#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/93/4339311.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4339311
loop_
_publ_author_name
'Natrajan, Louise S.'
'Timmins, Phillipa L.'
'Lunn, Matthew'
'Heath, Sarah L.'
_publ_section_title
;
 Luminescent dinuclear lanthanide complexes of 5-Me-HXTA.
;
_journal_issue                   25
_journal_name_full               'Inorganic chemistry'
_journal_page_first              10877
_journal_page_last               10886
_journal_paper_doi               10.1021/ic701366f
_journal_volume                  46
_journal_year                    2007
_chemical_formula_sum            'C34 H74.5 N4 Na4 O29.5 Yb2'
_chemical_formula_weight         1449.52
_chemical_name_common            'Compound 8'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.758(6)
_cell_angle_beta                 98.158(6)
_cell_angle_gamma                108.341(3)
_cell_formula_units_Z            4
_cell_length_a                   16.9226(10)
_cell_length_b                   17.0690(10)
_cell_length_c                   20.2256(15)
_cell_measurement_reflns_used    13865
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      31.90
_cell_measurement_theta_min      2.53
_cell_volume                     5344.8(6)
_computing_cell_refinement
'CrysAlis RED, Oxford Diffraction Ltd, Version 1.71.30.2'
_computing_data_collection
'CrysAlis CCD, Oxford Diffraction Ltd, Version 1.71.30.2'
_computing_data_reduction
'CrysAlis RED, Oxford Diffraction Ltd, Version 1.71.30.2'
_computing_molecular_graphics    'SHELXTL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXTL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.838
_diffrn_measured_fraction_theta_max 0.838
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0595
_diffrn_reflns_av_sigmaI/netI    0.2862
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            50944
_diffrn_reflns_theta_full        31.97
_diffrn_reflns_theta_max         31.97
_diffrn_reflns_theta_min         2.54
_exptl_absorpt_coefficient_mu    3.603
_exptl_absorpt_correction_T_max  1.066
_exptl_absorpt_correction_T_min  0.895
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Empirical using spherical harmonics'
_exptl_crystal_colour            Colourless
_exptl_crystal_density_diffrn    1.801
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Needle
_exptl_crystal_F_000             2906
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.08
_refine_diff_density_max         4.012
_refine_diff_density_min         -3.577
_refine_diff_density_rms         0.418
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.944
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1337
_refine_ls_number_reflns         31023
_refine_ls_number_restraints     942
_refine_ls_restrained_S_all      0.934
_refine_ls_R_factor_all          0.1902
_refine_ls_R_factor_gt           0.0694
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1178P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1883
_refine_ls_wR_factor_ref         0.2412
_reflns_number_gt                12157
_reflns_number_total             31023
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic701366f-file001.cif
_cod_data_source_block           osf11pb1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/automatic-downloads/retrospective/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/usr/data/users/saulius/automatic-downloads/retrospective/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C34 H74.50 N4 Na4 O29.50 Yb2'
_cod_database_code               4339311
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Yb1 Yb 0.32759(3) 0.37562(3) 0.59538(3) 0.02071(14) Uani 1 1 d .
Yb2 Yb 0.23408(4) 0.41878(3) 0.74815(3) 0.02579(16) Uani 1 1 d .
Yb3 Yb 0.25819(3) 0.78920(3) 1.12337(3) 0.01626(13) Uani 1 1 d .
Yb4 Yb 0.34155(3) 1.01059(3) 1.22906(3) 0.01894(14) Uani 1 1 d .
