#------------------------------------------------------------------------------
#$Date: 2016-03-23 21:51:50 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179458 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/55/4335548.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4335548
loop_
_publ_author_name
'Yuji Kikukawa'
'Kosuke Suzuki'
'Kazuya Yamaguchi'
'Noritaka Mizuno'
_publ_contact_author_address
;
Department of Applied Chemistry
School of Engineering
the University of Tokyo
7-3-1 Hongo, Bunkyoku
Tokyo, JAPAN
;
_publ_contact_author_email       tmizuno@mail.ecc.u-tokyo.ac.jp
_publ_contact_author_fax         81-3-5841-7220
_publ_contact_author_name        'Noritaka Mizuno'
_publ_contact_author_phone       81-3-5841-7272
_publ_section_title
;
 Synthesis, Structure Characterization, and Reversible Transformation of a
 Cobalt Salt of a Dilacunary γ-Keggin Silicotungstate and Sandwich-Type
 Di- and Tetracobalt-Containing Silicotungstate Dimers
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8644
_journal_page_last               8652
_journal_paper_doi               10.1021/ic4008075
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         'C196 Co4 N16 O152 Si4 W40'
_chemical_formula_sum            'C196 Co4 N16 O152 Si4 W40'
_chemical_formula_weight         12712.2
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             2013-02-26T13:07:41-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                98.9830(10)
_cell_angle_beta                 97.0030(10)
_cell_angle_gamma                96.09
_cell_formula_units_Z            2
_cell_length_a                   24.29700(10)
_cell_length_b                   25.1429(2)
_cell_length_c                   27.2971(2)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    123
_cell_measurement_theta_max      0
_cell_measurement_theta_min      0
_cell_volume                     16214.6(2)
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1986)'
_diffrn_ambient_temperature      123
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.926
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            84219
_diffrn_reflns_theta_full        25
_diffrn_reflns_theta_max         29.56
_diffrn_reflns_theta_min         1.85
_exptl_absorpt_coefficient_mu    14.416
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.604
_exptl_crystal_description       prism
_exptl_crystal_F_000             11256
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_refine_diff_density_max         10.781
_refine_diff_density_min         -4.604
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2115
_refine_ls_number_reflns         84219
_refine_ls_number_restraints     63
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_gt           0.0571
_refine_ls_shift/su_max          0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0519P)²+549.4132P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1516
_reflns_number_gt                67398
_reflns_number_total             84219
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic4008075_si_001_3.cif
_cod_data_source_block           Co2
_cod_original_cell_volume        16214.75(19)
_cod_database_code               4335548
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
W1A W 0.395023(18) 0.012715(19) 0.323090(17) 0.02695(9) Uani 1 d .
W2A W 0.340511(18) 0.08391(2) 0.415775(18) 0.02857(9) Uani 1 d .
W3A W 0.612967(17) 0.047153(18) 0.454323(16) 0.02427(8) Uani 1 d .
W4A W 0.556956(19) 0.124996(18) 0.540427(16) 0.02604(9) Uani 1 d .
W5A W 0.545744(18) 0.018228(18) 0.325945(16) 0.02449(8) Uani 1 d .
W6A W 0.43292(2) 0.187277(19) 0.508522(18) 0.02964(9) Uani 1 d .
W7A W 0.48902(2) 0.124552(19) 0.295374(17) 0.02838(9) Uani 1 d .
W8A W 0.42285(2) 0.207516(19) 0.391607(18) 0.02997(9) Uani 1 d .
W9A W 0.611134(19) 0.143857(19) 0.369309(18) 0.02828(9) Uani 1 d .
W10A W 0.54767(2) 0.233005(19) 0.465546(19) 0.03080(10) Uani 1 d .
W1B W 0.00111(2) -0.07451(2) -0.190436(17) 0.03173(10) Uani 1 d .
W2B W 0.00458(2) 0.06037(2) -0.169672(18) 0.03063(10) Uani 1 d .
W3B W 0.113204(18) -0.061453(18) 0.017090(16) 0.02445(8) Uani 1 d .
W4B W 0.121307(19) 0.073298(18) 0.030579(17) 0.02668(9) Uani 1 d .
W5B W 0.087530(19) -0.143012(19) -0.107140(17) 0.02791(9) Uani 1 d .
W6B W 0.11361(2) 0.142950(19) -0.075826(18) 0.03033(10) Uani 1 d .
W7B W 0.15108(2) -0.08010(2) -0.186643(18) 0.03368(11) Uani 1 d .
W8B W 0.15749(2) 0.07033(2) -0.171413(19) 0.03206(10) Uani 1 d .
W9B W 0.213935(19) -0.07220(2) -0.070252(19) 0.03023(10) Uani 1 d .
W10B W 0.225605(19) 0.07996(2) -0.054847(19) 0.03163(10) Uani 1 d .
W1C W 0.53503(2) 0.30662(2) -0.07321(2) 0.03831(11) Uani 1 d .
W2C W 0.47384(2) 0.36165(2) -0.16594(2) 0.03847(12) Uani 1 d .
W3C W 0.636436(19) 0.521165(18) 0.032244(17) 0.02674(9) Uani 1 d .
W4C W 0.575471(19) 0.577508(18) -0.059673(17) 0.02596(9) Uani 1 d .
W5C W 0.65745(2) 0.37944(2) 0.011280(18) 0.03046(10) Uani 1 d .
W6C W 0.52676(2) 0.497431(19) -0.182716(17) 0.02845(9) Uani 1 d .
W7C W 0.67542(2) 0.33928(2) -0.106298(19) 0.03397(11) Uani 1 d .
W8C W 0.60787(2) 0.40276(2) -0.208325(18) 0.03536(11) Uani 1 d .
W9C W 0.73384(2) 0.46217(2) -0.045319(19) 0.03219(10) Uani 1 d .
W10C W 0.66459(2) 0.52574(2) -0.148460(19) 0.03201(10) Uani 1 d .
W1D W 1.177372(19) 0.45110(2) 0.60179(2) 0.03347(10) Uani 1 d .
W2D W 1.11257(2) 0.53268(2) 0.677546(19) 0.03550(11) Uani 1 d .
W3D W 0.96339(2) 0.36726(2) 0.475319(18) 0.03117(10) Uani 1 d .
W4D W 0.898096(19) 0.44456(2) 0.553531(19) 0.03051(10) Uani 1 d .
W5D W 1.10077(2) 0.33274(2) 0.51676(2) 0.03928(12) Uani 1 d .
W6D W 0.96331(2) 0.49899(2) 0.680383(19) 0.03685(11) Uani 1 d .
W7D W 1.11568(2) 0.32550(2) 0.63690(2) 0.03698(11) Uani 1 d .
W8D W 1.04585(3) 0.41594(3) 0.72420(2) 0.04390(13) Uani 1 d .
W9D W 0.99344(2) 0.27776(2) 0.56487(2) 0.04000(12) Uani 1 d .
W10D W 0.92230(2) 0.36634(2) 0.65420(2) 0.04189(12) Uani 1 d .
Co1A Co 0.40782(6) -0.01172(6) 0.43999(6) 0.0250(3) Uani 1 d .
Co1B Co -0.04349(6) -0.00743(6) -0.09176(6) 0.0259(3) Uani 1 d .
Co1C Co 0.46174(7) 0.40549(6) -0.04987(6) 0.0276(3) Uani 1 d .
Co1D Co 1.09360(7) 0.53234(7) 0.55813(7) 0.0336(3) Uani 1 d .
Si1A Si 0.48920(12) 0.09670(12) 0.41969(11) 0.0221(5) Uani 1 d .
Si1B Si 0.09487(12) -0.00159(12) -0.08778(11) 0.0235(6) Uani 1 d .
Si1C Si 0.58705(13) 0.44087(12) -0.08198(11) 0.0241(6) Uani 1 d .
Si1D Si 1.03151(12) 0.42042(12) 0.59407(11) 0.0232(6) Uani 1 d .
O1A O 0.3840(3) -0.0451(3) 0.3659(3) 0.0275(16) Uiso 1 d .
O2A O 0.3359(3) 0.0233(3) 0.4411(3) 0.0264(15) Uiso 1 d .
O3A O 0.5752(3) -0.0173(3) 0.4837(3) 0.0253(15) Uiso 1 d .
O4A O 0.5270(3) 0.0551(3) 0.5590(3) 0.0256(15) Uiso 1 d .
O5A O 0.4296(3) 0.0571(3) 0.4042(3) 0.0236(14) Uiso 1 d .
O6A O 0.5302(3) 0.0775(3) 0.4629(3) 0.0239(15) Uiso 1 d .
O7A O 0.3631(4) -0.0259(4) 0.2680(3) 0.0369(19) Uiso 1 d .
O8A O 0.3342(3) 0.0426(3) 0.3472(3) 0.0305(17) Uiso 1 d .
O9A O 0.2743(4) 0.1008(4) 0.4150(4) 0.040(2) Uiso 1 d .
O13A O 0.4716(3) -0.0087(3) 0.3264(3) 0.0287(16) Uiso 1 d .
O14A O 0.3807(4) 0.1268(3) 0.4779(3) 0.0321(17) Uiso 1 d .
O15A O 0.5735(3) 0.0086(3) 0.3912(3) 0.0251(15) Uiso 1 d .
O16A O 0.4823(3) 0.1428(3) 0.5390(3) 0.0291(16) Uiso 1 d .
O10A O 0.6756(4) 0.0214(3) 0.4566(3) 0.0325(17) Uiso 1 d .
O11A O 0.6181(3) 0.0833(3) 0.5229(3) 0.0274(16) Uiso 1 d .
O12A O 0.5880(4) 0.1517(3) 0.6005(3) 0.0349(18) Uiso 1 d .
O17A O 0.5684(4) -0.0344(3) 0.2894(3) 0.0330(18) Uiso 1 d .
O18A O 0.4024(4) 0.2142(4) 0.5583(3) 0.0378(19) Uiso 1 d .
O19A O 0.4236(4) 0.0757(3) 0.3006(3) 0.0328(18) Uiso 1 d .
O20A O 0.3729(3) 0.1461(3) 0.3828(3) 0.0307(17) Uiso 1 d .
O21A O 0.6309(3) 0.1081(3) 0.4273(3) 0.0289(16) Uiso 1 d .
O22A O 0.5778(3) 0.1816(3) 0.5082(3) 0.0294(16) Uiso 1 d .
O23A O 0.5208(3) 0.0965(3) 0.3700(3) 0.0243(15) Uiso 1 d .
O24A O 0.4774(3) 0.1592(3) 0.4392(3) 0.0280(16) Uiso 1 d .
O25A O 0.5197(3) 0.0593(3) 0.2755(3) 0.0287(16) Uiso 1 d .
O26A O 0.4039(3) 0.2259(3) 0.4587(3) 0.0300(17) Uiso 1 d .
O27A O 0.6114(3) 0.0734(3) 0.3330(3) 0.0272(16) Uiso 1 d .
O28A O 0.4990(4) 0.2397(3) 0.5151(3) 0.0329(18) Uiso 1 d .
O29A O 0.4610(3) 0.1793(3) 0.3374(3) 0.0304(17) Uiso 1 d .
O30A O 0.5858(4) 0.1971(3) 0.4156(3) 0.0320(17) Uiso 1 d .
O31A O 0.5639(4) 0.1606(3) 0.3149(3) 0.0321(17) Uiso 1 d .
O32A O 0.4955(4) 0.2552(4) 0.4199(3) 0.0355(19) Uiso 1 d .
O33A O 0.4734(4) 0.1434(4) 0.2386(3) 0.0365(19) Uiso 1 d .
O34A O 0.3869(4) 0.2536(4) 0.3645(4) 0.040(2) Uiso 1 d .
O35A O 0.6738(4) 0.1750(4) 0.3620(3) 0.038(2) Uiso 1 d .
O36A O 0.5936(4) 0.2910(4) 0.4867(4) 0.040(2) Uiso 1 d .
O1B O -0.0639(3) -0.0697(3) -0.1520(3) 0.0312(17) Uiso 1 d .
O2B O -0.0556(3) 0.0473(3) -0.1394(3) 0.0306(17) Uiso 1 d .
O3B O 0.0322(3) -0.0583(3) 0.0342(3) 0.0263(15) Uiso 1 d .
O4B O 0.0423(3) 0.0618(3) 0.0447(3) 0.0265(15) Uiso 1 d .
O5B O 0.0343(3) -0.0062(3) -0.1226(3) 0.0265(15) Uiso 1 d .
O6B O 0.0896(3) 0.0004(3) -0.0290(3) 0.0248(15) Uiso 1 d .
O7B O -0.0318(4) -0.1218(4) -0.2393(4) 0.042(2) Uiso 1 d .
O8B O -0.0137(4) -0.0109(3) -0.2135(3) 0.0322(17) Uiso 1 d .
O9B O -0.0185(4) 0.0998(4) -0.2110(3) 0.0359(19) Uiso 1 d .
O13B O 0.0247(3) -0.1207(3) -0.1410(3) 0.0284(16) Uiso 1 d .
O14B O 0.0435(3) 0.1121(3) -0.1127(3) 0.0303(17) Uiso 1 d .
O15B O 0.0780(3) -0.1129(3) -0.0405(3) 0.0270(15) Uiso 1 d .
O16B O 0.0948(3) 0.1164(3) -0.0164(3) 0.0290(16) Uiso 1 d .
O10B O 0.1274(3) -0.1025(3) 0.0602(3) 0.0310(17) Uiso 1 d .
O11B O 0.1272(3) 0.0071(3) 0.0616(3) 0.0250(15) Uiso 1 d .
O12B O 0.1430(4) 0.1189(4) 0.0851(3) 0.0375(19) Uiso 1 d .
O17B O 0.0670(4) -0.2103(3) -0.1086(3) 0.0324(17) Uiso 1 d .
O18B O 0.1055(4) 0.2103(4) -0.0616(4) 0.042(2) Uiso 1 d .
O19B O 0.0742(4) -0.0710(3) -0.2058(3) 0.0330(18) Uiso 1 d .
O20B O 0.0815(4) 0.0543(3) -0.1916(3) 0.0346(18) Uiso 1 d .
O21B O 0.1801(3) -0.0566(3) -0.0076(3) 0.0299(16) Uiso 1 d .
O22B O 0.1876(3) 0.0694(3) 0.0046(3) 0.0297(16) Uiso 1 d .
O23B O 0.1259(3) -0.0545(3) -0.1067(3) 0.0262(15) Uiso 1 d .
O24B O 0.1339(3) 0.0531(3) -0.0949(3) 0.0282(16) Uiso 1 d .
O25B O 0.1204(4) -0.1460(3) -0.1682(3) 0.0338(18) Uiso 1 d .
O26B O 0.1442(4) 0.1400(3) -0.1374(3) 0.0320(17) Uiso 1 d .
O27B O 0.1667(3) -0.1388(3) -0.0788(3) 0.0320(17) Uiso 1 d .
O28B O 0.1898(4) 0.1446(3) -0.0469(3) 0.0344(18) Uiso 1 d .
O29B O 0.1682(4) -0.0044(3) -0.1827(3) 0.0333(18) Uiso 1 d .
O30B O 0.2318(3) 0.0044(3) -0.0625(3) 0.0310(17) Uiso 1 d .
O31B O 0.2175(4) -0.0816(4) -0.1400(3) 0.0358(19) Uiso 1 d .
O32B O 0.2277(4) 0.0832(3) -0.1225(3) 0.0350(18) Uiso 1 d .
O33B O 0.1724(4) -0.1049(4) -0.2419(4) 0.048(2) Uiso 1 d .
O34B O 0.1813(4) 0.0907(4) -0.2226(4) 0.041(2) Uiso 1 d .
O35B O 0.2763(4) -0.0916(4) -0.0484(4) 0.040(2) Uiso 1 d .
O36B O 0.2916(4) 0.1075(4) -0.0280(4) 0.043(2) Uiso 1 d .
O1C O 0.4756(3) 0.3291(3) -0.0408(3) 0.0313(17) Uiso 1 d .
O2C O 0.4207(4) 0.3759(3) -0.1203(3) 0.0341(18) Uiso 1 d .
O3C O 0.5609(3) 0.5200(3) 0.0572(3) 0.0261(15) Uiso 1 d .
O4C O 0.5064(3) 0.5698(3) -0.0246(3) 0.0273(16) Uiso 1 d .
O5C O 0.5328(3) 0.3952(3) -0.0895(3) 0.0284(16) Uiso 1 d .
O6C O 0.5812(3) 0.4938(3) -0.0416(3) 0.0243(15) Uiso 1 d .
O7C O 0.5303(4) 0.2400(4) -0.0659(4) 0.044(2) Uiso 1 d .
O8C O 0.4891(4) 0.2998(4) -0.1367(3) 0.0361(19) Uiso 1 d .
O9C O 0.4290(4) 0.3321(4) -0.2180(4) 0.047(2) Uiso 1 d .
O13C O 0.5864(4) 0.3429(3) -0.0131(3) 0.0347(18) Uiso 1 d .
O14C O 0.4792(4) 0.4389(3) -0.1717(3) 0.0326(17) Uiso 1 d .
O15C O 0.6317(3) 0.4466(3) 0.0379(3) 0.0279(16) Uiso 1 d .
O16C O 0.5270(3) 0.5410(3) -0.1184(3) 0.0269(15) Uiso 1 d .
O10C O 0.6720(4) 0.5525(4) 0.0899(3) 0.0367(19) Uiso 1 d .
O11C O 0.6146(3) 0.5868(3) 0.0085(3) 0.0268(15) Uiso 1 d .
O12C O 0.5709(4) 0.6446(4) -0.0631(3) 0.0369(19) Uiso 1 d .
O17C O 0.6743(4) 0.3533(4) 0.0646(4) 0.039(2) Uiso 1 d .
O18C O 0.4829(4) 0.5287(3) -0.2200(3) 0.0351(18) Uiso 1 d .
O19C O 0.6004(4) 0.3087(4) -0.1086(3) 0.0354(19) Uiso 1 d .
O20C O 0.5443(4) 0.3607(3) -0.1932(3) 0.0330(18) Uiso 1 d .
O21C O 0.6949(4) 0.5143(3) -0.0056(3) 0.0333(18) Uiso 1 d .
O22C O 0.6380(4) 0.5669(3) -0.0914(3) 0.0353(18) Uiso 1 d .
O23C O 0.6433(3) 0.4151(3) -0.0630(3) 0.0278(16) Uiso 1 d .
O24C O 0.5940(3) 0.4594(3) -0.1362(3) 0.0274(16) Uiso 1 d .
O25C O 0.6861(3) 0.3305(3) -0.0375(3) 0.0307(17) Uiso 1 d .
O26C O 0.5565(4) 0.4493(3) -0.2306(3) 0.0337(18) Uiso 1 d .
O27C O 0.7270(4) 0.4250(3) 0.0092(3) 0.0344(18) Uiso 1 d .
O28C O 0.5980(4) 0.5422(3) -0.1831(3) 0.0323(17) Uiso 1 d .
O29C O 0.6548(3) 0.3703(3) -0.1631(3) 0.0308(17) Uiso 1 d .
O30C O 0.7099(4) 0.4962(3) -0.1006(3) 0.0324(17) Uiso 1 d .
O31C O 0.7401(4) 0.3969(3) -0.0874(3) 0.0350(18) Uiso 1 d .
O32C O 0.6652(4) 0.4655(4) -0.1988(4) 0.039(2) Uiso 1 d .
O33C O 0.7071(4) 0.2858(4) -0.1315(4) 0.044(2) Uiso 1 d .
O34C O 0.6187(5) 0.3679(4) -0.2642(4) 0.051(2) Uiso 1 d .
O35C O 0.8021(4) 0.4915(4) -0.0306(4) 0.044(2) Uiso 1 d .
O36C O 0.7127(4) 0.5732(4) -0.1643(4) 0.042(2) Uiso 1 d .
O1D O 1.1717(4) 0.5074(3) 0.5611(3) 0.0342(18) Uiso 1 d .
O2D O 1.1157(4) 0.5763(3) 0.6287(3) 0.0348(18) Uiso 1 d .
O3D O 0.9805(4) 0.4355(4) 0.4470(3) 0.0359(19) Uiso 1 d .
O4D O 0.9231(4) 0.5044(3) 0.5149(3) 0.0331(18) Uiso 1 d .
O5D O 1.0854(3) 0.4676(3) 0.6036(3) 0.0285(16) Uiso 1 d .
O6D O 0.9854(3) 0.4263(3) 0.5473(3) 0.0251(15) Uiso 1 d .
O7D O 1.2467(4) 0.4471(4) 0.6027(4) 0.044(2) Uiso 1 d .
O8D O 1.1802(3) 0.5037(3) 0.6601(3) 0.0317(17) Uiso 1 d .
O9D O 1.1385(4) 0.5788(4) 0.7290(4) 0.048(2) Uiso 1 d .
O13D O 1.1443(4) 0.3989(4) 0.5406(3) 0.038(2) Uiso 1 d .
O14D O 1.0318(4) 0.5355(4) 0.6743(3) 0.0364(19) Uiso 1 d .
O15D O 1.0414(4) 0.3620(3) 0.4804(3) 0.0330(18) Uiso 1 d .
O16D O 0.9320(4) 0.4952(3) 0.6118(3) 0.0339(18) Uiso 1 d .
O10D O 0.9381(5) 0.3296(4) 0.4174(4) 0.053(3) Uiso 1 d .
O11D O 0.8960(3) 0.3989(3) 0.4885(3) 0.0318(17) Uiso 1 d .
O12D O 0.8302(4) 0.4583(4) 0.5466(4) 0.048(2) Uiso 1 d .
O17D O 1.1358(5) 0.3072(5) 0.4692(5) 0.059(3) Uiso 1 d .
O18D O 0.9324(5) 0.5520(5) 0.7095(4) 0.054(3) Uiso 1 d .
O19D O 1.1595(4) 0.3928(3) 0.6379(3) 0.0337(18) Uiso 1 d .
