0 . .
H54A C54 H54B 107.8 . .
Sn5 K4 Sn5 180.0 2 .
Sn5 K4 Sn4 49.112(9) 2 2
Sn5 K4 Sn4 130.887(9) . 2
Sn5 K4 Sn4 130.888(9) 2 .
Sn5 K4 Sn4 49.113(9) . .
Sn4 K4 Sn4 180.0 2 .
Sn5 K4 Sn6 52.077(9) 2 2
Sn5 K4 Sn6 127.923(9) . 2
Sn4 K4 Sn6 45.316(9) 2 2
Sn4 K4 Sn6 134.685(9) . 2
Sn5 K4 Sn6 127.923(9) 2 .
Sn5 K4 Sn6 52.078(9) . .
Sn4 K4 Sn6 134.684(9) 2 .
Sn4 K4 Sn6 45.315(9) . .
Sn6 K4 Sn6 180.0 2 .
Sn1 K5 Sn1 180.0 2_556 .
Sn1 K5 Sn3 50.437(9) 2_556 2_556
Sn1 K5 Sn3 129.563(10) . 2_556
Sn1 K5 Sn3 129.563(10) 2_556 .
Sn1 K5 Sn3 50.437(9) . .
Sn3 K5 Sn3 180.0 2_556 .
Sn1 K5 Sn7 133.895(10) 2_556 .
Sn1 K5 Sn7 46.105(10) . .
Sn3 K5 Sn7 135.368(9) 2_556 .
Sn3 K5 Sn7 44.632(9) . .
Sn1 K5 Sn7 46.104(10) 2_556 2_556
Sn1 K5 Sn7 133.896(10) . 2_556
Sn3 K5 Sn7 44.631(9) 2_556 2_556
Sn3 K5 Sn7 135.369(9) . 2_556
Sn7 K5 Sn7 180.0 . 2_556
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ni1 Sn5 2.5797(8) .
Ni1 Sn3 2.5846(8) .
Ni1 Sn6 2.5851(8) .
Ni1 Sn2 2.5935(8) .
Ni1 Sn7 2.6223(8) .
Ni1 Sn1 2.6255(8) .
Ni1 Sn8 2.6325(8) .
Ni1 Sn4 2.6402(8) .
Ni1 Sn9 2.7318(8) .
Sn1 Sn8 3.0004(6) .
Sn1 Sn2 3.0041(6) .
Sn1 Sn7 3.0635(6) .
Sn1 Sn3 3.0778(6) .
Sn1 K5 3.5073(4) .
Sn2 Sn9 2.9971(6) .
Sn2 Sn8 2.9974(6) .
Sn2 Sn5 3.2518(6) .
Sn2 Sn3 3.5892(6) .
Sn3 Sn9 2.9852(6) .
Sn3 Sn7 3.0174(6) .
Sn3 Sn6 3.3377(6) .
Sn3 K5 3.7042(5) .
Sn4 Sn8 3.0044(5) .
Sn4 Sn6 3.0212(6) .
Sn4 Sn7 3.0297(6) .
Sn4 Sn5 3.0639(6) .
Sn4 K4 3.7101(4) .
Sn5 Sn9 2.9773(6) .
Sn5 Sn8 3.0522(5) .
Sn5 Sn6 3.4202(6) .
Sn5 K4 3.6617(4) .
Sn6 Sn9 3.0187(6) .
Sn6 Sn7 3.0971(6) .
Sn6 K4 4.0820(5) .
Sn7 K5 4.1631(5) .
K1 O6 2.838(4) .
K1 O2 2.843(4) .
K1 O5 2.850(4) .
K1 O3 2.856(4) .
K1 O1 2.857(4) .
K1 O4 2.871(4) .
K1 N1 2.910(5) .
K1 N2 2.928(5) .
N1 C13 1.466(7) .
N1 C7 1.471(7) .
N1 C1 1.478(7) .
N2 C6 1.472(7) .
N2 C12 1.479(7) .
N2 C18 1.481(7) .
O1 C2 1.419(6) .
O1 C3 1.420(6) .
O2 C4 1.425(6) .
O2 C5 1.427(6) .
O3 C9 1.414(6) .
O3 C8 1.424(7) .
O4 C10 1.421(6) .
O4 C11 1.437(6) .
O5 C15 1.416(6) .
O5 C14 1.424(7) .
O6 C17 1.416(7) .
O6 C16 1.424(7) .
C1 C2 1.502(7) .
C1 H1A 0.9900 .
C1 H1B 0.9900 .
C2 H2A 0.9900 .
C2 H2B 0.9900 .
C3 C4 1.491(8) .
C3 H3A 0.9900 .
C3 H3B 0.9900 .
C4 H4A 0.9900 .
C4 H4B 0.9900 .
C5 C6 1.503(8) .
C5 H5A 0.9900 .
C5 H5B 0.9900 .
C6 H6A 0.9900 .
C6 H6B 0.9900 .
C7 C8 1.513(8) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 C10 1.501(8) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 H10A 0.9900 .
C10 H10B 0.9900 .
C11 C12 1.506(8) .
C11 H11A 0.9900 .
C11 H11B 0.9900 .
C12 H12A 0.9900 .
C12 H12B 0.9900 .
C13 C14 1.505(8) .
C13 H13A 0.9900 .
C13 H13B 0.9900 .
C14 H14A 0.9900 .
C14 H14B 0.9900 .
C15 C16 1.483(8) .
C15 H15A 0.9900 .
C15 H15B 0.9900 .
C16 H16A 0.9900 .
C16 H16B 0.9900 .
C17 C18 1.500(8) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 H18A 0.9900 .
C18 H18B 0.9900 .
K2 O11 2.788(4) .
K2 O9 2.798(4) .
K2 O8 2.815(4) .
K2 O12 2.816(4) .
K2 O10 2.837(4) .
K2 O7 2.874(4) .
K2 N4 3.043(4) .
K2 N3 3.056(5) .
N3 C24 1.465(7) .
N3 C36 1.467(8) .
N3 C30 1.473(8) .
N4 C19 1.478(7) .
N4 C25 1.480(7) .
N4 C31 1.483(7) .
O7 C20 1.421(7) .
O7 C21 1.432(7) .
O8 C23 1.410(7) .
O8 C22 1.421(7) .
O9 C27 1.420(6) .
O9 C26 1.426(6) .
O10 C28 1.415(7) .
O10 C29 1.427(7) .
O11 C33 1.416(7) .
O11 C32 1.426(7) .
O12 C34 1.424(7) .
O12 C35 1.437(7) .
C19 C20 1.503(8) .
C19 H19A 0.9900 .
C19 H19B 0.9900 .
C20 H20A 0.9900 .
C20 H20B 0.9900 .
C21 C22 1.484(8) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 H22A 0.9900 .
C22 H22B 0.9900 .
C23 C24 1.505(8) .
C23 H23A 0.9900 .
C23 H23B 0.9900 .
C24 H24A 0.9900 .
C24 H24B 0.9900 .
C25 C26 1.491(8) .
C25 H25A 0.9900 .
C25 H25B 0.9900 .
C26 H26A 0.9900 .
C26 H26B 0.9900 .
C27 C28 1.494(8) .
C27 H27A 0.9900 .
C27 H27B 0.9900 .
C28 H28A 0.9900 .
C28 H28B 0.9900 .
C29 C30 1.491(9) .
C29 H29A 0.9900 .
C29 H29B 0.9900 .
C30 H30A 0.9900 .
C30 H30B 0.9900 .
C31 C32 1.505(8) .
C31 H31A 0.9900 .
C31 H31B 0.9900 .
C32 H32A 0.9900 .
C32 H32B 0.9900 .
C33 C34 1.489(8) .
C33 H33A 0.9900 .
C33 H33B 0.9900 .
C34 H34A 0.9900 .
C34 H34B 0.9900 .
C35 C36 1.497(9) .
C35 H35A 0.9900 .
C35 H35B 0.9900 .
C36 H36A 0.9900 .
C36 H36B 0.9900 .
K3 O13 2.798(4) .
K3 O17 2.831(4) .
K3 O16 2.844(4) .
K3 O18 2.861(4) .
K3 O14 2.881(4) .
K3 O15 2.893(4) .
K3 N5 2.975(5) .
K3 N6 2.979(5) .
N5 C37 1.471(7) .
N5 C49 1.471(7) .
N5 C43 1.475(7) .
N6 C54 1.470(7) .
N6 C42 1.476(7) .
N6 C48 1.480(7) .
O13 C39 1.421(6) .
O13 C38 1.429(6) .
O14 C40 1.422(6) .
O14 C41 1.433(7) .
O15 C44 1.421(7) .
O15 C45 1.438(6) .
O16 C46 1.428(7) .
O16 C47 1.429(6) .
O17 C50 1.415(7) .
O17 C51 1.421(7) .
O18 C53 1.425(7) .
O18 C52 1.427(6) .
C37 C38 1.504(7) .
C37 H37A 0.9900 .
C37 H37B 0.9900 .
C38 H38A 0.9900 .
C38 H38B 0.9900 .
C39 C40 1.504(8) .
C39 H39A 0.9900 .
C39 H39B 0.9900 .
C40 H40A 0.9900 .
C40 H40B 0.9900 .
C41 C42 1.503(8) .
C41 H41A 0.9900 .
C41 H41B 0.9900 .
C42 H42A 0.9900 .
C42 H42B 0.9900 .
C43 C44 1.499(8) .
C43 H43A 0.9900 .
C43 H43B 0.9900 .
C44 H44A 0.9900 .
C44 H44B 0.9900 .
C45 C46 1.498(8) .
C45 H45A 0.9900 .
C45 H45B 0.9900 .
C46 H46A 0.9900 .
C46 H46B 0.9900 .
C47 C48 1.491(8) .
C47 H47A 0.9900 .
C47 H47B 0.9900 .
C48 H48A 0.9900 .
C48 H48B 0.9900 .
C49 C50 1.501(9) .
C49 H49A 0.9900 .
C49 H49B 0.9900 .
C50 H50A 0.9900 .
C50 H50B 0.9900 .
C51 C52 1.499(8) .
C51 H51A 0.9900 .
C51 H51B 0.9900 .
C52 H52A 0.9900 .
C52 H52B 0.9900 .
C53 C54 1.507(8) .
C53 H53A 0.9900 .
C53 H53B 0.9900 .
C54 H54A 0.9900 .
C54 H54B 0.9900 .
K4 Sn5 3.6617(4) 2
K4 Sn4 3.7100(4) 2
K4 Sn6 4.0820(5) 2
K5 Sn1 3.5073(4) 2_556
K5 Sn3 3.7042(5) 2_556
K5 Sn7 4.1631(5) 2_556
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_4
Sn5 Ni1 Sn1 Sn8 -29.30(4) .
Sn3 Ni1 Sn1 Sn8 -169.28(3) .
Sn6 Ni1 Sn1 Sn8 142.08(6) .
Sn2 Ni1 Sn1 Sn8 -75.26(2) .
Sn7 Ni1 Sn1 Sn8 115.61(2) .
Sn4 Ni1 Sn1 Sn8 56.65(2) .
Sn9 Ni1 Sn1 Sn8 -121.14(4) .
Sn5 Ni1 Sn1 Sn2 45.96(4) .
Sn3 Ni1 Sn1 Sn2 -94.02(2) .
Sn6 Ni1 Sn1 Sn2 -142.66(6) .
Sn7 Ni1 Sn1 Sn2 -169.12(3) .
Sn8 Ni1 Sn1 Sn2 75.26(2) .
Sn4 Ni1 Sn1 Sn2 131.91(3) .
Sn9 Ni1 Sn1 Sn2 -45.88(3) .
Sn5 Ni1 Sn1 Sn7 -144.92(5) .
Sn3 Ni1 Sn1 Sn7 75.11(2) .
Sn6 Ni1 Sn1 Sn7 26.46(4) .
Sn2 Ni1 Sn1 Sn7 169.12(3) .
Sn8 Ni1 Sn1 Sn7 -115.61(2) .
Sn4 Ni1 Sn1 Sn7 -58.97(2) .
Sn9 Ni1 Sn1 Sn7 123.24(4) .
Sn5 Ni1 Sn1 Sn3 139.98(5) .
Sn6 Ni1 Sn1 Sn3 -48.64(4) .
Sn2 Ni1 Sn1 Sn3 94.02(2) .
Sn7 Ni1 Sn1 Sn3 -75.11(2) .
Sn8 Ni1 Sn1 Sn3 169.28(3) .
Sn4 Ni1 Sn1 Sn3 -134.07(3) .
Sn9 Ni1 Sn1 Sn3 48.13(3) .
Sn5 Ni1 Sn1 K5 165.36(3) .
Sn3 Ni1 Sn1 K5 25.38(2) .
Sn6 Ni1 Sn1 K5 -23.26(6) .