N1 N 0.2218(7) 0.3672(7) 0.4902(6) 0.0335(8) Uani 1 1 d U
O1 O 0.2560(5) 0.4534(5) 0.6452(5) 0.0321(9) Uani 1 1 d U
C1 C 0.2183(8) 0.4999(8) 0.6154(8) 0.0329(8) Uani 1 1 d U
N2 N 0.2597(7) 0.5773(7) 0.7744(6) 0.0340(8) Uani 1 1 d U
O2 O 0.2310(6) 0.2416(6) 0.5504(5) 0.0342(10) Uani 1 1 d U
C2 C 0.1647(9) 0.4692(8) 0.5515(8) 0.0340(8) Uani 1 1 d U
N3 N 0.4292(7) 0.3019(6) 0.6275(6) 0.0266(7) Uani 1 1 d U
O3 O 0.1584(6) 0.1383(6) 0.4612(5) 0.0357(10) Uani 1 1 d U
C3 C 0.1286(8) 0.5199(8) 0.5229(8) 0.0347(8) Uani 1 1 d U
H3A H 0.0951 0.4981 0.4789 0.042 Uiso 1 1 calc R
N4 N 0.1185(7) 0.2824(7) 0.7531(6) 0.0323(7) Uani 1 1 d U
O4 O 0.3736(6) 0.4969(5) 0.5524(5) 0.0325(10) Uani 1 1 d U
C4 C 0.1385(9) 0.5998(8) 0.5545(8) 0.0350(8) Uani 1 1 d U
N5 N 0.4333(6) 1.1028(6) 1.1626(6) 0.0246(7) Uani 1 1 d U
O5 O 0.3502(6) 0.5776(6) 0.4845(5) 0.0337(10) Uani 1 1 d U
C5 C 0.1923(8) 0.6315(9) 0.6206(8) 0.0341(8) Uani 1 1 d U
H5A H 0.2014 0.6863 0.6441 0.041 Uiso 1 1 calc R
N6 N 0.3736(6) 0.7271(7) 1.1466(6) 0.0285(8) Uani 1 1 d U
O6 O 0.1698(6) 0.4647(6) 0.8358(5) 0.0353(10) Uani 1 1 d U
C6 C 0.2325(8) 0.5823(8) 0.6516(8) 0.0331(8) Uani 1 1 d U
N7 N 0.1517(6) 0.7831(6) 1.0183(5) 0.0233(7) Uani 1 1 d U
O7 O 0.0911(6) 0.5385(6) 0.8679(5) 0.0365(10) Uani 1 1 d U
C7 C 0.0963(9) 0.6567(8) 0.5242(8) 0.0357(10) Uani 1 1 d U
H7A H 0.0646 0.6281 0.4785 0.054 Uiso 1 1 calc R
H7B H 0.1393 0.7085 0.5228 0.054 Uiso 1 1 calc R
H7C H 0.0586 0.6692 0.5522 0.054 Uiso 1 1 calc R
N8 N 0.2300(6) 1.0194(6) 1.3013(6) 0.0260(7) Uani 1 1 d U
O8 O 0.3753(6) 0.5028(6) 0.7964(5) 0.0345(10) Uani 1 1 d U
C8 C 0.1458(8) 0.3803(8) 0.5155(8) 0.0339(8) Uani 1 1 d U
H8A H 0.0986 0.3646 0.4767 0.041 Uiso 1 1 calc R
H8B H 0.1287 0.3435 0.5464 0.041 Uiso 1 1 calc R
O9 O 0.4713(6) 0.6223(6) 0.8573(5) 0.0359(10) Uani 1 1 d U
C9 C 0.1944(9) 0.2783(8) 0.4482(8) 0.0340(9) Uani 1 1 d U
H9A H 0.1384 0.2642 0.4199 0.041 Uiso 1 1 calc R
H9B H 0.2335 0.2754 0.4179 0.041 Uiso 1 1 calc R
O10 O 0.2806(5) 0.3248(5) 0.6867(5) 0.0277(8) Uani 1 1 d U
C11 C 0.2613(8) 0.4345(8) 0.4537(7) 0.0333(9) Uani 1 1 d U
H10A H 0.2834 0.4098 0.4169 0.040 Uiso 1 1 calc R
H10B H 0.2175 0.4536 0.4330 0.040 Uiso 1 1 calc R
O12 O 0.3840(5) 0.3266(5) 0.5044(5) 0.0260(9) Uani 1 1 d U
