#------------------------------------------------------------------------------
#$Date: 2016-03-23 21:59:38 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179461 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/58/4335890.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4335890
loop_
_publ_author_name
'Dong Woo Lee'
'Kang Min Ok'
_publ_section_title
;
 New Selenites: Hydrothermal Syntheses, Crystal Structures, and
 Characterization of Rb3HGa2(OH)2(SeO3)4, Rb3Ga5(SeO3)8(HSeO3)2.0.5H2O,
 and RbGa(SeO3)2.H2O
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              10080
_journal_page_last               10086
_journal_paper_doi               10.1021/ic4013894
_journal_volume                  52
_journal_year                    2013
_chemical_formula_sum            'Ga3 H4.8 O20.4 Rb3 Se6'
_chemical_formula_weight         1270.56
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                105.622(4)
_cell_angle_beta                 90.210(4)
_cell_angle_gamma                116.385(2)
_cell_formula_units_Z            2
_cell_length_a                   8.7027(6)
_cell_length_b                   9.7622(7)
_cell_length_c                   15.3347(14)
_cell_measurement_temperature    298.0(2)
_cell_volume                     1112.42(15)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      298.0(2)
_diffrn_measured_fraction_theta_full 0.967
_diffrn_measured_fraction_theta_max 0.967
_diffrn_measurement_device_type  'Bruker SMART BREEZE'
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0584
_diffrn_reflns_av_unetI/netI     0.0783
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            20427
_diffrn_reflns_theta_full        28.38
_diffrn_reflns_theta_max         28.38
_diffrn_reflns_theta_min         1.39
_exptl_absorpt_coefficient_mu    20.007
_exptl_absorpt_correction_T_max  0.753
_exptl_absorpt_correction_T_min  0.58
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
; 
 SADABS(Blessing, 1995) 
;
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    3.779
_exptl_crystal_F_000             1142
_exptl_crystal_size_max          0.042
_exptl_crystal_size_mid          0.034
_exptl_crystal_size_min          0.022
_refine_diff_density_max         1.701
_refine_diff_density_min         -1.714
_refine_diff_density_rms         0.232
_refine_ls_extinction_coef       0.00289(15)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.953
_refine_ls_matrix_type           full
_refine_ls_number_parameters     330
_refine_ls_number_reflns         5381
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.953
_refine_ls_R_factor_all          0.0622
_refine_ls_R_factor_gt           0.038
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0290P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0731
_refine_ls_wR_factor_ref         0.0784
_reflns_number_gt                3766
_reflns_number_total             5381
_reflns_threshold_expression     >2sĬ)
_cod_data_source_file            ic4013894_si_002_3.cif
_cod_data_source_block           RbGaSe2O6(H2O)
_cod_database_code               4335890
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Rb1 Rb 0.3397(2) 0.56974(19) 0.32459(11) 0.0542(7) Uani 0.598(3) 1 d P
Rb2 Rb 0.9256(2) 0.5710(2) -0.00797(12) 0.0410(7) Uani 0.488(3) 1 d P
Rb3 Rb 0.0823(3) -0.0133(3) 0.06510(13) 0.0850(10) Uani 0.578(3) 1 d P
Rb4 Rb 0.5968(3) -0.0013(3) 0.43640(15) 0.1063(12) Uani 0.611(3) 1 d P
Rb5 Rb 1.1371(4) 0.5698(3) 0.48454(16) 0.0747(12) Uani 0.423(3) 1 d P
Rb6 Rb 0.5955(4) 0.5324(3) -0.0234(2) 0.0463(12) Uani 0.290(3) 1 d P
Se1 Se 0.14779(8) -0.20545(7) 0.23153(4) 0.01085(16) Uani 1 1 d .
Se2 Se 0.43081(8) 0.21746(7) 0.27651(4) 0.01113(16) Uani 1 1 d .
Se3 Se 0.85836(8) 0.21532(7) 0.26981(4) 0.01132(16) Uani 1 1 d .
Se4 Se 0.61771(8) 0.20992(7) 0.06077(4) 0.01145(16) Uani 1 1 d .
Se5 Se 0.71509(8) 0.79122(7) 0.22032(4) 0.01117(16) Uani 1 1 d .
Se6 Se 0.90449(8) 0.79145(7) 0.44118(4) 0.01160(16) Uani 1 1 d .
Ga1 Ga 0.07333(9) 0.07999(8) 0.34855(4) 0.00990(17) Uani 1 1 d .
Ga2 Ga 0.49229(9) -0.07693(8) 0.15081(4) 0.00983(17) Uani 1 1 d .
Ga3 Ga 0.78401(9) 0.50292(8) 0.24682(5) 0.01014(16) Uani 1 1 d .
O1 O 0.1926(6) -0.0549(5) 0.3317(3) 0.0142(10) Uani 1 1 d .
O2 O 0.0391(5) -0.3687(5) 0.2679(3) 0.0159(11) Uani 1 1 d .
O3 O 0.3424(5) -0.2074(5) 0.2264(3) 0.0134(10) Uani 1 1 d .
O4 O 0.3755(5) 0.0610(5) 0.1788(3) 0.0123(10) Uani 1 1 d .
O5 O 0.5275(5) 0.3721(5) 0.2315(3) 0.0139(10) Uani 1 1 d .
O6 O 0.2382(5) 0.2185(5) 0.2848(3) 0.0152(10) Uani 1 1 d .
O7 O 0.6575(5) 0.0630(5) 0.2638(3) 0.0127(10) Uani 1 1 d .
O8 O 0.8210(6) 0.3751(5) 0.3172(3) 0.0135(10) Uani 1 1 d .
O9 O 0.9562(5) 0.2180(5) 0.3660(3) 0.0148(10) Uani 1 1 d .
O10 O 0.6422(5) 0.0541(5) 0.0756(3) 0.0128(10) Uani 1 1 d .
O11 O 0.7999(5) 0.3663(5) 0.1285(3) 0.0139(10) Uani 1 1 d .
O12 O 0.6870(5) 0.2150(5) -0.0427(3) 0.0142(10) Uani 1 1 d .
O13 O 0.7491(5) 0.6299(5) 0.1734(3) 0.0140(10) Uani 1 1 d .
O14 O 0.9182(5) 0.9432(5) 0.2284(3) 0.0125(10) Uani 1 1 d .
O15 O 0.6150(5) 0.7919(5) 0.1248(3) 0.0126(10) Uani 1 1 d .
O16 O 0.7481(6) 0.6309(5) 0.3607(3) 0.0162(11) Uani 1 1 d .
O17 O 0.7862(5) 0.7888(5) 0.5297(3) 0.0144(10) Uani 1 1 d .
O18 O 0.8952(5) 0.9428(5) 0.4094(3) 0.0114(10) Uani 1 1 d .
OW1 O 0.479(4) 0.520(4) 0.521(2) 0.0387(13) Uani 0.201(12) 1 d P
OW2 O 0.2426(7) 0.4380(6) 0.1829(4) 0.0387(13) Uani 1 1 d .
OW3 O 0.6779(18) 0.6482(16) -0.0698(11) 0.0387(13) Uani 0.374(10) 1 d P
OW4 O 0.113(3) 0.317(3) 0.1028(18) 0.0387(13) Uani 0.226(9) 1 d P
OW5 O 0.4387(10) 0.5350(9) 0.4707(7) 0.0387(13) Uani 0.676(12) 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
OW2 Rb1 OW5 140.0(2) . .
OW2 Rb1 O3 71.30(16) . 1_565
OW5 Rb1 O3 147.5(2) . 1_565
OW2 Rb1 O6 67.63(16) . .