Sn2 Ni1 Sn1 K5 119.40(2) .
Sn7 Ni1 Sn1 K5 -49.72(2) .
Sn8 Ni1 Sn1 K5 -165.34(2) .
Sn4 Ni1 Sn1 K5 -108.69(3) .
Sn9 Ni1 Sn1 K5 73.52(4) .
Sn5 Ni1 Sn2 Sn9 71.025(19) .
Sn3 Ni1 Sn2 Sn9 -67.47(2) .
Sn6 Ni1 Sn2 Sn9 5.78(4) .
Sn7 Ni1 Sn2 Sn9 -123.33(5) .
Sn1 Ni1 Sn2 Sn9 -139.58(2) .
Sn8 Ni1 Sn2 Sn9 145.72(2) .
Sn4 Ni1 Sn2 Sn9 119.22(4) .
Sn5 Ni1 Sn2 Sn8 -74.691(19) .
Sn3 Ni1 Sn2 Sn8 146.82(3) .
Sn6 Ni1 Sn2 Sn8 -139.94(5) .
Sn7 Ni1 Sn2 Sn8 90.95(5) .
Sn1 Ni1 Sn2 Sn8 74.705(19) .
Sn4 Ni1 Sn2 Sn8 -26.50(3) .
Sn9 Ni1 Sn2 Sn8 -145.72(2) .
Sn5 Ni1 Sn2 Sn1 -149.40(3) .
Sn3 Ni1 Sn2 Sn1 72.11(2) .
Sn6 Ni1 Sn2 Sn1 145.36(5) .
Sn7 Ni1 Sn2 Sn1 16.25(4) .
Sn8 Ni1 Sn2 Sn1 -74.705(19) .
Sn4 Ni1 Sn2 Sn1 -101.21(4) .
Sn9 Ni1 Sn2 Sn1 139.58(2) .
Sn3 Ni1 Sn2 Sn5 -138.49(3) .
Sn6 Ni1 Sn2 Sn5 -65.25(4) .
Sn7 Ni1 Sn2 Sn5 165.64(6) .
Sn1 Ni1 Sn2 Sn5 149.40(3) .
Sn8 Ni1 Sn2 Sn5 74.691(19) .
Sn4 Ni1 Sn2 Sn5 48.19(3) .
Sn9 Ni1 Sn2 Sn5 -71.025(19) .
Sn5 Ni1 Sn2 Sn3 138.49(3) .
Sn6 Ni1 Sn2 Sn3 73.25(4) .
Sn7 Ni1 Sn2 Sn3 -55.86(4) .
Sn1 Ni1 Sn2 Sn3 -72.11(2) .
Sn8 Ni1 Sn2 Sn3 -146.82(3) .
Sn4 Ni1 Sn2 Sn3 -173.32(5) .
Sn9 Ni1 Sn2 Sn3 67.47(2) .
Sn8 Sn1 Sn2 Ni1 66.82(2) .
Sn7 Sn1 Sn2 Ni1 -9.26(2) .
Sn3 Sn1 Sn2 Ni1 -56.94(2) .
K5 Sn1 Sn2 Ni1 -98.31(3) .
Ni1 Sn1 Sn2 Sn9 34.38(2) .
Sn8 Sn1 Sn2 Sn9 101.202(18) .
Sn7 Sn1 Sn2 Sn9 25.13(2) .
Sn3 Sn1 Sn2 Sn9 -22.558(17) .
K5 Sn1 Sn2 Sn9 -63.92(2) .
Ni1 Sn1 Sn2 Sn8 -66.82(2) .
Sn7 Sn1 Sn2 Sn8 -76.075(18) .
Sn3 Sn1 Sn2 Sn8 -123.760(16) .
K5 Sn1 Sn2 Sn8 -165.13(2) .
Ni1 Sn1 Sn2 Sn5 -23.72(2) .
Sn8 Sn1 Sn2 Sn5 43.099(14) .
Sn7 Sn1 Sn2 Sn5 -32.98(2) .
Sn3 Sn1 Sn2 Sn5 -80.661(16) .
K5 Sn1 Sn2 Sn5 -122.026(18) .
Ni1 Sn1 Sn2 Sn3 56.94(2) .
Sn8 Sn1 Sn2 Sn3 123.760(16) .
Sn7 Sn1 Sn2 Sn3 47.685(15) .
K5 Sn1 Sn2 Sn3 -41.366(16) .
Sn5 Ni1 Sn3 Sn9 -2.17(4) .
Sn6 Ni1 Sn3 Sn9 -71.230(19) .
Sn2 Ni1 Sn3 Sn9 67.65(2) .
Sn7 Ni1 Sn3 Sn9 -146.43(2) .
Sn1 Ni1 Sn3 Sn9 137.66(2) .
Sn8 Ni1 Sn3 Sn9 121.73(5) .
Sn4 Ni1 Sn3 Sn9 -119.22(5) .
Sn5 Ni1 Sn3 Sn7 144.26(5) .
Sn6 Ni1 Sn3 Sn7 75.20(2) .
Sn2 Ni1 Sn3 Sn7 -145.92(3) .
Sn1 Ni1 Sn3 Sn7 -75.91(2) .
Sn8 Ni1 Sn3 Sn7 -91.85(5) .
Sn4 Ni1 Sn3 Sn7 27.20(3) .
Sn9 Ni1 Sn3 Sn7 146.43(2) .
Sn5 Ni1 Sn3 Sn1 -139.83(5) .
Sn6 Ni1 Sn3 Sn1 151.11(3) .
Sn2 Ni1 Sn3 Sn1 -70.01(2) .
Sn7 Ni1 Sn3 Sn1 75.91(2) .
Sn8 Ni1 Sn3 Sn1 -15.93(4) .
Sn4 Ni1 Sn3 Sn1 103.11(4) .
Sn9 Ni1 Sn3 Sn1 -137.66(2) .
Sn5 Ni1 Sn3 Sn6 69.06(4) .
Sn2 Ni1 Sn3 Sn6 138.88(3) .
Sn7 Ni1 Sn3 Sn6 -75.20(2) .
Sn1 Ni1 Sn3 Sn6 -151.11(3) .
Sn8 Ni1 Sn3 Sn6 -167.04(6) .
Sn4 Ni1 Sn3 Sn6 -47.99(4) .
Sn9 Ni1 Sn3 Sn6 71.230(19) .
Sn5 Ni1 Sn3 Sn2 -69.82(4) .
Sn6 Ni1 Sn3 Sn2 -138.88(3) .
Sn7 Ni1 Sn3 Sn2 145.92(3) .
Sn1 Ni1 Sn3 Sn2 70.01(2) .
Sn8 Ni1 Sn3 Sn2 54.08(4) .
Sn4 Ni1 Sn3 Sn2 173.13(5) .
Sn9 Ni1 Sn3 Sn2 -67.65(2) .
Sn5 Ni1 Sn3 K5 -162.78(3) .
Sn6 Ni1 Sn3 K5 128.156(19) .
Sn2 Ni1 Sn3 K5 -92.96(2) .
Sn7 Ni1 Sn3 K5 52.96(2) .
Sn1 Ni1 Sn3 K5 -22.95(2) .
Sn8 Ni1 Sn3 K5 -38.89(5) .
Sn4 Ni1 Sn3 K5 80.16(4) .
Sn9 Ni1 Sn3 K5 -160.614(18) .
Sn8 Sn1 Sn3 Ni1 9.25(2) .
Sn2 Sn1 Sn3 Ni1 58.31(2) .
Sn7 Sn1 Sn3 Ni1 -66.38(2) .
K5 Sn1 Sn3 Ni1 -155.68(2) .
Ni1 Sn1 Sn3 Sn9 -35.79(2) .
Sn8 Sn1 Sn3 Sn9 -26.54(2) .
Sn2 Sn1 Sn3 Sn9 22.517(17) .
Sn7 Sn1 Sn3 Sn9 -102.172(18) .
K5 Sn1 Sn3 Sn9 168.531(16) .
Ni1 Sn1 Sn3 Sn7 66.38(2) .
Sn8 Sn1 Sn3 Sn7 75.629(18) .
Sn2 Sn1 Sn3 Sn7 124.688(17) .
K5 Sn1 Sn3 Sn7 -89.297(13) .
Ni1 Sn1 Sn3 Sn6 21.98(2) .
Sn8 Sn1 Sn3 Sn6 31.23(2) .
Sn2 Sn1 Sn3 Sn6 80.289(16) .
Sn7 Sn1 Sn3 Sn6 -44.400(14) .
K5 Sn1 Sn3 Sn6 -133.697(14) .
Ni1 Sn1 Sn3 Sn2 -58.31(2) .
Sn8 Sn1 Sn3 Sn2 -49.060(15) .
Sn7 Sn1 Sn3 Sn2 -124.688(17) .
K5 Sn1 Sn3 Sn2 146.015(15) .
Ni1 Sn1 Sn3 K5 155.68(2) .
Sn8 Sn1 Sn3 K5 164.925(19) .
Sn2 Sn1 Sn3 K5 -146.015(15) .
Sn7 Sn1 Sn3 K5 89.297(13) .
Sn9 Sn2 Sn3 Ni1 78.73(3) .
Sn8 Sn2 Sn3 Ni1 -27.01(2) .
Sn1 Sn2 Sn3 Ni1 -73.39(3) .
Sn5 Sn2 Sn3 Ni1 30.94(2) .
Ni1 Sn2 Sn3 Sn9 -78.73(3) .
Sn8 Sn2 Sn3 Sn9 -105.740(18) .
Sn1 Sn2 Sn3 Sn9 -152.12(2) .
Sn5 Sn2 Sn3 Sn9 -47.786(15) .
Ni1 Sn2 Sn3 Sn7 27.52(2) .
Sn9 Sn2 Sn3 Sn7 106.245(18) .
Sn8 Sn2 Sn3 Sn7 0.505(17) .
Sn1 Sn2 Sn3 Sn7 -45.873(16) .
Sn5 Sn2 Sn3 Sn7 58.459(16) .
Ni1 Sn2 Sn3 Sn1 73.39(3) .
Sn9 Sn2 Sn3 Sn1 152.12(2) .
Sn8 Sn2 Sn3 Sn1 46.379(16) .
Sn5 Sn2 Sn3 Sn1 104.332(17) .
Ni1 Sn2 Sn3 Sn6 -30.17(2) .
Sn9 Sn2 Sn3 Sn6 48.561(15) .
Sn8 Sn2 Sn3 Sn6 -57.179(15) .
Sn1 Sn2 Sn3 Sn6 -103.557(17) .
Sn5 Sn2 Sn3 Sn6 0.775(14) .
Ni1 Sn2 Sn3 K5 104.29(2) .
Sn9 Sn2 Sn3 K5 -176.980(18) .
Sn8 Sn2 Sn3 K5 77.280(15) .
Sn1 Sn2 Sn3 K5 30.901(14) .
Sn5 Sn2 Sn3 K5 135.233(13) .
Sn5 Ni1 Sn4 Sn8 76.668(19) .
Sn3 Ni1 Sn4 Sn8 -143.64(5) .
Sn6 Ni1 Sn4 Sn8 165.40(3) .
Sn2 Ni1 Sn4 Sn8 26.60(3) .
Sn7 Ni1 Sn4 Sn8 -116.34(2) .
Sn1 Ni1 Sn4 Sn8 -56.71(2) .
Sn9 Ni1 Sn4 Sn8 121.01(4) .
Sn5 Ni1 Sn4 Sn6 -88.74(2) .
Sn3 Ni1 Sn4 Sn6 50.96(4) .
Sn2 Ni1 Sn4 Sn6 -138.81(5) .
Sn7 Ni1 Sn4 Sn6 78.25(2) .
Sn1 Ni1 Sn4 Sn6 137.88(3) .
Sn8 Ni1 Sn4 Sn6 -165.40(3) .
Sn9 Ni1 Sn4 Sn6 -44.39(3) .
Sn5 Ni1 Sn4 Sn7 -166.99(3) .
Sn3 Ni1 Sn4 Sn7 -27.30(3) .
Sn6 Ni1 Sn4 Sn7 -78.25(2) .
Sn2 Ni1 Sn4 Sn7 142.94(5) .
Sn1 Ni1 Sn4 Sn7 59.63(2) .
Sn8 Ni1 Sn4 Sn7 116.34(2) .
Sn9 Ni1 Sn4 Sn7 -122.65(4) .
Sn3 Ni1 Sn4 Sn5 139.69(5) .
Sn6 Ni1 Sn4 Sn5 88.74(2) .
Sn2 Ni1 Sn4 Sn5 -50.07(4) .
Sn7 Ni1 Sn4 Sn5 166.99(3) .
Sn1 Ni1 Sn4 Sn5 -133.38(3) .
Sn8 Ni1 Sn4 Sn5 -76.668(19) .