O20D O 1.0994(4) 0.4683(4) 0.7099(3) 0.038(2) Uiso 1 d .
O21D O 0.9530(4) 0.3150(3) 0.5160(3) 0.0339(18) Uiso 1 d .
O22D O 0.8926(4) 0.3891(4) 0.5893(3) 0.0362(19) Uiso 1 d .
O23D O 1.0530(3) 0.3605(3) 0.5830(3) 0.0268(15) Uiso 1 d .
O24D O 1.0017(3) 0.4239(3) 0.6451(3) 0.0307(17) Uiso 1 d .
O25D O 1.1375(4) 0.3056(4) 0.5727(4) 0.040(2) Uiso 1 d .
O26D O 1.0007(4) 0.4735(4) 0.7365(4) 0.043(2) Uiso 1 d .
O27D O 1.0434(4) 0.2718(4) 0.5179(4) 0.041(2) Uiso 1 d .
O28D O 0.9089(4) 0.4381(4) 0.6806(4) 0.043(2) Uiso 1 d .
O29D O 1.0782(4) 0.3592(4) 0.6869(4) 0.041(2) Uiso 1 d .
O30D O 0.9531(4) 0.3129(4) 0.6127(4) 0.040(2) Uiso 1 d .
O31D O 1.0514(4) 0.2696(4) 0.6158(4) 0.041(2) Uiso 1 d .
O32D O 0.9748(5) 0.3671(4) 0.7104(4) 0.050(2) Uiso 1 d .
O33D O 1.1587(5) 0.2907(4) 0.6699(4) 0.053(3) Uiso 1 d .
O34D O 1.0689(5) 0.4091(5) 0.7839(5) 0.061(3) Uiso 1 d .
O35D O 0.9572(5) 0.2147(5) 0.5519(4) 0.053(3) Uiso 1 d .
O36D O 0.8645(5) 0.3301(5) 0.6675(5) 0.059(3) Uiso 1 d .
N1A N -0.2042(5) -0.0126(5) -0.2248(5) 0.044(3) Uiso 1 d .
N1B N 0.0217(7) -0.2777(7) -0.2636(7) 0.073(4) Uiso 1 d .
N1C N 0.3788(6) -0.0428(5) -0.1672(5) 0.052(3) Uiso 1 d .
N1D N 0.8287(5) 0.2626(5) -0.0075(4) 0.041(2) Uiso 1 d .
N1E N 0.4261(6) 0.3324(6) 0.2583(6) 0.061(4) Uiso 1 d .
N1F N 0.5021(6) 0.2034(6) 0.7123(5) 0.053(3) Uiso 1 d .
N1G N 0.8496(8) 0.4756(8) 0.8146(7) 0.078(5) Uiso 1 d D
N1H N 1.0588(6) 0.1334(5) 0.6685(5) 0.050(3) Uiso 1 d .
N1I N 1.3064(5) 0.5191(5) 0.7814(5) 0.043(3) Uiso 1 d .
N1J N 0.2872(5) 0.2740(5) -0.0569(5) 0.048(3) Uiso 1 d .
N1K N 0.3186(6) 0.3472(6) 0.4913(5) 0.053(3) Uiso 1 d .
N1L N 0.7666(7) 0.2366(7) 0.5211(6) 0.071(4) Uiso 1 d .
C1A C -0.2230(7) 0.0407(7) -0.2348(6) 0.051(4) Uiso 1 d .
C2A C -0.1804(10) 0.0889(9) -0.2147(9) 0.077(6) Uiso 1 d .
C3A C -0.2055(11) 0.1421(11) -0.2149(10) 0.093(7) Uiso 1 d .
C4A C -0.2433(12) 0.1446(12) -0.1729(11) 0.104(8) Uiso 1 d .
C5A C -0.2521(7) -0.0554(6) -0.2480(6) 0.048(3) Uiso 1 d .
C6A C -0.2374(7) -0.1147(7) -0.2481(7) 0.055(4) Uiso 1 d .
C7A C -0.2887(7) -0.1531(7) -0.2740(7) 0.057(4) Uiso 1 d .
C8A C -0.3380(7) -0.1545(7) -0.2430(6) 0.055(4) Uiso 1 d .
C9A C -0.1496(7) -0.0209(6) -0.2456(6) 0.050(3) Uiso 1 d .
C10A C -0.1545(7) -0.0242(7) -0.3038(6) 0.053(4) Uiso 1 d .
C11A C -0.0999(8) -0.0369(8) -0.3205(7) 0.063(4) Uiso 1 d .
C12A C -0.1045(8) -0.0401(8) -0.3793(7) 0.065(5) Uiso 1 d .
C13A C -0.1908(7) -0.0130(7) -0.1684(6) 0.051(4) Uiso 1 d .
C14A C -0.2398(7) -0.0013(7) -0.1377(7) 0.057(4) Uiso 1 d .
C15A C -0.2631(8) -0.0536(8) -0.1201(7) 0.064(4) Uiso 1 d .
C16A C -0.2979(10) -0.0374(9) -0.0777(9) 0.080(6) Uiso 1 d .
C1B C 0.0170(10) -0.3336(9) -0.2517(9) 0.078(6) Uiso 1 d .
C2B C 0.0419(9) -0.3407(9) -0.2051(8) 0.073(5) Uiso 1 d .
C3B C 0.0247(13) -0.3982(13) -0.1894(12) 0.071(5) Uiso 0.68(2) d P
C4B C 0.0405(14) -0.4047(14) -0.1467(14) 0.071(5) Uiso 0.68(2) d P
C53B C 0.011(3) -0.351(3) -0.175(3) 0.071(5) Uiso 0.32(2) d P
C54B C 0.032(3) -0.395(3) -0.126(3) 0.071(5) Uiso 0.32(2) d P
C5B C -0.0044(9) -0.2818(8) -0.3144(8) 0.071(5) Uiso 1 d .
C6B C -0.0018(11) -0.2242(10) -0.3371(9) 0.087(7) Uiso 1 d .
C7B C -0.0367(10) -0.2353(10) -0.3877(9) 0.083(6) Uiso 1 d .
C8B C -0.0353(12) -0.1765(11) -0.4105(11) 0.100(8) Uiso 1 d .
C9B C -0.0082(9) -0.2409(9) -0.2259(8) 0.072(5) Uiso 1 d .
C10B C -0.0722(18) -0.2654(17) -0.2222(16) 0.094(6) Uiso 0.68(2) d P
C11B C -0.098(3) -0.222(2) -0.190(3) 0.094(6) Uiso 0.68(2) d P
C12B C -0.1420(17) -0.1946(16) -0.2101(15) 0.094(6) Uiso 0.68(2) d P
C60B C -0.070(4) -0.244(4) -0.240(3) 0.094(6) Uiso 0.31(2) d P
C61B C -0.094(7) -0.212(5) -0.191(6) 0.094(6) Uiso 0.31(2) d P
C62B C -0.097(4) -0.228(3) -0.153(3) 0.094(6) Uiso 0.31(2) d P
C13B C 0.0821(8) -0.2491(8) -0.2542(8) 0.069(5) Uiso 1 d D
C14B C 0.117(2) -0.281(3) -0.289(3) 0.086(5) Uiso 0.59(3) d PD
C15B C 0.175(3) -0.249(3) -0.276(2) 0.086(5) Uiso 0.59(3) d PD
C16B C 0.2121(17) -0.2631(18) -0.3173(15) 0.086(5) Uiso 0.59(3) d PD
C64B C 0.122(3) -0.281(4) -0.283(4) 0.086(5) Uiso 0.41(3) d PD
C65B C 0.182(4) -0.253(3) -0.282(4) 0.086(5) Uiso 0.41(3) d PD
C66B C 0.215(2) -0.298(2) -0.302(2) 0.086(5) Uiso 0.41(3) d PD
C1C C 0.4296(13) -0.0045(12) -0.1758(11) 0.048(2) Uiso 0.526(14) d P
C2C C 0.4821(14) -0.0034(13) -0.1594(12) 0.048(2) Uiso 0.526(14) d P
C3C C 0.5309(13) 0.0205(13) -0.1677(11) 0.048(2) Uiso 0.526(14) d P
C4C C 0.5862(13) 0.0368(12) -0.1563(11) 0.048(2) Uiso 0.526(14) d P
C51C C 0.4456(14) -0.0533(13) -0.1692(13) 0.048(2) Uiso 0.474(14) d P
C52C C 0.4840(15) -0.0256(15) -0.1589(14) 0.048(2) Uiso 0.474(14) d P
C53C C 0.5423(14) -0.0084(14) -0.1601(13) 0.048(2) Uiso 0.474(14) d P
C54C C 0.5886(14) -0.0034(13) -0.1632(13) 0.048(2) Uiso 0.474(14) d P
C5C C 0.3790(14) -0.0951(14) -0.1946(13) 0.074(4) Uiso 0.66(2) d P
C6C C 0.3261(15) -0.1347(14) -0.1922(13) 0.074(4) Uiso 0.66(2) d P
C7C C 0.3300(16) -0.1911(15) -0.2292(14) 0.074(4) Uiso 0.66(2) d P
C8C C 0.3840(15) -0.2156(14) -0.1990(13) 0.074(4) Uiso 0.66(2) d P
C55C C 0.353(3) -0.104(3) -0.169(3) 0.074(4) Uiso 0.34(2) d P
C56C C 0.346(3) -0.138(3) -0.224(3) 0.074(4) Uiso 0.34(2) d P
C57C C 0.329(3) -0.201(3) -0.211(3) 0.074(4) Uiso 0.34(2) d P
C58C C 0.362(3) -0.232(3) -0.224(3) 0.074(4) Uiso 0.34(2) d P
C9C C 0.3729(18) -0.0170(19) -0.1162(16) 0.065(3) Uiso 0.484(18) d P
C10C C 0.3859(17) 0.0132(17) -0.0754(16) 0.065(3) Uiso 0.484(18) d P
C11C C 0.379(2) 0.0169(19) -0.025(2) 0.065(3) Uiso 0.484(18) d P
C12C C 0.4231(17) -0.0212(17) 0.0085(15) 0.065(3) Uiso 0.484(18) d P
C59C C 0.3767(17) -0.0441(17) -0.1106(16) 0.065(3) Uiso 0.516(18) d P
C60C C 0.3964(16) -0.0307(16) -0.0732(15) 0.065(3) Uiso 0.516(18) d P
C61C C 0.388(2) 0.0032(18) -0.0237(19) 0.065(3) Uiso 0.516(18) d P
C62C C 0.4187(16) 0.0189(16) 0.0180(15) 0.065(3) Uiso 0.516(18) d P
C13C C 0.3251(14) -0.0166(13) -0.1870(13) 0.066(3) Uiso 0.610(18) d P
C14C C 0.3163(14) -0.0223(13) -0.2455(13) 0.066(3) Uiso 0.610(18) d P
C15C C 0.2790(16) 0.0202(14) -0.2609(14) 0.066(3) Uiso 0.610(18) d P
C16C C 0.2656(14) -0.0182(14) -0.3170(13) 0.066(3) Uiso 0.610(18) d P
C63C C 0.361(2) -0.021(2) -0.2125(19) 0.066(3) Uiso 0.390(18) d P
C64C C 0.299(2) -0.012(2) -0.216(2) 0.066(3) Uiso 0.390(18) d P
C65C C 0.269(2) 0.001(2) -0.268(2) 0.066(3) Uiso 0.390(18) d P
C66C C 0.264(2) 0.016(2) -0.316(2) 0.066(3) Uiso 0.390(18) d P
C1D C 0.8304(7) 0.2605(6) 0.0474(6) 0.048(3) Uiso 1 d .
C2D C 0.7842(8) 0.2862(7) 0.0735(7) 0.060(4) Uiso 1 d .
C3D C 0.7920(10) 0.2753(10) 0.1280(9) 0.083(6) Uiso 1 d .
C4D C 0.7494(12) 0.3016(12) 0.1572(11) 0.104(8) Uiso 1 d .
C5D C 0.8778(7) 0.2339(7) -0.0225(7) 0.057(4) Uiso 1 d .
C6D C 0.8860(9) 0.2326(9) -0.0784(8) 0.072(5) Uiso 1 d .
C7D C 0.9436(10) 0.2117(10) -0.0851(9) 0.082(6) Uiso 1 d .
C8D C 0.9546(12) 0.2121(11) -0.1401(11) 0.100(8) Uiso 1 d .
C9D C 0.7731(7) 0.2361(6) -0.0378(6) 0.049(3) Uiso 1 d .
C10D C 0.7554(8) 0.1787(7) -0.0306(7) 0.060(4) Uiso 1 d .
C11D C 0.691(3) 0.167(2) -0.060(2) 0.089(7) Uiso 0.52(3) d P
C12D C 0.658(2) 0.177(2) -0.0366(19) 0.089(7) Uiso 0.52(3) d P
C61D C 0.703(3) 0.151(3) -0.065(2) 0.089(7) Uiso 0.48(3) d P
C62D C 0.671(2) 0.111(2) -0.062(2) 0.089(7) Uiso 0.48(3) d P
C13D C 0.8352(7) 0.3209(6) -0.0161(6) 0.050(3) Uiso 1 d .
C14D C 0.8902(8) 0.3536(7) 0.0052(7) 0.060(4) Uiso 1 d .
C15D C 0.8904(10) 0.4108(9) -0.0085(9) 0.080(6) Uiso 1 d .
C16D C 0.9455(11) 0.4470(10) 0.0105(10) 0.090(7) Uiso 1 d .
C1E C 0.4318(10) 0.3149(10) 0.2026(9) 0.080(6) Uiso 1 d .
C2E C 0.4192(13) 0.2505(13) 0.1868(12) 0.095(5) Uiso 0.86(2) d P
C3E C 0.4315(14) 0.2297(14) 0.1364(13) 0.095(5) Uiso 0.86(2) d P
C4E C 0.4172(13) 0.1716(13) 0.1184(12) 0.095(5) Uiso 0.86(2) d P
C52E C 0.413(9) 0.283(9) 0.160(8) 0.095(5) Uiso 0.14(2) d P
C53E C 0.374(9) 0.257(8) 0.140(8) 0.095(5) Uiso 0.14(2) d P
C54E C 0.410(10) 0.247(9) 0.123(8) 0.095(5) Uiso 0.14(2) d P
C5E C 0.3672(8) 0.3106(8) 0.2665(7) 0.064(5) Uiso 1 d .
C6E C 0.3200(10) 0.3338(9) 0.2371(8) 0.077(6) Uiso 1 d .
C7E C 0.2659(11) 0.3160(11) 0.2539(10) 0.094(7) Uiso 1 d .
C8E C 0.2155(13) 0.3357(13) 0.2230(12) 0.114(9) Uiso 1 d .
C9E C 0.4367(9) 0.3947(8) 0.2697(8) 0.068(5) Uiso 1 d .
C10E C 0.4337(9) 0.4186(9) 0.3232(8) 0.074(5) Uiso 1 d .
C11E C 0.4373(11) 0.4803(11) 0.3246(10) 0.093(7) Uiso 1 d .
C12E C 0.4376(12) 0.5098(12) 0.3796(11) 0.102(8) Uiso 1 d .
C13E C 0.4666(8) 0.3059(7) 0.2919(7) 0.057(4) Uiso 1 d .
C14E C 0.5279(9) 0.3212(9) 0.2877(8) 0.073(5) Uiso 1 d .
C15E C 0.5661(11) 0.3006(10) 0.3272(9) 0.087(7) Uiso 1 d .
C16E C 0.5682(17) 0.3457(16) 0.3805(15) 0.067(7) Uiso 0.52(2) d P
C66E C 0.6200(18) 0.3031(17) 0.3180(16) 0.067(7) Uiso 0.48(2) d P
C1F C 0.4651(6) 0.1578(6) 0.6731(6) 0.046(3) Uiso 1 d .
C2F C 0.4032(7) 0.1627(7) 0.6638(7) 0.055(4) Uiso 1 d .
C3F C 0.3734(7) 0.1138(7) 0.6239(7) 0.055(4) Uiso 1 d .
C4F C 0.3124(11) 0.1212(10) 0.6093(9) 0.088(7) Uiso 1 d .
C5F C 0.5604(8) 0.1880(7) 0.7150(7) 0.060(4) Uiso 1 d .
C6F C 0.6044(9) 0.2265(9) 0.7536(8) 0.071(5) Uiso 1 d D
C7F C 0.6668(12) 0.2109(15) 0.7486(12) 0.093(7) Uiso 0.75(2) d PD
C8F C 0.6904(15) 0.2227(14) 0.6973(12) 0.093(7) Uiso 0.75(2) d PD
C57F C 0.640(4) 0.182(3) 0.774(3) 0.093(7) Uiso 0.25(2) d PD
C58F C 0.682(4) 0.162(4) 0.735(4) 0.093(7) Uiso 0.25(2) d PD
C9F C 0.4992(8) 0.2597(8) 0.6984(7) 0.061(4) Uiso 1 d .
C10F C 0.5198(7) 0.2655(7) 0.6489(6) 0.053(4) Uiso 1 d .
C11F C 0.494(3) 0.316(2) 0.626(2) 0.079(6) Uiso 0.43(3) d P
C12F C 0.459(2) 0.340(2) 0.636(2) 0.079(6) Uiso 0.43(3) d P
C61F C 0.520(2) 0.3229(18) 0.6358(17) 0.079(6) Uiso 0.57(3) d P
C62F C 0.4887(18) 0.3630(17) 0.6580(16) 0.079(6) Uiso 0.57(3) d P
C13F C 0.4800(9) 0.2053(8) 0.7628(8) 0.068(5) Uiso 1 d .
C14F C 0.4902(9) 0.1545(9) 0.7868(8) 0.073(5) Uiso 1 d .
C15F C 0.4532(13) 0.1572(12) 0.8326(12) 0.110(9) Uiso 1 d .
C16F C 0.3933(12) 0.1467(11) 0.8146(11) 0.101(8) Uiso 1 d .
C1G C 0.8391(9) 0.4927(9) 0.7634(8) 0.073(5) Uiso 1 d .
C2G C 0.7768(10) 0.5009(10) 0.7472(9) 0.081(6) Uiso 1 d .
C3G C 0.7776(12) 0.5213(11) 0.6958(11) 0.099(8) Uiso 1 d .
C4G C 0.7118(14) 0.5272(13) 0.6760(12) 0.119(10) Uiso 1 d .
C5G C 0.9116(11) 0.4667(11) 0.8188(10) 0.092(7) Uiso 1 d .
C6G C 0.9339(14) 0.4664(13) 0.8758(12) 0.119(10) Uiso 1 d .
C7G C 0.9909(12) 0.4377(11) 0.8745(10) 0.099(8) Uiso 1 d .
C8G C 0.9755(10) 0.3784(10) 0.8563(9) 0.084(6) Uiso 1 d .
C9G C 0.8144(10) 0.4270(9) 0.8142(9) 0.075(5) Uiso 1 d .
C10G C 0.8133(13) 0.3822(13) 0.7710(12) 0.072(4) Uiso 0.709(19) d P
C11G C 0.7854(13) 0.3273(12) 0.7804(12) 0.072(4) Uiso 0.709(19) d P
C12G C 0.8224(13) 0.3025(12) 0.8209(11) 0.072(4) Uiso 0.709(19) d P
C60G C 0.788(3) 0.397(3) 0.797(3) 0.072(4) Uiso 0.291(19) d P
C61G C 0.787(3) 0.351(3) 0.755(3) 0.072(4) Uiso 0.291(19) d P
C62G C 0.741(3) 0.313(3) 0.749(3) 0.072(4) Uiso 0.291(19) d P
C13G C 0.840(3) 0.510(2) 0.8634(19) 0.091(5) Uiso 0.35(2) d PD
C14G C 0.894(3) 0.548(3) 0.876(2) 0.091(5) Uiso 0.35(2) d PD
C15G C 0.882(3) 0.576(3) 0.925(2) 0.091(5) Uiso 0.35(2) d PD
C16G C 0.839(3) 0.615(3) 0.924(3) 0.091(5) Uiso 0.35(2) d PD
C63G C 0.8363(17) 0.5227(13) 0.8520(14) 0.091(5) Uiso 0.65(2) d PD
C64G C 0.8651(17) 0.5795(12) 0.8576(14) 0.091(5) Uiso 0.65(2) d PD
C65G C 0.8505(17) 0.6195(16) 0.8989(12) 0.091(5) Uiso 0.65(2) d PD
C66G C 0.8858(16) 0.6132(17) 0.9457(14) 0.091(5) Uiso 0.65(2) d PD
C1H C 0.9972(8) 0.1249(7) 0.6742(7) 0.058(4) Uiso 1 d .
C2H C 0.9687(9) 0.1724(8) 0.6716(8) 0.071(5) Uiso 1 d .
C3H C 0.9092(12) 0.1604(12) 0.6865(11) 0.103(8) Uiso 1 d .
C4H C 0.8817(13) 0.2088(13) 0.6894(12) 0.114(9) Uiso 1 d .
C5H C 1.0868(8) 0.0852(8) 0.6843(7) 0.064(5) Uiso 1 d .
C6H C 1.0674(15) 0.0279(14) 0.6561(14) 0.070(4) Uiso 0.64(2) d P
C7H C 1.0966(16) -0.0136(14) 0.6859(13) 0.070(4) Uiso 0.64(2) d P
C8H C 1.0652(14) -0.0700(13) 0.6696(12) 0.070(4) Uiso 0.64(2) d P
C56H C 1.044(3) 0.033(3) 0.656(2) 0.070(4) Uiso 0.36(2) d P
C57H C 1.065(3) -0.022(2) 0.677(2) 0.070(4) Uiso 0.36(2) d P
C58H C 1.125(3) -0.013(2) 0.668(2) 0.070(4) Uiso 0.36(2) d P
C9H C 1.0614(7) 0.1364(7) 0.6128(7) 0.057(4) Uiso 1 d .