OW5 Rb1 O6 73.1(2) . .
O3 Rb1 O6 138.92(13) 1_565 .
OW2 Rb1 Rb5 128.06(16) . 1_455
OW5 Rb1 Rb5 59.4(2) . 1_455
O3 Rb1 Rb5 112.89(11) 1_565 1_455
O6 Rb1 Rb5 92.25(10) . 1_455
OW2 Rb1 O2 71.75(17) . 1_565
OW5 Rb1 O2 133.4(2) . 1_565
O3 Rb1 O2 50.60(11) 1_565 1_565
O6 Rb1 O2 113.19(12) . 1_565
Rb5 Rb1 O2 74.08(10) 1_455 1_565
OW2 Rb1 O5 65.36(16) . .
OW5 Rb1 O5 83.7(2) . .
O3 Rb1 O5 112.31(12) 1_565 .
O6 Rb1 O5 49.34(11) . .
Rb5 Rb1 O5 134.66(10) 1_455 .
O2 Rb1 O5 137.10(12) 1_565 .
OW2 Rb1 OW1 128.3(5) . 2_666
OW5 Rb1 OW1 14.9(5) . 2_666
O3 Rb1 OW1 151.6(6) 1_565 2_666
O6 Rb1 OW1 64.8(5) . 2_666
Rb5 Rb1 OW1 73.2(5) 1_455 2_666
O2 Rb1 OW1 147.1(5) 1_565 2_666
O5 Rb1 OW1 68.9(5) . 2_666
OW2 Rb1 O16 107.41(17) . .
OW5 Rb1 O16 61.6(2) . .
O3 Rb1 O16 107.38(12) 1_565 .
O6 Rb1 O16 85.78(11) . .
Rb5 Rb1 O16 118.68(11) 1_455 .
O2 Rb1 O16 157.65(11) 1_565 .
O5 Rb1 O16 47.95(10) . .
OW1 Rb1 O16 50.8(5) 2_666 .
OW2 Rb1 OW1 139.4(5) . .
OW5 Rb1 OW1 1.0(5) . .
O3 Rb1 OW1 147.8(5) 1_565 .
O6 Rb1 OW1 72.6(5) . .
Rb5 Rb1 OW1 60.4(4) 1_455 .
O2 Rb1 OW1 134.4(4) 1_565 .
O5 Rb1 OW1 82.7(4) . .
OW1 Rb1 OW1 13.9(9) 2_666 .
O16 Rb1 OW1 60.8(5) . .
OW2 Rb1 OW4 9.5(4) . .
OW5 Rb1 OW4 136.9(4) . .
O3 Rb1 OW4 75.5(4) 1_565 .
O6 Rb1 OW4 63.8(4) . .
Rb5 Rb1 OW4 118.7(4) 1_455 .
O2 Rb1 OW4 67.4(4) 1_565 .
O5 Rb1 OW4 70.1(4) . .
OW1 Rb1 OW4 127.5(6) 2_666 .
O16 Rb1 OW4 114.8(4) . .
OW1 Rb1 OW4 136.5(6) . .
OW2 Rb1 Rb4 130.59(15) . 1_565
OW5 Rb1 Rb4 85.76(18) . 1_565
O3 Rb1 Rb4 61.81(9) 1_565 1_565
O6 Rb1 Rb4 156.23(11) . 1_565
Rb5 Rb1 Rb4 85.99(7) 1_455 1_565
O2 Rb1 Rb4 89.14(9) 1_565 1_565
O5 Rb1 Rb4 118.85(10) . 1_565
OW1 Rb1 Rb4 92.1(5) 2_666 1_565
O16 Rb1 Rb4 74.45(8) . 1_565
OW1 Rb1 Rb4 86.0(5) . 1_565
OW4 Rb1 Rb4 136.7(4) . 1_565
OW4 Rb2 Rb2 138.5(7) 2_665 2_765
OW4 Rb2 Rb6 68.6(6) 2_665 .
Rb2 Rb2 Rb6 139.98(12) 2_765 .
OW4 Rb2 OW3 39.7(7) 2_665 .
Rb2 Rb2 OW3 161.6(3) 2_765 .
Rb6 Rb2 OW3 29.6(3) . .
OW4 Rb2 O11 69.0(6) 2_665 2_765
Rb2 Rb2 O11 71.57(11) 2_765 2_765
Rb6 Rb2 O11 134.10(13) . 2_765
OW3 Rb2 O11 108.3(3) . 2_765
OW4 Rb2 OW2 27.3(6) 2_665 2_665
Rb2 Rb2 OW2 127.35(15) 2_765 2_665
Rb6 Rb2 OW2 59.21(12) . 2_665
OW3 Rb2 OW2 39.6(3) . 2_665
O11 Rb2 OW2 75.04(13) 2_765 2_665
OW4 Rb2 O12 96.2(6) 2_665 2_765
Rb2 Rb2 O12 67.69(11) 2_765 2_765
Rb6 Rb2 O12 150.65(12) . 2_765
OW3 Rb2 O12 127.3(3) . 2_765
O11 Rb2 O12 50.82(11) 2_765 2_765
OW2 Rb2 O12 117.01(13) 2_665 2_765
OW4 Rb2 O12 117.8(6) 2_665 .
Rb2 Rb2 O12 67.14(11) 2_765 .
Rb6 Rb2 O12 73.67(11) . .
OW3 Rb2 O12 97.1(3) . .
O11 Rb2 O12 112.76(12) 2_765 .
OW2 Rb2 O12 90.73(13) 2_665 .
O12 Rb2 O12 134.84(9) 2_765 .
OW4 Rb2 O11 153.3(6) 2_665 .
Rb2 Rb2 O11 63.74(11) 2_765 .
Rb6 Rb2 O11 84.83(11) . .
OW3 Rb2 O11 114.0(3) . .
O11 Rb2 O11 135.31(9) 2_765 .
OW2 Rb2 O11 133.92(13) 2_665 .
O12 Rb2 O11 108.41(12) 2_765 .
O12 Rb2 O11 49.18(10) . .
OW4 Rb2 O13 112.8(7) 2_665 .
Rb2 Rb2 O13 108.60(12) 2_765 .
Rb6 Rb2 O13 60.23(10) . .
OW3 Rb2 O13 78.7(3) . .
O11 Rb2 O13 157.62(12) 2_765 .
OW2 Rb2 O13 117.43(14) 2_665 .
O12 Rb2 O13 107.69(12) 2_765 .
O12 Rb2 O13 86.66(11) . .
O11 Rb2 O13 50.38(11) . .
OW4 Rb2 Rb3 61.7(7) 2_665 1_665
Rb2 Rb2 Rb3 127.29(10) 2_765 1_665
Rb6 Rb2 Rb3 89.52(8) . 1_665
OW3 Rb2 Rb3 70.4(3) . 1_665
O11 Rb2 Rb3 85.43(9) 2_765 1_665
OW2 Rb2 Rb3 88.31(11) 2_665 1_665
O12 Rb2 Rb3 61.17(9) 2_765 1_665
O12 Rb2 Rb3 160.86(11) . 1_665
O11 Rb2 Rb3 121.63(9) . 1_665
O13 Rb2 Rb3 76.88(8) . 1_665
OW4 Rb2 Se1 123.8(7) 2_665 1_665
Rb2 Rb2 Se1 79.91(9) 2_765 1_665
Rb6 Rb2 Se1 110.67(8) . 1_665
OW3 Rb2 Se1 116.7(3) . 1_665
O11 Rb2 Se1 106.87(9) 2_765 1_665
OW2 Rb2 Se1 149.60(11) 2_665 1_665
O12 Rb2 Se1 56.11(8) 2_765 1_665
O12 Rb2 Se1 114.91(9) . 1_665
O11 Rb2 Se1 66.17(8) . 1_665
O13 Rb2 Se1 52.57(8) . 1_665
Rb3 Rb2 Se1 62.04(4) 1_665 1_665
Rb3 Rb3 O4 154.44(16) 2 .