Sn9 Ni1 Sn4 Sn5 44.34(3) .
Sn5 Ni1 Sn4 K4 -35.833(19) .
Sn3 Ni1 Sn4 K4 103.86(4) .
Sn6 Ni1 Sn4 K4 52.903(19) .
Sn2 Ni1 Sn4 K4 -85.90(4) .
Sn7 Ni1 Sn4 K4 131.155(17) .
Sn1 Ni1 Sn4 K4 -169.21(2) .
Sn8 Ni1 Sn4 K4 -112.501(17) .
Sn9 Ni1 Sn4 K4 8.51(4) .
Sn3 Ni1 Sn5 Sn9 2.17(4) .
Sn6 Ni1 Sn5 Sn9 70.294(19) .
Sn2 Ni1 Sn5 Sn9 -71.411(19) .
Sn7 Ni1 Sn5 Sn9 122.89(5) .
Sn1 Ni1 Sn5 Sn9 -115.21(5) .
Sn8 Ni1 Sn5 Sn9 -144.10(2) .
Sn4 Ni1 Sn5 Sn9 142.18(2) .
Sn3 Ni1 Sn5 Sn8 146.27(5) .
Sn6 Ni1 Sn5 Sn8 -145.61(3) .
Sn2 Ni1 Sn5 Sn8 72.688(19) .
Sn7 Ni1 Sn5 Sn8 -93.01(5) .
Sn1 Ni1 Sn5 Sn8 28.89(4) .
Sn4 Ni1 Sn5 Sn8 -73.724(19) .
Sn9 Ni1 Sn5 Sn8 144.10(2) .
Sn3 Ni1 Sn5 Sn4 -140.01(5) .
Sn6 Ni1 Sn5 Sn4 -71.88(2) .
Sn2 Ni1 Sn5 Sn4 146.41(2) .
Sn7 Ni1 Sn5 Sn4 -19.29(4) .
Sn1 Ni1 Sn5 Sn4 102.62(5) .
Sn8 Ni1 Sn5 Sn4 73.724(19) .
Sn9 Ni1 Sn5 Sn4 -142.18(2) .
Sn3 Ni1 Sn5 Sn2 73.58(4) .
Sn6 Ni1 Sn5 Sn2 141.70(3) .
Sn7 Ni1 Sn5 Sn2 -165.70(5) .
Sn1 Ni1 Sn5 Sn2 -43.80(4) .
Sn8 Ni1 Sn5 Sn2 -72.688(19) .
Sn4 Ni1 Sn5 Sn2 -146.41(2) .
Sn9 Ni1 Sn5 Sn2 71.411(19) .
Sn3 Ni1 Sn5 Sn6 -68.12(4) .
Sn2 Ni1 Sn5 Sn6 -141.70(3) .
Sn7 Ni1 Sn5 Sn6 52.60(4) .
Sn1 Ni1 Sn5 Sn6 174.50(6) .
Sn8 Ni1 Sn5 Sn6 145.61(3) .
Sn4 Ni1 Sn5 Sn6 71.88(2) .
Sn9 Ni1 Sn5 Sn6 -70.294(19) .
Sn3 Ni1 Sn5 K4 -102.86(4) .
Sn6 Ni1 Sn5 K4 -34.73(2) .
Sn2 Ni1 Sn5 K4 -176.439(16) .
Sn7 Ni1 Sn5 K4 17.86(5) .
Sn1 Ni1 Sn5 K4 139.76(4) .
Sn8 Ni1 Sn5 K4 110.872(18) .
Sn4 Ni1 Sn5 K4 37.148(19) .
Sn9 Ni1 Sn5 K4 -105.029(18) .
Sn8 Sn4 Sn5 Ni1 -66.70(2) .
Sn6 Sn4 Sn5 Ni1 60.23(2) .
Sn7 Sn4 Sn5 Ni1 11.04(2) .
K4 Sn4 Sn5 Ni1 142.02(2) .
Ni1 Sn4 Sn5 Sn9 -32.63(2) .
Sn8 Sn4 Sn5 Sn9 -99.332(17) .
Sn6 Sn4 Sn5 Sn9 27.602(16) .
Sn7 Sn4 Sn5 Sn9 -21.59(2) .
K4 Sn4 Sn5 Sn9 109.384(15) .
Ni1 Sn4 Sn5 Sn8 66.70(2) .
Sn6 Sn4 Sn5 Sn8 126.935(16) .
Sn7 Sn4 Sn5 Sn8 77.746(17) .
K4 Sn4 Sn5 Sn8 -151.283(14) .
Ni1 Sn4 Sn5 Sn2 25.97(2) .
Sn8 Sn4 Sn5 Sn2 -40.727(14) .
Sn6 Sn4 Sn5 Sn2 86.207(16) .
Sn7 Sn4 Sn5 Sn2 37.019(19) .
K4 Sn4 Sn5 Sn2 167.990(14) .
Ni1 Sn4 Sn5 Sn6 -60.23(2) .
Sn8 Sn4 Sn5 Sn6 -126.935(16) .
Sn7 Sn4 Sn5 Sn6 -49.188(15) .
K4 Sn4 Sn5 Sn6 81.782(11) .
Ni1 Sn4 Sn5 K4 -142.02(2) .
Sn8 Sn4 Sn5 K4 151.283(14) .
Sn6 Sn4 Sn5 K4 -81.782(11) .
Sn7 Sn4 Sn5 K4 -130.971(15) .
Sn9 Sn2 Sn5 Ni1 -73.50(2) .
Sn8 Sn2 Sn5 Ni1 69.31(2) .
Sn1 Sn2 Sn5 Ni1 25.26(2) .
Sn3 Sn2 Sn5 Ni1 -28.49(2) .
Ni1 Sn2 Sn5 Sn9 73.50(2) .
Sn8 Sn2 Sn5 Sn9 142.815(18) .
Sn1 Sn2 Sn5 Sn9 98.755(18) .
Sn3 Sn2 Sn5 Sn9 45.014(13) .
Ni1 Sn2 Sn5 Sn8 -69.31(2) .
Sn9 Sn2 Sn5 Sn8 -142.815(18) .
Sn1 Sn2 Sn5 Sn8 -44.060(15) .
Sn3 Sn2 Sn5 Sn8 -97.801(15) .
Ni1 Sn2 Sn5 Sn4 -27.38(2) .
Sn9 Sn2 Sn5 Sn4 -100.885(17) .
Sn8 Sn2 Sn5 Sn4 41.930(15) .
Sn1 Sn2 Sn5 Sn4 -2.129(19) .
Sn3 Sn2 Sn5 Sn4 -55.871(15) .
Ni1 Sn2 Sn5 Sn6 27.73(2) .
Sn9 Sn2 Sn5 Sn6 -45.770(14) .
Sn8 Sn2 Sn5 Sn6 97.045(15) .
Sn1 Sn2 Sn5 Sn6 52.985(17) .
Sn3 Sn2 Sn5 Sn6 -0.756(13) .
Ni1 Sn2 Sn5 K4 10.85(5) .
Sn9 Sn2 Sn5 K4 -62.65(5) .
Sn8 Sn2 Sn5 K4 80.17(5) .
Sn1 Sn2 Sn5 K4 36.11(5) .
Sn3 Sn2 Sn5 K4 -17.64(5) .
Sn5 Ni1 Sn6 Sn9 -69.223(19) .
Sn3 Ni1 Sn6 Sn9 70.26(2) .
Sn2 Ni1 Sn6 Sn9 -5.75(4) .
Sn7 Ni1 Sn6 Sn9 143.00(3) .
Sn1 Ni1 Sn6 Sn9 116.78(5) .
Sn8 Ni1 Sn6 Sn9 -121.94(5) .
Sn4 Ni1 Sn6 Sn9 -142.44(2) .
Sn5 Ni1 Sn6 Sn4 73.22(2) .
Sn3 Ni1 Sn6 Sn4 -147.30(3) .
Sn2 Ni1 Sn6 Sn4 136.69(5) .
Sn7 Ni1 Sn6 Sn4 -74.563(19) .
Sn1 Ni1 Sn6 Sn4 -100.78(5) .
Sn8 Ni1 Sn6 Sn4 20.50(4) .
Sn9 Ni1 Sn6 Sn4 142.44(2) .
Sn5 Ni1 Sn6 Sn7 147.78(3) .
Sn3 Ni1 Sn6 Sn7 -72.74(2) .
Sn2 Ni1 Sn6 Sn7 -148.75(5) .
Sn1 Ni1 Sn6 Sn7 -26.22(4) .
Sn8 Ni1 Sn6 Sn7 95.06(5) .
Sn4 Ni1 Sn6 Sn7 74.563(19) .
Sn9 Ni1 Sn6 Sn7 -143.00(3) .
Sn5 Ni1 Sn6 Sn3 -139.48(3) .
Sn2 Ni1 Sn6 Sn3 -76.01(4) .
Sn7 Ni1 Sn6 Sn3 72.74(2) .
Sn1 Ni1 Sn6 Sn3 46.52(4) .
Sn8 Ni1 Sn6 Sn3 167.80(5) .
Sn4 Ni1 Sn6 Sn3 147.30(3) .
Sn9 Ni1 Sn6 Sn3 -70.26(2) .
Sn3 Ni1 Sn6 Sn5 139.48(3) .
Sn2 Ni1 Sn6 Sn5 63.47(4) .
Sn7 Ni1 Sn6 Sn5 -147.78(3) .
Sn1 Ni1 Sn6 Sn5 -174.00(6) .
Sn8 Ni1 Sn6 Sn5 -52.72(4) .
Sn4 Ni1 Sn6 Sn5 -73.22(2) .
Sn9 Ni1 Sn6 Sn5 69.223(19) .
Sn5 Ni1 Sn6 K4 28.92(2) .
Sn3 Ni1 Sn6 K4 168.403(17) .
Sn2 Ni1 Sn6 K4 92.39(4) .
Sn7 Ni1 Sn6 K4 -118.858(17) .
Sn1 Ni1 Sn6 K4 -145.07(4) .
Sn8 Ni1 Sn6 K4 -23.80(5) .
Sn4 Ni1 Sn6 K4 -44.295(16) .
Sn9 Ni1 Sn6 K4 98.145(17) .
Sn8 Sn4 Sn6 Ni1 -12.54(2) .
Sn7 Sn4 Sn6 Ni1 65.12(2) .
Sn5 Sn4 Sn6 Ni1 -59.37(2) .
K4 Sn4 Sn6 Ni1 -127.94(2) .
Ni1 Sn4 Sn6 Sn9 32.17(2) .
Sn8 Sn4 Sn6 Sn9 19.63(2) .
Sn7 Sn4 Sn6 Sn9 97.290(18) .
Sn5 Sn4 Sn6 Sn9 -27.197(16) .
K4 Sn4 Sn6 Sn9 -95.769(15) .
Ni1 Sn4 Sn6 Sn7 -65.12(2) .
Sn8 Sn4 Sn6 Sn7 -77.656(17) .
Sn5 Sn4 Sn6 Sn7 -124.487(16) .
K4 Sn4 Sn6 Sn7 166.941(14) .
Ni1 Sn4 Sn6 Sn3 -24.72(2) .
Sn8 Sn4 Sn6 Sn3 -37.256(19) .
Sn7 Sn4 Sn6 Sn3 40.400(15) .
Sn5 Sn4 Sn6 Sn3 -84.087(15) .
K4 Sn4 Sn6 Sn3 -152.659(13) .
Ni1 Sn4 Sn6 Sn5 59.37(2) .
Sn8 Sn4 Sn6 Sn5 46.831(15) .
Sn7 Sn4 Sn6 Sn5 124.487(16) .
K4 Sn4 Sn6 Sn5 -68.572(10) .
Ni1 Sn4 Sn6 K4 127.94(2) .
Sn8 Sn4 Sn6 K4 115.403(15) .
Sn7 Sn4 Sn6 K4 -166.941(14) .
Sn5 Sn4 Sn6 K4 68.572(10) .
Sn9 Sn3 Sn6 Ni1 74.33(2) .
Sn7 Sn3 Sn6 Ni1 -69.24(2) .
Sn1 Sn3 Sn6 Ni1 -23.49(2) .
Sn2 Sn3 Sn6 Ni1 28.36(2) .
K5 Sn3 Sn6 Ni1 -83.34(3) .
Ni1 Sn3 Sn6 Sn9 -74.33(2) .
Sn7 Sn3 Sn6 Sn9 -143.574(18) .
Sn1 Sn3 Sn6 Sn9 -97.819(18) .
Sn2 Sn3 Sn6 Sn9 -45.968(13) .
K5 Sn3 Sn6 Sn9 -157.67(2) .
Ni1 Sn3 Sn6 Sn4 26.84(2) .
Sn9 Sn3 Sn6 Sn4 101.172(17) .
Sn7 Sn3 Sn6 Sn4 -42.401(15) .