C10 C 0.1914(9) 0.2151(9) 0.4897(8) 0.0345(9) Uani 1 1 d U
O11 O 0.4256(5) 0.2250(5) 0.4512(5) 0.0266(9) Uani 1 1 d U
C12 C 0.3319(9) 0.5097(9) 0.4994(8) 0.0330(9) Uani 1 1 d U
O13 O 0.4529(5) 0.4674(5) 0.6708(5) 0.0276(10) Uani 1 1 d U
C13 C 0.2915(9) 0.6220(8) 0.7228(7) 0.0329(8) Uani 1 1 d U
H13A H 0.3414 0.6688 0.7319 0.039 Uiso 1 1 calc R
O14 O 0.5846(5) 0.4928(5) 0.7240(5) 0.0291(10) Uani 1 1 d U
C14 C 0.1767(9) 0.5873(8) 0.7898(8) 0.0351(8) Uani 1 1 d U
H14A H 0.1876 0.6450 0.8140 0.042 Uiso 1 1 calc R
H14B H 0.1357 0.5749 0.7474 0.042 Uiso 1 1 calc R
O16 O 0.2781(6) 0.3573(6) 0.8325(5) 0.0355(10) Uani 1 1 d U
C16 C 0.3253(8) 0.6149(9) 0.8385(8) 0.0350(8) Uani 1 1 d U
H15A H 0.3017 0.5996 0.8774 0.042 Uiso 1 1 calc R
H15B H 0.3472 0.6762 0.8462 0.042 Uiso 1 1 calc R
O15 O 0.2594(6) 0.2610(6) 0.8928(5) 0.0376(10) Uani 1 1 d U
C15 C 0.1423(9) 0.5269(8) 0.8331(8) 0.0356(9) Uani 1 1 d U
O17 O 0.1037(6) 0.4018(5) 0.6872(5) 0.0332(10) Uani 1 1 d U
C17 C 0.3973(9) 0.5780(9) 0.8288(8) 0.0350(9) Uani 1 1 d U
O18 O -0.0376(6) 0.3540(6) 0.6695(5) 0.0345(10) Uani 1 1 d U
C18 C 0.2725(8) 0.2434(8) 0.6939(7) 0.0282(7) Uani 1 1 d U
O19 O 0.3777(5) 0.9094(5) 1.1679(4) 0.0243(8) Uani 1 1 d U
C19 C 0.3403(8) 0.2131(8) 0.6967(7) 0.0278(7) Uani 1 1 d U
O20 O 0.4860(5) 1.0565(5) 1.2791(5) 0.0262(10) Uani 1 1 d U
C20 C 0.3300(8) 0.1325(8) 0.7049(7) 0.0283(8) Uani 1 1 d U
H20A H 0.3749 0.1123 0.7039 0.034 Uiso 1 1 calc R
O21 O 0.6222(5) 1.1303(5) 1.2867(5) 0.0266(10) Uani 1 1 d U
C21 C 0.2545(8) 0.0821(8) 0.7143(7) 0.0291(8) Uani 1 1 d U
O22 O 0.2650(5) 1.0600(5) 1.1534(4) 0.0247(9) Uani 1 1 d U
C22 C 0.1878(8) 0.1102(8) 0.7099(7) 0.0293(8) Uani 1 1 d U
H22A H 0.1355 0.0740 0.7138 0.035 Uiso 1 1 calc R
O23 O 0.2553(5) 1.1645(5) 1.1037(5) 0.0257(9) Uani 1 1 d U
C23 C 0.1937(8) 0.1908(8) 0.6998(7) 0.0293(7) Uani 1 1 d U
O24 O 0.2256(5) 0.6535(6) 1.0571(5) 0.0299(10) Uani 1 1 d U
C24 C 0.2429(8) -0.0065(8) 0.7219(7) 0.0295(9) Uani 1 1 d U
H24A H 0.2957 -0.0164 0.7219 0.044 Uiso 1 1 calc R
H24B H 0.2001 -0.0462 0.6843 0.044 Uiso 1 1 calc R
H24C H 0.2256 -0.0137 0.7643 0.044 Uiso 1 1 calc R
O25 O 0.2719(5) 0.5640(6) 0.9958(5) 0.0317(10) Uani 1 1 d U
C25 C 0.4267(8) 0.2715(8) 0.6924(7) 0.0270(7) Uani 1 1 d U