Rb3 Rb3 O14 118.14(14) 2 1_445
O4 Rb3 O14 82.56(12) . 1_445
Rb3 Rb3 OW4 67.1(5) 2 .
O4 Rb3 OW4 99.3(5) . .
O14 Rb3 OW4 92.0(5) 1_445 .
Rb3 Rb3 OW4 62.9(4) 2 2
O4 Rb3 OW4 126.4(5) . 2
O14 Rb3 OW4 110.9(4) 1_445 2
OW4 Rb3 OW4 130.0(4) . 2
Rb3 Rb3 OW3 77.8(3) 2 2_665
O4 Rb3 OW3 79.5(3) . 2_665
O14 Rb3 OW3 115.7(3) 1_445 2_665
OW4 Rb3 OW3 33.4(5) . 2_665
OW4 Rb3 OW3 129.2(5) 2 2_665
Rb3 Rb3 O10 88.79(12) 2 2_655
O4 Rb3 O10 75.16(12) . 2_655
O14 Rb3 O10 150.92(14) 1_445 2_655
OW4 Rb3 O10 109.6(5) . 2_655
OW4 Rb3 O10 70.0(4) 2 2_655
OW3 Rb3 O10 78.6(3) 2_665 2_655
Rb3 Rb3 O12 127.03(14) 2 2_655
O4 Rb3 O12 52.45(11) . 2_655
O14 Rb3 O12 104.78(12) 1_445 2_655
OW4 Rb3 O12 143.3(5) . 2_655
OW4 Rb3 O12 74.1(4) 2 2_655
OW3 Rb3 O12 110.9(3) 2_665 2_655
O10 Rb3 O12 46.50(10) 2_655 2_655
Rb3 Rb3 O6 131.39(16) 2 .
O4 Rb3 O6 48.62(12) . .
O14 Rb3 O6 51.96(10) 1_445 .
OW4 Rb3 O6 66.2(5) . .
OW4 Rb3 O6 160.1(4) 2 .
OW3 Rb3 O6 70.7(3) 2_665 .
O10 Rb3 O6 118.98(12) 2_655 .
O12 Rb3 O6 98.91(11) 2_655 .
Rb3 Rb3 Rb2 98.97(12) 2 1_445
O4 Rb3 Rb2 97.07(11) . 1_445
O14 Rb3 Rb2 86.36(10) 1_445 1_445
OW4 Rb3 Rb2 163.2(5) . 1_445
OW4 Rb3 Rb2 37.3(4) 2 1_445
OW3 Rb3 Rb2 156.7(3) 2_665 1_445
O10 Rb3 Rb2 78.22(9) 2_655 1_445
O12 Rb3 Rb2 52.57(8) 2_655 1_445
O6 Rb3 Rb2 123.98(9) . 1_445
Rb3 Rb3 Se1 156.35(13) 2 .
O4 Rb3 Se1 48.62(9) . .
O14 Rb3 Se1 50.99(9) 1_445 .
OW4 Rb3 Se1 128.3(5) . .
OW4 Rb3 Se1 99.3(4) 2 .
OW3 Rb3 Se1 125.3(3) 2_665 .
O10 Rb3 Se1 99.94(10) 2_655 .
O12 Rb3 Se1 54.16(7) 2_655 .
O6 Rb3 Se1 62.54(8) . .
Rb2 Rb3 Se1 62.03(5) 1_445 .
Rb3 Rb3 Se2 144.95(14) 2 .
O4 Rb3 Se2 23.74(9) . .
O14 Rb3 Se2 70.88(9) 1_445 .
OW4 Rb3 Se2 79.2(5) . .
OW4 Rb3 Se2 149.5(4) 2 .
OW3 Rb3 Se2 68.5(3) 2_665 .
O10 Rb3 Se2 93.76(9) 2_655 .
O12 Rb3 Se2 76.06(8) 2_655 .
O6 Rb3 Se2 26.06(8) . .
Rb2 Rb3 Se2 115.79(6) 1_445 .
Se1 Rb3 Se2 56.96(3) . .
Rb4 Rb4 O7 142.52(17) 2_656 .
Rb4 Rb4 O18 135.90(15) 2_656 1_545
O7 Rb4 O18 81.47(13) . 1_545
Rb4 Rb4 O9 144.14(18) 2_656 .
O7 Rb4 O9 49.01(11) . .
O18 Rb4 O9 52.60(11) 1_545 .
Rb4 Rb4 O3 109.81(15) 2_656 .
O7 Rb4 O3 50.64(11) . .
O18 Rb4 O3 102.82(12) 1_545 .
O9 Rb4 O3 97.87(11) . .
Rb4 Rb4 O1 73.03(12) 2_656 .
O7 Rb4 O1 73.07(12) . .
O18 Rb4 O1 146.45(13) 1_545 .
O9 Rb4 O1 117.68(11) . .
O3 Rb4 O1 43.85(10) . .
Rb4 Rb4 Rb5 93.25(14) 2_656 2_766
O7 Rb4 Rb5 79.83(10) . 2_766
O18 Rb4 Rb5 92.43(11) 1_545 2_766
O9 Rb4 Rb5 51.60(9) . 2_766
O3 Rb4 Rb5 123.86(10) . 2_766
O1 Rb4 Rb5 103.91(10) . 2_766
Rb4 Rb4 Rb1 93.50(13) 2_656 1_545
O7 Rb4 Rb1 92.08(10) . 1_545
O18 Rb4 Rb1 85.82(10) 1_545 1_545
O9 Rb4 Rb1 122.14(10) . 1_545
O3 Rb4 Rb1 49.22(8) . 1_545
O1 Rb4 Rb1 73.87(9) . 1_545
Rb5 Rb4 Rb1 171.89(7) 2_766 1_545
Rb4 Rb4 Se5 152.73(16) 2_656 1_545
O7 Rb4 Se5 47.64(9) . 1_545
O18 Rb4 Se5 49.98(8) 1_545 1_545
O9 Rb4 Se5 63.08(8) . 1_545
O3 Rb4 Se5 53.13(8) . 1_545
O1 Rb4 Se5 96.47(9) . 1_545
Rb5 Rb4 Se5 113.86(7) 2_766 1_545
Rb1 Rb4 Se5 59.23(5) 1_545 1_545
Rb4 Rb4 Se3 146.77(14) 2_656 .
O7 Rb4 Se3 24.12(8) . .
O18 Rb4 Se3 69.98(9) 1_545 .
O9 Rb4 Se3 25.84(8) . .
O3 Rb4 Se3 74.65(7) . .
O1 Rb4 Se3 92.64(8) . .
Rb5 Rb4 Se3 60.57(5) 2_766 .
Rb1 Rb4 Se3 111.49(6) 1_545 .
Se5 Rb4 Se3 56.20(3) 1_545 .