C10H C 1.1218(8) 0.1497(7) 0.6009(7) 0.058(4) Uiso 1 d .
C11H C 1.1159(9) 0.1484(8) 0.5427(8) 0.069(5) Uiso 1 d .
C12H C 1.1719(10) 0.1695(9) 0.5266(9) 0.081(6) Uiso 1 d .
C13H C 1.0886(7) 0.1853(7) 0.7005(6) 0.053(4) Uiso 1 d .
C14H C 1.0827(7) 0.1911(7) 0.7559(7) 0.057(4) Uiso 1 d .
C15H C 1.0958(14) 0.2561(13) 0.7702(13) 0.050(4) Uiso 0.509(19) d P
C16H C 1.0908(13) 0.2676(13) 0.8265(12) 0.050(4) Uiso 0.509(19) d P
C65H C 1.1062(14) 0.2433(14) 0.7924(14) 0.050(4) Uiso 0.491(19) d P
C66H C 1.0689(14) 0.2845(13) 0.7859(12) 0.050(4) Uiso 0.491(19) d P
C1I C 1.3582(6) 0.5437(6) 0.8194(6) 0.044(3) Uiso 1 d .
C2I C 1.3724(7) 0.6054(6) 0.8253(6) 0.049(3) Uiso 1 d .
C3I C 1.4263(6) 0.6229(6) 0.8641(6) 0.044(3) Uiso 1 d .
C4I C 1.4380(8) 0.6841(7) 0.8774(7) 0.061(4) Uiso 1 d .
C5I C 1.3032(7) 0.4583(7) 0.7836(6) 0.052(4) Uiso 1 d .
C6I C 1.2549(10) 0.4240(10) 0.7448(9) 0.081(6) Uiso 1 d .
C7I C 1.2477(10) 0.3675(10) 0.7621(9) 0.086(6) Uiso 1 d .
C8I C 1.2129(10) 0.3700(10) 0.8067(9) 0.084(6) Uiso 1 d .
C9I C 1.2539(8) 0.5409(7) 0.7965(7) 0.060(4) Uiso 1 d .
C10I C 1.2432(9) 0.5364(9) 0.8485(8) 0.075(5) Uiso 1 d .
C11I C 1.1785(15) 0.5343(14) 0.8419(14) 0.055(4) Uiso 0.51(2) d P
C12I C 1.1659(14) 0.5313(14) 0.8969(13) 0.055(4) Uiso 0.51(2) d P
C61I C 1.1876(15) 0.5528(15) 0.8687(15) 0.055(4) Uiso 0.49(2) d P
C62I C 1.1456(15) 0.5091(14) 0.8443(14) 0.055(4) Uiso 0.49(2) d P
C13I C 1.3101(8) 0.5295(8) 0.7288(7) 0.065(5) Uiso 1 d .
C14I C 1.3589(10) 0.5062(9) 0.7045(9) 0.077(6) Uiso 1 d .
C15I C 1.3637(10) 0.5274(9) 0.6537(9) 0.078(6) Uiso 1 d .
C16I C 1.4076(13) 0.5000(12) 0.6264(11) 0.107(9) Uiso 1 d .
C1J C 0.3520(7) 0.2812(6) -0.0516(6) 0.049(3) Uiso 1 d .
C2J C 0.3781(7) 0.2277(7) -0.0566(6) 0.054(4) Uiso 1 d .
C3J C 0.4057(8) 0.2152(8) -0.0064(8) 0.066(5) Uiso 1 d .
C4J C 0.4342(10) 0.1623(9) -0.0191(9) 0.080(6) Uiso 1 d .
C5J C 0.2711(6) 0.3315(6) -0.0580(6) 0.046(3) Uiso 1 d .
C6J C 0.2076(7) 0.3333(7) -0.0655(7) 0.055(4) Uiso 1 d .
C7J C 0.1961(8) 0.3912(8) -0.0529(7) 0.062(4) Uiso 1 d .
C8J C 0.1324(11) 0.3965(10) -0.0673(9) 0.088(7) Uiso 1 d .
C9J C 0.2612(7) 0.2353(7) -0.1040(6) 0.052(4) Uiso 1 d .
C10J C 0.2830(7) 0.2488(7) -0.1523(7) 0.056(4) Uiso 1 d .
C11J C 0.2553(9) 0.2039(8) -0.1957(8) 0.068(5) Uiso 1 d .
C12J C 0.2687(10) 0.2166(9) -0.2473(9) 0.081(6) Uiso 1 d .
C13J C 0.2674(7) 0.2508(7) -0.0138(7) 0.056(4) Uiso 1 d .
C14J C 0.2829(9) 0.2880(8) 0.0377(8) 0.071(5) Uiso 1 d .
C15J C 0.2618(13) 0.2578(13) 0.0796(11) 0.107(9) Uiso 1 d .
C16J C 0.209(2) 0.246(2) 0.075(2) 0.096(10) Uiso 0.51(3) d P
C66J C 0.264(2) 0.209(2) 0.090(2) 0.096(10) Uiso 0.49(3) d P
C1K C 0.3056(14) 0.4067(13) 0.5119(12) 0.062(3) Uiso 0.581(17) d P
C2K C 0.3123(15) 0.4445(14) 0.4768(14) 0.062(3) Uiso 0.581(17) d P
C3K C 0.2890(15) 0.4928(14) 0.4828(14) 0.062(3) Uiso 0.581(17) d P
C4K C 0.3099(14) 0.5441(13) 0.4704(13) 0.062(3) Uiso 0.581(17) d P
C51K C 0.3040(19) 0.3945(18) 0.4671(17) 0.062(3) Uiso 0.419(17) d P
C52K C 0.324(2) 0.454(2) 0.4980(19) 0.062(3) Uiso 0.419(17) d P
C53K C 0.305(2) 0.503(2) 0.5056(19) 0.062(3) Uiso 0.419(17) d P
C54K C 0.3068(19) 0.5502(19) 0.5084(18) 0.062(3) Uiso 0.419(17) d P
C5K C 0.3689(15) 0.3471(14) 0.4664(13) 0.059(3) Uiso 0.526(15) d P
C6K C 0.4204(15) 0.3720(14) 0.4995(15) 0.059(3) Uiso 0.526(15) d P
C7K C 0.4868(15) 0.3805(14) 0.4926(14) 0.059(3) Uiso 0.526(15) d P
C8K C 0.5235(15) 0.3961(14) 0.4579(13) 0.059(3) Uiso 0.526(15) d P
C55K C 0.3862(17) 0.3547(16) 0.5080(15) 0.059(3) Uiso 0.474(15) d P
C56K C 0.4224(17) 0.3700(16) 0.4691(16) 0.059(3) Uiso 0.474(15) d P
C57K C 0.4667(17) 0.3858(16) 0.4660(16) 0.059(3) Uiso 0.474(15) d P
C58K C 0.5219(16) 0.4152(16) 0.4961(15) 0.059(3) Uiso 0.474(15) d P
C9K C 0.3211(17) 0.3146(16) 0.5337(15) 0.079(4) Uiso 0.61(2) d P
C10K C 0.2726(17) 0.3111(16) 0.5613(15) 0.079(4) Uiso 0.61(2) d P
C11K C 0.276(2) 0.2783(18) 0.6002(17) 0.079(4) Uiso 0.61(2) d P
C12K C 0.3216(17) 0.3007(17) 0.6465(15) 0.079(4) Uiso 0.61(2) d P
C59K C 0.293(3) 0.341(2) 0.535(2) 0.079(4) Uiso 0.39(2) d P
C60K C 0.308(3) 0.296(2) 0.560(2) 0.079(4) Uiso 0.39(2) d P
C61K C 0.284(3) 0.292(3) 0.614(3) 0.079(4) Uiso 0.39(2) d P
C62K C 0.308(3) 0.334(3) 0.648(2) 0.079(4) Uiso 0.39(2) d P
C13K C 0.2653(16) 0.3223(16) 0.4520(14) 0.074(4) Uiso 0.585(18) d P
C14K C 0.258(2) 0.2628(17) 0.4355(18) 0.074(4) Uiso 0.585(18) d P
C15K C 0.2415(17) 0.2266(16) 0.4024(16) 0.074(4) Uiso 0.585(18) d P
C16K C 0.1920(16) 0.1955(15) 0.3722(14) 0.074(4) Uiso 0.585(18) d P
C63K C 0.311(2) 0.293(2) 0.452(2) 0.074(4) Uiso 0.415(18) d P
C64K C 0.252(3) 0.278(2) 0.430(3) 0.074(4) Uiso 0.415(18) d P
C65K C 0.213(2) 0.252(2) 0.387(2) 0.074(4) Uiso 0.415(18) d P
C66K C 0.246(2) 0.230(2) 0.374(2) 0.074(4) Uiso 0.415(18) d P
C1L C 0.7319(10) 0.2534(9) 0.4786(9) 0.078(6) Uiso 1 d .
C2L C 0.7528(12) 0.3049(11) 0.4660(11) 0.094(7) Uiso 1 d .
C3L C 0.7161(18) 0.3185(16) 0.4174(15) 0.093(7) Uiso 0.69(3) d P
C4L C 0.7343(17) 0.3663(16) 0.3908(16) 0.093(7) Uiso 0.69(3) d P
C53L C 0.754(4) 0.318(4) 0.439(4) 0.093(7) Uiso 0.31(3) d P
C54L C 0.748(4) 0.375(4) 0.420(4) 0.093(7) Uiso 0.31(3) d P
C5L C 0.7759(13) 0.2872(12) 0.5653(11) 0.105(8) Uiso 1 d .
C6L C 0.715(4) 0.292(3) 0.584(3) 0.106(7) Uiso 0.39(3) d P
C7L C 0.743(4) 0.377(4) 0.611(3) 0.106(7) Uiso 0.39(3) d P
C8L C 0.659(4) 0.360(3) 0.624(3) 0.106(7) Uiso 0.39(3) d P
C56L C 0.719(2) 0.314(2) 0.574(2) 0.106(7) Uiso 0.61(3) d P
C57L C 0.728(2) 0.351(2) 0.619(2) 0.106(7) Uiso 0.61(3) d P
C58L C 0.686(2) 0.378(2) 0.638(2) 0.106(7) Uiso 0.61(3) d P
C9L C 0.7367(9) 0.1854(9) 0.5343(8) 0.071(5) Uiso 1 d .
C10L C 0.7691(10) 0.1608(10) 0.5760(9) 0.081(6) Uiso 1 d .
C11L C 0.7359(9) 0.1100(9) 0.5865(8) 0.074(5) Uiso 1 d .
C12L C 0.7666(10) 0.0849(10) 0.6270(9) 0.085(6) Uiso 1 d .
C13L C 0.8256(11) 0.2306(11) 0.5076(10) 0.095(7) Uiso 1 d .
C14L C 0.812(2) 0.185(2) 0.455(2) 0.112(8) Uiso 0.63(3) d P
C15L C 0.877(2) 0.194(2) 0.431(2) 0.112(8) Uiso 0.63(3) d P
C16L C 0.859(2) 0.150(2) 0.3860(19) 0.112(8) Uiso 0.63(3) d P
C64L C 0.833(4) 0.189(4) 0.473(4) 0.112(8) Uiso 0.37(3) d P
C65L C 0.841(4) 0.210(4) 0.426(3) 0.112(8) Uiso 0.37(3) d P
C66L C 0.860(4) 0.159(4) 0.444(3) 0.112(8) Uiso 0.37(3) d P
O1M O 0.0016(8) -0.2891(8) -0.0399(7) 0.105(5) Uiso 1 d .
O2M O -0.0514(10) -0.2871(10) -0.1111(9) 0.138(8) Uiso 1 d .
N1M N -0.0313(9) -0.2675(8) -0.0663(8) 0.088(5) Uiso 1 d .
C1M C -0.0454(9) -0.2112(8) -0.0470(8) 0.068(5) Uiso 1 d .
O1N O 0.6488(15) 0.1917(13) 0.0827(12) 0.189(12) Uiso 1 d .
O2N O 0.5579(14) 0.1611(13) 0.0856(12) 0.183(11) Uiso 1 d .
N1N N 0.5971(18) 0.1822(15) 0.0693(14) 0.158(12) Uiso 1 d .
C1N C 0.5788(18) 0.2147(17) 0.0222(16) 0.159(15) Uiso 1 d .
O1O O 0.1854(13) 0.0223(13) 0.5641(12) 0.176(11) Uiso 1 d .
O2O O 0.2185(10) 0.0245(9) 0.4867(9) 0.132(7) Uiso 1 d .
N1O N 0.1884(15) -0.0102(16) 0.5212(14) 0.157(12) Uiso 1 d .
C1O C 0.1789(18) -0.0572(19) 0.5018(16) 0.158(15) Uiso 1 d .
O1P O 0.959(4) -0.004(3) 0.474(3) 0.20(2) Uiso 0.46(3) d P
O51P O 0.927(3) -0.003(3) 0.499(3) 0.20(2) Uiso 0.54(3) d P
O2P O 0.9546(13) 0.0818(13) 0.4869(12) 0.181(11) Uiso 1 d .
N1P N 0.958(2) 0.036(2) 0.530(2) 0.24(2) Uiso 1 d .
C1P C 0.924(2) 0.071(2) 0.5588(19) 0.182(18) Uiso 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.849 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O7A W1A O8A 100.8(4) . .
O7A W1A O19A 100.9(4) . .
O8A W1A O19A 94.9(4) . .
O7A W1A O13A 101.5(4) . .
O8A W1A O13A 156.8(3) . .
O19A W1A O13A 87.4(3) . .
O7A W1A O1A 96.5(4) . .
O8A W1A O1A 88.3(3) . .
O19A W1A O1A 161.4(3) . .
O13A W1A O1A 82.6(3) . .
O7A W1A O5A 171.2(4) . .
O8A W1A O5A 75.1(3) . .
O19A W1A O5A 87.3(3) . .
O13A W1A O5A 81.9(3) . .
O1A W1A O5A 75.8(3) . .
O9A W2A O2A 102.5(4) . .
O9A W2A O14A 103.6(4) . .
O2A W2A O14A 93.0(4) . .
O9A W2A O8A 99.8(4) . .
O2A W2A O8A 91.3(3) . .
O14A W2A O8A 154.6(3) . .
O9A W2A O20A 97.6(4) . .
O2A W2A O20A 159.8(3) . .
O14A W2A O20A 84.9(3) . .
O8A W2A O20A 82.5(3) . .
O9A W2A O5A 171.9(4) . .
O2A W2A O5A 80.1(3) . .
O14A W2A O5A 83.8(3) . .
O8A W2A O5A 72.3(3) . .
O20A W2A O5A 79.6(3) . .
O10A W3A O21A 100.0(4) . .
O10A W3A O15A 102.0(4) . .
O21A W3A O15A 92.1(3) . .
O10A W3A O11A 100.2(4) . .
O21A W3A O11A 96.9(3) . .
O15A W3A O11A 154.2(3) . .
O10A W3A O3A 92.3(4) . .
O21A W3A O3A 167.7(3) . .
O15A W3A O3A 84.3(3) . .
O11A W3A O3A 81.8(3) . .
O10A W3A O6A 171.3(3) . .
O21A W3A O6A 86.6(3) . .
O15A W3A O6A 83.3(3) . .
O11A W3A O6A 73.1(3) . .
O3A W3A O6A 81.3(3) . .
O12A W4A O22A 99.9(4) . .
O12A W4A O16A 103.8(4) . .
O22A W4A O16A 92.0(3) . .
O12A W4A O11A 95.5(4) . .
O22A W4A O11A 95.3(3) . .
O16A W4A O11A 157.9(3) . .
O12A W4A O4A 93.5(4) . .
O22A W4A O4A 166.6(3) . .
O16A W4A O4A 85.9(3) . .
O11A W4A O4A 82.2(3) . .
O12A W4A O6A 167.5(3) . .
O22A W4A O6A 85.0(3) . .
O16A W4A O6A 87.4(3) . .
O11A W4A O6A 72.6(3) . .
O4A W4A O6A 81.6(3) . .
O17A W5A O13A 101.7(4) . .
O17A W5A O15A 102.2(4) . .
O13A W5A O15A 97.3(3) . .
O17A W5A O25A 100.4(4) . .
O13A W5A O25A 88.0(3) . .
O15A W5A O25A 155.1(3) . .
O17A W5A O27A 99.8(4) . .
O13A W5A O27A 157.1(3) . .
O15A W5A O27A 85.6(3) . .
O25A W5A O27A 80.5(3) . .
O17A W5A O23A 173.0(3) . .
O13A W5A O23A 83.4(3) . .
O15A W5A O23A 81.7(3) . .
O25A W5A O23A 74.8(3) . .
O27A W5A O23A 74.6(3) . .
O18A W6A O14A 102.7(4) . .
O18A W6A O26A 100.8(4) . .
O14A W6A O26A 88.5(4) . .
O18A W6A O16A 101.7(4) . .
O14A W6A O16A 92.7(3) . .
O26A W6A O16A 156.7(3) . .
O18A W6A O28A 100.7(4) . .
O14A W6A O28A 156.4(4) . .
O26A W6A O28A 84.2(4) . .
O16A W6A O28A 85.5(3) . .
O18A W6A O24A 174.3(4) . .
O14A W6A O24A 81.7(3) . .
O26A W6A O24A 75.5(3) . .
O16A W6A O24A 81.6(3) . .
O28A W6A O24A 74.8(3) . .
O33A W7A O29A 100.8(4) . .
O33A W7A O25A 100.0(4) . .
O29A W7A O25A 158.9(4) . .
O33A W7A O31A 100.5(4) . .
O29A W7A O31A 91.1(4) . .
O25A W7A O31A 88.3(3) . .
O33A W7A O19A 103.6(4) . .
O29A W7A O19A 88.1(4) . .
O25A W7A O19A 84.0(3) . .
O31A W7A O19A 155.7(4) . .
O33A W7A O23A 173.0(4) . .
O29A W7A O23A 84.5(3) . .
O25A W7A O23A 75.0(3) . .
O31A W7A O23A 74.7(3) . .
O19A W7A O23A 81.1(3) . .
O34A W8A O20A 105.0(4) . .
O34A W8A O29A 100.5(4) . .
O20A W8A O29A 93.1(4) . .
O34A W8A O26A 97.6(4) . .
O20A W8A O26A 88.3(4) . .
O29A W8A O26A 160.9(3) . .
O34A W8A O32A 99.8(4) . .
O20A W8A O32A 154.9(4) . .
O29A W8A O32A 86.3(3) . .
O26A W8A O32A 84.5(3) . .
O34A W8A O24A 169.6(4) . .
O20A W8A O24A 83.0(3) . .
O29A W8A O24A 85.6(3) . .
O26A W8A O24A 75.6(3) . .
O32A W8A O24A 71.9(3) . .
O35A W9A O27A 101.7(4) . .
O35A W9A O31A 101.7(4) . .
O27A W9A O31A 89.7(3) . .
O35A W9A O30A 102.1(4) . .
O27A W9A O30A 155.3(3) . .
O31A W9A O30A 91.9(4) . .
O35A W9A O21A 101.9(4) . .
O27A W9A O21A 82.7(3) . .
O31A W9A O21A 156.2(3) . .
O30A W9A O21A 85.9(3) . .
O35A W9A O23A 173.7(4) . .
O27A W9A O23A 74.3(3) . .
O31A W9A O23A 73.7(3) . .
O30A W9A O23A 82.6(3) . .
O21A W9A O23A 82.5(3) . .
O36A W10A O32A 102.7(4) . .
O36A W10A O28A 99.8(4) . .
O32A W10A O28A 90.9(4) . .
O36A W10A O30A 100.5(4) . .
O32A W10A O30A 94.6(4) . .
O28A W10A O30A 157.3(4) . .
O36A W10A O22A 101.9(4) . .
O32A W10A O22A 155.0(4) . .
O28A W10A O22A 80.8(3) . .
O30A W10A O22A 85.1(3) . .
O36A W10A O24A 174.0(4) . .
O32A W10A O24A 73.9(3) . .
O28A W10A O24A 75.4(3) . .
O30A W10A O24A 84.9(3) . .
O22A W10A O24A 81.2(3) . .
O7B W1B O8B 100.7(4) . .
O7B W1B O19B 99.9(4) . .
O8B W1B O19B 94.9(4) . .
O7B W1B O13B 101.5(4) . .
O8B W1B O13B 157.1(3) . .
O19B W1B O13B 86.9(4) . .
O7B W1B O1B 96.8(4) . .
O8B W1B O1B 89.2(4) . .
O19B W1B O1B 161.7(4) . .
O13B W1B O1B 82.5(3) . .
O7B W1B O5B 172.2(4) . .
O8B W1B O5B 75.6(3) . .
O19B W1B O5B 87.4(3) . .
O13B W1B O5B 81.6(3) . .
O1B W1B O5B 76.4(3) . .
O9B W2B O2B 102.1(4) . .
O9B W2B O14B 104.0(4) . .
O2B W2B O14B 93.3(4) . .
O9B W2B O8B 98.8(4) . .
O2B W2B O8B 90.7(4) . .
O14B W2B O8B 155.6(3) . .
O9B W2B O20B 97.4(4) . .
O2B W2B O20B 160.0(4) . .
O14B W2B O20B 86.1(3) . .
O8B W2B O20B 82.1(3) . .
O9B W2B O5B 171.1(3) . .
O2B W2B O5B 79.7(3) . .
O14B W2B O5B 84.6(3) . .
O8B W2B O5B 72.4(3) . .
O20B W2B O5B 80.4(3) . .
O10B W3B O21B 99.5(4) . .
O10B W3B O15B 102.0(4) . .
O21B W3B O15B 91.9(3) . .
O10B W3B O11B 98.3(4) . .
O21B W3B O11B 96.7(3) . .
O15B W3B O11B 156.2(3) . .
O10B W3B O3B 91.7(3) . .
O21B W3B O3B 168.7(3) . .