H25A H 0.4454 0.3203 0.7307 0.032 Uiso 1 1 calc R
H25B H 0.4669 0.2420 0.6972 0.032 Uiso 1 1 calc R
O26 O 0.2688(5) 0.7627(6) 1.2304(5) 0.0317(10) Uani 1 1 d U
C26 C 0.4140(8) 0.2290(8) 0.5658(7) 0.0264(8) Uani 1 1 d U
H26A H 0.4605 0.2072 0.5704 0.032 Uiso 1 1 calc R
H26B H 0.3616 0.1833 0.5637 0.032 Uiso 1 1 calc R
O27 O 0.3276(5) 0.7101(6) 1.3123(5) 0.0349(10) Uani 1 1 d U
C28 C 0.5156(8) 0.3668(8) 0.6379(7) 0.0273(8) Uani 1 1 d U
H27A H 0.5578 0.3474 0.6609 0.033 Uiso 1 1 calc R
H27B H 0.5286 0.3745 0.5938 0.033 Uiso 1 1 calc R
O28 O 0.2211(5) 0.8967(5) 1.1701(4) 0.0235(8) Uani 1 1 d U
C27 C 0.4084(8) 0.2619(8) 0.5011(7) 0.0263(9) Uani 1 1 d U
O29 O 0.3190(5) 0.8169(5) 1.0314(4) 0.0229(10) Uani 1 1 d U
C29 C 0.5192(8) 0.4489(8) 0.6799(7) 0.0279(9) Uani 1 1 d U
O30 O 0.3176(5) 0.8000(5) 0.9213(4) 0.0233(9) Uani 1 1 d U
C30 C 0.1176(8) 0.2189(8) 0.6926(7) 0.0305(7) Uani 1 1 d U
H30A H 0.1151 0.2429 0.6525 0.037 Uiso 1 1 calc R
H30B H 0.0664 0.1696 0.6848 0.037 Uiso 1 1 calc R
O31 O 0.1214(5) 0.7192(5) 1.1309(4) 0.0229(9) Uani 1 1 d U
C31 C 0.1376(8) 0.2570(8) 0.8159(7) 0.0339(8) Uani 1 1 d U
H31A H 0.1182 0.1956 0.8065 0.041 Uiso 1 1 calc R
H31B H 0.1059 0.2757 0.8478 0.041 Uiso 1 1 calc R
O32 O -0.0176(5) 0.6639(5) 1.0909(4) 0.0245(10) Uani 1 1 d U
C33 C 0.0372(8) 0.2947(8) 0.7440(7) 0.0330(8) Uani 1 1 d U
H32A H 0.0283 0.3192 0.7880 0.040 Uiso 1 1 calc R
H32B H -0.0082 0.2405 0.7254 0.040 Uiso 1 1 calc R
O33 O 0.3632(5) 1.1474(5) 1.2904(4) 0.0263(9) Uani 1 1 d U
C32 C 0.2338(9) 0.2926(9) 0.8510(8) 0.0356(9) Uani 1 1 d U
O34 O 0.3036(5) 1.2444(5) 1.3098(5) 0.0266(9) Uani 1 1 d U
C34 C 0.0349(9) 0.3539(8) 0.6949(8) 0.0334(9) Uani 1 1 d U
O35 O 0.3491(5) 0.9497(5) 1.3209(5) 0.0279(9) Uani 1 1 d U
C35 C 0.4500(7) 0.9190(8) 1.1441(7) 0.0247(7) Uani 1 1 d U
O36 O 0.3478(5) 0.9595(5) 1.4325(5) 0.0293(10) Uani 1 1 d U
C36 C 0.4830(7) 0.9869(8) 1.1129(7) 0.0247(7) Uani 1 1 d U
C37 C 0.5575(7) 0.9977(8) 1.0891(7) 0.0250(7) Uani 1 1 d U
H37A H 0.5770 1.0403 1.0660 0.030 Uiso 1 1 calc R
C38 C 0.6031(7) 0.9442(8) 1.0998(7) 0.0253(8) Uani 1 1 d U
C39 C 0.5702(7) 0.8758(8) 1.1286(7) 0.0252(7) Uani 1 1 d U
H39A H 0.6004 0.8395 1.1342 0.030 Uiso 1 1 calc R