Rb4 Rb4 Se6 118.27(11) 2_656 1_545
O7 Rb4 Se6 98.69(10) . 1_545
O18 Rb4 Se6 21.69(8) 1_545 1_545
O9 Rb4 Se6 74.18(9) . 1_545
O3 Rb4 Se6 104.13(9) . 1_545
O1 Rb4 Se6 144.65(10) . 1_545
Rb5 Rb4 Se6 108.39(8) 2_766 1_545
Rb1 Rb4 Se6 72.13(5) 1_545 1_545
Se5 Rb4 Se6 57.43(3) 1_545 1_545
Se3 Rb4 Se6 90.92(4) . 1_545
Rb4 Rb4 Se6 107.86(13) 2_656 2_766
O7 Rb4 Se6 99.34(10) . 2_766
O18 Rb4 Se6 43.26(9) 1_545 2_766
O9 Rb4 Se6 50.78(8) . 2_766
O3 Rb4 Se6 142.04(9) . 2_766
O1 Rb4 Se6 161.39(10) . 2_766
Rb5 Rb4 Se6 57.62(6) 2_766 2_766
Rb1 Rb4 Se6 124.05(7) 1_545 2_766
Se5 Rb4 Se6 90.13(4) 1_545 2_766
Se3 Rb4 Se6 76.60(4) . 2_766
Se6 Rb4 Se6 52.09(3) 1_545 2_766
Rb5 Rb5 OW5 137.4(2) 2_766 1_655
Rb5 Rb5 O8 75.32(14) 2_766 2_766
OW5 Rb5 O8 91.1(3) 1_655 2_766
Rb5 Rb5 O9 68.82(14) 2_766 2_766
OW5 Rb5 O9 131.1(2) 1_655 2_766
O8 Rb5 O9 50.69(12) 2_766 2_766
Rb5 Rb5 Rb1 138.96(16) 2_766 1_655
OW5 Rb5 Rb1 51.9(2) 1_655 1_655
O8 Rb5 Rb1 140.98(15) 2_766 1_655
O9 Rb5 Rb1 143.22(13) 2_766 1_655
Rb5 Rb5 O9 67.01(14) 2_766 .
OW5 Rb5 O9 84.3(2) 1_655 .
O8 Rb5 O9 115.86(14) 2_766 .
O9 Rb5 O9 135.83(12) 2_766 .
Rb1 Rb5 O9 76.88(10) 1_655 .
Rb5 Rb5 O8 61.40(14) 2_766 .
OW5 Rb5 O8 120.2(2) 1_655 .
O8 Rb5 O8 136.72(12) 2_766 .
O9 Rb5 O8 108.60(14) 2_766 .
Rb1 Rb5 O8 80.18(10) 1_655 .
O9 Rb5 O8 47.73(12) . .
Rb5 Rb5 OW1 127.9(6) 2_766 1_655
OW5 Rb5 OW1 14.6(5) 1_655 1_655
O8 Rb5 OW1 77.0(6) 2_766 1_655
O9 Rb5 OW1 120.8(6) 2_766 1_655
Rb1 Rb5 OW1 66.5(6) 1_655 1_655
O9 Rb5 OW1 87.3(6) . 1_655
O8 Rb5 OW1 129.7(6) . 1_655
Rb5 Rb5 Rb4 126.29(16) 2_766 2_766
OW5 Rb5 Rb4 89.06(18) 1_655 2_766
O8 Rb5 Rb4 79.66(10) 2_766 2_766
O9 Rb5 Rb4 58.57(9) 2_766 2_766
Rb1 Rb5 Rb4 86.86(8) 1_655 2_766
O9 Rb5 Rb4 163.16(12) . 2_766
O8 Rb5 Rb4 125.62(12) . 2_766
OW1 Rb5 Rb4 90.2(6) 1_655 2_766
Rb5 Rb5 Se6 75.67(15) 2_766 .
OW5 Rb5 Se6 146.4(2) 1_655 .
O8 Rb5 Se6 106.57(11) 2_766 .
O9 Rb5 Se6 56.04(9) 2_766 .
Rb1 Rb5 Se6 101.37(8) 1_655 .
O9 Rb5 Se6 111.50(12) . .
O8 Rb5 Se6 64.27(9) . .
OW1 Rb5 Se6 155.4(6) 1_655 .
Rb4 Rb5 Se6 67.15(6) 2_766 .
Rb5 Rb5 Se3 75.07(11) 2_766 2_766
OW5 Rb5 Se3 108.9(2) 1_655 2_766
O8 Rb5 Se3 25.74(9) 2_766 2_766
O9 Rb5 Se3 25.86(8) 2_766 2_766
Rb1 Rb5 Se3 145.82(10) 1_655 2_766
O9 Rb5 Se3 134.10(12) . 2_766
O8 Rb5 Se3 129.42(12) . 2_766
OW1 Rb5 Se3 96.6(6) 1_655 2_766
Rb4 Rb5 Se3 62.73(5) 2_766 2_766
Se6 Rb5 Se3 81.78(6) . 2_766
Rb5 Rb5 Se6 69.24(13) 2_766 2_766
OW5 Rb5 Se6 68.47(18) 1_655 2_766
O8 Rb5 Se6 64.82(9) 2_766 2_766
O9 Rb5 Se6 108.95(11) 2_766 2_766
Rb1 Rb5 Se6 104.91(8) 1_655 2_766
O9 Rb5 Se6 54.17(9) . 2_766
O8 Rb5 Se6 97.76(10) . 2_766
OW1 Rb5 Se6 59.1(6) 1_655 2_766
Rb4 Rb5 Se6 136.55(8) 2_766 2_766
Se6 Rb5 Se6 144.91(9) . 2_766
Se3 Rb5 Se6 89.14(6) 2_766 2_766
OW3 Rb6 Rb6 134.6(7) . 2_665
OW3 Rb6 Rb2 78.6(6) . .
Rb6 Rb6 Rb2 143.6(3) 2_665 .
OW3 Rb6 OW4 34.3(8) . 2_665
Rb6 Rb6 OW4 168.8(5) 2_665 2_665
Rb2 Rb6 OW4 45.7(5) . 2_665
OW3 Rb6 O15 119.8(6) . 2_665
Rb6 Rb6 O15 73.10(18) 2_665 2_665
Rb2 Rb6 O15 105.82(14) . 2_665
OW4 Rb6 O15 112.8(5) 2_665 2_665
OW3 Rb6 OW2 40.1(6) . 2_665
Rb6 Rb6 OW2 147.6(3) 2_665 2_665
Rb2 Rb6 OW2 65.40(13) . 2_665
OW4 Rb6 OW2 30.5(5) 2_665 2_665
O15 Rb6 OW2 86.06(15) 2_665 2_665
OW3 Rb6 O15 86.2(6) . .
Rb6 Rb6 O15 71.39(19) 2_665 .
Rb2 Rb6 O15 102.62(13) . .
OW4 Rb6 O15 102.2(5) 2_665 .
O15 Rb6 O15 144.49(13) 2_665 .
OW2 Rb6 O15 125.52(16) 2_665 .
OW3 Rb6 OW3 155.0(4) . 2_665
Rb6 Rb6 OW3 20.3(3) 2_665 2_665
Rb2 Rb6 OW3 125.1(3) . 2_665
OW4 Rb6 OW3 170.6(6) 2_665 2_665
O15 Rb6 OW3 65.5(3) 2_665 2_665
OW2 Rb6 OW3 151.1(3) 2_665 2_665
O15 Rb6 OW3 80.9(3) . 2_665
OW3 Rb6 O13 115.3(6) . .
Rb6 Rb6 O13 81.6(2) 2_665 .
Rb2 Rb6 O13 68.04(11) . .
OW4 Rb6 O13 101.9(6) 2_665 .
O15 Rb6 O13 121.92(16) 2_665 .
OW2 Rb6 O13 130.74(17) 2_665 .
O15 Rb6 O13 52.24(13) . .