Sn1 Sn3 Sn6 Sn4 3.353(19) .
Sn2 Sn3 Sn6 Sn4 55.205(15) .
K5 Sn3 Sn6 Sn4 -56.50(2) .
Ni1 Sn3 Sn6 Sn7 69.24(2) .
Sn9 Sn3 Sn6 Sn7 143.574(18) .
Sn1 Sn3 Sn6 Sn7 45.755(15) .
Sn2 Sn3 Sn6 Sn7 97.606(15) .
K5 Sn3 Sn6 Sn7 -14.094(17) .
Ni1 Sn3 Sn6 Sn5 -29.10(2) .
Sn9 Sn3 Sn6 Sn5 45.231(13) .
Sn7 Sn3 Sn6 Sn5 -98.343(15) .
Sn1 Sn3 Sn6 Sn5 -52.588(16) .
Sn2 Sn3 Sn6 Sn5 -0.736(13) .
K5 Sn3 Sn6 Sn5 -112.436(18) .
Ni1 Sn3 Sn6 K4 -21.77(3) .
Sn9 Sn3 Sn6 K4 52.57(3) .
Sn7 Sn3 Sn6 K4 -91.01(3) .
Sn1 Sn3 Sn6 K4 -45.25(3) .
Sn2 Sn3 Sn6 K4 6.60(3) .
K5 Sn3 Sn6 K4 -105.10(3) .
Sn9 Sn5 Sn6 Ni1 -75.75(2) .
Sn8 Sn5 Sn6 Ni1 27.79(2) .
Sn4 Sn5 Sn6 Ni1 71.39(2) .
Sn2 Sn5 Sn6 Ni1 -28.93(2) .
K4 Sn5 Sn6 Ni1 145.62(2) .
Ni1 Sn5 Sn6 Sn9 75.75(2) .
Sn8 Sn5 Sn6 Sn9 103.547(17) .
Sn4 Sn5 Sn6 Sn9 147.147(18) .
Sn2 Sn5 Sn6 Sn9 46.824(14) .
K4 Sn5 Sn6 Sn9 -138.624(14) .
Ni1 Sn5 Sn6 Sn4 -71.39(2) .
Sn9 Sn5 Sn6 Sn4 -147.147(18) .
Sn8 Sn5 Sn6 Sn4 -43.600(14) .
Sn2 Sn5 Sn6 Sn4 -100.323(15) .
K4 Sn5 Sn6 Sn4 74.229(12) .
Ni1 Sn5 Sn6 Sn7 -25.79(2) .
Sn9 Sn5 Sn6 Sn7 -101.540(18) .
Sn8 Sn5 Sn6 Sn7 2.008(17) .
Sn4 Sn5 Sn6 Sn7 45.607(14) .
Sn2 Sn5 Sn6 Sn7 -54.716(17) .
K4 Sn5 Sn6 Sn7 119.837(14) .
Ni1 Sn5 Sn6 Sn3 29.74(2) .
Sn9 Sn5 Sn6 Sn3 -46.011(14) .
Sn8 Sn5 Sn6 Sn3 57.537(16) .
Sn4 Sn5 Sn6 Sn3 101.137(15) .
Sn2 Sn5 Sn6 Sn3 0.813(14) .
K4 Sn5 Sn6 Sn3 175.366(13) .
Ni1 Sn5 Sn6 K4 -145.62(2) .
Sn9 Sn5 Sn6 K4 138.624(14) .
Sn8 Sn5 Sn6 K4 -117.829(14) .
Sn4 Sn5 Sn6 K4 -74.229(12) .
Sn2 Sn5 Sn6 K4 -174.553(13) .
Sn5 Ni1 Sn7 Sn3 -141.07(5) .
Sn6 Ni1 Sn7 Sn3 -85.54(2) .
Sn2 Ni1 Sn7 Sn3 61.12(4) .
Sn1 Ni1 Sn7 Sn3 77.25(2) .
Sn8 Ni1 Sn7 Sn3 138.71(3) .
Sn4 Ni1 Sn7 Sn3 -160.55(3) .
Sn9 Ni1 Sn7 Sn3 -40.37(3) .
Sn5 Ni1 Sn7 Sn4 19.48(4) .
Sn3 Ni1 Sn7 Sn4 160.55(3) .
Sn6 Ni1 Sn7 Sn4 75.01(2) .
Sn2 Ni1 Sn7 Sn4 -138.33(5) .
Sn1 Ni1 Sn7 Sn4 -122.20(2) .
Sn8 Ni1 Sn7 Sn4 -60.74(2) .
Sn9 Ni1 Sn7 Sn4 120.17(4) .
Sn5 Ni1 Sn7 Sn1 141.67(5) .
Sn3 Ni1 Sn7 Sn1 -77.25(2) .
Sn6 Ni1 Sn7 Sn1 -162.79(3) .
Sn2 Ni1 Sn7 Sn1 -16.13(4) .
Sn8 Ni1 Sn7 Sn1 61.46(2) .
Sn4 Ni1 Sn7 Sn1 122.20(2) .
Sn9 Ni1 Sn7 Sn1 -117.63(4) .
Sn5 Ni1 Sn7 Sn6 -55.53(4) .
Sn3 Ni1 Sn7 Sn6 85.54(2) .
Sn2 Ni1 Sn7 Sn6 146.66(5) .
Sn1 Ni1 Sn7 Sn6 162.79(3) .
Sn8 Ni1 Sn7 Sn6 -135.75(3) .
Sn4 Ni1 Sn7 Sn6 -75.01(2) .
Sn9 Ni1 Sn7 Sn6 45.17(3) .
Sn5 Ni1 Sn7 K5 177.11(4) .
Sn3 Ni1 Sn7 K5 -41.822(17) .
Sn6 Ni1 Sn7 K5 -127.363(18) .
Sn2 Ni1 Sn7 K5 19.30(5) .
Sn1 Ni1 Sn7 K5 35.431(17) .
Sn8 Ni1 Sn7 K5 96.89(2) .
Sn4 Ni1 Sn7 K5 157.629(16) .
Sn9 Ni1 Sn7 K5 -82.20(3) .
Sn9 Sn3 Sn7 Ni1 29.32(2) .
Sn1 Sn3 Sn7 Ni1 -65.18(2) .
Sn6 Sn3 Sn7 Ni1 60.46(2) .
Sn2 Sn3 Sn7 Ni1 -23.98(2) .
K5 Sn3 Sn7 Ni1 -130.18(2) .
Ni1 Sn3 Sn7 Sn4 -16.59(2) .
Sn9 Sn3 Sn7 Sn4 12.74(2) .
Sn1 Sn3 Sn7 Sn4 -81.770(17) .
Sn6 Sn3 Sn7 Sn4 43.872(15) .
Sn2 Sn3 Sn7 Sn4 -40.566(18) .
K5 Sn3 Sn7 Sn4 -146.762(15) .
Ni1 Sn3 Sn7 Sn1 65.18(2) .
Sn9 Sn3 Sn7 Sn1 94.505(18) .
Sn6 Sn3 Sn7 Sn1 125.642(16) .
Sn2 Sn3 Sn7 Sn1 41.204(14) .
K5 Sn3 Sn7 Sn1 -64.992(11) .
Ni1 Sn3 Sn7 Sn6 -60.46(2) .
Sn9 Sn3 Sn7 Sn6 -31.136(16) .
Sn1 Sn3 Sn7 Sn6 -125.642(16) .
Sn2 Sn3 Sn7 Sn6 -84.437(14) .
K5 Sn3 Sn7 Sn6 169.366(13) .
Ni1 Sn3 Sn7 K5 130.18(2) .
Sn9 Sn3 Sn7 K5 159.498(17) .
Sn1 Sn3 Sn7 K5 64.992(11) .
Sn6 Sn3 Sn7 K5 -169.366(13) .
Sn2 Sn3 Sn7 K5 106.196(12) .
Sn8 Sn4 Sn7 Ni1 47.37(2) .
Sn6 Sn4 Sn7 Ni1 -63.99(2) .
Sn5 Sn4 Sn7 Ni1 -10.84(2) .
K4 Sn4 Sn7 Ni1 -81.45(3) .
Ni1 Sn4 Sn7 Sn3 16.35(2) .
Sn8 Sn4 Sn7 Sn3 63.725(18) .
Sn6 Sn4 Sn7 Sn3 -47.637(16) .
Sn5 Sn4 Sn7 Sn3 5.51(2) .
K4 Sn4 Sn7 Sn3 -65.10(2) .
Ni1 Sn4 Sn7 Sn1 -43.44(2) .
Sn8 Sn4 Sn7 Sn1 3.932(15) .
Sn6 Sn4 Sn7 Sn1 -107.430(16) .
Sn5 Sn4 Sn7 Sn1 -54.285(18) .
K4 Sn4 Sn7 Sn1 -124.895(19) .
Ni1 Sn4 Sn7 Sn6 63.99(2) .
Sn8 Sn4 Sn7 Sn6 111.362(16) .
Sn5 Sn4 Sn7 Sn6 53.145(16) .
K4 Sn4 Sn7 Sn6 -17.465(18) .
Ni1 Sn4 Sn7 K5 -43.44(3) .
Sn8 Sn4 Sn7 K5 3.94(3) .
Sn6 Sn4 Sn7 K5 -107.43(3) .
Sn5 Sn4 Sn7 K5 -54.28(3) .
K4 Sn4 Sn7 K5 -124.89(2) .
Sn8 Sn1 Sn7 Ni1 -47.92(2) .
Sn2 Sn1 Sn7 Ni1 9.27(2) .
Sn3 Sn1 Sn7 Ni1 64.68(2) .
K5 Sn1 Sn7 Ni1 136.02(2) .
Ni1 Sn1 Sn7 Sn3 -64.68(2) .
Sn8 Sn1 Sn7 Sn3 -112.599(16) .
Sn2 Sn1 Sn7 Sn3 -55.407(17) .
K5 Sn1 Sn7 Sn3 71.338(12) .
Ni1 Sn1 Sn7 Sn4 43.98(2) .
Sn8 Sn1 Sn7 Sn4 -3.939(15) .
Sn2 Sn1 Sn7 Sn4 53.253(19) .
Sn3 Sn1 Sn7 Sn4 108.660(16) .
K5 Sn1 Sn7 Sn4 179.997(13) .
Ni1 Sn1 Sn7 Sn6 -14.19(2) .
Sn8 Sn1 Sn7 Sn6 -62.106(18) .
Sn2 Sn1 Sn7 Sn6 -4.91(2) .
Sn3 Sn1 Sn7 Sn6 50.493(16) .
K5 Sn1 Sn7 Sn6 121.831(15) .
Ni1 Sn1 Sn7 K5 -136.02(2) .
Sn8 Sn1 Sn7 K5 176.063(16) .
Sn2 Sn1 Sn7 K5 -126.745(19) .
Sn3 Sn1 Sn7 K5 -71.338(12) .
Sn9 Sn6 Sn7 Ni1 -31.56(2) .
Sn4 Sn6 Sn7 Ni1 67.49(2) .
Sn3 Sn6 Sn7 Ni1 -61.87(2) .
Sn5 Sn6 Sn7 Ni1 23.71(2) .
K4 Sn6 Sn7 Ni1 80.51(2) .
Ni1 Sn6 Sn7 Sn3 61.87(2) .
Sn9 Sn6 Sn7 Sn3 30.315(16) .
Sn4 Sn6 Sn7 Sn3 129.360(17) .
Sn5 Sn6 Sn7 Sn3 85.587(15) .
K4 Sn6 Sn7 Sn3 142.381(16) .
Ni1 Sn6 Sn7 Sn4 -67.49(2) .
Sn9 Sn6 Sn7 Sn4 -99.045(17) .
Sn3 Sn6 Sn7 Sn4 -129.360(17) .
Sn5 Sn6 Sn7 Sn4 -43.773(14) .
K4 Sn6 Sn7 Sn4 13.021(14) .
Ni1 Sn6 Sn7 Sn1 14.44(2) .
Sn9 Sn6 Sn7 Sn1 -17.11(2) .
Sn4 Sn6 Sn7 Sn1 81.932(17) .
Sn3 Sn6 Sn7 Sn1 -47.428(15) .
Sn5 Sn6 Sn7 Sn1 38.159(19) .
K4 Sn6 Sn7 Sn1 94.953(18) .
Ni1 Sn6 Sn7 K5 73.05(2) .
Sn9 Sn6 Sn7 K5 41.49(2) .
Sn4 Sn6 Sn7 K5 140.535(19) .
Sn3 Sn6 Sn7 K5 11.176(14) .
Sn5 Sn6 Sn7 K5 96.762(17) .
K4 Sn6 Sn7 K5 153.557(11) .
Sn5 Ni1 Sn8 Sn2 83.42(2) .
Sn3 Ni1 Sn8 Sn2 -59.45(4) .