C40 C 0.4918(7) 0.8603(8) 1.1493(7) 0.0253(7) Uani 1 1 d U
C41 C 0.6891(7) 0.9562(8) 1.0773(7) 0.0256(9) Uani 1 1 d U
H41A H 0.7046 1.0058 1.0587 0.038 Uiso 1 1 calc R
H41B H 0.6836 0.9074 1.0430 0.038 Uiso 1 1 calc R
H41C H 0.7323 0.9629 1.1163 0.038 Uiso 1 1 calc R
C42 C 0.4349(7) 1.0457(8) 1.0996(7) 0.0247(7) Uani 1 1 d U
H42A H 0.4608 1.0797 1.0693 0.030 Uiso 1 1 calc R
H42B H 0.3768 1.0120 1.0762 0.030 Uiso 1 1 calc R
C43 C 0.5217(7) 1.1497(8) 1.2042(7) 0.0252(8) Uani 1 1 d U
H43A H 0.5261 1.2071 1.2243 0.030 Uiso 1 1 calc R
H43B H 0.5616 1.1531 1.1739 0.030 Uiso 1 1 calc R
C44 C 0.3927(7) 1.1621(8) 1.1428(7) 0.0249(8) Uani 1 1 d U
H44A H 0.4091 1.1772 1.1013 0.030 Uiso 1 1 calc R
H44B H 0.4129 1.2135 1.1788 0.030 Uiso 1 1 calc R
C45 C 0.5472(7) 1.1094(8) 1.2612(7) 0.0259(9) Uani 1 1 d U
C46 C 0.2973(7) 1.1249(8) 1.1306(7) 0.0250(8) Uani 1 1 d U
C47 C 0.4583(7) 0.7898(8) 1.1826(7) 0.0264(7) Uani 1 1 d U
H47A H 0.4547 0.8134 1.2287 0.032 Uiso 1 1 calc R
H47B H 0.4988 0.7604 1.1865 0.032 Uiso 1 1 calc R
C48 C 0.3737(8) 0.6754(8) 1.0811(7) 0.0291(8) Uani 1 1 d U
H48A H 0.4035 0.6368 1.0894 0.035 Uiso 1 1 calc R
H48B H 0.4037 0.7118 1.0540 0.035 Uiso 1 1 calc R
C49 C 0.3472(8) 0.6713(8) 1.1933(7) 0.0310(8) Uani 1 1 d U
H49A H 0.3955 0.6596 1.2155 0.037 Uiso 1 1 calc R
H49B H 0.3040 0.6180 1.1680 0.037 Uiso 1 1 calc R
C50 C 0.2852(8) 0.6258(8) 1.0420(7) 0.0302(9) Uani 1 1 d U
C51 C 0.3106(8) 0.7181(9) 1.2481(8) 0.0326(9) Uani 1 1 d U
C52 C 0.1429(7) 0.9050(8) 1.1547(7) 0.0238(7) Uani 1 1 d U
C53 C 0.1031(7) 0.8914(8) 1.0852(7) 0.0240(7) Uani 1 1 d U
C54 C 0.0248(7) 0.9010(7) 1.0715(7) 0.0245(7) Uani 1 1 d U
H54A H -0.0032 0.8896 1.0261 0.029 Uiso 1 1 calc R
C55 C -0.0135(7) 0.9270(8) 1.1226(7) 0.0249(8) Uani 1 1 d U
C56 C 0.0279(7) 0.9399(7) 1.1906(7) 0.0246(8) Uani 1 1 d U
H56A H 0.0019 0.9559 1.2255 0.030 Uiso 1 1 calc R
C57 C 0.1052(7) 0.9302(8) 1.2085(7) 0.0243(7) Uani 1 1 d U
C58 C -0.0979(7) 0.9398(8) 1.1056(7) 0.0253(9) Uani 1 1 d U
H58A H -0.1143 0.9586 1.1473 0.038 Uiso 1 1 calc R
H58B H -0.1405 0.8873 1.0800 0.038 Uiso 1 1 calc R
H58C H -0.0925 0.9818 1.0787 0.038 Uiso 1 1 calc R
C59 C 0.1453(7) 0.8695(7) 1.0275(7) 0.0237(7) Uani 1 1 d U
H59A H 0.1136 0.8735 0.9852 0.028 Uiso 1 1 calc R