O15B W3B O3B 84.7(3) . .
O11B W3B O3B 82.5(3) . .
O10B W3B O6B 170.7(3) . .
O21B W3B O6B 86.7(3) . .
O15B W3B O6B 84.5(3) . .
O11B W3B O6B 73.9(3) . .
O3B W3B O6B 82.2(3) . .
O12B W4B O22B 101.0(4) . .
O12B W4B O16B 104.3(4) . .
O22B W4B O16B 92.1(4) . .
O12B W4B O11B 95.8(4) . .
O22B W4B O11B 93.8(3) . .
O16B W4B O11B 157.5(3) . .
O12B W4B O4B 93.3(4) . .
O22B W4B O4B 165.4(3) . .
O16B W4B O4B 86.5(3) . .
O11B W4B O4B 82.4(3) . .
O12B W4B O6B 167.2(4) . .
O22B W4B O6B 84.1(3) . .
O16B W4B O6B 87.1(3) . .
O11B W4B O6B 72.0(3) . .
O4B W4B O6B 81.3(3) . .
O17B W5B O13B 102.7(4) . .
O17B W5B O15B 101.4(4) . .
O13B W5B O15B 98.1(3) . .
O17B W5B O25B 100.6(4) . .
O13B W5B O25B 87.8(4) . .
O15B W5B O25B 155.3(3) . .
O17B W5B O27B 99.6(4) . .
O13B W5B O27B 156.6(3) . .
O15B W5B O27B 84.5(3) . .
O25B W5B O27B 81.0(4) . .
O17B W5B O23B 173.2(3) . .
O13B W5B O23B 82.7(3) . .
O15B W5B O23B 81.8(3) . .
O25B W5B O23B 75.2(3) . .
O27B W5B O23B 74.6(3) . .
O18B W6B O14B 102.6(4) . .
O18B W6B O26B 102.1(4) . .
O14B W6B O26B 89.1(4) . .
O18B W6B O28B 100.5(4) . .
O14B W6B O28B 156.7(4) . .
O26B W6B O28B 84.0(4) . .
O18B W6B O16B 101.7(4) . .
O14B W6B O16B 91.9(3) . .
O26B W6B O16B 155.4(3) . .
O28B W6B O16B 85.5(4) . .
O18B W6B O24B 174.6(4) . .
O14B W6B O24B 82.2(3) . .
O26B W6B O24B 75.4(3) . .
O28B W6B O24B 74.5(3) . .
O16B W6B O24B 80.4(3) . .
O33B W7B O29B 102.3(4) . .
O33B W7B O25B 100.3(4) . .
O29B W7B O25B 157.2(4) . .
O33B W7B O19B 103.5(4) . .
O29B W7B O19B 87.3(4) . .
O25B W7B O19B 84.5(4) . .
O33B W7B O31B 100.9(4) . .
O29B W7B O31B 90.8(4) . .
O25B W7B O31B 88.0(4) . .
O19B W7B O31B 155.4(4) . .
O33B W7B O23B 173.2(4) . .
O29B W7B O23B 83.0(3) . .
O25B W7B O23B 74.7(3) . .
O19B W7B O23B 80.8(3) . .
O31B W7B O23B 74.7(3) . .
O34B W8B O20B 102.9(4) . .
O34B W8B O29B 100.7(4) . .
O20B W8B O29B 92.3(4) . .
O34B W8B O26B 98.5(4) . .
O20B W8B O26B 88.3(4) . .
O29B W8B O26B 160.2(4) . .
O34B W8B O32B 101.3(4) . .
O20B W8B O32B 155.5(4) . .
O29B W8B O32B 87.2(4) . .
O26B W8B O32B 84.1(4) . .
O34B W8B O24B 171.7(4) . .
O20B W8B O24B 83.3(3) . .
O29B W8B O24B 84.5(3) . .
O26B W8B O24B 75.8(3) . .
O32B W8B O24B 72.3(3) . .
O35B W9B O27B 100.5(4) . .
O35B W9B O31B 101.2(4) . .
O27B W9B O31B 90.7(4) . .
O35B W9B O30B 102.1(4) . .
O27B W9B O30B 156.2(4) . .
O31B W9B O30B 92.3(4) . .
O35B W9B O21B 101.6(4) . .
O27B W9B O21B 82.9(3) . .
O31B W9B O21B 157.1(4) . .
O30B W9B O21B 85.3(3) . .
O35B W9B O23B 173.7(4) . .
O27B W9B O23B 74.8(3) . .
O31B W9B O23B 75.1(3) . .
O30B W9B O23B 83.2(3) . .
O21B W9B O23B 82.1(3) . .
O36B W10B O32B 102.5(4) . .
O36B W10B O30B 101.5(4) . .
O32B W10B O30B 94.2(4) . .
O36B W10B O28B 98.8(4) . .
O32B W10B O28B 90.7(4) . .
O30B W10B O28B 157.5(4) . .
O36B W10B O22B 102.6(4) . .
O32B W10B O22B 154.4(4) . .
O30B W10B O22B 86.0(3) . .
O28B W10B O22B 80.2(3) . .
O36B W10B O24B 172.6(4) . .
O32B W10B O24B 74.1(3) . .
O30B W10B O24B 85.4(3) . .
O28B W10B O24B 74.9(3) . .
O22B W10B O24B 80.4(3) . .
O7C W1C O1C 100.6(4) . .
O7C W1C O8C 100.1(4) . .
O1C W1C O8C 89.8(4) . .
O7C W1C O19C 98.4(4) . .
O1C W1C O19C 161.0(4) . .
O8C W1C O19C 88.2(4) . .
O7C W1C O13C 102.3(4) . .
O1C W1C O13C 88.2(4) . .
O8C W1C O13C 157.5(4) . .
O19C W1C O13C 86.4(4) . .
O7C W1C O5C 173.9(4) . .
O1C W1C O5C 77.6(3) . .
O8C W1C O5C 74.1(3) . .
O19C W1C O5C 83.7(3) . .
O13C W1C O5C 83.6(3) . .
O9C W2C O8C 101.0(4) . .
O9C W2C O2C 99.3(4) . .
O8C W2C O2C 89.1(4) . .
O9C W2C O20C 99.6(4) . .
O8C W2C O20C 89.2(4) . .
O2C W2C O20C 161.0(4) . .
O9C W2C O14C 102.3(4) . .
O8C W2C O14C 156.7(4) . .
O2C W2C O14C 87.3(4) . .
O20C W2C O14C 86.8(3) . .
O9C W2C O5C 174.1(4) . .
O8C W2C O5C 73.9(3) . .
O2C W2C O5C 78.0(3) . .
O20C W2C O5C 83.4(3) . .
O14C W2C O5C 82.9(3) . .
O10C W3C O21C 101.3(4) . .
O10C W3C O15C 102.4(4) . .
O21C W3C O15C 91.0(4) . .
O10C W3C O11C 97.5(4) . .
O21C W3C O11C 95.2(3) . .
O15C W3C O11C 157.6(3) . .
O10C W3C O3C 92.9(4) . .
O21C W3C O3C 165.8(3) . .
O15C W3C O3C 86.3(3) . .
O11C W3C O3C 82.5(3) . .
O10C W3C O6C 169.3(4) . .
O21C W3C O6C 84.7(3) . .
O15C W3C O6C 86.2(3) . .
O11C W3C O6C 73.0(3) . .
O3C W3C O6C 81.2(3) . .
O12C W4C O22C 100.5(4) . .
O12C W4C O16C 102.2(4) . .
O22C W4C O16C 90.9(4) . .
O12C W4C O11C 98.7(4) . .
O22C W4C O11C 96.0(4) . .
O16C W4C O11C 156.4(3) . .
O12C W4C O4C 93.1(4) . .
O22C W4C O4C 166.3(3) . .
O16C W4C O4C 85.2(3) . .
O11C W4C O4C 82.9(3) . .
O12C W4C O6C 170.5(4) . .
O22C W4C O6C 85.2(3) . .
O16C W4C O6C 85.1(3) . .
O11C W4C O6C 73.1(3) . .
O4C W4C O6C 81.4(3) . .
O17C W5C O13C 102.2(4) . .
O17C W5C O25C 101.5(4) . .
O13C W5C O25C 88.2(4) . .
O17C W5C O15C 101.5(4) . .
O13C W5C O15C 95.2(4) . .
O25C W5C O15C 155.4(3) . .
O17C W5C O27C 101.0(4) . .
O13C W5C O27C 156.3(4) . .
O25C W5C O27C 82.6(4) . .
O15C W5C O27C 84.8(3) . .
O17C W5C O23C 174.5(4) . .
O13C W5C O23C 82.1(3) . .
O25C W5C O23C 75.1(3) . .
O15C W5C O23C 81.3(3) . .
O27C W5C O23C 74.4(3) . .
O18C W6C O14C 102.2(4) . .
O18C W6C O26C 102.3(4) . .
O14C W6C O26C 89.0(4) . .
O18C W6C O16C 100.9(4) . .
O14C W6C O16C 95.8(3) . .
O26C W6C O16C 154.7(4) . .
O18C W6C O28C 99.7(4) . .
O14C W6C O28C 157.5(4) . .
O26C W6C O28C 81.7(4) . .
O16C W6C O28C 84.7(3) . .
O18C W6C O24C 173.7(4) . .
O14C W6C O24C 83.4(3) . .
O26C W6C O24C 74.9(3) . .
O16C W6C O24C 81.0(3) . .
O28C W6C O24C 74.4(3) . .
O33C W7C O29C 101.5(4) . .
O33C W7C O19C 103.7(4) . .
O29C W7C O19C 90.1(4) . .
O33C W7C O25C 99.2(4) . .
O29C W7C O25C 159.2(3) . .
O19C W7C O25C 86.8(4) . .
O33C W7C O31C 100.9(4) . .
O29C W7C O31C 88.4(4) . .
O19C W7C O31C 155.2(4) . .
O25C W7C O31C 85.9(4) . .
O33C W7C O23C 171.8(4) . .
O29C W7C O23C 84.1(3) . .
O19C W7C O23C 82.1(3) . .
O25C W7C O23C 75.1(3) . .
O31C W7C O23C 73.1(3) . .
O34C W8C O20C 102.8(4) . .
O34C W8C O26C 100.5(5) . .
O20C W8C O26C 85.9(4) . .
O34C W8C O29C 100.5(4) . .
O20C W8C O29C 89.4(4) . .
O26C W8C O29C 159.0(4) . .
O34C W8C O32C 101.5(5) . .
O20C W8C O32C 155.4(4) . .
O26C W8C O32C 86.5(4) . .
O29C W8C O32C 89.5(4) . .
O34C W8C O24C 173.3(4) . .
O20C W8C O24C 81.6(3) . .
O26C W8C O24C 74.7(3) . .
O29C W8C O24C 84.4(3) . .
O32C W8C O24C 73.8(3) . .
O35C W9C O31C 102.3(4) . .
O35C W9C O27C 100.5(4) . .
O31C W9C O27C 90.8(4) . .
O35C W9C O30C 100.4(4) . .
O31C W9C O30C 92.6(4) . .
O27C W9C O30C 157.5(4) . .
O35C W9C O21C 102.0(4) . .
O31C W9C O21C 155.6(4) . .
O27C W9C O21C 81.9(4) . .
O30C W9C O21C 85.9(4) . .
O35C W9C O23C 174.8(4) . .
O31C W9C O23C 74.7(3) . .
O27C W9C O23C 75.5(3) . .
O30C W9C O23C 84.0(3) . .
O21C W9C O23C 80.9(3) . .
O36C W10C O32C 101.8(4) . .
O36C W10C O28C 100.3(4) . .
O32C W10C O28C 90.3(4) . .
O36C W10C O30C 101.2(4) . .
O32C W10C O30C 92.3(4) . .
O28C W10C O30C 157.3(4) . .
O36C W10C O22C 102.3(4) . .
O32C W10C O22C 155.7(4) . .
O28C W10C O22C 82.3(4) . .
O30C W10C O22C 86.2(4) . .
O36C W10C O24C 173.6(4) . .
O32C W10C O24C 74.3(3) . .
O28C W10C O24C 74.9(3) . .
O30C W10C O24C 84.1(3) . .
O22C W10C O24C 81.4(3) . .
O7D W1D O8D 99.4(4) . .
O7D W1D O19D 98.4(4) . .
O8D W1D O19D 91.4(4) . .
O7D W1D O1D 97.9(4) . .
O8D W1D O1D 89.8(4) . .
O19D W1D O1D 163.2(4) . .
O7D W1D O13D 102.3(4) . .
O8D W1D O13D 158.3(4) . .
O19D W1D O13D 86.0(4) . .
O1D W1D O13D 86.8(4) . .
O7D W1D O5D 173.2(4) . .
O8D W1D O5D 75.4(3) . .
O19D W1D O5D 86.1(3) . .
O1D W1D O5D 78.0(3) . .
O13D W1D O5D 82.9(3) . .
O9D W2D O2D 100.1(5) . .
O9D W2D O8D 101.1(4) . .
O2D W2D O8D 90.4(4) . .
O9D W2D O14D 102.2(4) . .
O2D W2D O14D 90.2(4) . .
O8D W2D O14D 156.2(4) . .
O9D W2D O20D 98.7(4) . .
O2D W2D O20D 161.2(4) . .
O8D W2D O20D 85.9(4) . .
O14D W2D O20D 85.9(4) . .
O9D W2D O5D 174.3(4) . .
O2D W2D O5D 78.9(3) . .
O8D W2D O5D 73.4(3) . .
O14D W2D O5D 83.4(3) . .
O20D W2D O5D 82.4(3) . .
O10D W3D O21D 100.6(5) . .
O10D W3D O15D 102.6(5) . .
O21D W3D O15D 91.4(4) . .
O10D W3D O11D 98.1(5) . .
O21D W3D O11D 94.3(4) . .
O15D W3D O11D 157.1(4) . .
O10D W3D O3D 92.9(5) . .
O21D W3D O3D 166.4(4) . .
O15D W3D O3D 86.6(4) . .
O11D W3D O3D 82.7(4) . .
O10D W3D O6D 169.8(4) . .
O21D W3D O6D 85.3(3) . .
O15D W3D O6D 85.4(3) . .
O11D W3D O6D 73.1(3) . .
O3D W3D O6D 81.2(3) . .
O12D W4D O22D 100.8(5) . .
O12D W4D O16D 103.0(4) . .
O22D W4D O16D 91.8(4) . .
O12D W4D O11D 98.1(4) . .
O22D W4D O11D 96.2(4) . .
O16D W4D O11D 155.6(4) . .
O12D W4D O4D 92.3(4) . .
O22D W4D O4D 166.9(4) . .
O16D W4D O4D 84.9(4) . .
O11D W4D O4D 82.1(3) . .
O12D W4D O6D 169.5(4) . .
O22D W4D O6D 86.1(3) . .
O16D W4D O6D 84.6(3) . .
O11D W4D O6D 73.0(3) . .
O4D W4D O6D 81.0(3) . .
O17D W5D O13D 100.7(5) . .
O17D W5D O15D 101.4(5) . .
O13D W5D O15D 95.6(4) . .
O17D W5D O25D 101.6(5) . .
O13D W5D O25D 88.0(4) . .
O15D W5D O25D 155.6(4) . .
O17D W5D O27D 102.5(5) . .
O13D W5D O27D 156.2(4) . .
O15D W5D O27D 85.1(4) . .
O25D W5D O27D 82.1(4) . .
O17D W5D O23D 175.4(4) . .
O13D W5D O23D 82.6(3) . .
O15D W5D O23D 81.4(3) . .
O25D W5D O23D 75.2(3) . .
O27D W5D O23D 74.0(3) . .
O18D W6D O14D 100.3(5) . .
O18D W6D O28D 101.5(5) . .
O14D W6D O28D 157.5(4) . .
O18D W6D O16D 101.2(5) . .
O14D W6D O16D 95.2(4) . .
O28D W6D O16D 86.0(4) . .
O18D W6D O26D 101.9(5) . .
O14D W6D O26D 87.3(4) . .
O28D W6D O26D 82.8(4) . .
O16D W6D O26D 155.9(4) . .
O18D W6D O24D 175.7(4) . .
O14D W6D O24D 83.0(3) . .
O28D W6D O24D 75.0(4) . .
O16D W6D O24D 81.1(3) . .
O26D W6D O24D 75.4(4) . .
O33D W7D O29D 101.7(5) . .
O33D W7D O19D 104.2(5) . .
O29D W7D O19D 89.5(4) . .
O33D W7D O25D 98.7(5) . .
O29D W7D O25D 159.5(4) . .
O19D W7D O25D 84.9(4) . .
O33D W7D O31D 99.5(5) . .
O29D W7D O31D 89.7(4) . .
O19D W7D O31D 156.0(4) . .
O25D W7D O31D 87.6(4) . .
O33D W7D O23D 171.1(4) . .
O29D W7D O23D 84.1(4) . .
O19D W7D O23D 82.4(3) . .
O25D W7D O23D 75.6(3) . .
O31D W7D O23D 73.7(3) . .
O34D W8D O20D 103.9(5) . .
O34D W8D O29D 101.1(5) . .
O20D W8D O29D 90.8(4) . .
O34D W8D O26D 100.4(5) . .
O20D W8D O26D 86.6(4) . .
O29D W8D O26D 158.4(4) . .
O34D W8D O32D 101.4(5) . .
O20D W8D O32D 154.5(4) . .
O29D W8D O32D 87.5(4) . .
O26D W8D O32D 85.7(4) . .
O34D W8D O24D 172.1(5) . .
O20D W8D O24D 82.4(4) . .
O29D W8D O24D 83.4(4) . .
O26D W8D O24D 75.0(4) . .
O32D W8D O24D 72.2(4) . .
O35D W9D O27D 100.9(5) . .
O35D W9D O30D 101.0(5) . .
O27D W9D O30D 157.3(4) . .
O35D W9D O31D 101.6(5) . .
O27D W9D O31D 89.8(4) . .
O30D W9D O31D 91.7(4) . .
O35D W9D O21D 101.9(5) . .
O27D W9D O21D 83.1(4) . .
O30D W9D O21D 86.5(4) . .
O31D W9D O21D 156.4(4) . .
O35D W9D O23D 173.6(4) . .
O27D W9D O23D 74.9(3) . .
O30D W9D O23D 83.8(3) . .
O31D W9D O23D 73.7(3) . .
O21D W9D O23D 82.6(3) . .
O36D W10D O32D 102.8(5) . .
O36D W10D O30D 102.1(5) . .
O32D W10D O30D 94.3(4) . .
O36D W10D O28D 99.7(5) . .
O32D W10D O28D 90.1(4) . .
O30D W10D O28D 156.1(4) . .
O36D W10D O22D 101.6(5) . .
O32D W10D O22D 155.2(4) . .
O30D W10D O22D 84.9(4) . .
O28D W10D O22D 81.4(4) . .
O36D W10D O24D 172.9(5) . .
O32D W10D O24D 73.6(4) . .
O30D W10D O24D 84.4(3) . .
O28D W10D O24D 74.4(4) . .
O22D W10D O24D 81.7(3) . .
O4A Co1A O2A 172.4(3) 2_656 .
O4A Co1A O1A 89.0(3) 2_656 .
O2A Co1A O1A 90.5(3) . .
O4A Co1A O3A 92.9(3) 2_656 2_656
O2A Co1A O3A 86.8(3) . 2_656
O1A Co1A O3A 174.2(3) . 2_656
O4A Co1A O5A 107.2(3) 2_656 .
O2A Co1A O5A 80.2(3) . .
O1A Co1A O5A 78.9(3) . .
O3A Co1A O5A 105.7(3) 2_656 .
O4A Co1A O11A 74.7(3) 2_656 2_656
O2A Co1A O11A 97.9(3) . 2_656
O1A Co1A O11A 100.7(3) . 2_656
O3A Co1A O11A 74.6(3) 2_656 2_656
O5A Co1A O11A 178.1(3) . 2_656
O4B Co1B O2B 172.7(3) 2 .
O4B Co1B O1B 90.1(3) 2 .
O2B Co1B O1B 89.3(3) . .
O4B Co1B O3B 93.3(3) 2 2
O2B Co1B O3B 86.5(3) . 2
O1B Co1B O3B 172.9(3) . 2
O4B Co1B O5B 107.0(3) 2 .
O2B Co1B O5B 80.1(3) . .
O1B Co1B O5B 79.1(3) . .
O3B Co1B O5B 105.7(3) 2 .
O4B Co1B O11B 75.2(3) 2 2
O2B Co1B O11B 97.7(3) . 2
O1B Co1B O11B 100.4(3) . 2
O3B Co1B O11B 74.6(3) 2 2
O5B Co1B O11B 177.7(3) . 2
O1C Co1C O3C 173.6(3) . 2_665
O1C Co1C O2C 90.0(3) . .
O3C Co1C O2C 88.9(3) 2_665 .
O1C Co1C O4C 87.4(3) . 2_665
O3C Co1C O4C 92.8(3) 2_665 2_665
O2C Co1C O4C 172.0(3) . 2_665
O1C Co1C O5C 78.9(3) . .
O3C Co1C O5C 107.1(3) 2_665 .
O2C Co1C O5C 80.5(3) . .
O4C Co1C O5C 106.3(3) 2_665 .
O1C Co1C O11C 99.4(3) . 2_665
O3C Co1C O11C 74.6(3) 2_665 2_665
O2C Co1C O11C 98.6(3) . 2_665
O4C Co1C O11C 74.4(3) 2_665 2_665
O5C Co1C O11C 178.0(3) . 2_665
O4D Co1D O2D 173.4(4) 2_766 .
O4D Co1D O3D 91.2(4) 2_766 2_766
O2D Co1D O3D 89.5(4) . 2_766
O4D Co1D O1D 88.8(3) 2_766 .
O2D Co1D O1D 89.8(4) . .
O3D Co1D O1D 174.0(4) 2_766 .