Sn6 Ni1 Sn8 Sn2 139.70(5) .
Sn7 Ni1 Sn8 Sn2 -138.36(3) .
Sn1 Ni1 Sn8 Sn2 -75.66(2) .
Sn4 Ni1 Sn8 Sn2 160.36(3) .
Sn9 Ni1 Sn8 Sn2 40.74(3) .
Sn5 Ni1 Sn8 Sn1 159.09(3) .
Sn3 Ni1 Sn8 Sn1 16.21(4) .
Sn6 Ni1 Sn8 Sn1 -144.63(5) .
Sn2 Ni1 Sn8 Sn1 75.66(2) .
Sn7 Ni1 Sn8 Sn1 -62.69(2) .
Sn4 Ni1 Sn8 Sn1 -123.97(2) .
Sn9 Ni1 Sn8 Sn1 116.41(4) .
Sn5 Ni1 Sn8 Sn4 -76.940(19) .
Sn3 Ni1 Sn8 Sn4 140.19(5) .
Sn6 Ni1 Sn8 Sn4 -20.66(4) .
Sn2 Ni1 Sn8 Sn4 -160.36(3) .
Sn7 Ni1 Sn8 Sn4 61.28(2) .
Sn1 Ni1 Sn8 Sn4 123.97(2) .
Sn9 Ni1 Sn8 Sn4 -119.62(4) .
Sn3 Ni1 Sn8 Sn5 -142.87(6) .
Sn6 Ni1 Sn8 Sn5 56.28(4) .
Sn2 Ni1 Sn8 Sn5 -83.42(2) .
Sn7 Ni1 Sn8 Sn5 138.22(3) .
Sn1 Ni1 Sn8 Sn5 -159.09(3) .
Sn4 Ni1 Sn8 Sn5 76.940(19) .
Sn9 Ni1 Sn8 Sn5 -42.68(3) .
Sn9 Sn2 Sn8 Ni1 -29.81(2) .
Sn1 Sn2 Sn8 Ni1 66.41(2) .
Sn5 Sn2 Sn8 Ni1 -61.56(2) .
Sn3 Sn2 Sn8 Ni1 23.33(2) .
Ni1 Sn2 Sn8 Sn1 -66.41(2) .
Sn9 Sn2 Sn8 Sn1 -96.223(19) .
Sn5 Sn2 Sn8 Sn1 -127.968(17) .
Sn3 Sn2 Sn8 Sn1 -43.079(14) .
Ni1 Sn2 Sn8 Sn4 16.85(2) .
Sn9 Sn2 Sn8 Sn4 -12.96(2) .
Sn1 Sn2 Sn8 Sn4 83.260(18) .
Sn5 Sn2 Sn8 Sn4 -44.708(15) .
Sn3 Sn2 Sn8 Sn4 40.181(18) .
Ni1 Sn2 Sn8 Sn5 61.56(2) .
Sn9 Sn2 Sn8 Sn5 31.745(16) .
Sn1 Sn2 Sn8 Sn5 127.968(17) .
Sn3 Sn2 Sn8 Sn5 84.889(14) .
Sn2 Sn1 Sn8 Ni1 -65.30(2) .
Sn7 Sn1 Sn8 Ni1 47.09(2) .
Sn3 Sn1 Sn8 Ni1 -9.00(2) .
K5 Sn1 Sn8 Ni1 62.40(6) .
Ni1 Sn1 Sn8 Sn2 65.30(2) .
Sn7 Sn1 Sn8 Sn2 112.388(16) .
Sn3 Sn1 Sn8 Sn2 56.301(17) .
K5 Sn1 Sn8 Sn2 127.70(7) .
Ni1 Sn1 Sn8 Sn4 -43.11(2) .
Sn2 Sn1 Sn8 Sn4 -108.411(16) .
Sn7 Sn1 Sn8 Sn4 3.977(15) .
Sn3 Sn1 Sn8 Sn4 -52.110(19) .
K5 Sn1 Sn8 Sn4 19.29(7) .
Ni1 Sn1 Sn8 Sn5 17.32(2) .
Sn2 Sn1 Sn8 Sn5 -47.977(16) .
Sn7 Sn1 Sn8 Sn5 64.410(18) .
Sn3 Sn1 Sn8 Sn5 8.32(2) .
K5 Sn1 Sn8 Sn5 79.72(7) .
Sn6 Sn4 Sn8 Ni1 12.33(2) .
Sn7 Sn4 Sn8 Ni1 -46.94(2) .
Sn5 Sn4 Sn8 Ni1 63.59(2) .
K4 Sn4 Sn8 Ni1 93.19(2) .
Ni1 Sn4 Sn8 Sn2 -16.64(2) .
Sn6 Sn4 Sn8 Sn2 -4.31(2) .
Sn7 Sn4 Sn8 Sn2 -63.585(18) .
Sn5 Sn4 Sn8 Sn2 46.948(16) .
K4 Sn4 Sn8 Sn2 76.547(19) .
Ni1 Sn4 Sn8 Sn1 42.92(2) .
Sn6 Sn4 Sn8 Sn1 55.252(19) .
Sn7 Sn4 Sn8 Sn1 -4.020(16) .
Sn5 Sn4 Sn8 Sn1 106.513(16) .
K4 Sn4 Sn8 Sn1 136.112(15) .
Ni1 Sn4 Sn8 Sn5 -63.59(2) .
Sn6 Sn4 Sn8 Sn5 -51.260(16) .
Sn7 Sn4 Sn8 Sn5 -110.533(16) .
K4 Sn4 Sn8 Sn5 29.599(14) .
Sn9 Sn5 Sn8 Ni1 31.17(2) .
Sn4 Sn5 Sn8 Ni1 -66.73(2) .
Sn2 Sn5 Sn8 Ni1 63.00(2) .
Sn6 Sn5 Sn8 Ni1 -25.29(2) .
K4 Sn5 Sn8 Ni1 -96.79(2) .
Ni1 Sn5 Sn8 Sn2 -63.00(2) .
Sn9 Sn5 Sn8 Sn2 -31.827(16) .
Sn4 Sn5 Sn8 Sn2 -129.724(17) .
Sn6 Sn5 Sn8 Sn2 -88.285(16) .
K4 Sn5 Sn8 Sn2 -159.791(17) .
Ni1 Sn5 Sn8 Sn1 -17.72(2) .
Sn9 Sn5 Sn8 Sn1 13.45(2) .
Sn4 Sn5 Sn8 Sn1 -84.445(18) .
Sn2 Sn5 Sn8 Sn1 45.279(16) .
Sn6 Sn5 Sn8 Sn1 -43.006(19) .
K4 Sn5 Sn8 Sn1 -114.512(17) .
Ni1 Sn5 Sn8 Sn4 66.73(2) .
Sn9 Sn5 Sn8 Sn4 97.897(17) .
Sn2 Sn5 Sn8 Sn4 129.724(17) .
Sn6 Sn5 Sn8 Sn4 41.439(14) .
K4 Sn5 Sn8 Sn4 -30.067(14) .
Sn3 Ni1 Sn9 Sn5 -178.39(3) .
Sn6 Ni1 Sn9 Sn5 -90.65(2) .
Sn2 Ni1 Sn9 Sn5 85.16(2) .
Sn7 Ni1 Sn9 Sn5 -137.19(4) .
Sn1 Ni1 Sn9 Sn5 131.77(4) .
Sn8 Ni1 Sn9 Sn5 43.91(3) .
Sn4 Ni1 Sn9 Sn5 -45.71(3) .
Sn5 Ni1 Sn9 Sn3 178.39(3) .
Sn6 Ni1 Sn9 Sn3 87.73(2) .
Sn2 Ni1 Sn9 Sn3 -96.45(2) .
Sn7 Ni1 Sn9 Sn3 41.20(3) .
Sn1 Ni1 Sn9 Sn3 -49.84(3) .
Sn8 Ni1 Sn9 Sn3 -137.70(4) .
Sn4 Ni1 Sn9 Sn3 132.68(4) .
Sn5 Ni1 Sn9 Sn2 -85.16(2) .
Sn3 Ni1 Sn9 Sn2 96.45(2) .
Sn6 Ni1 Sn9 Sn2 -175.82(3) .
Sn7 Ni1 Sn9 Sn2 137.65(4) .
Sn1 Ni1 Sn9 Sn2 46.61(3) .
Sn8 Ni1 Sn9 Sn2 -41.25(3) .
Sn4 Ni1 Sn9 Sn2 -130.87(4) .
Sn5 Ni1 Sn9 Sn6 90.65(2) .
Sn3 Ni1 Sn9 Sn6 -87.73(2) .
Sn2 Ni1 Sn9 Sn6 175.82(3) .
Sn7 Ni1 Sn9 Sn6 -46.53(3) .
Sn1 Ni1 Sn9 Sn6 -137.58(4) .
Sn8 Ni1 Sn9 Sn6 134.56(4) .
Sn4 Ni1 Sn9 Sn6 44.94(3) .
Sn8 Sn5 Sn9 Ni1 -29.85(2) .
Sn4 Sn5 Sn9 Ni1 31.24(2) .
Sn2 Sn5 Sn9 Ni1 -61.42(2) .
Sn6 Sn5 Sn9 Ni1 58.64(2) .
K4 Sn5 Sn9 Ni1 101.27(2) .
Ni1 Sn5 Sn9 Sn3 -1.36(2) .
Sn8 Sn5 Sn9 Sn3 -31.21(2) .
Sn4 Sn5 Sn9 Sn3 29.88(2) .
Sn2 Sn5 Sn9 Sn3 -62.776(17) .
Sn6 Sn5 Sn9 Sn3 57.279(16) .
K4 Sn5 Sn9 Sn3 99.914(17) .
Ni1 Sn5 Sn9 Sn2 61.42(2) .
Sn8 Sn5 Sn9 Sn2 31.569(15) .
Sn4 Sn5 Sn9 Sn2 92.660(17) .
Sn6 Sn5 Sn9 Sn2 120.055(16) .
K4 Sn5 Sn9 Sn2 162.689(16) .
Ni1 Sn5 Sn9 Sn6 -58.64(2) .
Sn8 Sn5 Sn9 Sn6 -88.486(16) .
Sn4 Sn5 Sn9 Sn6 -27.394(15) .
Sn2 Sn5 Sn9 Sn6 -120.055(16) .
K4 Sn5 Sn9 Sn6 42.635(14) .
Sn7 Sn3 Sn9 Ni1 -28.23(2) .
Sn1 Sn3 Sn9 Ni1 34.02(2) .
Sn6 Sn3 Sn9 Ni1 -59.89(2) .
Sn2 Sn3 Sn9 Ni1 56.41(2) .
K5 Sn3 Sn9 Ni1 64.93(5) .
Ni1 Sn3 Sn9 Sn5 1.36(2) .
Sn7 Sn3 Sn9 Sn5 -26.87(2) .
Sn1 Sn3 Sn9 Sn5 35.37(2) .
Sn6 Sn3 Sn9 Sn5 -58.538(16) .
Sn2 Sn3 Sn9 Sn5 57.768(15) .
K5 Sn3 Sn9 Sn5 66.29(5) .
Ni1 Sn3 Sn9 Sn2 -56.41(2) .
Sn7 Sn3 Sn9 Sn2 -84.637(18) .
Sn1 Sn3 Sn9 Sn2 -22.393(17) .
Sn6 Sn3 Sn9 Sn2 -116.306(16) .
K5 Sn3 Sn9 Sn2 8.52(5) .
Ni1 Sn3 Sn9 Sn6 59.89(2) .
Sn7 Sn3 Sn9 Sn6 31.669(16) .
Sn1 Sn3 Sn9 Sn6 93.913(17) .
Sn2 Sn3 Sn9 Sn6 116.306(16) .
K5 Sn3 Sn9 Sn6 124.83(5) .
Sn8 Sn2 Sn9 Ni1 28.95(2) .
Sn1 Sn2 Sn9 Ni1 -33.24(2) .
Sn5 Sn2 Sn9 Ni1 61.32(2) .
Sn3 Sn2 Sn9 Ni1 -56.35(2) .
Ni1 Sn2 Sn9 Sn5 -61.32(2) .
Sn8 Sn2 Sn9 Sn5 -32.372(16) .
Sn1 Sn2 Sn9 Sn5 -94.555(18) .
Sn3 Sn2 Sn9 Sn5 -117.668(16) .
Ni1 Sn2 Sn9 Sn3 56.35(2) .
Sn8 Sn2 Sn9 Sn3 85.296(18) .
Sn1 Sn2 Sn9 Sn3 23.113(17) .
Sn5 Sn2 Sn9 Sn3 117.668(16) .
Ni1 Sn2 Sn9 Sn6 -3.49(2) .
Sn8 Sn2 Sn9 Sn6 25.45(2) .