OW3 Rb6 O13 72.8(3) 2_665 .
OW3 Rb6 O13 88.7(6) . 2_665
Rb6 Rb6 O13 66.6(2) 2_665 2_665
Rb2 Rb6 O13 140.84(13) . 2_665
OW4 Rb6 O13 109.3(5) 2_665 2_665
O15 Rb6 O13 49.81(12) 2_665 2_665
OW2 Rb6 O13 81.04(15) 2_665 2_665
O15 Rb6 O13 113.47(16) . 2_665
OW3 Rb6 O13 77.0(3) 2_665 2_665
O13 Rb6 O13 148.22(12) . 2_665
OW3 Rb6 O12 122.4(6) . .
Rb6 Rb6 O12 100.5(2) 2_665 .
Rb2 Rb6 O12 57.34(10) . .
OW4 Rb6 O12 90.5(5) 2_665 .
O15 Rb6 O12 53.23(12) 2_665 .
OW2 Rb6 O12 85.46(14) 2_665 .
O15 Rb6 O12 134.76(15) . .
OW3 Rb6 O12 81.2(3) 2_665 .
O13 Rb6 O12 82.78(13) . .
O13 Rb6 O12 102.36(12) 2_665 .
OW3 Rb6 Se5 97.5(6) . 2_665
Rb6 Rb6 Se5 78.11(17) 2_665 2_665
Rb2 Rb6 Se5 117.46(10) . 2_665
OW4 Rb6 Se5 103.0(5) 2_665 2_665
O15 Rb6 Se5 26.28(9) 2_665 2_665
OW2 Rb6 Se5 72.62(12) 2_665 2_665
O15 Rb6 Se5 139.73(15) . 2_665
OW3 Rb6 Se5 79.3(3) 2_665 2_665
O13 Rb6 Se5 146.97(13) . 2_665
O13 Rb6 Se5 27.44(8) 2_665 2_665
O12 Rb6 Se5 75.70(8) . 2_665
O2 Se1 O3 99.1(2) . .
O2 Se1 O1 100.2(2) . .
O3 Se1 O1 101.1(2) . .
O2 Se1 Rb3 140.36(15) . .
O3 Se1 Rb3 110.00(14) . .
O1 Se1 Rb3 99.90(15) . .
O2 Se1 Rb2 92.60(14) . 1_445
O3 Se1 Rb2 102.37(14) . 1_445
O1 Se1 Rb2 151.05(16) . 1_445
Rb3 Se1 Rb2 55.93(5) . 1_445
O2 Se1 Rb1 52.83(16) . 1_545
O3 Se1 Rb1 47.74(14) . 1_545
O1 Se1 Rb1 96.67(15) . 1_545
Rb3 Se1 Rb1 154.84(4) . 1_545
Rb2 Se1 Rb1 111.66(4) 1_445 1_545
O2 Se1 Rb2 77.53(15) . 2_655
O3 Se1 Rb2 74.25(14) . 2_655
O1 Se1 Rb2 174.25(16) . 2_655
Rb3 Se1 Rb2 84.98(5) . 2_655
Rb2 Se1 Rb2 34.70(6) 1_445 2_655
Rb1 Se1 Rb2 77.74(4) 1_545 2_655
O6 Se2 O5 98.4(2) . .
O6 Se2 O4 99.8(2) . .
O5 Se2 O4 98.96(19) . .
O6 Se2 Rb1 51.81(14) . .
O5 Se2 Rb1 55.73(15) . .
O4 Se2 Rb1 129.69(15) . .
O6 Se2 Rb3 61.86(15) . .
O5 Se2 Rb3 89.44(14) . .
O4 Se2 Rb3 40.88(16) . .
Rb1 Se2 Rb3 91.77(5) . .
O9 Se3 O7 99.6(2) . .
O9 Se3 O8 97.5(2) . .
O7 Se3 O8 99.6(2) . .
O9 Se3 Rb5 51.39(15) . 2_766
O7 Se3 Rb5 92.62(14) . 2_766
O8 Se3 Rb5 48.30(14) . 2_766
O9 Se3 Rb4 58.22(15) . .
O7 Se3 Rb4 43.81(14) . .
O8 Se3 Rb4 90.67(14) . .
Rb5 Se3 Rb4 56.70(6) 2_766 .
O9 Se3 Rb5 49.50(15) . .
O7 Se3 Rb5 127.03(14) . .
O8 Se3 Rb5 55.39(15) . .
Rb5 Se3 Rb5 34.78(9) 2_766 .
Rb4 Se3 Rb5 86.74(6) . .
O9 Se3 Rb1 71.44(14) . 1_655
O7 Se3 Rb1 170.77(14) . 1_655
O8 Se3 Rb1 79.79(14) . 1_655
Rb5 Se3 Rb1 80.09(5) 2_766 1_655
Rb4 Se3 Rb1 126.99(5) . 1_655
Rb5 Se3 Rb1 45.34(5) . 1_655
O10 Se4 O11 99.8(2) . .
O10 Se4 O12 101.1(2) . .
O11 Se4 O12 98.20(19) . .
O10 Se4 Rb6 167.21(14) . .
O11 Se4 Rb6 83.50(15) . .
O12 Se4 Rb6 66.15(16) . .
O10 Se4 Rb2 130.79(14) . .
O11 Se4 Rb2 55.29(14) . .
O12 Se4 Rb2 51.75(13) . .
Rb6 Se4 Rb2 42.20(6) . .
O10 Se4 Rb2 95.08(14) . 2_765
O11 Se4 Rb2 49.02(14) . 2_765
O12 Se4 Rb2 50.98(14) . 2_765
Rb6 Se4 Rb2 77.64(6) . 2_765
Rb2 Se4 Rb2 35.80(6) . 2_765
O10 Se4 Rb6 161.22(15) . 2_665
O11 Se4 Rb6 95.80(16) . 2_665
O12 Se4 Rb6 86.92(16) . 2_665
Rb6 Se4 Rb6 26.07(9) . 2_665
Rb2 Se4 Rb6 67.27(5) . 2_665
Rb2 Se4 Rb6 103.07(6) 2_765 2_665
O10 Se4 Rb3 51.65(14) . 2_655
O11 Se4 Rb3 89.04(15) . 2_655
O12 Se4 Rb3 52.69(16) . 2_655
Rb6 Se4 Rb3 116.44(6) . 2_655
Rb2 Se4 Rb3 83.42(5) . 2_655
Rb2 Se4 Rb3 52.42(4) 2_765 2_655
Rb6 Se4 Rb3 139.57(5) 2_665 2_655
O13 Se5 O15 98.8(2) . .
O13 Se5 O14 100.2(2) . .
O15 Se5 O14 100.86(19) . .
O13 Se5 Rb1 94.29(14) . .
O15 Se5 Rb1 101.10(14) . .
O14 Se5 Rb1 151.39(14) . .
O13 Se5 Rb6 61.69(15) . 2_665
O15 Se5 Rb6 47.14(14) . 2_665
O14 Se5 Rb6 132.37(14) . 2_665
Rb1 Se5 Rb6 76.24(6) . 2_665
O13 Se5 Rb6 52.26(15) . .
O15 Se5 Rb6 46.55(15) . .
O14 Se5 Rb6 106.20(14) . .
Rb1 Se5 Rb6 102.20(6) . .
Rb6 Se5 Rb6 26.92(10) 2_665 .