O4D Co1D O5D 106.7(3) 2_766 .
O2D Co1D O5D 79.2(3) . .
O3D Co1D O5D 107.4(3) 2_766 .
O1D Co1D O5D 78.4(3) . .
O4D Co1D O11D 74.1(3) 2_766 2_766
O2D Co1D O11D 99.9(3) . 2_766
O3D Co1D O11D 73.4(3) 2_766 2_766
O1D Co1D O11D 100.8(3) . 2_766
O5D Co1D O11D 178.8(3) . 2_766
O6A Si1A O5A 112.6(4) . .
O6A Si1A O23A 108.5(4) . .
O5A Si1A O23A 108.8(4) . .
O6A Si1A O24A 109.1(4) . .
O5A Si1A O24A 109.5(4) . .
O23A Si1A O24A 108.2(4) . .
O6B Si1B O5B 112.8(4) . .
O6B Si1B O24B 109.4(4) . .
O5B Si1B O24B 108.9(4) . .
O6B Si1B O23B 108.2(4) . .
O5B Si1B O23B 109.1(4) . .
O24B Si1B O23B 108.3(4) . .
O6C Si1C O5C 112.0(4) . .
O6C Si1C O23C 108.8(4) . .
O5C Si1C O23C 109.8(4) . .
O6C Si1C O24C 109.2(4) . .
O5C Si1C O24C 108.6(4) . .
O23C Si1C O24C 108.4(4) . .
O6D Si1D O5D 112.8(4) . .
O6D Si1D O23D 108.8(4) . .
O5D Si1D O23D 109.3(4) . .
O6D Si1D O24D 109.0(4) . .
O5D Si1D O24D 108.7(4) . .
O23D Si1D O24D 108.0(4) . .
W1A O1A Co1A 109.7(4) . .
W2A O2A Co1A 111.7(4) . .
Co1A O3A W3A 101.7(3) 2_656 .
W4A O4A Co1A 104.2(3) . 2_656
Si1A O5A Co1A 123.2(4) . .
Si1A O5A W1A 124.3(4) . .
Co1A O5A W1A 95.4(3) . .
Si1A O5A W2A 125.2(4) . .
Co1A O5A W2A 87.9(3) . .
W1A O5A W2A 90.9(3) . .
Si1A O6A W4A 124.6(4) . .
Si1A O6A W3A 126.1(4) . .
W4A O6A W3A 95.7(3) . .
W1A O8A W2A 121.6(4) . .
W5A O13A W1A 142.5(4) . .
W6A O14A W2A 147.2(5) . .
W5A O15A W3A 142.5(4) . .
W4A O16A W6A 140.8(5) . .
W3A O11A W4A 117.4(4) . .
W3A O11A Co1A 100.2(3) . 2_656
W4A O11A Co1A 96.3(3) . 2_656
W1A O19A W7A 147.2(5) . .
W8A O20A W2A 145.5(5) . .
W3A O21A W9A 143.0(5) . .
W4A O22A W10A 143.2(5) . .
Si1A O23A W5A 122.9(4) . .
Si1A O23A W7A 127.4(4) . .
W5A O23A W7A 90.7(3) . .
Si1A O23A W9A 124.7(4) . .
W5A O23A W9A 90.7(3) . .
W7A O23A W9A 89.6(3) . .
Si1A O24A W8A 123.8(4) . .
Si1A O24A W10A 124.2(4) . .
W8A O24A W10A 92.9(3) . .
Si1A O24A W6A 125.5(4) . .
W8A O24A W6A 90.1(3) . .
W10A O24A W6A 90.1(3) . .
W7A O25A W5A 119.1(4) . .
W6A O26A W8A 118.1(4) . .
W9A O27A W5A 120.3(4) . .
W10A O28A W6A 119.6(4) . .
W7A O29A W8A 155.2(5) . .
W9A O30A W10A 163.7(5) . .
W9A O31A W7A 121.3(4) . .
W10A O32A W8A 120.8(5) . .
W1B O1B Co1B 109.1(4) . .
W2B O2B Co1B 111.4(4) . .
Co1B O3B W3B 101.9(3) 2 .
W4B O4B Co1B 104.3(4) . 2
Si1B O5B Co1B 122.6(4) . .
Si1B O5B W1B 124.5(4) . .
Co1B O5B W1B 95.2(3) . .
Si1B O5B W2B 125.4(4) . .
Co1B O5B W2B 88.8(3) . .
W1B O5B W2B 90.5(3) . .
Si1B O6B W3B 126.2(4) . .
Si1B O6B W4B 123.8(4) . .
W3B O6B W4B 96.3(3) . .
W1B O8B W2B 121.4(4) . .
W5B O13B W1B 143.0(4) . .
W6B O14B W2B 146.1(5) . .
W5B O15B W3B 142.5(4) . .
W4B O16B W6B 141.0(4) . .
W3B O11B W4B 116.8(4) . .
W3B O11B Co1B 99.7(3) . 2
W4B O11B Co1B 95.5(3) . 2
W1B O19B W7B 148.3(5) . .
W8B O20B W2B 144.5(5) . .
W3B O21B W9B 142.6(5) . .
W4B O22B W10B 143.9(5) . .
Si1B O23B W5B 123.0(4) . .
Si1B O23B W7B 126.9(4) . .
W5B O23B W7B 90.4(3) . .
Si1B O23B W9B 125.3(4) . .
W5B O23B W9B 91.0(3) . .
W7B O23B W9B 89.5(3) . .
Si1B O24B W8B 124.1(4) . .
Si1B O24B W10B 124.1(4) . .
W8B O24B W10B 92.3(3) . .
Si1B O24B W6B 126.1(4) . .
W8B O24B W6B 89.7(3) . .
W10B O24B W6B 90.2(3) . .
W7B O25B W5B 119.4(4) . .
W6B O26B W8B 118.3(4) . .
W9B O27B W5B 119.7(4) . .
W6B O28B W10B 120.4(4) . .
W7B O29B W8B 157.9(5) . .
W10B O30B W9B 162.4(5) . .
W9B O31B W7B 120.0(5) . .
W10B O32B W8B 120.9(5) . .
W1C O1C Co1C 111.7(4) . .
W2C O2C Co1C 109.9(4) . .
W3C O3C Co1C 103.7(3) . 2_665
W4C O4C Co1C 103.1(3) . 2_665
Si1C O5C Co1C 123.1(4) . .
Si1C O5C W1C 124.8(4) . .
Co1C O5C W1C 91.7(3) . .
Si1C O5C W2C 125.4(4) . .
Co1C O5C W2C 91.5(3) . .
W1C O5C W2C 90.3(3) . .
Si1C O6C W3C 125.0(4) . .
Si1C O6C W4C 124.7(4) . .
W3C O6C W4C 95.9(3) . .
W2C O8C W1C 121.7(5) . .
W5C O13C W1C 145.6(5) . .
W6C O14C W2C 143.9(5) . .
W3C O15C W5C 142.2(4) . .
W4C O16C W6C 142.7(4) . .
W4C O11C W3C 117.0(4) . .
W4C O11C Co1C 97.7(3) . 2_665
W3C O11C Co1C 97.2(3) . 2_665
W7C O19C W1C 145.6(5) . .
W8C O20C W2C 146.4(5) . .
W3C O21C W9C 144.3(5) . .
W4C O22C W10C 144.3(5) . .
Si1C O23C W7C 125.1(4) . .
Si1C O23C W9C 125.1(4) . .
W7C O23C W9C 91.4(3) . .
Si1C O23C W5C 124.5(4) . .
W7C O23C W5C 89.8(3) . .
W9C O23C W5C 90.4(3) . .
Si1C O24C W6C 124.5(4) . .
Si1C O24C W8C 125.8(4) . .
W6C O24C W8C 90.2(3) . .
Si1C O24C W10C 124.2(4) . .
W6C O24C W10C 90.9(3) . .
W8C O24C W10C 90.8(3) . .
W5C O25C W7C 119.4(4) . .
W6C O26C W8C 119.6(5) . .
W9C O27C W5C 119.7(5) . .
W10C O28C W6C 119.7(4) . .
W7C O29C W8C 157.3(5) . .
W10C O30C W9C 162.3(5) . .
W9C O31C W7C 120.3(5) . .
W10C O32C W8C 120.6(5) . .
W1D O1D Co1D 110.6(4) . .
W2D O2D Co1D 111.9(4) . .
W3D O3D Co1D 104.2(4) . 2_766
Co1D O4D W4D 103.9(4) 2_766 .
Si1D O5D Co1D 123.2(4) . .
Si1D O5D W1D 124.7(4) . .
Co1D O5D W1D 93.0(3) . .
Si1D O5D W2D 125.3(4) . .
Co1D O5D W2D 90.0(3) . .
W1D O5D W2D 90.6(3) . .
Si1D O6D W4D 125.1(4) . .
Si1D O6D W3D 125.5(4) . .
W4D O6D W3D 95.8(3) . .
W1D O8D W2D 120.5(4) . .
W5D O13D W1D 144.5(5) . .
W6D O14D W2D 146.0(5) . .
W3D O15D W5D 142.8(5) . .
W4D O16D W6D 141.9(5) . .
W3D O11D W4D 117.1(4) . .
W3D O11D Co1D 97.4(3) . 2_766
W4D O11D Co1D 97.7(3) . 2_766
W7D O19D W1D 146.5(5) . .
W8D O20D W2D 145.8(5) . .
W3D O21D W9D 142.6(5) . .
W4D O22D W10D 143.1(5) . .
Si1D O23D W5D 123.9(4) . .
Si1D O23D W7D 125.9(4) . .
W5D O23D W7D 90.2(3) . .
Si1D O23D W9D 124.3(4) . .
W5D O23D W9D 90.7(3) . .
W7D O23D W9D 91.4(3) . .
Si1D O24D W6D 124.4(4) . .
Si1D O24D W8D 125.2(4) . .
W6D O24D W8D 90.2(3) . .
Si1D O24D W10D 124.5(4) . .
W6D O24D W10D 90.5(3) . .
W8D O24D W10D 91.6(3) . .
W7D O25D W5D 118.6(5) . .
W6D O26D W8D 118.8(5) . .
W9D O27D W5D 120.3(5) . .
W10D O28D W6D 120.1(5) . .
W7D O29D W8D 157.9(6) . .
W9D O30D W10D 163.1(6) . .
W9D O31D W7D 120.5(5) . .
W10D O32D W8D 122.1(6) . .
C5A N1A C1A 105.6(12) . .
C5A N1A C9A 113.9(12) . .
C1A N1A C9A 110.4(12) . .
C5A N1A C13A 110.4(12) . .
C1A N1A C13A 111.6(12) . .
C9A N1A C13A 105.1(12) . .
C5B N1B C1B 106.9(17) . .
C5B N1B C13B 113.2(16) . .
C1B N1B C13B 113.2(16) . .
C5B N1B C9B 111.7(16) . .
C1B N1B C9B 108.8(16) . .
C13B N1B C9B 102.9(15) . .
C5C N1C C63C 92(3) . .
C5C N1C C9C 139(3) . .
C63C N1C C9C 124(3) . .
C5C N1C C1C 110(2) . .
C63C N1C C1C 74(2) . .
C9C N1C C1C 99(2) . .
C5C N1C C59C 112(2) . .
C63C N1C C59C 150(3) . .
C9C N1C C59C 27.8(19) . .
C1C N1C C59C 112(2) . .
C5C N1C C55C 39(2) . .
C63C N1C C55C 113(3) . .
C9C N1C C55C 103(3) . .
C1C N1C C55C 146(3) . .
C59C N1C C55C 79(3) . .
C5C N1C C13C 111(2) . .
C63C N1C C13C 45(2) . .
C9C N1C C13C 88(2) . .
C1C N1C C13C 105.3(18) . .
C59C N1C C13C 107(2) . .
C55C N1C C13C 102(3) . .
C5C N1C C51C 72.0(19) . .
C63C N1C C51C 106(2) . .
C9C N1C C51C 109(2) . .
C1C N1C C51C 49.5(16) . .
C59C N1C C51C 99(2) . .
C55C N1C C51C 98(3) . .
C13C N1C C51C 150.4(19) . .
C1D N1D C13D 110.6(11) . .
C1D N1D C9D 112.2(11) . .
C13D N1D C9D 105.9(11) . .
C1D N1D C5D 104.4(12) . .
C13D N1D C5D 111.3(12) . .
C9D N1D C5D 112.7(12) . .
C5E N1E C9E 112.2(14) . .
C5E N1E C13E 105.9(14) . .
C9E N1E C13E 112.6(14) . .
C5E N1E C1E 108.2(15) . .
C9E N1E C1E 107.3(15) . .
C13E N1E C1E 110.6(15) . .
C5F N1F C9F 112.0(13) . .
C5F N1F C13F 111.8(14) . .
C9F N1F C13F 106.2(13) . .
C5F N1F C1F 105.6(12) . .
C9F N1F C1F 112.4(13) . .
C13F N1F C1F 108.9(13) . .
C9G N1G C13G 102(3) . .
C9G N1G C63G 112(2) . .
C13G N1G C63G 19(3) . .
C9G N1G C1G 108.9(17) . .
C13G N1G C1G 124(3) . .
C63G N1G C1G 105(2) . .
C9G N1G C5G 111.7(18) . .
C13G N1G C5G 108(3) . .
C63G N1G C5G 115(2) . .
C1G N1G C5G 102.6(17) . .
C13H N1H C1H 112.0(13) . .
C13H N1H C5H 108.7(13) . .
C1H N1H C5H 108.9(13) . .
C13H N1H C9H 109.3(12) . .
C1H N1H C9H 106.4(13) . .
C5H N1H C9H 111.6(13) . .
C13I N1I C9I 106.6(13) . .
C13I N1I C5I 111.1(12) . .
C9I N1I C5I 110.5(12) . .
C13I N1I C1I 114.0(12) . .
C9I N1I C1I 111.7(12) . .
C5I N1I C1I 103.0(11) . .
C13J N1J C9J 106.8(12) . .
C13J N1J C5J 111.8(12) . .
C9J N1J C5J 111.3(12) . .
C13J N1J C1J 110.7(12) . .
C9J N1J C1J 111.6(12) . .
C5J N1J C1J 104.8(11) . .
C59K N1K C5K 149(3) . .
C59K N1K C51K 115(3) . .
C5K N1K C51K 89(2) . .
C59K N1K C9K 40(3) . .
C5K N1K C9K 112(2) . .
C51K N1K C9K 154(3) . .
C59K N1K C63K 113(3) . .
C5K N1K C63K 73(2) . .
C51K N1K C63K 112(3) . .
C9K N1K C63K 90(3) . .
C59K N1K C13K 96(3) . .
C5K N1K C13K 110(2) . .
C51K N1K C13K 77(2) . .
C9K N1K C13K 108(2) . .
C63K N1K C13K 52(2) . .
C59K N1K C1K 76(3) . .
C5K N1K C1K 113(2) . .
C51K N1K C1K 46(2) . .
C9K N1K C1K 109(2) . .
C63K N1K C1K 154(3) . .
C13K N1K C1K 104(2) . .
C59K N1K C55K 108(3) . .
C5K N1K C55K 42.7(19) . .
C51K N1K C55K 108(2) . .
C9K N1K C55K 81(2) . .
C63K N1K C55K 100(3) . .
C13K N1K C55K 150(2) . .
C1K N1K C55K 100(2) . .
C1L N1L C9L 109.3(16) . .
C1L N1L C13L 109.4(18) . .
C9L N1L C13L 114.0(17) . .
C1L N1L C5L 105.8(18) . .
C9L N1L C5L 113.6(17) . .
C13L N1L C5L 104.3(18) . .
C2A C1A N1A 113.8(15) . .
C1A C2A C3A 111.7(19) . .
C2A C3A C4A 105(2) . .
N1A C5A C6A 113.2(13) . .
C7A C6A C5A 107.1(14) . .
C6A C7A C8A 113.9(14) . .
N1A C9A C10A 113.6(13) . .
C11A C10A C9A 108.8(14) . .
C10A C11A C12A 109.0(15) . .
N1A C13A C14A 114.9(13) . .
C15A C14A C13A 109.8(14) . .
C16A C15A C14A 108.1(16) . .
C2B C1B N1B 118(2) . .
C53B C2B C1B 117(4) . .
C53B C2B C3B 52(3) . .
C1B C2B C3B 116(2) . .
C4B C3B C53B 93(4) . .
C4B C3B C2B 119(3) . .
C53B C3B C2B 48(3) . .
C4B C3B C54B 17(3) . .
C53B C3B C54B 79(4) . .
C2B C3B C54B 113(3) . .
C54B C4B C3B 129(9) . .
C54B C4B C53B 88(9) . .
C3B C4B C53B 45(3) . .
C2B C53B C3B 79(4) . .
C2B C53B C4B 105(5) . .
C3B C53B C4B 42(3) . .
C2B C53B C54B 121(5) . .
C3B C53B C54B 60(4) . .
C4B C53B C54B 19(2) . .
C4B C54B C3B 34(7) . .
C4B C54B C53B 72(8) . .
C3B C54B C53B 41(3) . .
N1B C5B C6B 115.7(18) . .
C7B C6B C5B 107.8(19) . .
C6B C7B C8B 108(2) . .
C60B C9B N1B 115(4) . .
C60B C9B C10B 28(3) . .
N1B C9B C10B 114(2) . .
C60B C10B C11B 84(9) . .
C60B C10B C9B 66(8) . .
C11B C10B C9B 108(4) . .
C60B C10B C61B 76(9) . .
C11B C10B C61B 9(7) . .
C9B C10B C61B 101(6) . .
C62B C11B C12B 117(9) . .
C62B C11B C10B 114(8) . .
C12B C11B C10B 122(6) . .
C62B C11B C60B 140(9) . .
C12B C11B C60B 102(6) . .
C10B C11B C60B 28(3) . .
C61B C12B C11B 11(7) . .
C10B C60B C9B 86(9) . .
C10B C60B C11B 67(8) . .
C9B C60B C11B 109(6) . .
C10B C60B C61B 76(9) . .
C9B C60B C61B 107(8) . .
C11B C60B C61B 10(6) . .
C62B C61B C12B 114(10) . .
C62B C61B C10B 98(9) . .
C12B C61B C10B 119(10) . .
C62B C61B C60B 125(10) . .
C12B C61B C60B 105(10) . .
C10B C61B C60B 27(4) . .
C11B C62B C61B 13(10) . .
C14B C13B C64B 7(7) . .
C14B C13B N1B 109(3) . .
C64B C13B N1B 113(4) . .
C13B C14B C15B 104(3) . .
C13B C14B C65B 112(5) . .
C15B C14B C65B 8(4) . .
C64B C15B C16B 115(5) . .
C64B C15B C14B 6(8) . .
C16B C15B C14B 112(4) . .
C64B C15B C66B 100(5) . .
C16B C15B C66B 36(2) . .
C14B C15B C66B 100(4) . .
C66B C16B C65B 82(5) . .
C66B C16B C15B 84(5) . .
C65B C16B C15B 3(7) . .
C15B C64B C13B 109(6) . .
C15B C64B C65B 9(3) . .
C13B C64B C65B 118(5) . .
C16B C65B C64B 124(7) . .
C16B C65B C66B 42(3) . .
C64B C65B C66B 106(5) . .
C16B C65B C14B 120(7) . .
C64B C65B C14B 5(8) . .
C66B C65B C14B 106(7) . .
C16B C66B C65B 56(5) . .
C16B C66B C15B 60(4) . .
C65B C66B C15B 3(6) . .
C2C C1C C51C 65(2) . .
C2C C1C C52C 21.3(18) . .
C51C C1C C52C 44(2) . .
C2C C1C N1C 129(3) . .
C51C C1C N1C 70(2) . .
C52C C1C N1C 111(2) . .
C2C C1C C63C 163(3) . .
C51C C1C C63C 104(3) . .
C52C C1C C63C 146(3) . .
N1C C1C C63C 50.8(19) . .
C52C C2C C1C 103(6) . .
C52C C2C C3C 108(6) . .
C1C C2C C3C 138(3) . .
C52C C2C C51C 43(5) . .
C1C C2C C51C 60(2) . .
C3C C2C C51C 144(3) . .
C52C C2C C53C 75(6) . .
C1C C2C C53C 159(3) . .
C3C C2C C53C 34.6(18) . .
C51C C2C C53C 116(3) . .
C53C C3C C2C 82(4) . .
C53C C3C C4C 80(4) . .
C2C C3C C4C 154(3) . .
C53C C3C C54C 44(3) . .
C2C C3C C54C 126(3) . .
C4C C3C C54C 39.2(18) . .
C53C C3C C52C 63(3) . .
C2C C3C C52C 19.6(18) . .
C4C C3C C52C 141(3) . .
C54C C3C C52C 107(3) . .
C54C C4C C3C 83(3) . .
C54C C4C C53C 51(3) . .
C3C C4C C53C 35.1(18) . .
C52C C51C C1C 76(3) . .
C52C C51C C2C 21(2) . .
C1C C51C C2C 55(2) . .
C52C C51C N1C 131(3) . .
C1C C51C N1C 60.3(19) . .
C2C C51C N1C 112(2) . .
C52C C51C C5C 172(4) . .
C1C C51C C5C 98(3) . .
C2C C51C C5C 153(3) . .
N1C C51C C5C 47.1(14) . .
C2C C52C C51C 116(7) . .
C2C C52C C53C 83(6) . .
C51C C52C C53C 154(4) . .
C2C C52C C1C 56(5) . .
C51C C52C C1C 60(3) . .
C53C C52C C1C 134(3) . .
C2C C52C C3C 52(5) . .
C51C C52C C3C 154(4) . .
C53C C52C C3C 31.8(17) . .
C1C C52C C3C 103(3) . .
C3C C53C C54C 105(4) . .
C3C C53C C52C 85(4) . .
C54C C53C C52C 169(4) . .
C3C C53C C4C 65(3) . .
C54C C53C C4C 44(2) . .