Sn1 Sn2 Sn9 Sn6 -36.73(2) .
Sn5 Sn2 Sn9 Sn6 57.826(16) .
Sn3 Sn2 Sn9 Sn6 -59.842(16) .
Sn4 Sn6 Sn9 Ni1 -31.27(2) .
Sn7 Sn6 Sn9 Ni1 30.07(2) .
Sn3 Sn6 Sn9 Ni1 60.40(2) .
Sn5 Sn6 Sn9 Ni1 -59.10(2) .
K4 Sn6 Sn9 Ni1 -93.89(2) .
Ni1 Sn6 Sn9 Sn5 59.10(2) .
Sn4 Sn6 Sn9 Sn5 27.820(16) .
Sn7 Sn6 Sn9 Sn5 89.170(16) .
Sn3 Sn6 Sn9 Sn5 119.495(15) .
K4 Sn6 Sn9 Sn5 -34.793(12) .
Ni1 Sn6 Sn9 Sn3 -60.40(2) .
Sn4 Sn6 Sn9 Sn3 -91.675(17) .
Sn7 Sn6 Sn9 Sn3 -30.326(15) .
Sn5 Sn6 Sn9 Sn3 -119.495(15) .
K4 Sn6 Sn9 Sn3 -154.288(13) .
Ni1 Sn6 Sn9 Sn2 3.51(2) .
Sn4 Sn6 Sn9 Sn2 -27.76(2) .
Sn7 Sn6 Sn9 Sn2 33.59(2) .
Sn3 Sn6 Sn9 Sn2 63.914(17) .
Sn5 Sn6 Sn9 Sn2 -55.582(16) .
K4 Sn6 Sn9 Sn2 -90.375(17) .
O6 K1 N1 C13 -34.6(4) .
O2 K1 N1 C13 -154.0(3) .
O5 K1 N1 C13 -20.4(3) .
O3 K1 N1 C13 102.5(3) .
O1 K1 N1 C13 -138.4(4) .
O4 K1 N1 C13 88.2(3) .
N2 K1 N1 C13 86(10) .
O6 K1 N1 C7 -153.4(3) .
O2 K1 N1 C7 87.1(3) .
O5 K1 N1 C7 -139.2(4) .
O3 K1 N1 C7 -16.3(3) .
O1 K1 N1 C7 102.7(4) .
O4 K1 N1 C7 -30.7(4) .
N2 K1 N1 C7 -33(10) .
O6 K1 N1 C1 85.3(3) .
O2 K1 N1 C1 -34.1(4) .
O5 K1 N1 C1 99.6(3) .
O3 K1 N1 C1 -137.6(4) .
O1 K1 N1 C1 -18.5(3) .
O4 K1 N1 C1 -151.9(3) .
N2 K1 N1 C1 -154(9) .
O6 K1 N2 C6 -133.8(4) .
O2 K1 N2 C6 -15.2(3) .
O5 K1 N2 C6 -148.9(3) .
O3 K1 N2 C6 88.8(4) .
O1 K1 N2 C6 -30.0(4) .
O4 K1 N2 C6 103.0(4) .
N1 K1 N2 C6 105(10) .
O6 K1 N2 C12 106.4(4) .
O2 K1 N2 C12 -135.0(4) .
O5 K1 N2 C12 91.4(4) .
O3 K1 N2 C12 -31.0(4) .
O1 K1 N2 C12 -149.8(3) .
O4 K1 N2 C12 -16.8(3) .
N1 K1 N2 C12 -15(10) .
O6 K1 N2 C18 -13.8(3) .
O2 K1 N2 C18 104.9(4) .
O5 K1 N2 C18 -28.8(4) .
O3 K1 N2 C18 -151.1(3) .
O1 K1 N2 C18 90.0(4) .
O4 K1 N2 C18 -136.9(4) .
N1 K1 N2 C18 -135(10) .
O6 K1 O1 C2 -123.5(3) .
O2 K1 O1 C2 151.3(4) .
O5 K1 O1 C2 -64.6(3) .
O3 K1 O1 C2 37.4(3) .
O4 K1 O1 C2 87.8(4) .
N1 K1 O1 C2 -12.7(3) .
N2 K1 O1 C2 166.7(3) .
O6 K1 O1 C3 100.0(3) .
O2 K1 O1 C3 14.9(3) .
O5 K1 O1 C3 159.0(3) .
O3 K1 O1 C3 -99.0(3) .
O4 K1 O1 C3 -48.6(4) .
N1 K1 O1 C3 -149.1(4) .
N2 K1 O1 C3 30.2(4) .
O6 K1 O2 C4 -96.2(3) .
O5 K1 O2 C4 -45.7(4) .
O3 K1 O2 C4 101.6(3) .
O1 K1 O2 C4 17.4(3) .
O4 K1 O2 C4 161.2(3) .
N1 K1 O2 C4 33.4(4) .
N2 K1 O2 C4 -147.4(4) .
O6 K1 O2 C5 35.2(4) .
O5 K1 O2 C5 85.7(4) .
O3 K1 O2 C5 -127.0(3) .
O1 K1 O2 C5 148.8(4) .
O4 K1 O2 C5 -67.4(4) .
N1 K1 O2 C5 164.8(3) .
N2 K1 O2 C5 -16.0(3) .
O6 K1 O3 C9 -51.8(4) .
O2 K1 O3 C9 98.2(4) .
O5 K1 O3 C9 -102.7(4) .
O1 K1 O3 C9 157.5(4) .
O4 K1 O3 C9 13.4(3) .
N1 K1 O3 C9 -151.8(4) .
N2 K1 O3 C9 28.0(4) .
O6 K1 O3 C8 85.7(4) .
O2 K1 O3 C8 -124.3(4) .
O5 K1 O3 C8 34.8(4) .
O1 K1 O3 C8 -65.0(4) .
O4 K1 O3 C8 151.0(4) .
N1 K1 O3 C8 -14.2(4) .
N2 K1 O3 C8 165.5(4) .
O6 K1 O4 C10 166.3(3) .
O2 K1 O4 C10 -93.3(3) .
O5 K1 O4 C10 106.2(3) .
O3 K1 O4 C10 20.4(3) .
O1 K1 O4 C10 -42.5(4) .
N1 K1 O4 C10 34.9(4) .
N2 K1 O4 C10 -145.1(4) .
O6 K1 O4 C11 -63.1(4) .
O2 K1 O4 C11 37.4(4) .
O5 K1 O4 C11 -123.2(4) .
O3 K1 O4 C11 151.0(4) .
O1 K1 O4 C11 88.1(4) .
N1 K1 O4 C11 165.6(3) .
N2 K1 O4 C11 -14.5(3) .
O6 K1 O5 C15 21.7(3) .
O2 K1 O5 C15 -41.8(4) .
O3 K1 O5 C15 168.3(4) .
O1 K1 O5 C15 -92.3(4) .
O4 K1 O5 C15 107.7(4) .
N1 K1 O5 C15 -143.7(4) .
N2 K1 O5 C15 37.2(4) .
O6 K1 O5 C14 155.4(4) .
O2 K1 O5 C14 92.0(4) .
O3 K1 O5 C14 -58.0(4) .
O1 K1 O5 C14 41.5(4) .
O4 K1 O5 C14 -118.5(4) .
N1 K1 O5 C14 -10.0(3) .
N2 K1 O5 C14 170.9(3) .
O2 K1 O6 C17 -69.4(4) .
O5 K1 O6 C17 146.7(4) .
O3 K1 O6 C17 83.2(4) .
O1 K1 O6 C17 -129.0(4) .
O4 K1 O6 C17 30.7(4) .
N1 K1 O6 C17 161.4(4) .
N2 K1 O6 C17 -17.8(4) .
O2 K1 O6 C16 154.8(4) .
O5 K1 O6 C16 10.9(4) .
O3 K1 O6 C16 -52.6(5) .
O1 K1 O6 C16 95.2(4) .
O4 K1 O6 C16 -105.1(4) .
N1 K1 O6 C16 25.6(4) .
N2 K1 O6 C16 -153.6(4) .
C13 N1 C1 C2 168.3(5) .
C7 N1 C1 C2 -72.7(6) .
K1 N1 C1 C2 50.2(5) .
C3 O1 C2 C1 -179.4(4) .
K1 O1 C2 C1 41.9(5) .
N1 C1 C2 O1 -63.9(6) .
C2 O1 C3 C4 177.3(4) .
K1 O1 C3 C4 -44.0(5) .
C5 O2 C4 C3 179.4(5) .
K1 O2 C4 C3 -46.7(5) .
O1 C3 C4 O2 59.6(6) .
C4 O2 C5 C6 -180.0(5) .
K1 O2 C5 C6 45.5(6) .
C12 N2 C6 C5 166.7(5) .
C18 N2 C6 C5 -73.0(6) .
K1 N2 C6 C5 46.6(5) .
O2 C5 C6 N2 -64.5(7) .
C13 N1 C7 C8 -72.7(6) .
C1 N1 C7 C8 166.8(5) .
K1 N1 C7 C8 45.9(6) .
C9 O3 C8 C7 -178.0(5) .
K1 O3 C8 C7 41.9(6) .
N1 C7 C8 O3 -59.2(7) .
C8 O3 C9 C10 175.6(5) .
K1 O3 C9 C10 -43.7(5) .
C11 O4 C10 C9 175.3(5) .
K1 O4 C10 C9 -51.4(5) .
O3 C9 C10 O4 63.4(6) .
C10 O4 C11 C12 175.9(5) .
K1 O4 C11 C12 43.8(5) .
C6 N2 C12 C11 -71.3(6) .
C18 N2 C12 C11 168.1(5) .
K1 N2 C12 C11 48.0(5) .
O4 C11 C12 N2 -63.5(6) .
C7 N1 C13 C14 173.2(5) .
C1 N1 C13 C14 -67.0(6) .
K1 N1 C13 C14 51.9(5) .
C15 O5 C14 C13 174.0(5) .
K1 O5 C14 C13 38.8(5) .
N1 C13 C14 O5 -63.9(6) .
C14 O5 C15 C16 172.5(5) .
K1 O5 C15 C16 -51.6(5) .
C17 O6 C16 C15 -178.3(5) .
K1 O6 C16 C15 -40.1(6) .
O5 C15 C16 O6 60.0(6) .
C16 O6 C17 C18 -173.6(5) .
K1 O6 C17 C18 47.1(6) .
C6 N2 C18 C17 164.4(5) .
C12 N2 C18 C17 -75.4(6) .
K1 N2 C18 C17 45.1(6) .
O6 C17 C18 N2 -63.8(7) .
O11 K2 N3 C24 -143.5(4) .
O9 K2 N3 C24 98.7(4) .
O8 K2 N3 C24 -14.6(3) .
O12 K2 N3 C24 -132.5(4) .
O10 K2 N3 C24 110.5(4) .
O7 K2 N3 C24 -25.9(4) .
N4 K2 N3 C24 3(8) .
O11 K2 N3 C36 -23.1(5) .
O9 K2 N3 C36 -140.9(4) .
O8 K2 N3 C36 105.8(4) .
O12 K2 N3 C36 -12.1(4) .
O10 K2 N3 C36 -129.1(4) .
O7 K2 N3 C36 94.5(4) .
N4 K2 N3 C36 124(7) .
O11 K2 N3 C30 98.1(4) .
O9 K2 N3 C30 -19.7(4) .
O8 K2 N3 C30 -133.0(4) .
O12 K2 N3 C30 109.0(4) .
O10 K2 N3 C30 -8.0(3) .
O7 K2 N3 C30 -144.4(3) .
N4 K2 N3 C30 -115(7) .
O11 K2 N4 C19 109.4(4) .
O9 K2 N4 C19 -133.8(4) .
O8 K2 N4 C19 -20.0(4) .
O12 K2 N4 C19 97.7(4) .
O10 K2 N4 C19 -144.3(3) .
O7 K2 N4 C19 -8.2(3) .
N3 K2 N4 C19 -38(8) .
O11 K2 N4 C25 -130.1(4) .
O9 K2 N4 C25 -13.3(3) .
O8 K2 N4 C25 100.5(3) .
O12 K2 N4 C25 -141.8(3) .
O10 K2 N4 C25 -23.8(4) .
O7 K2 N4 C25 112.3(4) .
N3 K2 N4 C25 83(8) .
O11 K2 N4 C31 -10.8(3) .
O9 K2 N4 C31 106.0(3) .
O8 K2 N4 C31 -140.2(3) .
O12 K2 N4 C31 -22.5(4) .
O10 K2 N4 C31 95.5(3) .
O7 K2 N4 C31 -128.4(4) .
N3 K2 N4 C31 -158(7) .
O11 K2 O7 C20 -76.6(3) .
O9 K2 O7 C20 20.0(4) .
O8 K2 O7 C20 142.5(4) .
O12 K2 O7 C20 -136.9(3) .