O13 Se5 Rb4 141.86(14) . 1_565
O15 Se5 Rb4 111.40(15) . 1_565
O14 Se5 Rb4 96.47(14) . 1_565
Rb1 Se5 Rb4 58.29(5) . 1_565
Rb6 Se5 Rb4 125.58(7) 2_665 1_565
Rb6 Se5 Rb4 150.53(7) . 1_565
O13 Se5 Rb3 81.59(14) . 1_665
O15 Se5 Rb3 71.43(14) . 1_665
O14 Se5 Rb3 37.96(14) . 1_665
Rb1 Se5 Rb3 170.64(4) . 1_665
Rb6 Se5 Rb3 94.42(6) 2_665 1_665
Rb6 Se5 Rb3 68.62(6) . 1_665
Rb4 Se5 Rb3 129.17(5) 1_565 1_665
O16 Se6 O17 97.9(2) . .
O16 Se6 O18 99.6(2) . .
O17 Se6 O18 99.6(2) . .
O16 Se6 Rb5 94.64(16) . .
O17 Se6 Rb5 101.85(16) . .
O18 Se6 Rb5 152.27(15) . .
O16 Se6 Rb5 76.40(16) . 2_766
O17 Se6 Rb5 75.08(15) . 2_766
O18 Se6 Rb5 172.63(15) . 2_766
Rb5 Se6 Rb5 35.09(9) . 2_766
O16 Se6 Rb4 85.35(16) . 1_565
O17 Se6 Rb4 66.14(15) . 1_565
O18 Se6 Rb4 38.70(14) . 1_565
Rb5 Se6 Rb4 167.81(5) . 1_565
Rb5 Se6 Rb4 134.10(6) 2_766 1_565
O16 Se6 Rb4 145.27(16) . 2_766
O17 Se6 Rb4 104.50(14) . 2_766
O18 Se6 Rb4 102.32(14) . 2_766
Rb5 Se6 Rb4 55.24(6) . 2_766
Rb5 Se6 Rb4 84.10(6) 2_766 2_766
Rb4 Se6 Rb4 127.91(3) 1_565 2_766
O6 Ga1 O18 176.25(19) . 1_445
O6 Ga1 O1 91.04(18) . .
O18 Ga1 O1 92.11(17) 1_445 .
O6 Ga1 O17 93.50(17) . 2_666
O18 Ga1 O17 88.53(16) 1_445 2_666
O1 Ga1 O17 90.43(18) . 2_666
O6 Ga1 O9 88.48(18) . 1_455
O18 Ga1 O9 88.40(17) 1_445 1_455
O1 Ga1 O9 179.29(17) . 1_455
O17 Ga1 O9 89.08(18) 2_666 1_455
O6 Ga1 O14 89.37(17) . 1_445
O18 Ga1 O14 88.52(16) 1_445 1_445
O1 Ga1 O14 91.16(17) . 1_445
O17 Ga1 O14 176.70(17) 2_666 1_445
O9 Ga1 O14 89.35(17) 1_455 1_445
O6 Ga1 Rb4 138.00(14) . 1_455
O18 Ga1 Rb4 38.49(13) 1_445 1_455
O1 Ga1 Rb4 129.66(12) . 1_455
O17 Ga1 Rb4 95.74(13) 2_666 1_455
O9 Ga1 Rb4 50.92(12) 1_455 1_455
O14 Ga1 Rb4 81.02(12) 1_445 1_455
O6 Ga1 Rb3 52.38(13) . .
O18 Ga1 Rb3 126.19(12) 1_445 .
O1 Ga1 Rb3 81.13(12) . .
O17 Ga1 Rb3 144.27(12) 2_666 .
O9 Ga1 Rb3 98.98(12) 1_455 .
O14 Ga1 Rb3 38.94(12) 1_445 .
Rb4 Ga1 Rb3 116.38(5) 1_455 .
O15 Ga2 O7 89.95(17) 1_545 .
O15 Ga2 O12 93.52(18) 1_545 2_655
O7 Ga2 O12 175.67(19) . 2_655
O15 Ga2 O4 178.27(16) 1_545 .
O7 Ga2 O4 88.59(17) . .
O12 Ga2 O4 87.98(18) 2_655 .
O15 Ga2 O10 88.57(17) 1_545 .
O7 Ga2 O10 92.31(16) . .
O12 Ga2 O10 90.37(16) 2_655 .
O4 Ga2 O10 90.55(17) . .
O15 Ga2 O3 91.55(17) 1_545 .
O7 Ga2 O3 87.56(16) . .
O12 Ga2 O3 89.76(16) 2_655 .
O4 Ga2 O3 89.33(17) . .
O10 Ga2 O3 179.82(18) . .
O15 Ga2 Rb6 39.28(12) 1_545 2_655
O7 Ga2 Rb6 123.71(14) . 2_655
O12 Ga2 Rb6 58.65(14) 2_655 2_655
O4 Ga2 Rb6 142.45(12) . 2_655
O10 Ga2 Rb6 105.15(13) . 2_655
O3 Ga2 Rb6 75.02(13) . 2_655
O15 Ga2 Rb3 146.16(12) 1_545 .
O7 Ga2 Rb3 123.88(14) . .
O12 Ga2 Rb3 52.67(14) 2_655 .
O4 Ga2 Rb3 35.31(12) . .
O10 Ga2 Rb3 90.28(14) . .
O3 Ga2 Rb3 89.69(13) . .
Rb6 Ga2 Rb3 109.36(6) 2_655 .
O16 Ga3 O8 88.59(17) . .
O16 Ga3 O2 94.92(17) . 1_665
O8 Ga3 O2 85.78(17) . 1_665
O16 Ga3 O11 175.36(18) . .
O8 Ga3 O11 92.96(17) . .
O2 Ga3 O11 89.56(17) 1_665 .
O16 Ga3 O5 83.47(17) . .
O8 Ga3 O5 91.93(17) . .
O2 Ga3 O5 177.23(17) 1_665 .
O11 Ga3 O5 92.11(17) . .
O16 Ga3 O13 92.71(18) . .
O8 Ga3 O13 178.66(18) . .
O2 Ga3 O13 93.75(17) 1_665 .
O11 Ga3 O13 85.77(17) . .
O5 Ga3 O13 88.58(17) . .
O16 Ga3 Rb2 135.76(13) . .
O8 Ga3 Rb2 131.72(13) . .
O2 Ga3 Rb2 74.39(12) 1_665 .
O11 Ga3 Rb2 44.60(12) . .
O5 Ga3 Rb2 108.33(12) . .
O13 Ga3 Rb2 46.94(12) . .
Se1 O1 Ga1 120.8(2) . .
Se1 O1 Rb4 102.53(19) . .
Ga1 O1 Rb4 133.96(17) . .
Se1 O2 Ga3 123.8(3) . 1_445
Se1 O2 Rb1 101.27(18) . 1_545
Ga3 O2 Rb1 133.52(18) 1_445 1_545
Se1 O3 Ga2 113.5(2) . .
Se1 O3 Rb1 106.98(17) . 1_545
Ga2 O3 Rb1 139.3(2) . 1_545
Se1 O3 Rb4 109.96(17) . .
Ga2 O3 Rb4 99.93(15) . .
Rb1 O3 Rb4 68.97(10) 1_545 .
Se2 O4 Ga2 124.0(2) . .
Se2 O4 Rb3 115.4(2) . .
Ga2 O4 Rb3 120.29(17) . .
Se2 O5 Ga3 122.3(2) . .
Se2 O5 Rb1 97.51(18) . .
Ga3 O5 Rb1 113.25(16) . .
Se2 O6 Ga1 118.3(2) . .
Se2 O6 Rb1 102.12(17) . .
Ga1 O6 Rb1 123.64(19) . .