C52C C53C C4C 147(3) . .
C3C C53C C2C 63(3) . .
C54C C53C C2C 168(4) . .
C52C C53C C2C 22.3(16) . .
C4C C53C C2C 125(3) . .
C4C C54C C53C 85(3) . .
C4C C54C C3C 58(3) . .
C53C C54C C3C 31(2) . .
C55C C5C C56C 81(5) . .
C55C C5C N1C 80(4) . .
C56C C5C N1C 143(4) . .
C55C C5C C6C 41(4) . .
C56C C5C C6C 41(3) . .
N1C C5C C6C 113(3) . .
C55C C5C C51C 116(5) . .
C56C C5C C51C 155(4) . .
N1C C5C C51C 60.9(17) . .
C6C C5C C51C 155(3) . .
C56C C6C C55C 100(6) . .
C56C C6C C5C 60(4) . .
C55C C6C C5C 41(4) . .
C56C C6C C7C 54(4) . .
C55C C6C C7C 138(5) . .
C5C C6C C7C 107(3) . .
C56C C6C C57C 73(5) . .
C55C C6C C57C 133(5) . .
C5C C6C C57C 117(4) . .
C7C C6C C57C 21(2) . .
C57C C7C C56C 117(10) . .
C57C C7C C58C 64(9) . .
C56C C7C C58C 129(5) . .
C57C C7C C6C 83(9) . .
C56C C7C C6C 39(3) . .
C58C C7C C6C 132(4) . .
C57C C7C C8C 55(9) . .
C56C C7C C8C 105(4) . .
C58C C7C C8C 30(3) . .
C6C C7C C8C 103(3) . .
C58C C8C C57C 59(6) . .
C58C C8C C7C 54(5) . .
C57C C8C C7C 20(3) . .
C5C C55C C6C 98(7) . .
C5C C55C C56C 59(5) . .
C6C C55C C56C 40(4) . .
C5C C55C N1C 61(4) . .
C6C C55C N1C 140(6) . .
C56C C55C N1C 112(5) . .
C5C C55C C59C 104(5) . .
C6C C55C C59C 155(6) . .
C56C C55C C59C 162(5) . .
N1C C55C C59C 50(2) . .
C6C C56C C7C 87(5) . .
C6C C56C C5C 80(5) . .
C7C C56C C5C 145(6) . .
C6C C56C C55C 40(4) . .
C7C C56C C55C 118(6) . .
C5C C56C C55C 40(3) . .
C6C C56C C57C 72(5) . .
C7C C56C C57C 18(3) . .
C5C C56C C57C 129(6) . .
C55C C56C C57C 100(5) . .
C7C C57C C58C 90(10) . .
C7C C57C C8C 105(10) . .
C58C C57C C8C 36(4) . .
C7C C57C C6C 76(9) . .
C58C C57C C6C 141(7) . .
C8C C57C C6C 113(5) . .
C7C C57C C56C 45(8) . .
C58C C57C C56C 112(6) . .
C8C C57C C56C 100(5) . .
C6C C57C C56C 36(3) . .
C8C C58C C57C 85(7) . .
C8C C58C C7C 96(7) . .
C57C C58C C7C 26(4) . .
C59C C9C C10C 104(6) . .
C59C C9C C60C 51(5) . .
C10C C9C C60C 53(3) . .
C59C C9C N1C 83(6) . .
C10C C9C N1C 158(4) . .
C60C C9C N1C 126(4) . .
C60C C10C C9C 69(4) . .
C60C C10C C11C 86(4) . .
C9C C10C C11C 142(5) . .
C60C C10C C61C 70(3) . .
C9C C10C C61C 132(4) . .
C11C C10C C61C 17(2) . .
C60C C10C C59C 42(3) . .
C9C C10C C59C 27(2) . .
C11C C10C C59C 120(4) . .
C61C C10C C59C 107(3) . .
C10C C11C C62C 130(4) . .
C10C C11C C60C 41(2) . .
C62C C11C C60C 108(3) . .
C10C C11C C12C 113(4) . .
C62C C11C C12C 35(2) . .
C60C C11C C12C 77(3) . .
C62C C12C C61C 60(4) . .
C62C C12C C11C 53(3) . .
C61C C12C C11C 8(3) . .
C9C C59C C60C 96(6) . .
C9C C59C N1C 70(5) . .
C60C C59C N1C 147(4) . .
C9C C59C C10C 49(5) . .
C60C C59C C10C 48(3) . .
N1C C59C C10C 115(3) . .
C9C C59C C55C 114(6) . .
C60C C59C C55C 149(5) . .
N1C C59C C55C 51(2) . .
C10C C59C C55C 163(4) . .
C59C C60C C10C 90(4) . .
C59C C60C C9C 33(3) . .
C10C C60C C9C 58(3) . .
C59C C60C C61C 142(5) . .
C10C C60C C61C 64(3) . .
C9C C60C C61C 118(4) . .
C59C C60C C11C 131(4) . .
C10C C60C C11C 53(3) . .
C9C C60C C11C 105(3) . .
C61C C60C C11C 13(3) . .
C62C C61C C12C 45(3) . .
C62C C61C C10C 139(5) . .
C12C C61C C10C 136(4) . .
C62C C61C C60C 134(4) . .
C12C C61C C60C 98(3) . .
C10C C61C C60C 46(3) . .
C12C C62C C61C 75(4) . .
C12C C62C C11C 92(4) . .
C61C C62C C11C 18(3) . .
C64C C13C C63C 89(5) . .
C64C C13C C14C 36(3) . .
C63C C13C C14C 55(3) . .
C64C C13C N1C 147(5) . .
C63C C13C N1C 62(3) . .
C14C C13C N1C 112(2) . .
C64C C14C C63C 83(5) . .
C64C C14C C65C 80(5) . .
C63C C14C C65C 153(4) . .
C64C C14C C15C 76(4) . .
C63C C14C C15C 135(4) . .
C65C C14C C15C 19(2) . .
C64C C14C C13C 37(4) . .
C63C C14C C13C 47(3) . .
C65C C14C C13C 116(4) . .
C15C C14C C13C 109(3) . .
C65C C15C C66C 72(10) . .
C65C C15C C14C 71(10) . .
C66C C15C C14C 114(3) . .
C65C C15C C64C 80(10) . .
C66C C15C C64C 146(4) . .
C14C C15C C64C 35(2) . .
C65C C15C C16C 45(9) . .
C66C C15C C16C 32(2) . .
C14C C15C C16C 87(3) . .
C64C C15C C16C 114(3) . .
C66C C16C C65C 76(5) . .
C66C C16C C15C 63(4) . .
C65C C16C C15C 16(3) . .
C13C C63C C14C 78(4) . .
C13C C63C N1C 73(3) . .
C14C C63C N1C 141(4) . .
C13C C63C C64C 40(3) . .
C14C C63C C64C 38(3) . .
N1C C63C C64C 112(4) . .
C13C C63C C1C 111(4) . .
C14C C63C C1C 164(4) . .
N1C C63C C1C 55(2) . .
C64C C63C C1C 146(4) . .
C14C C64C C13C 107(6) . .
C14C C64C C63C 58(4) . .
C13C C64C C63C 50(4) . .
C14C C64C C65C 64(4) . .
C13C C64C C65C 168(6) . .
C63C C64C C65C 119(5) . .
C14C C64C C15C 69(4) . .
C13C C64C C15C 153(5) . .
C63C C64C C15C 115(4) . .
C65C C64C C15C 18(2) . .
C15C C65C C16C 119(10) . .
C15C C65C C66C 88(10) . .
C16C C65C C66C 37(3) . .
C15C C65C C14C 89(10) . .
C16C C65C C14C 103(4) . .
C66C C65C C14C 124(5) . .
C15C C65C C64C 82(10) . .
C16C C65C C64C 137(5) . .
C66C C65C C64C 157(5) . .
C14C C65C C64C 36(2) . .
C16C C66C C65C 68(5) . .
C16C C66C C15C 85(5) . .
C65C C66C C15C 20(3) . .
N1D C1D C2D 116.4(13) . .
C1D C2D C3D 106.8(16) . .
C4D C3D C2D 110(2) . .
N1D C5D C6D 114.0(15) . .
C5D C6D C7D 107.5(17) . .
C8D C7D C6D 109(2) . .
C10D C9D N1D 114.8(13) . .
C9D C10D C61D 114(3) . .
C9D C10D C11D 102(2) . .
C61D C10D C11D 19(3) . .
C61D C11D C12D 139(10) . .
C61D C11D C62D 57(10) . .
C12D C11D C62D 87(5) . .
C61D C11D C10D 67(10) . .
C12D C11D C10D 116(6) . .
C62D C11D C10D 109(4) . .
C11D C12D C61D 13(5) . .
C11D C12D C62D 54(4) . .
C61D C12D C62D 43(3) . .
C11D C61D C62D 102(10) . .
C11D C61D C10D 94(10) . .
C62D C61D C10D 132(6) . .
C11D C61D C12D 28(10) . .
C62D C61D C12D 78(5) . .
C10D C61D C12D 100(4) . .
C61D C62D C11D 21(4) . .
C61D C62D C12D 59(4) . .
C11D C62D C12D 39(3) . .
C14D C13D N1D 115.7(14) . .
C13D C14D C15D 108.9(16) . .
C16D C15D C14D 112.9(19) . .
C52E C1E N1E 148(10) . .
C52E C1E C2E 47(9) . .
N1E C1E C2E 111(2) . .
C52E C2E C3E 70(10) . .
C52E C2E C1E 53(10) . .
C3E C2E C1E 114(3) . .
C52E C2E C53E 44(10) . .
C3E C2E C53E 63(8) . .
C1E C2E C53E 91(8) . .
C52E C2E C54E 46(10) . .
C3E C2E C54E 28(8) . .
C1E C2E C54E 98(8) . .
C53E C2E C54E 38(9) . .
C54E C3E C4E 112(10) . .
C54E C3E C2E 93(10) . .
C4E C3E C2E 117(3) . .
C54E C3E C52E 54(10) . .
C4E C3E C52E 148(8) . .
C2E C3E C52E 46(8) . .
C54E C3E C53E 36(10) . .
C4E C3E C53E 109(8) . .
C2E C3E C53E 63(8) . .
C52E C3E C53E 41(9) . .
C3E C4E C54E 23(7) . .
C53E C52E C2E 89(10) . .
C53E C52E C54E 54(10) . .
C2E C52E C54E 90(10) . .
C53E C52E C1E 141(10) . .
C2E C52E C1E 80(10) . .
C54E C52E C1E 161(10) . .
C53E C52E C3E 74(10) . .
C2E C52E C3E 64(10) . .
C54E C52E C3E 31(10) . .
C1E C52E C3E 131(10) . .
C54E C53E C52E 69(10) . .
C54E C53E C2E 76(10) . .
C52E C53E C2E 47(10) . .
C54E C53E C3E 26(10) . .
C52E C53E C3E 65(10) . .
C2E C53E C3E 54(7) . .
C3E C54E C53E 119(10) . .
C3E C54E C52E 95(10) . .
C53E C54E C52E 57(10) . .
C3E C54E C2E 59(10) . .
C53E C54E C2E 66(10) . .
C52E C54E C2E 43(10) . .
C3E C54E C4E 45(10) . .
C53E C54E C4E 111(10) . .
C52E C54E C4E 130(10) . .
C2E C54E C4E 87(10) . .
N1E C5E C6E 114.1(16) . .
C7E C6E C5E 108.9(19) . .
C6E C7E C8E 111(2) . .
C10E C9E N1E 114.1(17) . .
C9E C10E C11E 105.5(18) . .
C10E C11E C12E 110(2) . .
C14E C13E N1E 114.0(15) . .
C13E C14E C15E 111.6(18) . .
C66E C15E C14E 113(3) . .
C66E C15E C16E 105(3) . .
C14E C15E C16E 105(2) . .
C2F C1F N1F 116.7(13) . .
C1F C2F C3F 109.2(14) . .
C4F C3F C2F 110.3(16) . .
N1F C5F C6F 114.9(15) . .
C5F C6F C57F 99(4) . .
C5F C6F C7F 110.8(19) . .
C57F C6F C7F 46(3) . .
C57F C7F C58F 77(4) . .
C57F C7F C6F 66.9(18) . .
C58F C7F C6F 128(5) . .
C57F C7F C8F 153(5) . .
C58F C7F C8F 83(4) . .
C6F C7F C8F 115(3) . .
C7F C8F C58F 42(3) . .
C7F C57F C58F 53(5) . .
C7F C57F C6F 66.9(19) . .
C58F C57F C6F 110(6) . .
C7F C58F C57F 50(4) . .
C7F C58F C8F 55(4) . .
C57F C58F C8F 104(6) . .
C10F C9F N1F 113.7(14) . .
C9F C10F C61F 114(2) . .
C9F C10F C11F 110(2) . .
C61F C10F C11F 23(2) . .
C61F C11F C12F 124(10) . .
C61F C11F C62F 80(8) . .
C12F C11F C62F 44(4) . .
C61F C11F C10F 69(8) . .
C12F C11F C10F 132(6) . .
C62F C11F C10F 120(4) . .
C62F C12F C11F 83(6) . .
C62F C12F C61F 63(4) . .
C11F C12F C61F 20(4) . .
C11F C61F C62F 73(8) . .
C11F C61F C10F 88(8) . .
C62F C61F C10F 125(4) . .
C11F C61F C12F 36(7) . .
C62F C61F C12F 37(2) . .
C10F C61F C12F 109(3) . .
C12F C62F C11F 53(4) . .
C12F C62F C61F 80(5) . .
C11F C62F C61F 27(3) . .
N1F C13F C14F 112.4(16) . .
C13F C14F C15F 105.2(18) . .
C16F C15F C14F 112(2) . .
N1G C1G C2G 114.0(18) . .
C1G C2G C3G 104.2(19) . .
C2G C3G C4G 106(2) . .
N1G C5G C6G 108(2) . .
C5G C6G C7G 105(2) . .
C8G C7G C6G 109(2) . .
C60G C9G N1G 151(5) . .
C60G C9G C10G 45(5) . .
N1G C9G C10G 117(2) . .
C61G C10G C60G 96(7) . .
C61G C10G C9G 136(6) . .
C60G C10G C9G 39(4) . .
C61G C10G C11G 39(5) . .
C60G C10G C11G 82(5) . .
C9G C10G C11G 112(3) . .
C61G C11G C62G 74(6) . .
C61G C11G C10G 37(5) . .
C62G C11G C10G 109(4) . .
C61G C11G C12G 143(6) . .
C62G C11G C12G 138(4) . .
C10G C11G C12G 113(3) . .
C61G C11G C60G 59(5) . .
C62G C11G C60G 105(5) . .
C10G C11G C60G 37(3) . .
C12G C11G C60G 112(3) . .
C9G C60G C10G 96(7) . .
C9G C60G C61G 135(8) . .
C10G C60G C61G 39(4) . .
C9G C60G C11G 137(7) . .
C10G C60G C11G 61(4) . .
C61G C60G C11G 35(3) . .
C10G C61G C11G 104(8) . .
C10G C61G C62G 156(9) . .
C11G C61G C62G 62(6) . .
C10G C61G C60G 44(5) . .
C11G C61G C60G 86(6) . .
C62G C61G C60G 113(7) . .
C11G C62G C61G 44(4) . .
C14G C13G N1G 102(4) . .
C14G C13G C64G 42(3) . .
N1G C13G C64G 105(4) . .
C64G C14G C15G 85(5) . .
C64G C14G C13G 83(5) . .
C15G C14G C13G 97(5) . .
C64G C14G C63G 66(4) . .
C15G C14G C63G 102(5) . .
C13G C14G C63G 19(4) . .
C66G C15G C14G 141(8) . .
C66G C15G C16G 55(4) . .
C14G C15G C16G 117(6) . .
C66G C15G C65G 65(4) . .
C14G C15G C65G 92(5) . .
C16G C15G C65G 29(3) . .
C66G C15G C64G 111(6) . .
C14G C15G C64G 42(3) . .
C16G C15G C64G 76(4) . .
C65G C15G C64G 50(2) . .
C65G C16G C66G 93(7) . .
C65G C16G C15G 83(6) . .
C66G C16G C15G 41(3) . .
C14G C63G C64G 49(3) . .
C14G C63G N1G 101(3) . .
C64G C63G N1G 123(3) . .
C14G C64G C65G 108(4) . .
C14G C64G C63G 66(4) . .
C65G C64G C63G 116(3) . .
C14G C64G C13G 54(3) . .
C65G C64G C13G 112(3) . .
C63G C64G C13G 13(3) . .
C14G C64G C15G 53(3) . .
C65G C64G C15G 56(3) . .
C63G C64G C15G 86(3) . .
C13G C64G C15G 75(3) . .
C16G C65G C66G 55(5) . .
C16G C65G C64G 130(7) . .
C66G C65G C64G 107(3) . .
C16G C65G C15G 68(5) . .
C66G C65G C15G 37(3) . .
C64G C65G C15G 74(3) . .
C15G C66G C16G 84(4) . .
C15G C66G C65G 78(5) . .
C16G C66G C65G 32(4) . .
C2H C1H N1H 114.5(15) . .
C1H C2H C3H 108.4(19) . .
C4H C3H C2H 110(2) . .
C6H C5H N1H 120(2) . .
C6H C5H C56H 22(2) . .
N1H C5H C56H 103(3) . .
C56H C6H C57H 101(9) . .
C56H C6H C5H 88(8) . .
C57H C6H C5H 127(4) . .
C56H C6H C7H 127(9) . .
C57H C6H C7H 29(3) . .
C5H C6H C7H 109(3) . .
C56H C6H C58H 155(9) . .
C57H C6H C58H 53(3) . .
C5H C6H C58H 107(3) . .
C7H C6H C58H 29(2) . .
C57H C7H C58H 129(8) . .
C57H C7H C8H 52(5) . .
C58H C7H C8H 105(5) . .
C57H C7H C6H 65(6) . .
C58H C7H C6H 92(5) . .
C8H C7H C6H 110(3) . .
C57H C7H C56H 54(6) . .
C58H C7H C56H 105(5) . .
C8H C7H C56H 103(3) . .
C6H C7H C56H 14(2) . .
C57H C8H C7H 31(3) . .
C57H C8H C58H 51(4) . .
C7H C8H C58H 27(2) . .
C6H C56H C5H 70(8) . .
C6H C56H C57H 58(8) . .
C5H C56H C57H 108(4) . .
C6H C56H C7H 39(7) . .
C5H C56H C7H 88(3) . .
C57H C56H C7H 22(2) . .
C7H C57H C8H 97(7) . .
C7H C57H C6H 85(6) . .
C8H C57H C6H 148(6) . .
C7H C57H C58H 27(5) . .
C8H C57H C58H 91(5) . .
C6H C57H C58H 77(4) . .
C7H C57H C56H 104(7) . .
C8H C57H C56H 149(6) . .
C6H C57H C56H 21(3) . .
C58H C57H C56H 97(5) . .
C7H C58H C57H 23(4) . .
C7H C58H C6H 59(4) . .
C57H C58H C6H 50(3) . .
C7H C58H C8H 48(4) . .
C57H C58H C8H 38(3) . .
C6H C58H C8H 84(3) . .
N1H C9H C10H 113.4(14) . .
C9H C10H C11H 105.8(15) . .
C12H C11H C10H 111.3(17) . .
N1H C13H C14H 115.0(14) . .
C13H C14H C65H 121.3(19) . .
C13H C14H C15H 98.4(18) . .
C65H C14H C15H 27.8(15) . .
C65H C15H C66H 103(5) . .
C65H C15H C16H 46(4) . .
C66H C15H C16H 57(3) . .
C65H C15H C14H 70(4) . .
C66H C15H C14H 128(3) . .
C16H C15H C14H 104(2) . .
C65H C16H C66H 72(3) . .
C65H C16H C15H 28(2) . .
C66H C16H C15H 44(2) . .
C15H C65H C16H 105(5) . .
C15H C65H C66H 47(4) . .
C16H C65H C66H 59(3) . .
C15H C65H C14H 82(4) . .
C16H C65H C14H 134(3) . .
C66H C65H C14H 109(3) . .
C15H C66H C16H 79(3) . .
C15H C66H C65H 30(2) . .
C16H C66H C65H 49(2) . .
C2I C1I N1I 115.1(12) . .
C1I C2I C3I 108.0(13) . .
C4I C3I C2I 110.8(13) . .
N1I C5I C6I 112.1(14) . .
C5I C6I C7I 104.5(18) . .
C8I C7I C6I 110(2) . .
C10I C9I N1I 115.4(16) . .
C9I C10I C11I 100(2) . .
C9I C10I C61I 122(2) . .
C11I C10I C61I 29.3(16) . .
C61I C11I C62I 107(6) . .
C61I C11I C10I 78(4) . .
C62I C11I C10I 139(4) . .
C61I C11I C12I 44(4) . .
C62I C11I C12I 65(3) . .
C10I C11I C12I 102(3) . .
C61I C12I C62I 65(3) . .
C61I C12I C11I 29(2) . .
C62I C12I C11I 37.5(19) . .
C11I C61I C12I 107(5) . .
C11I C61I C62I 41(4) . .
C12I C61I C62I 68(3) . .
C11I C61I C10I 73(4) . .
C12I C61I C10I 124(3) . .
C62I C61I C10I 104(3) . .
C11I C62I C61I 32(3) . .
C11I C62I C12I 78(4) . .
C61I C62I C12I 47(2) . .
N1I C13I C14I 115.0(16) . .
C13I C14I C15I 109.8(18) . .
C16I C15I C14I 110(2) . .
C2J C1J N1J 114.6(13) . .
C1J C2J C3J 113.8(14) . .
C2J C3J C4J 106.8(16) . .
C6J C5J N1J 113.4(12) . .
C7J C6J C5J 109.4(14) . .
C6J C7J C8J 111.6(16) . .
N1J C9J C10J 114.2(13) . .