O10 K2 O7 C20 75.8(4) .
N4 K2 O7 C20 -25.7(3) .
N3 K2 O7 C20 153.7(3) .
O11 K2 O7 C21 155.0(3) .
O9 K2 O7 C21 -108.4(3) .
O8 K2 O7 C21 14.1(3) .
O12 K2 O7 C21 94.7(4) .
O10 K2 O7 C21 -52.6(4) .
N4 K2 O7 C21 -154.0(4) .
N3 K2 O7 C21 25.4(4) .
O11 K2 O8 C23 86.3(4) .
O9 K2 O8 C23 -125.8(4) .
O12 K2 O8 C23 32.7(4) .
O10 K2 O8 C23 -63.3(4) .
O7 K2 O8 C23 151.3(4) .
N4 K2 O8 C23 163.0(4) .
N3 K2 O8 C23 -17.4(4) .
O11 K2 O8 C22 -45.1(4) .
O9 K2 O8 C22 102.8(4) .
O12 K2 O8 C22 -98.7(4) .
O10 K2 O8 C22 165.3(4) .
O7 K2 O8 C22 19.9(3) .
N4 K2 O8 C22 31.5(4) .
N3 K2 O8 C22 -148.9(4) .
O11 K2 O9 C27 -97.1(3) .
O8 K2 O9 C27 104.6(3) .
O12 K2 O9 C27 -43.7(4) .
O10 K2 O9 C27 21.2(3) .
O7 K2 O9 C27 166.3(3) .
N4 K2 O9 C27 -148.5(4) .
N3 K2 O9 C27 32.7(4) .
O11 K2 O9 C26 33.2(4) .
O8 K2 O9 C26 -125.1(4) .
O12 K2 O9 C26 86.6(4) .
O10 K2 O9 C26 151.5(4) .
O7 K2 O9 C26 -63.4(4) .
N4 K2 O9 C26 -18.2(4) .
N3 K2 O9 C26 163.1(4) .
O11 K2 O10 C28 94.2(3) .
O9 K2 O10 C28 13.3(3) .
O8 K2 O10 C28 -109.0(3) .
O12 K2 O10 C28 154.2(3) .
O7 K2 O10 C28 -54.5(4) .
N4 K2 O10 C28 23.7(4) .
N3 K2 O10 C28 -155.1(4) .
O11 K2 O10 C29 -135.8(4) .
O9 K2 O10 C29 143.4(4) .
O8 K2 O10 C29 21.0(4) .
O12 K2 O10 C29 -75.7(4) .
O7 K2 O10 C29 75.6(4) .
N4 K2 O10 C29 153.7(4) .
N3 K2 O10 C29 -25.1(4) .
O9 K2 O11 C33 155.1(4) .
O8 K2 O11 C33 -51.5(4) .
O12 K2 O11 C33 14.5(4) .
O10 K2 O11 C33 94.4(4) .
O7 K2 O11 C33 -104.2(4) .
N4 K2 O11 C33 -154.0(4) .
N3 K2 O11 C33 25.3(4) .
O9 K2 O11 C32 -73.5(4) .
O8 K2 O11 C32 80.0(4) .
O12 K2 O11 C32 146.0(4) .
O10 K2 O11 C32 -134.1(3) .
O7 K2 O11 C32 27.3(4) .
N4 K2 O11 C32 -22.6(3) .
N3 K2 O11 C32 156.7(3) .
O11 K2 O12 C34 19.8(4) .
O9 K2 O12 C34 -45.9(5) .
O8 K2 O12 C34 160.4(4) .
O10 K2 O12 C34 -98.9(4) .
O7 K2 O12 C34 100.4(4) .
N4 K2 O12 C34 31.5(4) .
N3 K2 O12 C34 -149.4(4) .
O11 K2 O12 C35 148.0(5) .
O9 K2 O12 C35 82.3(5) .
O8 K2 O12 C35 -71.5(4) .
O10 K2 O12 C35 29.2(4) .
O7 K2 O12 C35 -131.5(4) .
N4 K2 O12 C35 159.6(4) .
N3 K2 O12 C35 -21.2(4) .
C25 N4 C19 C20 -80.6(6) .
C31 N4 C19 C20 159.1(5) .
K2 N4 C19 C20 39.7(5) .
C21 O7 C20 C19 -172.7(5) .
K2 O7 C20 C19 58.0(5) .
N4 C19 C20 O7 -66.3(6) .
C20 O7 C21 C22 -176.2(5) .
K2 O7 C21 C22 -45.6(5) .
C23 O8 C22 C21 171.1(5) .
K2 O8 C22 C21 -53.0(5) .
O7 C21 C22 O8 67.9(6) .
C22 O8 C23 C24 179.7(5) .
K2 O8 C23 C24 47.2(6) .
C36 N3 C24 C23 -73.5(7) .
C30 N3 C24 C23 164.2(5) .
K2 N3 C24 C23 45.2(6) .
O8 C23 C24 N3 -63.8(7) .
C19 N4 C25 C26 164.8(5) .
C31 N4 C25 C26 -75.2(6) .
K2 N4 C25 C26 43.1(5) .
C27 O9 C26 C25 179.4(5) .
K2 O9 C26 C25 48.4(6) .
N4 C25 C26 O9 -62.2(7) .
C26 O9 C27 C28 171.4(5) .
K2 O9 C27 C28 -53.7(5) .
C29 O10 C28 C27 -177.6(5) .
K2 O10 C28 C27 -45.7(5) .
O9 C27 C28 O10 68.8(6) .
C28 O10 C29 C30 -172.6(5) .
K2 O10 C29 C30 57.1(6) .
C24 N3 C30 C29 -78.3(6) .
C36 N3 C30 C29 159.2(5) .
K2 N3 C30 C29 39.4(6) .
O10 C29 C30 N3 -65.8(7) .
C19 N4 C31 C32 -79.1(6) .
C25 N4 C31 C32 161.0(5) .
K2 N4 C31 C32 42.2(5) .
C33 O11 C32 C31 -172.3(5) .
K2 O11 C32 C31 54.6(5) .
N4 C31 C32 O11 -66.4(6) .
C32 O11 C33 C34 179.1(5) .
K2 O11 C33 C34 -46.6(6) .
C35 O12 C34 C33 176.0(6) .
K2 O12 C34 C33 -51.7(6) .
O11 C33 C34 O12 67.3(7) .
C34 O12 C35 C36 -178.2(6) .
K2 O12 C35 C36 52.7(7) .
C24 N3 C36 C35 162.4(6) .
C30 N3 C36 C35 -76.4(7) .
K2 N3 C36 C35 44.2(7) .
O12 C35 C36 N3 -66.2(8) .
O13 K3 N5 C37 -11.3(3) .
O17 K3 N5 C37 103.2(4) .
O16 K3 N5 C37 -147.2(3) .
O18 K3 N5 C37 90.5(3) .
O14 K3 N5 C37 -24.6(4) .
O15 K3 N5 C37 -134.4(4) .
N6 K3 N5 C37 -165(6) .
O13 K3 N5 C49 -131.6(4) .
O17 K3 N5 C49 -17.1(3) .
O16 K3 N5 C49 92.5(4) .
O18 K3 N5 C49 -29.7(4) .
O14 K3 N5 C49 -144.9(3) .
O15 K3 N5 C49 105.3(4) .
N6 K3 N5 C49 75(6) .
O13 K3 N5 C43 108.2(3) .
O17 K3 N5 C43 -137.3(4) .
O16 K3 N5 C43 -27.7(4) .
O18 K3 N5 C43 -149.9(3) .
O14 K3 N5 C43 94.9(3) .
O15 K3 N5 C43 -14.9(3) .
N6 K3 N5 C43 -45(6) .
O13 K3 N6 C54 91.4(3) .
O17 K3 N6 C54 -24.1(4) .
O16 K3 N6 C54 -133.2(3) .
O18 K3 N6 C54 -10.0(3) .
O14 K3 N6 C54 104.0(3) .
O15 K3 N6 C54 -145.4(3) .
N5 K3 N6 C54 -115(6) .
O13 K3 N6 C42 -28.6(4) .
O17 K3 N6 C42 -144.2(3) .
O16 K3 N6 C42 106.8(4) .
O18 K3 N6 C42 -130.1(4) .
O14 K3 N6 C42 -16.1(3) .
O15 K3 N6 C42 94.5(3) .
N5 K3 N6 C42 125(6) .
O13 K3 N6 C48 -147.8(3) .
O17 K3 N6 C48 96.7(3) .
O16 K3 N6 C48 -12.4(3) .
O18 K3 N6 C48 110.7(3) .
O14 K3 N6 C48 -135.3(4) .
O15 K3 N6 C48 -24.6(4) .
N5 K3 N6 C48 6(6) .
O17 K3 O13 C39 152.3(4) .
O16 K3 O13 C39 -54.9(4) .
O18 K3 O13 C39 93.0(4) .
O14 K3 O13 C39 11.7(3) .
O15 K3 O13 C39 -107.3(4) .
N5 K3 O13 C39 -154.9(4) .
N6 K3 O13 C39 24.4(4) .
O17 K3 O13 C38 -74.2(3) .
O16 K3 O13 C38 78.5(4) .
O18 K3 O13 C38 -133.6(3) .
O14 K3 O13 C38 145.2(4) .
O15 K3 O13 C38 26.2(3) .
N5 K3 O13 C38 -21.5(3) .
N6 K3 O13 C38 157.9(3) .
O13 K3 O14 C40 23.4(3) .
O17 K3 O14 C40 -40.1(4) .
O16 K3 O14 C40 167.8(3) .
O18 K3 O14 C40 -90.9(3) .
O15 K3 O14 C40 107.7(3) .
N5 K3 O14 C40 36.9(4) .
N6 K3 O14 C40 -144.0(4) .
O13 K3 O14 C41 151.3(4) .
O17 K3 O14 C41 87.9(4) .
O16 K3 O14 C41 -64.3(4) .
O18 K3 O14 C41 37.0(4) .
O15 K3 O14 C41 -124.3(3) .
N5 K3 O14 C41 164.8(3) .
N6 K3 O14 C41 -16.1(3) .
O13 K3 O15 C44 -64.5(3) .
O17 K3 O15 C44 32.1(3) .
O16 K3 O15 C44 150.7(4) .
O18 K3 O15 C44 85.1(4) .
O14 K3 O15 C44 -125.5(3) .
N5 K3 O15 C44 -16.1(3) .
N6 K3 O15 C44 163.1(3) .
O13 K3 O15 C45 164.3(3) .
O17 K3 O15 C45 -99.1(3) .
O16 K3 O15 C45 19.5(3) .
O18 K3 O15 C45 -46.1(4) .
O14 K3 O15 C45 103.3(3) .
N5 K3 O15 C45 -147.4(4) .
N6 K3 O15 C45 31.9(4) .
O13 K3 O16 C46 -51.4(4) .
O17 K3 O16 C46 97.1(3) .
O18 K3 O16 C46 158.4(3) .
O14 K3 O16 C46 -105.2(3) .
O15 K3 O16 C46 13.9(3) .
N5 K3 O16 C46 26.8(4) .
N6 K3 O16 C46 -153.6(4) .
O13 K3 O16 C47 83.7(4) .
O17 K3 O16 C47 -127.8(3) .
O18 K3 O16 C47 -66.5(3) .
O14 K3 O16 C47 29.9(3) .
O15 K3 O16 C47 149.0(4) .
N5 K3 O16 C47 161.9(3) .
N6 K3 O16 C47 -18.5(3) .
O13 K3 O17 C50 39.6(4) .
O16 K3 O17 C50 -121.3(4) .
O18 K3 O17 C50 153.6(4) .
O14 K3 O17 C50 90.5(4) .
O15 K3 O17 C50 -61.7(4) .
N5 K3 O17 C50 -13.7(4) .
N6 K3 O17 C50 167.8(4) .
O13 K3 O17 C51 -94.6(4) .
O16 K3 O17 C51 104.5(4) .
O18 K3 O17 C51 19.4(3) .
O14 K3 O17 C51 -43.7(4) .
O15 K3 O17 C51 164.1(3) .
N5 K3 O17 C51 -147.9(4) .
N6 K3 O17 C51 33.6(4) .
O13 K3 O18 C53 -135.5(3) .
O17 K3 O18 C53 142.8(4) .
O16 K3 O18 C53 24.9(3) .
O14 K3 O18 C53 -76.4(3) .
O15 K3 O18 C53 77.4(4) .
N5 K3 O18 C53 155.5(3) .
N6 K3 O18 C53 -23.1(3) .
O13 K3 O18 C52 95.8(4) .
O17 K3 O18 C52 14.0(3) .
O16 K3 O18 C52 -103.9(3) .
O14 K3 O18 C52 154.8(3) .
O15 K3 O18 C52 -51.4(4) .