H59B H 0.2022 0.9110 1.0360 0.028 Uiso 1 1 calc R
C60 C 0.1859(7) 0.7654(8) 0.9571(7) 0.0232(8) Uani 1 1 d U
H60A H 0.1641 0.7906 0.9225 0.028 Uiso 1 1 calc R
H60B H 0.1655 0.7046 0.9390 0.028 Uiso 1 1 calc R
C61 C 0.0692(7) 0.7190(8) 1.0162(7) 0.0235(8) Uani 1 1 d U
H61A H 0.0640 0.6665 0.9856 0.028 Uiso 1 1 calc R
H61B H 0.0242 0.7378 0.9973 0.028 Uiso 1 1 calc R
C62 C 0.2807(7) 0.7982(8) 0.9701(7) 0.0230(8) Uani 1 1 d U
C63 C 0.0564(7) 0.7016(8) 1.0863(7) 0.0236(8) Uani 1 1 d U
C64 C 0.1512(7) 0.9459(8) 1.2803(7) 0.0250(7) Uani 1 1 d U
H64A H 0.1134 0.9535 1.3107 0.030 Uiso 1 1 calc R
H64B H 0.1645 0.8960 1.2863 0.030 Uiso 1 1 calc R
C65 C 0.2182(7) 1.1008(7) 1.2970(7) 0.0259(8) Uani 1 1 d U
H65A H 0.1938 1.1182 1.3350 0.031 Uiso 1 1 calc R
H65B H 0.1783 1.0927 1.2548 0.031 Uiso 1 1 calc R
C66 C 0.2706(8) 1.0282(8) 1.3720(7) 0.0276(8) Uani 1 1 d U
H66A H 0.2276 1.0109 1.3988 0.033 Uiso 1 1 calc R
H66B H 0.3054 1.0870 1.3922 0.033 Uiso 1 1 calc R
C67 C 0.2994(8) 1.1695(8) 1.2987(7) 0.0263(9) Uani 1 1 d U
C68 C 0.3246(8) 0.9741(8) 1.3731(7) 0.0282(9) Uani 1 1 d U
Na1 Na -0.1372(3) 0.5458(3) 1.0526(3) 0.0372(14) Uani 1 1 d .
Na2 Na 0.4644(3) 0.2799(3) 0.3558(3) 0.0314(13) Uani 1 1 d .
Na3 Na 0.6484(4) 0.6264(4) 0.7121(4) 0.0583(18) Uani 1 1 d U
Na4 Na 0.5000 1.0000 1.5000 0.113(5) Uani 1 2 d S
Na5 Na 0.4741(6) 0.7746(6) 0.9682(5) 0.098(3) Uani 1 1 d U
Na6 Na 0.2510(5) 0.8127(6) 0.7937(5) 0.091(3) Uani 1 1 d .
Na7 Na 0.1021(7) 0.5924(7) 1.2028(6) 0.042(3) Uani 0.50 1 d PU
Na8 Na 0.1886(8) 0.7841(8) 1.3428(7) 0.053(3) Uani 0.50 1 d PU
Na9 Na 0.0931(8) 1.1184(8) 1.1180(9) 0.065(4) Uani 0.50 1 d P
Na10 Na 0.5306(8) 0.5563(12) 0.9466(7) 0.080(3) Uani 0.50 1 d PU
Na11 Na 0.5479(15) 0.5120(15) 0.8413(8) 0.104(5) Uani 0.50 1 d PU
O1W O -0.1790(9) 0.6479(9) 0.9967(7) 0.082(4) Uani 1 1 d .
O2W O -0.0813(6) 0.4901(6) 0.9637(5) 0.039(3) Uani 1 1 d .
O3W O 0.4488(5) 0.4110(5) 0.4062(5) 0.027(2) Uani 1 1 d .
O4W O 0.4902(5) 0.3606(5) 0.2721(4) 0.028(2) Uani 1 1 d .
O5W O 0.6002(6) 0.2912(7) 0.4031(6) 0.046(3) Uani 1 1 d .
O6W O 0.3764(7) 0.9125(9) 1.5150(8) 0.101(6) Uani 1 1 d .
O7W O 0.5240(13) 0.9440(14) 1.3721(10) 0.152(9) Uani 1 1 d .
O8W O 0.5528(11) 0.6753(8) 1.033(2) 0.43(3) Uani 1 1 d .