C11J C10J C9J 107.4(14) . .
C10J C11J C12J 112.0(17) . .
N1J C13J C14J 115.1(15) . .
C13J C14J C15J 109.7(18) . .
C16J C15J C66J 86(4) . .
C16J C15J C14J 114(3) . .
C66J C15J C14J 134(4) . .
C15J C16J C66J 48(3) . .
C15J C66J C16J 46(3) . .
C51K C1K C52K 77(4) . .
C51K C1K C2K 54(3) . .
C52K C1K C2K 25(2) . .
C51K C1K N1K 63(3) . .
C52K C1K N1K 128(3) . .
C2K C1K N1K 113(3) . .
C51K C1K C59K 105(4) . .
C52K C1K C59K 171(4) . .
C2K C1K C59K 159(3) . .
N1K C1K C59K 48(2) . .
C52K C2K C51K 114(8) . .
C52K C2K C3K 82(7) . .
C51K C2K C3K 147(4) . .
C52K C2K C1K 67(7) . .
C51K C2K C1K 52(3) . .
C3K C2K C1K 120(3) . .
C52K C2K C53K 57(7) . .
C51K C2K C53K 155(4) . .
C3K C2K C53K 25(2) . .
C1K C2K C53K 107(3) . .
C53K C3K C2K 95(6) . .
C53K C3K C52K 70(6) . .
C2K C3K C52K 25(2) . .
C53K C3K C4K 83(6) . .
C2K C3K C4K 128(3) . .
C52K C3K C4K 124(3) . .
C53K C3K C54K 49(5) . .
C2K C3K C54K 137(4) . .
C52K C3K C54K 116(4) . .
C4K C3K C54K 41(2) . .
C54K C4K C3K 72(3) . .
C54K C4K C53K 50(3) . .
C3K C4K C53K 27(2) . .
C1K C51K C2K 74(3) . .
C1K C51K N1K 71(3) . .
C2K C51K N1K 138(4) . .
C1K C51K C52K 55(3) . .
C2K C51K C52K 20(3) . .
N1K C51K C52K 118(4) . .
C1K C51K C13K 104(3) . .
C2K C51K C13K 160(4) . .
N1K C51K C13K 53.5(19) . .
C52K C51K C13K 157(4) . .
C2K C52K C1K 89(7) . .
C2K C52K C53K 101(8) . .
C1K C52K C53K 131(5) . .
C2K C52K C3K 73(7) . .
C1K C52K C3K 126(4) . .
C53K C52K C3K 28(2) . .
C2K C52K C51K 45(6) . .
C1K C52K C51K 48(3) . .
C53K C52K C51K 139(5) . .
C3K C52K C51K 113(4) . .
C3K C53K C54K 104(7) . .
C3K C53K C52K 82(6) . .
C54K C53K C52K 157(5) . .
C3K C53K C4K 70(6) . .
C54K C53K C4K 43(3) . .
C52K C53K C4K 124(4) . .
C3K C53K C2K 60(5) . .
C54K C53K C2K 152(5) . .
C52K C53K C2K 22(2) . .
C4K C53K C2K 109(4) . .
C4K C54K C53K 87(5) . .
C4K C54K C3K 66(3) . .
C53K C54K C3K 26(3) . .
C55K C5K C56K 75(3) . .
C55K C5K C6K 41(3) . .
C56K C5K C6K 34(2) . .
C55K C5K N1K 76(3) . .
C56K C5K N1K 145(3) . .
C6K C5K N1K 114(3) . .
C55K C5K C63K 111(4) . .
C56K C5K C63K 157(3) . .
C6K C5K C63K 148(3) . .
N1K C5K C63K 56(2) . .
C56K C6K C55K 116(6) . .
C56K C6K C5K 65(4) . .
C55K C6K C5K 51(3) . .
C56K C6K C57K 43(4) . .
C55K C6K C57K 158(5) . .
C5K C6K C57K 108(3) . .
C56K C6K C7K 72(4) . .
C55K C6K C7K 158(4) . .
C5K C6K C7K 134(3) . .
C57K C6K C7K 30.9(18) . .
C57K C7K C58K 99(5) . .
C57K C7K C8K 71(4) . .
C58K C7K C8K 48(3) . .
C57K C7K C56K 43(4) . .
C58K C7K C56K 135(4) . .
C8K C7K C56K 113(3) . .
C57K C7K C6K 70(4) . .
C58K C7K C6K 138(4) . .
C8K C7K C6K 142(3) . .
C56K C7K C6K 29.7(17) . .
C58K C8K C57K 74(3) . .
C58K C8K C7K 51(3) . .
C57K C8K C7K 35(2) . .
C6K C55K C5K 88(4) . .
C6K C55K C56K 29(3) . .
C5K C55K C56K 59(3) . .
C6K C55K N1K 141(4) . .
C5K C55K N1K 61(3) . .
C56K C55K N1K 117(3) . .
C6K C55K C9K 172(5) . .
C5K C55K C9K 99(3) . .
C56K C55K C9K 156(3) . .
N1K C55K C9K 47.2(16) . .
C6K C56K C57K 107(5) . .
C6K C56K C5K 81(4) . .
C57K C56K C5K 172(5) . .
C6K C56K C55K 35(4) . .
C57K C56K C55K 141(5) . .
C5K C56K C55K 46(2) . .
C6K C56K C7K 78(4) . .
C57K C56K C7K 31(3) . .
C5K C56K C7K 153(4) . .
C55K C56K C7K 110(3) . .
C7K C57K C56K 106(5) . .
C7K C57K C8K 74(4) . .
C56K C57K C8K 170(4) . .
C7K C57K C58K 47(4) . .
C56K C57K C58K 144(4) . .
C8K C57K C58K 43(2) . .
C7K C57K C6K 79(4) . .
C56K C57K C6K 30(3) . .
C8K C57K C6K 152(4) . .
C58K C57K C6K 114(3) . .
C8K C58K C7K 81(4) . .
C8K C58K C57K 63(3) . .
C7K C58K C57K 34(2) . .
C60K C9K C59K 95(6) . .
C60K C9K C10K 41(4) . .
C59K C9K C10K 55(4) . .
C60K C9K N1K 158(6) . .
C59K C9K N1K 66(4) . .
C10K C9K N1K 118(3) . .
C60K C9K C55K 147(5) . .
C59K C9K C55K 104(5) . .
C10K C9K C55K 154(3) . .
N1K C9K C55K 52.2(18) . .
C60K C10K C59K 83(6) . .
C60K C10K C11K 75(5) . .
C59K C10K C11K 154(5) . .
C60K C10K C9K 41(4) . .
C59K C10K C9K 43(3) . .
C11K C10K C9K 116(4) . .
C60K C10K C61K 77(6) . .
C59K C10K C61K 143(5) . .
C11K C10K C61K 17(3) . .
C9K C10K C61K 115(4) . .
C10K C11K C60K 39(3) . .
C10K C11K C12K 115(4) . .
C60K C11K C12K 97(4) . .
C10K C11K C62K 94(3) . .
C60K C11K C62K 94(4) . .
C12K C11K C62K 31(2) . .
C62K C12K C61K 76(6) . .
C62K C12K C11K 88(5) . .
C61K C12K C11K 11(5) . .
C9K C59K C10K 82(5) . .
C9K C59K N1K 74(5) . .
C10K C59K N1K 149(6) . .
C9K C59K C60K 42(4) . .
C10K C59K C60K 41(3) . .
N1K C59K C60K 115(5) . .
C9K C59K C1K 120(6) . .
C10K C59K C1K 155(5) . .
N1K C59K C1K 56(2) . .
C60K C59K C1K 155(5) . .
C10K C60K C9K 98(7) . .
C10K C60K C59K 56(5) . .
C9K C60K C59K 43(4) . .
C10K C60K C11K 66(5) . .
C9K C60K C11K 164(7) . .
C59K C60K C11K 121(5) . .
C10K C60K C61K 68(5) . .
C9K C60K C61K 156(7) . .
C59K C60K C61K 116(5) . .
C11K C60K C61K 16(3) . .
C12K C61K C62K 43(4) . .
C12K C61K C10K 134(6) . .
C62K C61K C10K 109(6) . .
C12K C61K C60K 108(6) . .
C62K C61K C60K 109(6) . .
C10K C61K C60K 35(3) . .
C12K C62K C61K 60(5) . .
C12K C62K C11K 61(5) . .
C61K C62K C11K 2(5) . .
C64K C13K C63K 69(4) . .
C64K C13K C14K 15(4) . .
C63K C13K C14K 58(3) . .
C64K C13K N1K 130(4) . .
C63K C13K N1K 63(3) . .
C14K C13K N1K 116(3) . .
C64K C13K C51K 158(5) . .
C63K C13K C51K 99(3) . .
C14K C13K C51K 157(3) . .
N1K C13K C51K 49.7(18) . .
C15K C14K C63K 133(5) . .
C15K C14K C13K 146(4) . .
C63K C14K C13K 58(3) . .
C15K C14K C65K 43(3) . .
C63K C14K C65K 138(4) . .
C13K C14K C65K 104(3) . .
C15K C14K C66K 24(3) . .
C63K C14K C66K 117(4) . .
C13K C14K C66K 126(4) . .
C65K C14K C66K 38(3) . .
C66K C15K C65K 69(6) . .
C66K C15K C14K 120(7) . .
C65K C15K C14K 88(5) . .
C66K C15K C64K 107(6) . .
C65K C15K C64K 70(4) . .
C14K C15K C64K 19(4) . .
C66K C15K C16K 76(5) . .
C65K C15K C16K 68(4) . .
C14K C15K C16K 145(5) . .
C64K C15K C16K 133(4) . .
C65K C16K C15K 44(3) . .
C65K C16K C66K 44(3) . .
C15K C16K C66K 32(2) . .
C13K C63K C14K 64(3) . .
C13K C63K C64K 48(3) . .
C14K C63K C64K 19(3) . .
C13K C63K N1K 64(3) . .
C14K C63K N1K 122(4) . .
C64K C63K N1K 111(4) . .
C13K C63K C5K 102(4) . .
C14K C63K C5K 164(4) . .
C64K C63K C5K 145(4) . .
N1K C63K C5K 51(2) . .
C13K C64K C15K 174(7) . .
C13K C64K C65K 136(6) . .
C15K C64K C65K 45(3) . .
C13K C64K C63K 63(4) . .
C15K C64K C63K 113(5) . .
C65K C64K C63K 147(6) . .
C13K C64K C66K 150(6) . .
C15K C64K C66K 26(3) . .
C65K C64K C66K 38(3) . .
C63K C64K C66K 111(5) . .
C15K C65K C66K 44(4) . .
C15K C65K C64K 65(4) . .
C66K C65K C64K 89(5) . .
C15K C65K C16K 68(4) . .
C66K C65K C16K 69(4) . .
C64K C65K C16K 129(5) . .
C15K C65K C14K 48(3) . .
C66K C65K C14K 79(5) . .
C64K C65K C14K 17(3) . .
C16K C65K C14K 112(4) . .
C15K C66K C65K 67(6) . .
C15K C66K C16K 72(5) . .
C65K C66K C16K 67(4) . .
C15K C66K C14K 36(4) . .
C65K C66K C14K 63(4) . .
C16K C66K C14K 102(4) . .
C15K C66K C64K 47(5) . .
C65K C66K C64K 53(4) . .
C16K C66K C64K 105(4) . .
C14K C66K C64K 15(2) . .
C2L C1L N1L 115(2) . .
C53L C2L C1L 136(8) . .
C53L C2L C3L 35(7) . .
C1L C2L C3L 112(2) . .
C53L C3L C54L 75(7) . .
C53L C3L C4L 98(7) . .
C54L C3L C4L 30(3) . .
C53L C3L C2L 28(6) . .
C54L C3L C2L 95(4) . .
C4L C3L C2L 123(3) . .
C54L C4L C3L 74(8) . .
C54L C4L C53L 52(8) . .
C3L C4L C53L 31(3) . .
C2L C53L C3L 117(10) . .
C2L C53L C54L 138(10) . .
C3L C53L C54L 66(7) . .
C2L C53L C4L 155(10) . .
C3L C53L C4L 51(5) . .
C54L C53L C4L 23(4) . .
C4L C54L C3L 76(8) . .
C4L C54L C53L 104(10) . .
C3L C54L C53L 38(4) . .
N1L C5L C56L 113(3) . .
N1L C5L C6L 106(4) . .
C56L C5L C6L 24(3) . .
C56L C6L C57L 60(10) . .
C56L C6L C5L 76(10) . .
C57L C6L C5L 99(5) . .
C57L C7L C58L 58(8) . .
C57L C7L C56L 51(8) . .
C58L C7L C56L 93(5) . .
C58L C8L C57L 50(7) . .
C6L C56L C57L 96(10) . .
C6L C56L C5L 80(10) . .
C57L C56L C5L 110(4) . .
C6L C56L C7L 120(10) . .
C57L C56L C7L 25(3) . .
C5L C56L C7L 104(4) . .
C7L C57L C58L 94(9) . .
C7L C57L C56L 103(10) . .
C58L C57L C56L 123(5) . .
C7L C57L C6L 126(10) . .
C58L C57L C6L 121(6) . .
C56L C57L C6L 24(4) . .
C7L C57L C8L 109(10) . .
C58L C57L C8L 26(3) . .
C56L C57L C8L 98(5) . .
C6L C57L C8L 95(5) . .
C8L C58L C57L 104(9) . .
C8L C58L C7L 119(10) . .
C57L C58L C7L 28(3) . .
N1L C9L C10L 115.7(18) . .
C11L C10L C9L 111.7(19) . .
C12L C11L C10L 112.9(19) . .
C64L C13L N1L 120(5) . .
C64L C13L C14L 23(5) . .
N1L C13L C14L 102(3) . .
C64L C14L C65L 93(10) . .
C64L C14L C66L 64(10) . .
C65L C14L C66L 68(6) . .
C64L C14L C13L 50(10) . .
C65L C14L C13L 100(5) . .
C66L C14L C13L 112(5) . .
C64L C14L C15L 69(10) . .
C65L C14L C15L 34(4) . .
C66L C14L C15L 37(4) . .
C13L C14L C15L 100(3) . .
C65L C15L C66L 97(9) . .
C65L C15L C16L 93(7) . .
C66L C15L C16L 72(6) . .
C65L C15L C64L 63(7) . .
C66L C15L C64L 51(6) . .
C16L C15L C64L 111(5) . .
C65L C15L C14L 47(6) . .
C66L C15L C14L 54(6) . .
C16L C15L C14L 95(4) . .
C64L C15L C14L 22(3) . .
C15L C16L C66L 40(4) . .
C15L C16L C65L 33(3) . .
C66L C16L C65L 53(5) . .
C14L C64L C66L 88(10) . .
C14L C64L C13L 107(10) . .
C66L C64L C13L 158(10) . .
C14L C64L C65L 60(10) . .
C66L C64L C65L 66(7) . .
C13L C64L C65L 107(8) . .
C14L C64L C15L 89(10) . .
C66L C64L C15L 39(5) . .
C13L C64L C15L 123(7) . .
C65L C64L C15L 36(4) . .
C15L C65L C14L 100(9) . .
C15L C65L C64L 80(8) . .
C14L C65L C64L 26(4) . .
C15L C65L C66L 43(6) . .
C14L C65L C66L 60(6) . .
C64L C65L C66L 50(5) . .
C15L C65L C16L 54(6) . .
C14L C65L C16L 99(6) . .
C64L C65L C16L 102(6) . .
C66L C65L C16L 54(5) . .
C15L C66L C64L 90(9) . .
C15L C66L C14L 90(8) . .
C64L C66L C14L 28(5) . .
C15L C66L C65L 40(5) . .
C64L C66L C65L 64(7) . .
C14L C66L C65L 52(5) . .
C15L C66L C16L 67(6) . .
C64L C66L C16L 133(8) . .
C14L C66L C16L 108(6) . .
C65L C66L C16L 73(6) . .
O1M N1M O2M 124(2) . .
O1M N1M C1M 120(2) . .
O2M N1M C1M 116(2) . .
O2N N1N O1N 136(4) . .
O2N N1N C1N 114(4) . .
O1N N1N C1N 110(4) . .
C1O N1O O1O 141(4) . .
C1O N1O O2O 111(4) . .
O1O N1O O2O 108(3) . .
O51P O1P N1P 49(5) . .
O1P O51P N1P 90(7) . .
O51P N1P C1P 112(6) . .
O51P N1P O1P 40(4) . .
C1P N1P O1P 145(6) . .
O51P N1P O2P 95(5) . .
C1P N1P O2P 87(4) . .
O1P N1P O2P 77(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1A O7A 1.704(9) .
W1A O8A 1.871(8) .
W1A O19A 1.881(8) .
W1A O13A 1.985(8) .
W1A O1A 2.017(8) .
W1A O5A 2.330(7) .
W2A O9A 1.706(9) .
W2A O2A 1.769(8) .
W2A O14A 1.947(8) .
W2A O8A 1.974(8) .
W2A O20A 2.055(8) .
W2A O5A 2.377(7) .
W3A O10A 1.712(8) .
W3A O21A 1.837(8) .
W3A O15A 1.925(8) .
W3A O11A 1.932(8) .
W3A O3A 2.091(8) .
W3A O6A 2.251(7) .
W4A O12A 1.719(9) .
W4A O22A 1.845(8) .
W4A O16A 1.912(8) .
W4A O11A 1.971(8) .
W4A O4A 1.993(8) .
W4A O6A 2.246(7) .
W5A O17A 1.709(8) .
W5A O13A 1.859(8) .
W5A O15A 1.888(8) .
W5A O25A 1.933(8) .
W5A O27A 1.969(8) .
W5A O23A 2.318(7) .
W6A O18A 1.709(9) .
W6A O14A 1.886(8) .
W6A O26A 1.900(8) .
W6A O16A 1.927(8) .
W6A O28A 1.937(8) .
W6A O24A 2.345(8) .
W7A O33A 1.702(9) .
W7A O29A 1.890(8) .
W7A O25A 1.903(8) .
W7A O31A 1.918(8) .
W7A O19A 1.937(8) .
W7A O23A 2.329(8) .
W8A O34A 1.725(9) .
W8A O20A 1.825(8) .
W8A O29A 1.923(8) .
W8A O26A 1.940(8) .
W8A O32A 2.020(9) .
W8A O24A 2.310(8) .
W9A O35A 1.686(9) .
W9A O27A 1.891(8) .
W9A O31A 1.893(9) .
W9A O30A 1.900(8) .
W9A O21A 1.973(8) .
W9A O23A 2.388(7) .
W10A O36A 1.714(9) .
W10A O32A 1.857(9) .
W10A O28A 1.902(9) .
W10A O30A 1.905(8) .
W10A O22A 2.006(8) .
W10A O24A 2.343(8) .
W1B O7B 1.695(10) .
W1B O8B 1.863(8) .
W1B O19B 1.870(8) .
W1B O13B 1.984(8) .
W1B O1B 2.004(8) .
W1B O5B 2.320(8) .
W2B O9B 1.697(9) .
W2B O2B 1.790(8) .
W2B O14B 1.938(8) .
W2B O8B 1.967(8) .
W2B O20B 2.044(9) .
W2B O5B 2.382(8) .
W3B O10B 1.710(8) .
W3B O21B 1.835(8) .
W3B O15B 1.918(8) .
W3B O11B 1.919(7) .
W3B O3B 2.084(8) .
W3B O6B 2.226(8) .
W4B O12B 1.719(9) .
W4B O22B 1.844(8) .
W4B O16B 1.900(8) .
W4B O11B 1.994(8) .
W4B O4B 2.005(8) .
W4B O6B 2.249(7) .
W5B O17B 1.706(8) .
W5B O13B 1.872(8) .
W5B O15B 1.910(8) .
W5B O25B 1.928(9) .
W5B O27B 1.969(8) .
W5B O23B 2.317(8) .
W6B O18B 1.714(9) .
W6B O14B 1.890(8) .
W6B O26B 1.913(8) .
W6B O28B 1.915(9) .
W6B O16B 1.934(8) .
W6B O24B 2.355(8) .
W7B O33B 1.702(11) .
W7B O29B 1.888(8) .
W7B O25B 1.908(9) .
W7B O19B 1.925(9) .
W7B O31B 1.938(9) .
W7B O23B 2.350(8) .
W8B O34B 1.705(10) .
W8B O20B 1.844(9) .
W8B O29B 1.906(8) .
W8B O26B 1.930(8) .
W8B O32B 1.996(9) .
W8B O24B 2.325(8) .
W9B O35B 1.708(10) .
W9B O27B 1.891(8) .
W9B O31B 1.895(9) .
W9B O30B 1.903(8) .
W9B O21B 1.988(8) .
W9B O23B 2.364(8) .
W10B O36B 1.705(10) .
W10B O32B 1.868(9) .
W10B O30B 1.902(8) .
W10B O28B 1.918(9) .
W10B O22B 2.000(8) .
W10B O24B 2.340(8) .
W1C O7C 1.712(10) .
W1C O1C 1.876(8) .
W1C O8C 1.918(9) .
W1C O19C 1.957(9) .
W1C O13C 1.968(9) .
W1C O5C 2.344(8) .
W2C O9C 1.697(10) .
W2C O8C 1.904(9) .
W2C O2C 1.923(9) .
W2C O20C 1.949(9) .
W2C O14C 1.964(8) .
W2C O5C 2.364(8) .
W3C O10C 1.728(9) .
W3C O21C 1.862(9) .
W3C O15C 1.898(8) .
W3C O11C 1.964(8) .
W3C O3C 2.033(8) .
W3C O6C 2.246(7) .
W4C O12C 1.718(9) .
W4C O22C 1.861(9) .
W4C O16C 1.911(8) .
W4C O11C 1.952(8) .
W4C O4C 2.037(8) .
W4C O6C 2.251(7) .
W5C O17C 1.711(9) .
W5C O13C 1.860(9) .