N5 K3 O18 C52 26.7(4) .
N6 K3 O18 C52 -151.8(4) .
C49 N5 C37 C38 162.0(5) .
C43 N5 C37 C38 -77.6(6) .
K3 N5 C37 C38 42.9(5) .
C39 O13 C38 C37 -171.5(5) .
K3 O13 C38 C37 52.1(5) .
N5 C37 C38 O13 -65.5(6) .
C38 O13 C39 C40 -179.7(4) .
K3 O13 C39 C40 -43.9(5) .
C41 O14 C40 C39 174.8(4) .
K3 O14 C40 C39 -55.2(4) .
O13 C39 C40 O14 67.0(5) .
C40 O14 C41 C42 174.6(4) .
K3 O14 C41 C42 46.8(5) .
C54 N6 C42 C41 -72.2(6) .
C48 N6 C42 C41 167.8(5) .
K3 N6 C42 C41 48.3(5) .
O14 C41 C42 N6 -66.7(6) .
C37 N5 C43 C44 164.9(5) .
C49 N5 C43 C44 -74.1(6) .
K3 N5 C43 C44 45.4(5) .
C45 O15 C44 C43 178.2(5) .
K3 O15 C44 C43 45.3(5) .
N5 C43 C44 O15 -62.5(6) .
C44 O15 C45 C46 175.9(5) .
K3 O15 C45 C46 -49.9(5) .
C47 O16 C46 C45 177.5(4) .
K3 O16 C46 C45 -44.4(5) .
O15 C45 C46 O16 62.4(6) .
C46 O16 C47 C48 -174.1(4) .
K3 O16 C47 C48 47.6(5) .
C54 N6 C48 C47 164.3(5) .
C42 N6 C48 C47 -75.8(6) .
K3 N6 C48 C47 43.1(5) .
O16 C47 C48 N6 -62.2(6) .
C37 N5 C49 C50 -71.6(6) .
C43 N5 C49 C50 168.4(5) .
K3 N5 C49 C50 47.6(6) .
C51 O17 C50 C49 178.0(5) .
K3 O17 C50 C49 42.3(6) .
N5 C49 C50 O17 -62.1(7) .
C50 O17 C51 C52 171.5(5) .
K3 O17 C51 C52 -50.6(5) .
C53 O18 C52 C51 -174.7(4) .
K3 O18 C52 C51 -44.3(5) .
O17 C51 C52 O18 63.9(6) .
C52 O18 C53 C54 -174.3(4) .
K3 O18 C53 C54 54.6(5) .
C42 N6 C54 C53 161.2(5) .
C48 N6 C54 C53 -79.1(6) .
K3 N6 C54 C53 41.7(5) .
O18 C53 C54 N6 -66.8(6) .
Ni1 Sn5 K4 Sn5 143(6) 2
Sn9 Sn5 K4 Sn5 79(6) 2
Sn8 Sn5 K4 Sn5 -157(6) 2
Sn4 Sn5 K4 Sn5 176(6) 2
Sn2 Sn5 K4 Sn5 134(6) 2
Sn6 Sn5 K4 Sn5 116(6) 2
Ni1 Sn5 K4 Sn4 147.300(19) 2
Sn9 Sn5 K4 Sn4 83.792(17) 2
Sn8 Sn5 K4 Sn4 -152.074(14) 2
Sn4 Sn5 K4 Sn4 180.0 2
Sn2 Sn5 K4 Sn4 138.25(4) 2
Sn6 Sn5 K4 Sn4 120.302(12) 2
Ni1 Sn5 K4 Sn4 -32.699(19) .
Sn9 Sn5 K4 Sn4 -96.207(17) .
Sn8 Sn5 K4 Sn4 27.927(14) .
Sn2 Sn5 K4 Sn4 -41.75(4) .
Sn6 Sn5 K4 Sn4 -59.696(12) .
Ni1 Sn5 K4 Sn6 -153.002(19) 2
Sn9 Sn5 K4 Sn6 143.490(14) 2
Sn8 Sn5 K4 Sn6 -92.376(17) 2
Sn4 Sn5 K4 Sn6 -120.303(12) 2
Sn2 Sn5 K4 Sn6 -162.05(4) 2
Sn6 Sn5 K4 Sn6 180.0 2
Ni1 Sn5 K4 Sn6 26.997(19) .
Sn9 Sn5 K4 Sn6 -36.511(14) .
Sn8 Sn5 K4 Sn6 87.623(17) .
Sn4 Sn5 K4 Sn6 59.696(12) .
Sn2 Sn5 K4 Sn6 17.95(4) .
Ni1 Sn4 K4 Sn5 -148.770(19) 2
Sn8 Sn4 K4 Sn5 151.623(14) 2
Sn6 Sn4 K4 Sn5 -106.681(14) 2
Sn7 Sn4 K4 Sn5 -90.73(2) 2
Sn5 Sn4 K4 Sn5 180.0 2
Ni1 Sn4 K4 Sn5 31.230(19) .
Sn8 Sn4 K4 Sn5 -28.377(14) .
Sn6 Sn4 K4 Sn5 73.319(14) .
Sn7 Sn4 K4 Sn5 89.27(2) .
Ni1 Sn4 K4 Sn4 -49(3) 2
Sn8 Sn4 K4 Sn4 -108(3) 2
Sn6 Sn4 K4 Sn4 -7(3) 2
Sn7 Sn4 K4 Sn4 9(3) 2
Sn5 Sn4 K4 Sn4 -80(3) 2
Ni1 Sn4 K4 Sn6 137.913(19) 2
Sn8 Sn4 K4 Sn6 78.306(18) 2
Sn6 Sn4 K4 Sn6 180.0 2
Sn7 Sn4 K4 Sn6 -164.051(17) 2
Sn5 Sn4 K4 Sn6 106.683(14) 2
Ni1 Sn4 K4 Sn6 -42.088(19) .
Sn8 Sn4 K4 Sn6 -101.695(18) .
Sn7 Sn4 K4 Sn6 15.948(17) .
Sn5 Sn4 K4 Sn6 -73.319(14) .
Ni1 Sn6 K4 Sn5 154.619(19) 2
Sn9 Sn6 K4 Sn5 -146.557(12) 2
Sn4 Sn6 K4 Sn5 113.361(13) 2
Sn7 Sn6 K4 Sn5 100.534(16) 2
Sn3 Sn6 K4 Sn5 171.31(2) 2
Sn5 Sn6 K4 Sn5 180.0 2
Ni1 Sn6 K4 Sn5 -25.382(19) .
Sn9 Sn6 K4 Sn5 33.442(12) .
Sn4 Sn6 K4 Sn5 -66.640(13) .
Sn7 Sn6 K4 Sn5 -79.466(16) .
Sn3 Sn6 K4 Sn5 -8.69(2) .
Ni1 Sn6 K4 Sn4 -138.742(19) 2
Sn9 Sn6 K4 Sn4 -79.918(16) 2
Sn4 Sn6 K4 Sn4 180.0 2
Sn7 Sn6 K4 Sn4 167.173(14) 2
Sn3 Sn6 K4 Sn4 -122.05(2) 2
Sn5 Sn6 K4 Sn4 -113.361(13) 2
Ni1 Sn6 K4 Sn4 41.258(19) .
Sn9 Sn6 K4 Sn4 100.082(16) .
Sn7 Sn6 K4 Sn4 -12.827(14) .
Sn3 Sn6 K4 Sn4 57.95(2) .
Sn5 Sn6 K4 Sn4 66.640(13) .
Ni1 Sn6 K4 Sn6 133(2) 2
Sn9 Sn6 K4 Sn6 -169(2) 2
Sn4 Sn6 K4 Sn6 91(2) 2
Sn7 Sn6 K4 Sn6 78(2) 2
Sn3 Sn6 K4 Sn6 149(2) 2
Sn5 Sn6 K4 Sn6 158(2) 2
Ni1 Sn1 K5 Sn1 118(21) 2_556
Sn8 Sn1 K5 Sn1 63(21) 2_556
Sn2 Sn1 K5 Sn1 -178(21) 2_556
Sn7 Sn1 K5 Sn1 78(21) 2_556
Sn3 Sn1 K5 Sn1 139(21) 2_556
Ni1 Sn1 K5 Sn3 158.29(2) 2_556
Sn8 Sn1 K5 Sn3 103.46(6) 2_556
Sn2 Sn1 K5 Sn3 -137.262(18) 2_556
Sn7 Sn1 K5 Sn3 119.083(14) 2_556
Sn3 Sn1 K5 Sn3 180.0 2_556
Ni1 Sn1 K5 Sn3 -21.71(2) .
Sn8 Sn1 K5 Sn3 -76.55(6) .
Sn2 Sn1 K5 Sn3 42.737(18) .
Sn7 Sn1 K5 Sn3 -60.918(14) .
Ni1 Sn1 K5 Sn7 39.21(2) .
Sn8 Sn1 K5 Sn7 -15.63(6) .
Sn2 Sn1 K5 Sn7 103.66(2) .
Sn3 Sn1 K5 Sn7 60.918(14) .
Ni1 Sn1 K5 Sn7 -140.79(2) 2_556
Sn8 Sn1 K5 Sn7 164.37(6) 2_556
Sn2 Sn1 K5 Sn7 -76.35(2) 2_556
Sn7 Sn1 K5 Sn7 180.0 2_556
Sn3 Sn1 K5 Sn7 -119.083(14) 2_556
Ni1 Sn3 K5 Sn1 -158.84(2) 2_556
Sn9 Sn3 K5 Sn1 145.08(4) 2_556
Sn7 Sn3 K5 Sn1 -116.313(15) 2_556
Sn1 Sn3 K5 Sn1 180.0 2_556
Sn6 Sn3 K5 Sn1 -104.00(2) 2_556
Sn2 Sn3 K5 Sn1 152.214(13) 2_556
Ni1 Sn3 K5 Sn1 21.16(2) .
Sn9 Sn3 K5 Sn1 -34.92(4) .
Sn7 Sn3 K5 Sn1 63.687(15) .
Sn6 Sn3 K5 Sn1 76.00(2) .
Sn2 Sn3 K5 Sn1 -27.786(13) .
Ni1 Sn3 K5 Sn3 96(5) 2_556
Sn9 Sn3 K5 Sn3 40(5) 2_556
Sn7 Sn3 K5 Sn3 138(5) 2_556
Sn1 Sn3 K5 Sn3 75(5) 2_556
Sn6 Sn3 K5 Sn3 151(5) 2_556
Sn2 Sn3 K5 Sn3 47(5) 2_556
Ni1 Sn3 K5 Sn7 -42.53(2) .
Sn9 Sn3 K5 Sn7 -98.61(5) .
Sn1 Sn3 K5 Sn7 -63.687(15) .
Sn6 Sn3 K5 Sn7 12.310(15) .
Sn2 Sn3 K5 Sn7 -91.473(15) .
Ni1 Sn3 K5 Sn7 137.47(2) 2_556
Sn9 Sn3 K5 Sn7 81.39(5) 2_556
Sn7 Sn3 K5 Sn7 180.0 2_556
Sn1 Sn3 K5 Sn7 116.314(15) 2_556
Sn6 Sn3 K5 Sn7 -167.689(15) 2_556
Sn2 Sn3 K5 Sn7 88.527(15) 2_556
Ni1 Sn7 K5 Sn1 145.190(19) 2_556
Sn3 Sn7 K5 Sn1 106.469(15) 2_556
Sn4 Sn7 K5 Sn1 180.00(2) 2_556
Sn1 Sn7 K5 Sn1 180.0 2_556
Sn6 Sn7 K5 Sn1 94.608(19) 2_556
Ni1 Sn7 K5 Sn1 -34.811(19) .
Sn3 Sn7 K5 Sn1 -73.531(15) .
Sn4 Sn7 K5 Sn1 0.00(2) .
Sn6 Sn7 K5 Sn1 -85.392(19) .
Ni1 Sn7 K5 Sn3 -141.279(18) 2_556
Sn3 Sn7 K5 Sn3 180.0 2_556
Sn4 Sn7 K5 Sn3 -106.47(3) 2_556
Sn1 Sn7 K5 Sn3 -106.468(15) 2_556
Sn6 Sn7 K5 Sn3 168.140(15) 2_556
Ni1 Sn7 K5 Sn3 38.721(18) .
Sn4 Sn7 K5 Sn3 73.53(3) .
Sn1 Sn7 K5 Sn3 73.531(15) .
Sn6 Sn7 K5 Sn3 -11.861(15) .
Ni1 Sn7 K5 Sn7 -157(9) 2_556
Sn3 Sn7 K5 Sn7 164(68) 2_556
Sn4 Sn7 K5 Sn7 -123(9) 2_556
Sn1 Sn7 K5 Sn7 -123(9) 2_556
Sn6 Sn7 K5 Sn7 152(9) 2_556