Se2 O6 Rb3 92.08(17) . .
Ga1 O6 Rb3 100.32(15) . .
Rb1 O6 Rb3 116.56(14) . .
Se3 O7 Ga2 125.6(2) . .
Se3 O7 Rb4 112.07(19) . .
Ga2 O7 Rb4 121.85(17) . .
Se3 O8 Ga3 123.9(2) . .
Se3 O8 Rb5 105.97(19) . 2_766
Ga3 O8 Rb5 129.85(18) . 2_766
Se3 O8 Rb5 98.87(19) . .
Ga3 O8 Rb5 116.32(16) . .
Rb5 O8 Rb5 43.28(12) 2_766 .
Se3 O9 Ga1 115.9(2) . 1_655
Se3 O9 Rb5 102.7(2) . 2_766
Ga1 O9 Rb5 141.14(19) 1_655 2_766
Se3 O9 Rb5 105.73(19) . .
Ga1 O9 Rb5 121.91(19) 1_655 .
Rb5 O9 Rb5 44.17(12) 2_766 .
Se3 O9 Rb4 95.94(17) . .
Ga1 O9 Rb4 101.14(16) 1_655 .
Rb5 O9 Rb4 69.83(11) 2_766 .
Rb5 O9 Rb4 113.22(15) . .
Se4 O10 Ga2 120.5(2) . .
Se4 O10 Rb3 104.65(17) . 2_655
Ga2 O10 Rb3 134.21(19) . 2_655
Se4 O11 Ga3 120.6(2) . .
Se4 O11 Rb2 105.34(17) . 2_765
Ga3 O11 Rb2 131.25(17) . 2_765
Se4 O11 Rb2 98.26(17) . .
Ga3 O11 Rb2 109.05(16) . .
Rb2 O11 Rb2 44.69(9) 2_765 .
Se4 O12 Ga2 115.7(2) . 2_655
Se4 O12 Rb2 103.11(17) . 2_765
Ga2 O12 Rb2 141.01(19) 2_655 2_765
Se4 O12 Rb2 102.15(17) . .
Ga2 O12 Rb2 124.33(18) 2_655 .
Rb2 O12 Rb2 45.16(9) 2_765 .
Se4 O12 Rb3 103.38(18) . 2_655
Ga2 O12 Rb3 99.27(16) 2_655 2_655
Rb2 O12 Rb3 66.26(11) 2_765 2_655
Rb2 O12 Rb3 110.37(14) . 2_655
Se4 O12 Rb6 87.13(17) . .
Ga2 O12 Rb6 92.21(16) 2_655 .
Rb2 O12 Rb6 93.83(11) 2_765 .
Rb2 O12 Rb6 48.99(9) . .
Rb3 O12 Rb6 158.99(14) 2_655 .
Se5 O13 Ga3 122.9(2) . .
Se5 O13 Rb6 101.25(19) . .
Ga3 O13 Rb6 130.95(18) . .
Se5 O13 Rb2 126.12(19) . .
Ga3 O13 Rb2 106.15(17) . .
Rb6 O13 Rb2 51.73(10) . .
Se5 O13 Rb6 90.87(18) . 2_665
Ga3 O13 Rb6 120.07(17) . 2_665
Rb6 O13 Rb6 31.78(12) . 2_665
Rb2 O13 Rb6 82.00(11) . 2_665
Se5 O14 Ga1 122.9(2) . 1_665
Se5 O14 Rb3 121.02(19) . 1_665
Ga1 O14 Rb3 115.43(17) 1_665 1_665
Se5 O15 Ga2 113.7(2) . 1_565
Se5 O15 Rb6 106.58(19) . 2_665
Ga2 O15 Rb6 114.48(18) 1_565 2_665
Se5 O15 Rb6 107.7(2) . .
Ga2 O15 Rb6 135.8(2) 1_565 .
Rb6 O15 Rb6 35.51(13) 2_665 .
Se6 O16 Ga3 126.5(2) . .
Se6 O16 Rb1 123.9(2) . .
Ga3 O16 Rb1 105.62(16) . .
Se6 O17 Ga1 114.3(2) . 2_666
Se6 O18 Ga1 124.0(2) . 1_665
Se6 O18 Rb4 119.61(19) . 1_565
Ga1 O18 Rb4 116.33(18) 1_665 1_565
OW1 OW1 OW5 77(5) 2_666 .
OW1 OW1 OW5 55(4) 2_666 2_666
OW5 OW1 OW5 132(3) . 2_666
OW1 OW1 Rb5 123(6) 2_666 1_455
OW5 OW1 Rb5 50.4(17) . 1_455
OW5 OW1 Rb5 162(2) 2_666 1_455
OW1 OW1 Rb1 92(5) 2_666 2_666
OW5 OW1 Rb1 169(2) . 2_666
OW5 OW1 Rb1 36.8(18) 2_666 2_666
Rb5 OW1 Rb1 139.4(10) 1_455 2_666
OW1 OW1 Rb1 75(5) 2_666 .
OW5 OW1 Rb1 2.8(14) . .
OW5 OW1 Rb1 129(2) 2_666 .
Rb5 OW1 Rb1 53.1(6) 1_455 .
Rb1 OW1 Rb1 166.1(9) 2_666 .
OW4 OW2 Rb1 156.7(10) . .
OW4 OW2 Rb6 72.4(9) . 2_665
Rb1 OW2 Rb6 130.8(2) . 2_665
OW4 OW2 Rb2 41.5(9) . 2_665
Rb1 OW2 Rb2 145.2(2) . 2_665
Rb6 OW2 Rb2 55.39(13) 2_665 2_665
Rb6 OW3 OW4 119.3(11) . 2_665
Rb6 OW3 Rb2 71.7(6) . .
OW4 OW3 Rb2 49.5(8) 2_665 .
Rb6 OW3 Rb6 25.0(4) . 2_665
OW4 OW3 Rb6 144.3(10) 2_665 2_665
Rb2 OW3 Rb6 95.7(4) . 2_665
Rb6 OW3 Rb3 150.2(9) . 2_665
OW4 OW3 Rb3 67.1(8) 2_665 2_665
Rb2 OW3 Rb3 101.1(4) . 2_665
Rb6 OW3 Rb3 139.4(5) 2_665 2_665
OW2 OW4 OW3 73.7(11) . 2_665
OW2 OW4 Rb2 111.2(12) . 2_665
OW3 OW4 Rb2 90.7(11) 2_665 2_665
OW2 OW4 Rb6 77.1(9) . 2_665
OW3 OW4 Rb6 26.4(6) 2_665 2_665
Rb2 OW4 Rb6 65.7(6) 2_665 2_665
OW2 OW4 Rb3 113.8(12) . .
OW3 OW4 Rb3 79.4(9) 2_665 .
Rb2 OW4 Rb3 128.7(11) 2_665 .
Rb6 OW4 Rb3 101.8(7) 2_665 .
OW2 OW4 Rb3 161.6(14) . 2
OW3 OW4 Rb3 92.9(11) 2_665 2
Rb2 OW4 Rb3 81.0(8) 2_665 2
Rb6 OW4 Rb3 96.7(7) 2_665 2
Rb3 OW4 Rb3 50.0(4) . 2
OW2 OW4 Rb1 13.8(6) . .
OW3 OW4 Rb1 86.3(10) 2_665 .
Rb2 OW4 Rb1 117.6(8) 2_665 .
Rb6 OW4 Rb1 90.8(6) 2_665 .
Rb3 OW4 Rb1 111.8(7) . .
Rb3 OW4 Rb1 161.3(8) 2 .