O9W O 0.0819(9) 0.7707(12) 0.7656(10) 0.122(7) Uani 1 1 d .
O10W O 0.3917(11) 0.4986(11) 0.9618(9) 0.121(6) Uani 1 1 d .
O11W O 0.5256(10) 1.1330(10) 1.4718(10) 0.115(6) Uani 1 1 d .
O12W O 0.7118(10) 0.6699(9) 0.8275(8) 0.097(5) Uani 1 1 d .
O13W O 0.8345(17) 0.6558(19) 0.753(3) 0.59(5) Uani 1 1 d .
O14W O 0.7465(14) 0.5214(18) 0.728(2) 0.35(3) Uani 1 1 d .
O15W O 0.661(2) 0.5602(16) 0.9107(19) 0.43(3) Uani 1 1 d .
O16W O 0.5191(13) 0.585(2) 1.1500(10) 0.234(17) Uani 1 1 d .
O17W O 0.1957(9) 0.0723(11) 0.5564(8) 0.102(5) Uani 1 1 d .
O18W O 0.3075(12) 1.0053(12) 1.5535(9) 0.144(8) Uani 1 1 d .
O19W O 0.3342(18) 0.8556(12) 1.5871(9) 0.185(11) Uani 1 1 d .
O20W O 0.0175(19) 0.4891(13) 0.3598(13) 0.265(18) Uani 1 1 d .
O21W O 0.0038(15) 0.3596(15) 1.1804(13) 0.063(7) Uiso 0.50 1 d PU
O22W O 0.1597(14) 0.6118(14) 1.3203(12) 0.057(6) Uiso 0.50 1 d P
O23W O 0.3875(10) 0.8402(10) 1.3983(9) 0.107(5) Uiso 1 1 d .
O24W O 0.0279(17) 0.4490(17) 1.1483(14) 0.212(11) Uiso 1 1 d U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Yb1 O2 106.7(3) . .
O1 Yb1 O10 69.4(3) . .
O2 Yb1 O10 73.6(3) . .
O1 Yb1 O4 79.4(3) . .
O2 Yb1 O4 134.0(3) . .
O10 Yb1 O4 144.3(3) . .
O1 Yb1 O13 88.8(3) . .
O2 Yb1 O13 150.2(3) . .
O10 Yb1 O13 89.0(3) . .
O4 Yb1 O13 73.0(3) . .
O1 Yb1 O12 153.1(3) . .
O2 Yb1 O12 77.7(3) . .
O10 Yb1 O12 135.5(3) . .
O4 Yb1 O12 79.1(3) . .
O13 Yb1 O12 100.0(3) . .
O1 Yb1 N3 140.1(3) . .
O2 Yb1 N3 85.0(3) . .
O10 Yb1 N3 78.1(3) . .
O4 Yb1 N3 119.9(3) . .
O13 Yb1 N3 67.5(3) . .
O12 Yb1 N3 66.0(3) . .
O1 Yb1 N1 80.8(4) . .
O2 Yb1 N1 67.1(3) . .
O10 Yb1 N1 120.3(3) . .
O4 Yb1 N1 69.2(3) . .
O13 Yb1 N1 142.0(3) . .
O12 Yb1 N1 76.6(3) . .
N3 Yb1 N1 137.3(4) . .
O1 Yb1 C10 107.5(3) . .
O2 Yb1 C10 18.9(4) . .
O10 Yb1 C10 91.2(3) . .
O4 Yb1 C10 115.1(4) . .
O13 Yb1 C10 162.5(3) . .
O12 Yb1 C10 68.0(3) . .
N3 Yb1 C10 95.5(4) . .
N1 Yb1 C10 50.1(4) . .
O1 Yb1 C29 107.7(3) . .
O2 Yb1 C29 134.0(3) . .
O10 Yb1 C29 90.8(3) . .
O4 Yb1 C29 82.2(3) . .
O13 Yb1 C29 19.5(3) . .
O12 Yb1 C29 85.2(3) . .
N3 Yb1 C29 49.1(3) . .
N1 Yb1 C29 148.4(3) . .
C10 Yb1 C29 143.0(3) . .
O1 Yb1 Yb2 35.6(2) . .