W5C O25C 1.915(8) .
W5C O15C 1.929(8) .
W5C O27C 1.951(9) .
W5C O23C 2.343(8) .
W6C O18C 1.719(9) .
W6C O14C 1.859(8) .
W6C O26C 1.903(9) .
W6C O16C 1.917(8) .
W6C O28C 1.964(8) .
W6C O24C 2.323(8) .
W7C O33C 1.711(10) .
W7C O29C 1.879(8) .
W7C O19C 1.891(9) .
W7C O25C 1.916(8) .
W7C O31C 1.979(9) .
W7C O23C 2.340(8) .
W8C O34C 1.700(11) .
W8C O20C 1.902(8) .
W8C O26C 1.908(9) .
W8C O29C 1.913(8) .
W8C O32C 1.952(9) .
W8C O24C 2.325(8) .
W9C O35C 1.715(10) .
W9C O31C 1.882(9) .
W9C O27C 1.891(9) .
W9C O30C 1.908(9) .
W9C O21C 1.965(8) .
W9C O23C 2.341(8) .
W10C O36C 1.721(10) .
W10C O32C 1.884(9) .
W10C O28C 1.891(9) .
W10C O30C 1.896(9) .
W10C O22C 1.948(9) .
W10C O24C 2.355(8) .
W1D O7D 1.696(10) .
W1D O8D 1.894(8) .
W1D O19D 1.932(9) .
W1D O1D 1.937(9) .
W1D O13D 1.981(9) .
W1D O5D 2.322(8) .
W2D O9D 1.684(11) .
W2D O2D 1.857(9) .
W2D O8D 1.947(8) .
W2D O14D 1.963(9) .
W2D O20D 1.978(9) .
W2D O5D 2.367(8) .
W3D O10D 1.717(11) .
W3D O21D 1.866(9) .
W3D O15D 1.903(9) .
W3D O11D 1.944(8) .
W3D O3D 2.014(9) .
W3D O6D 2.240(7) .
W4D O12D 1.715(11) .
W4D O22D 1.826(9) .
W4D O16D 1.913(9) .
W4D O11D 1.950(8) .
W4D O4D 2.051(9) .
W4D O6D 2.238(7) .
W5D O17D 1.716(12) .
W5D O13D 1.851(9) .
W5D O15D 1.927(9) .
W5D O25D 1.927(10) .
W5D O27D 1.965(9) .
W5D O23D 2.323(8) .
W6D O18D 1.733(11) .
W6D O14D 1.851(9) .
W6D O28D 1.915(10) .
W6D O16D 1.916(9) .
W6D O26D 1.916(10) .
W6D O24D 2.322(8) .
W7D O33D 1.697(11) .
W7D O29D 1.876(10) .
W7D O19D 1.895(9) .
W7D O25D 1.901(9) .
W7D O31D 1.950(10) .
W7D O23D 2.325(8) .
W8D O34D 1.699(13) .
W8D O20D 1.870(9) .
W8D O29D 1.914(9) .
W8D O26D 1.920(10) .
W8D O32D 1.970(11) .
W8D O24D 2.337(8) .
W9D O35D 1.692(11) .
W9D O27D 1.871(10) .
W9D O30D 1.892(9) .
W9D O31D 1.907(10) .
W9D O21D 1.971(9) .
W9D O23D 2.353(8) .
W10D O36D 1.700(12) .
W10D O32D 1.868(11) .
W10D O30D 1.896(9) .
W10D O28D 1.912(10) .
W10D O22D 2.019(9) .
W10D O24D 2.348(8) .
Co1A O4A 2.015(8) 2_656
Co1A O2A 2.039(8) .
Co1A O1A 2.053(8) .
Co1A O3A 2.073(8) 2_656
Co1A O5A 2.164(7) .
Co1A O11A 2.269(8) 2_656
Co1B O4B 2.017(8) 2
Co1B O2B 2.054(8) .
Co1B O1B 2.058(8) .
Co1B O3B 2.065(8) 2
Co1B O5B 2.158(8) .
Co1B O11B 2.286(8) 2
Co1C O1C 2.033(8) .
Co1C O3C 2.040(8) 2_665
Co1C O2C 2.042(9) .
Co1C O4C 2.059(8) 2_665
Co1C O5C 2.164(8) .
Co1C O11C 2.296(8) 2_665
Co1D O4D 2.035(9) 2_766
Co1D O2D 2.045(9) .
Co1D O3D 2.048(9) 2_766
Co1D O1D 2.058(9) .
Co1D O5D 2.204(8) .
Co1D O11D 2.311(9) 2_766
Si1A O6A 1.615(8) .
Si1A O5A 1.637(8) .
Si1A O23A 1.638(8) .
Si1A O24A 1.644(8) .
Si1B O6B 1.619(8) .
Si1B O5B 1.635(8) .
Si1B O24B 1.637(8) .
Si1B O23B 1.641(8) .
Si1C O6C 1.620(8) .
Si1C O5C 1.623(8) .
Si1C O23C 1.637(8) .
Si1C O24C 1.642(8) .
Si1D O6D 1.628(8) .
Si1D O5D 1.636(8) .
Si1D O23D 1.641(8) .
Si1D O24D 1.642(9) .
O3A Co1A 2.073(8) 2_656
O4A Co1A 2.015(8) 2_656
O11A Co1A 2.269(8) 2_656
O3B Co1B 2.065(8) 2
O4B Co1B 2.017(8) 2
O11B Co1B 2.286(8) 2
O3C Co1C 2.040(8) 2_665
O4C Co1C 2.059(8) 2_665
O11C Co1C 2.296(8) 2_665
O3D Co1D 2.048(9) 2_766
O4D Co1D 2.035(9) 2_766
O11D Co1D 2.311(9) 2_766
N1A C5A 1.502(19) .
N1A C1A 1.52(2) .
N1A C9A 1.53(2) .
N1A C13A 1.53(2) .
N1B C5B 1.43(3) .
N1B C1B 1.49(3) .
N1B C13B 1.54(3) .
N1B C9B 1.57(3) .
N1C C5C 1.41(3) .
N1C C63C 1.46(5) .
N1C C9C 1.47(4) .
N1C C1C 1.55(3) .
N1C C59C 1.56(4) .
N1C C55C 1.59(7) .
N1C C13C 1.60(4) .
N1C C51C 1.68(4) .
N1D C1D 1.504(19) .
N1D C13D 1.517(19) .
N1D C9D 1.522(19) .
N1D C5D 1.52(2) .
N1E C5E 1.53(2) .
N1E C9E 1.54(2) .
N1E C13E 1.54(2) .
N1E C1E 1.54(3) .
N1F C5F 1.51(2) .
N1F C9F 1.53(2) .
N1F C13F 1.53(2) .
N1F C1F 1.56(2) .
N1G C9G 1.41(3) .
N1G C13G 1.52(3) .
N1G C63G 1.53(3) .
N1G C1G 1.53(3) .
N1G C5G 1.54(3) .
N1H C13H 1.51(2) .
N1H C1H 1.52(2) .
N1H C5H 1.54(2) .
N1H C9H 1.54(2) .
N1I C13I 1.51(2) .
N1I C9I 1.52(2) .
N1I C5I 1.53(2) .
N1I C1I 1.536(19) .
N1J C13J 1.50(2) .
N1J C9J 1.51(2) .
N1J C5J 1.541(19) .
N1J C1J 1.55(2) .
N1K C59K 1.44(6) .
N1K C5K 1.47(4) .
N1K C51K 1.50(5) .
N1K C9K 1.52(4) .
N1K C63K 1.57(5) .
N1K C13K 1.58(4) .
N1K C1K 1.59(3) .
N1K C55K 1.63(4) .
N1L C1L 1.49(3) .
N1L C9L 1.53(3) .
N1L C13L 1.54(3) .
N1L C5L 1.59(3) .
C1A C2A 1.49(3) .
C2A C3A 1.53(3) .
C3A C4A 1.55(4) .
C5A C6A 1.57(2) .
C6A C7A 1.52(2) .
C7A C8A 1.55(2) .
C9A C10A 1.57(2) .
C10A C11A 1.51(2) .
C11A C12A 1.59(3) .
C13A C14A 1.57(2) .
C14A C15A 1.54(3) .
C15A C16A 1.54(3) .
C1B C2B 1.39(3) .
C2B C53B 1.21(7) .
C2B C3B 1.60(4) .
C3B C4B 1.22(4) .
C3B C53B 1.29(7) .
C3B C54B 1.70(8) .
C4B C54B 0.64(7) .
C4B C53B 1.83(8) .
C53B C54B 1.92(10) .
C5B C6B 1.66(3) .
C6B C7B 1.50(3) .
C7B C8B 1.69(4) .
C9B C60B 1.50(9) .
C9B C10B 1.63(5) .
C10B C60B 0.78(9) .
C10B C11B 1.52(8) .
C10B C61B 1.66(17) .
C11B C62B 1.05(10) .
C11B C12B 1.45(9) .
C11B C60B 1.64(12) .
C12B C61B 1.36(17) .
C60B C61B 1.66(19) .
C61B C62B 1.19(19) .
C13B C14B 1.53(2) .
C13B C64B 1.53(2) .
C14B C15B 1.54(2) .
C14B C65B 1.64(15) .
C15B C64B 1.43(15) .
C15B C16B 1.54(2) .
C15B C66B 1.77(9) .
C16B C66B 1.04(6) .
C16B C65B 1.29(8) .
C64B C65B 1.54(2) .
C65B C66B 1.54(2) .
C1C C2C 1.29(4) .
C1C C51C 1.36(4) .
C1C C52C 1.52(5) .
C1C C63C 1.82(6) .
C2C C52C 0.57(4) .
C2C C3C 1.33(4) .
C2C C51C 1.43(5) .
C2C C53C 1.48(5) .
C3C C53C 0.85(4) .
C3C C4C 1.34(4) .
C3C C54C 1.58(4) .
C3C C52C 1.60(5) .
C4C C54C 1.01(4) .
C4C C53C 1.45(4) .
C51C C52C 1.08(5) .
C51C C5C 1.83(5) .
C52C C53C 1.44(5) .
C53C C54C 1.13(4) .
C5C C55C 1.02(7) .
C5C C56C 1.36(7) .
C5C C6C 1.55(5) .
C6C C56C 1.03(7) .
C6C C55C 1.03(7) .
C6C C7C 1.63(5) .
C6C C57C 1.67(8) .
C7C C57C 0.59(7) .
C7C C56C 1.32(7) .
C7C C58C 1.37(7) .
C7C C8C 1.69(5) .
C8C C58C 0.84(7) .
C8C C57C 1.43(8) .
C55C C56C 1.57(9) .
C55C C59C 2.00(8) .
C56C C57C 1.67(10) .
C57C C58C 1.24(9) .
C9C C59C 0.73(5) .
C9C C10C 1.23(6) .
C9C C60C 1.35(6) .
C10C C60C 1.17(5) .
C10C C11C 1.40(7) .
C10C C61C 1.47(6) .
C10C C59C 1.58(6) .
C11C C62C 1.41(6) .
C11C C60C 1.77(6) .
C11C C12C 1.77(6) .
C12C C62C 1.02(5) .
C12C C61C 1.40(6) .
C59C C60C 1.06(5) .
C60C C61C 1.53(6) .
C61C C62C 1.26(6) .
C13C C64C 0.99(6) .
C13C C63C 1.18(6) .
C13C C14C 1.57(5) .
C14C C64C 0.96(5) .
C14C C63C 1.31(6) .
C14C C65C 1.47(7) .
C14C C15C 1.55(5) .
C15C C65C 0.51(6) .
C15C C66C 1.48(6) .
C15C C64C 1.61(7) .
C15C C16C 1.65(5) .
C16C C66C 0.87(5) .
C16C C65C 1.34(6) .
C63C C64C 1.53(7) .
C64C C65C 1.60(8) .
C65C C66C 1.41(8) .
C1D C2D 1.54(2) .
C2D C3D 1.55(3) .
C3D C4D 1.52(4) .
C5D C6D 1.56(3) .
C6D C7D 1.57(3) .
C7D C8D 1.56(3) .
C9D C10D 1.51(2) .
C10D C61D 1.52(7) .
C10D C11D 1.65(6) .
C11D C61D 0.53(8) .
C11D C12D 1.12(7) .
C11D C62D 1.43(8) .
C12D C61D 1.56(8) .
C12D C62D 1.77(7) .
C61D C62D 1.23(8) .
C13D C14D 1.49(2) .
C14D C15D 1.54(3) .
C15D C16D 1.52(3) .
C1E C52E 1.3(2) .
C1E C2E 1.59(4) .
C2E C52E 1.2(2) .
C2E C3E 1.47(4) .
C2E C53E 1.6(2) .
C2E C54E 1.7(2) .
C3E C54E 0.8(2) .
C3E C4E 1.46(4) .
C3E C52E 1.5(2) .
C3E C53E 1.6(2) .
C4E C54E 1.9(2) .
C52E C53E 1.1(3) .
C52E C54E 1.2(3) .
C53E C54E 1.1(3) .
C5E C6E 1.54(3) .
C6E C7E 1.49(3) .
C7E C8E 1.57(4) .
C9E C10E 1.50(3) .
C10E C11E 1.54(3) .
C11E C12E 1.57(4) .
C13E C14E 1.52(3) .
C14E C15E 1.52(3) .
C15E C66E 1.36(5) .
C15E C16E 1.69(5) .
C1F C2F 1.52(2) .
C2F C3F 1.56(2) .
C3F C4F 1.52(3) .
C5F C6F 1.54(3) .
C6F C57F 1.62(3) .
C6F C7F 1.62(3) .
C7F C57F 1.27(9) .
C7F C58F 1.32(10) .
C7F C8F 1.63(3) .
C8F C58F 1.97(11) .
C57F C58F 1.62(3) .
C9F C10F 1.52(3) .
C10F C61F 1.54(5) .
C10F C11F 1.65(6) .
C11F C61F 0.65(6) .
C11F C12F 1.11(7) .
C11F C62F 1.38(7) .
C12F C62F 0.96(6) .
C12F C61F 1.57(7) .
C61F C62F 1.42(6) .
C13F C14F 1.55(3) .
C14F C15F 1.62(4) .
C15F C16F 1.46(4) .
C1G C2G 1.57(3) .
C2G C3G 1.57(3) .
C3G C4G 1.65(4) .
C5G C6G 1.59(4) .
C6G C7G 1.63(4) .
C7G C8G 1.49(3) .
C9G C60G 0.95(7) .
C9G C10G 1.49(4) .
C10G C61G 0.96(8) .
C10G C60G 1.06(8) .
C10G C11G 1.54(4) .
C11G C61G 1.00(8) .
C11G C62G 1.28(8) .
C11G C12G 1.58(4) .
C11G C60G 1.75(8) .
C60G C61G 1.50(11) .
C61G C62G 1.39(10) .
C13G C14G 1.49(3) .
C13G C64G 1.83(8) .
C14G C64G 1.24(8) .
C14G C15G 1.49(3) .
C14G C63G 1.50(8) .
C15G C66G 0.99(7) .
C15G C16G 1.49(3) .
C15G C65G 1.60(8) .
C15G C64G 1.86(8) .
C16G C65G 0.79(8) .
C16G C66G 1.22(8) .
C63G C64G 1.50(2) .
C64G C65G 1.49(2) .
C65G C66G 1.49(2) .
C1H C2H 1.45(3) .
C2H C3H 1.56(3) .
C3H C4H 1.45(4) .
C5H C6H 1.52(4) .
C5H C56H 1.61(7) .
C6H C56H 0.60(6) .
C6H C57H 1.45(7) .
C6H C7H 1.59(5) .
C6H C58H 1.85(7) .
C7H C57H 0.78(6) .
C7H C58H 0.90(6) .
C7H C8H 1.51(5) .
C7H C56H 2.01(7) .
C8H C57H 1.19(6) .
C8H C58H 1.95(7) .
C56H C57H 1.68(9) .
C57H C58H 1.53(9) .
C9H C10H 1.55(2) .
C10H C11H 1.57(3) .
C11H C12H 1.55(3) .
C13H C14H 1.52(2) .
C14H C65H 1.53(4) .
C14H C15H 1.61(4) .
C15H C65H 0.76(4) .
C15H C66H 1.09(4) .
C15H C16H 1.54(5) .
C16H C65H 1.15(4) .
C16H C66H 1.32(5) .
C65H C66H 1.46(5) .
C1I C2I 1.53(2) .
C2I C3I 1.56(2) .
C3I C4I 1.51(2) .
C5I C6I 1.56(3) .
C6I C7I 1.56(3) .
C7I C8I 1.56(3) .
C9I C10I 1.49(3) .
C10I C11I 1.55(4) .
C10I C61I 1.59(4) .
C11I C61I 0.79(4) .
C11I C62I 0.98(4) .
C11I C12I 1.58(5) .
C12I C61I 1.15(5) .
C12I C62I 1.46(5) .
C61I C62I 1.44(5) .
C13I C14I 1.55(3) .
C14I C15I 1.58(3) .
C15I C16I 1.54(4) .
C1J C2J 1.54(2) .
C2J C3J 1.54(3) .
C3J C4J 1.58(3) .
C5J C6J 1.54(2) .
C6J C7J 1.51(2) .
C7J C8J 1.57(3) .
C9J C10J 1.55(2) .
C10J C11J 1.54(3) .
C11J C12J 1.56(3) .
C13J C14J 1.54(3) .
C14J C15J 1.57(4) .
C15J C16J 1.27(6) .
C15J C66J 1.31(6) .
C16J C66J 1.75(8) .
C1K C51K 1.21(5) .
C1K C52K 1.34(6) .
C1K C2K 1.46(5) .
C1K C59K 1.87(7) .
C2K C52K 0.61(5) .
C2K C51K 1.23(5) .
C2K C3K 1.39(5) .
C2K C53K 1.60(6) .
C3K C53K 0.69(5) .
C3K C52K 1.44(6) .
C3K C4K 1.44(5) .
C3K C54K 1.50(6) .
C4K C54K 1.04(5) .
C4K C53K 1.52(6) .
C51K C52K 1.58(7) .
C51K C13K 1.91(6) .
C52K C53K 1.37(7) .
C53K C54K 1.17(6) .
C5K C55K 1.14(5) .
C5K C56K 1.35(5) .
C5K C6K 1.47(5) .
C5K C63K 1.81(6) .
C6K C56K 0.83(4) .
C6K C55K 0.97(5) .
C6K C57K 1.58(5) .
C6K C7K 1.64(5) .
C7K C57K 0.86(4) .
C7K C58K 1.14(5) .
C7K C8K 1.45(5) .
C7K C56K 1.59(5) .
C8K C58K 1.09(5) .
C8K C57K 1.43(5) .
C55K C56K 1.53(6) .
C55K C9K 2.04(6) .
C56K C57K 1.12(5) .
C57K C58K 1.53(6) .
C9K C60K 0.98(6) .
C9K C59K 1.01(6) .
C9K C10K 1.48(6) .
C10K C60K 0.98(6) .
C10K C59K 1.22(7) .
C10K C11K 1.44(6) .
C10K C61K 1.59(8) .
C11K C60K 1.52(8) .
C11K C12K 1.57(6) .
C11K C62K 1.79(7) .
C12K C62K 0.92(6) .
C12K C61K 1.17(7) .
C59K C60K 1.47(9) .
C60K C61K 1.67(10) .
C61K C62K 1.31(8) .
C13K C64K 1.16(7) .
C13K C63K 1.39(6) .
C13K C14K 1.48(6) .
C14K C15K 1.18(6) .
C14K C63K 1.40(7) .
C14K C65K 1.57(7) .
C14K C66K 1.74(7) .
C15K C66K 0.81(6) .
C15K C65K 1.08(6) .
C15K C64K 1.38(8) .
C15K C16K 1.45(5) .
C16K C65K 1.45(6) .
C16K C66K 1.48(6) .
C63K C64K 1.46(9) .
C64K C65K 1.43(8) .
C64K C66K 1.79(9) .
C65K C66K 1.09(7) .
C1L C2L 1.45(3) .
C2L C53L 0.84(9) .
C2L C3L 1.61(5) .
C3L C53L 1.04(9) .
C3L C54L 1.53(10) .
C3L C4L 1.55(5) .
C4L C54L 0.81(9) .
C4L C53L 1.99(11) .
C53L C54L 1.62(13) .
C5L C56L 1.62(6) .
C5L C6L 1.64(9) .
C6L C56L 0.67(9) .
C6L C57L 1.62(10) .
C7L C57L 0.78(8) .
C7L C58L 1.64(10) .
C7L C56L 1.76(10) .
C8L C58L 0.79(8) .
C8L C57L 1.75(10) .
C56L C57L 1.41(7) .
C57L C58L 1.39(7) .
C9L C10L 1.55(3) .
C10L C11L 1.52(3) .
C11L C12L 1.52(3) .
C13L C64L 1.33(10) .
C13L C14L 1.66(6) .
C14L C64L 0.67(10) .
C14L C65L 1.32(10) .
C14L C66L 1.43(10) .
C14L C15L 1.78(8) .
C15L C65L 1.00(9) .
C15L C66L 1.06(9) .
C15L C16L 1.51(7) .
C15L C64L 1.67(11) .
C16L C66L 1.56(10) .
C16L C65L 1.85(10) .
C64L C66L 1.29(12) .
C64L C65L 1.51(13) .
C65L C66L 1.54(13) .
O1M N1M 1.24(2) .
O2M N1M 1.26(3) .
N1M C1M 1.52(3) .
O1N N1N 1.25(4) .
O2N N1N 1.21(4) .
N1N C1N 1.67(5) .
O1O N1O 1.33(4) .
O2O N1O 1.57(4) .
N1O C1O 1.20(5) .
O1P O51P 1.11(9) .
O1P N1P 1.71(9) .
O51P N1P 1.30(7) .
O2P N1P 1.76(5) .
N1P C1P 1.48(6) .