OW1 OW5 OW1 48(3) . 2_666
OW1 OW5 Rb1 176.2(19) . .
OW1 OW5 Rb1 128(2) 2_666 .
OW1 OW5 Rb5 115.0(19) . 1_455
OW1 OW5 Rb5 154.0(18) 2_666 1_455
Rb1 OW5 Rb5 68.7(2) . 1_455
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Rb1 OW2 2.146(6) .
Rb1 OW5 2.555(11) .
Rb1 O3 2.954(4) 1_565
Rb1 O6 3.014(4) .
Rb1 Rb5 3.026(3) 1_455
Rb1 O2 3.102(5) 1_565
Rb1 O5 3.125(5) .
Rb1 OW1 3.35(4) 2_666
Rb1 O16 3.349(5) .
Rb1 OW1 3.47(4) .
Rb1 OW4 3.56(3) .
Rb1 Rb4 3.641(3) 1_565
Rb2 OW4 2.14(2) 2_665
Rb2 Rb2 2.332(4) 2_765
Rb2 Rb6 2.727(4) .
Rb2 OW3 2.815(14) .
Rb2 O11 2.974(4) 2_765
Rb2 OW2 3.012(6) 2_665
Rb2 O12 3.030(4) 2_765
Rb2 O12 3.042(4) .
Rb2 O11 3.146(4) .
Rb2 O13 3.221(4) .
Rb2 Rb3 3.493(3) 1_665
Rb2 Se1 3.7243(19) 1_665
Rb3 Rb3 2.588(4) 2
Rb3 O4 2.778(5) .
Rb3 O14 2.924(4) 1_445
Rb3 OW4 3.01(2) .
Rb3 OW4 3.11(3) 2
Rb3 OW3 3.212(13) 2_665
Rb3 O10 3.314(5) 2_655
Rb3 O12 3.343(5) 2_655
Rb3 O6 3.383(5) .
Rb3 Rb2 3.493(3) 1_445
Rb3 Se1 3.724(2) .
Rb3 Se2 3.835(2) .
Rb4 Rb4 2.584(4) 2_656
Rb4 O7 2.879(4) .
Rb4 O18 2.891(5) 1_545
Rb4 O9 3.294(5) .
Rb4 O3 3.438(5) .
Rb4 O1 3.618(5) .
Rb4 Rb5 3.624(4) 2_766
Rb4 Rb1 3.641(3) 1_545
Rb4 Se5 3.795(2) 1_545
Rb4 Se3 3.854(2) .
Rb4 Se6 4.020(2) 1_545
Rb4 Se6 4.065(3) 2_766
Rb5 Rb5 2.290(6) 2_766
Rb5 OW5 2.795(9) 1_655
Rb5 O8 2.933(5) 2_766
Rb5 O9 3.026(5) 2_766
Rb5 Rb1 3.026(3) 1_655
Rb5 O9 3.064(5) .
Rb5 O8 3.231(5) .
Rb5 OW1 3.29(3) 1_655
Rb5 Rb4 3.624(4) 2_766
Rb5 Se6 3.725(3) .
Rb5 Se3 3.776(2) 2_766
Rb5 Se6 3.860(3) 2_766
Rb6 OW3 1.419(13) .
Rb6 Rb6 1.730(6) 2_665
Rb6 OW4 2.78(2) 2_665
Rb6 O15 2.823(5) 2_665
Rb6 OW2 2.846(6) 2_665
Rb6 O15 2.850(5) .
Rb6 OW3 2.908(14) 2_665
Rb6 O13 3.015(5) .
Rb6 O13 3.249(5) 2_665
Rb6 O12 3.468(5) .
Rb6 Se5 3.690(3) 2_665
Se1 O2 1.700(4) .
Se1 O3 1.704(4) .
Se1 O1 1.715(4) .
Se1 Rb2 3.7243(19) 1_445
Se1 Rb1 3.8171(18) 1_545
Se1 Rb2 4.0331(19) 2_655
Se2 O6 1.686(4) .
Se2 O5 1.703(4) .
Se2 O4 1.709(4) .
Se3 O9 1.689(4) .
Se3 O7 1.700(4) .
Se3 O8 1.706(4) .
Se3 Rb5 3.776(2) 2_766
Se3 Rb1 3.9688(18) 1_655
Se4 O10 1.699(4) .
Se4 O11 1.705(4) .
Se4 O12 1.705(4) .
Se4 Rb2 3.7985(17) 2_765
Se4 Rb6 3.875(4) 2_665
Se4 Rb3 4.089(2) 2_655
Se5 O13 1.701(4) .
Se5 O15 1.705(4) .
Se5 O14 1.706(4) .
Se5 Rb6 3.690(3) 2_665
Se5 Rb4 3.795(2) 1_565
Se5 Rb3 4.075(2) 1_665
Se6 O16 1.697(4) .
Se6 O17 1.706(4) .
Se6 O18 1.709(4) .
Se6 Rb5 3.860(3) 2_766
Se6 Rb4 4.020(2) 1_565
Se6 Rb4 4.065(3) 2_766
Ga1 O6 1.960(4) .
Ga1 O18 1.976(4) 1_445
Ga1 O1 1.978(4) .
Ga1 O17 1.981(4) 2_666
Ga1 O9 1.988(5) 1_455
Ga1 O14 2.013(4) 1_445
Ga1 Rb4 4.164(2) 1_455
Ga2 O15 1.971(4) 1_545
Ga2 O7 1.974(4) .
Ga2 O12 1.977(4) 2_655
Ga2 O4 1.984(4) .
Ga2 O10 1.997(4) .
Ga2 O3 1.998(4) .
Ga2 Rb6 4.057(3) 2_655
Ga3 O16 1.971(4) .
Ga3 O8 1.977(4) .
Ga3 O2 1.977(4) 1_665
Ga3 O11 1.988(4) .
Ga3 O5 1.992(4) .
Ga3 O13 1.995(4) .
O2 Ga3 1.977(4) 1_445
O2 Rb1 3.102(5) 1_545
O3 Rb1 2.954(4) 1_545
O8 Rb5 2.933(5) 2_766
O9 Ga1 1.988(5) 1_655
O9 Rb5 3.026(5) 2_766
O10 Rb3 3.314(5) 2_655
O11 Rb2 2.974(4) 2_765
O12 Ga2 1.977(4) 2_655
O12 Rb2 3.030(4) 2_765
O12 Rb3 3.343(5) 2_655
O13 Rb6 3.249(5) 2_665
O14 Ga1 2.013(4) 1_665
O14 Rb3 2.924(4) 1_665
O15 Ga2 1.971(4) 1_565
O15 Rb6 2.823(5) 2_665
O17 Ga1 1.981(4) 2_666
O18 Ga1 1.976(4) 1_665
O18 Rb4 2.891(5) 1_565
OW1 OW1 0.83(5) 2_666
OW1 OW5 0.92(4) .
OW1 OW5 1.09(4) 2_666
OW1 Rb5 3.29(3) 1_455
OW1 Rb1 3.35(4) 2_666
OW2 OW4 1.48(3) .
OW2 Rb6 2.846(6) 2_665
OW2 Rb2 3.012(6) 2_665
OW3 OW4 1.80(3) 2_665
OW3 Rb6 2.908(14) 2_665
OW3 Rb3 3.212(13) 2_665
OW4 OW3 1.80(3) 2_665
OW4 Rb2 2.14(2) 2_665
OW4 Rb6 2.78(2) 2_665
OW4 Rb3 3.11(3) 2
OW5 OW1 1.09(4) 2_666
OW5 Rb5 2.795(9) 1_455