O2 Yb1 Yb2 95.7(2) . .
O10 Yb1 Yb2 34.9(2) . .
O4 Yb1 Yb2 110.5(2) . .
O13 Yb1 Yb2 82.1(2) . .
O12 Yb1 Yb2 170.3(2) . .
N3 Yb1 Yb2 106.7(3) . .
N1 Yb1 Yb2 107.6(3) . .
C10 Yb1 Yb2 107.6(3) . .
C29 Yb1 Yb2 94.7(2) . .
O10 Yb2 O17 106.1(3) . .
O10 Yb2 O16 79.3(3) . .
O17 Yb2 O16 133.0(3) . .
O10 Yb2 O1 69.5(3) . .
O17 Yb2 O1 73.9(3) . .
O16 Yb2 O1 144.5(3) . .
O10 Yb2 O8 88.9(3) . .
O17 Yb2 O8 150.3(3) . .
O16 Yb2 O8 74.1(3) . .
O1 Yb2 O8 88.4(3) . .
O10 Yb2 O6 154.1(3) . .
O17 Yb2 O6 78.7(3) . .
O16 Yb2 O6 79.2(3) . .
O1 Yb2 O6 134.9(3) . .
O8 Yb2 O6 99.0(3) . .
O10 Yb2 N2 139.3(3) . .
O17 Yb2 N2 86.5(3) . .
O16 Yb2 N2 120.2(4) . .
O1 Yb2 N2 77.6(3) . .
O8 Yb2 N2 66.3(3) . .
O6 Yb2 N2 65.4(3) . .
O10 Yb2 N4 81.6(3) . .
O17 Yb2 N4 66.9(3) . .
O16 Yb2 N4 67.9(3) . .
O1 Yb2 N4 121.6(4) . .
O8 Yb2 N4 141.9(4) . .
O6 Yb2 N4 76.9(3) . .
N2 Yb2 N4 137.6(3) . .
O10 Yb2 C34 105.9(3) . .
O17 Yb2 C34 18.8(3) . .
O16 Yb2 C34 114.2(3) . .
O1 Yb2 C34 91.0(3) . .
O8 Yb2 C34 163.8(3) . .
O6 Yb2 C34 70.4(3) . .
N2 Yb2 C34 97.8(4) . .
N4 Yb2 C34 49.3(4) . .
O10 Yb2 C17 107.5(3) . .
O17 Yb2 C17 134.8(3) . .
O16 Yb2 C17 82.7(4) . .
O1 Yb2 C17 90.5(3) . .
O8 Yb2 C17 19.1(3) . .
O6 Yb2 C17 84.0(3) . .
N2 Yb2 C17 48.5(4) . .
N4 Yb2 C17 147.4(4) . .
C34 Yb2 C17 144.8(4) . .
O10 Yb2 C15 171.1(3) . .
O17 Yb2 C15 68.7(4) . .
O16 Yb2 C15 98.9(4) . .
O1 Yb2 C15 114.5(3) . .
O8 Yb2 C15 99.0(3) . .
O6 Yb2 C15 20.5(3) . .
N2 Yb2 C15 49.0(3) . .
N4 Yb2 C15 89.6(3) . .
C34 Yb2 C15 66.7(4) . .
C17 Yb2 C15 80.8(4) . .
O10 Yb2 Yb1 35.6(2) . .
O17 Yb2 Yb1 95.6(2) . .
O16 Yb2 Yb1 110.6(2) . .
O1 Yb2 Yb1 35.0(2) . .
O8 Yb2 Yb1 81.7(2) . .
O6 Yb2 Yb1 169.9(2) . .
N2 Yb2 Yb1 106.1(3) . .
N4 Yb2 Yb1 108.8(3) . .
C34 Yb2 Yb1 106.6(3) . .
C17 Yb2 Yb1 94.4(3) . .
C15 Yb2 Yb1 149.4(3) . .
O28 Yb3 O26 84.6(3) . .
O28 Yb3 O31 79.0(3) . .
O26 Yb3 O31 75.0(3) . .
O28 Yb3 O29 111.1(3) . .
O26 Yb3 O29 149.7(3) . .
O31 Yb3 O29 132.1(3) . .
O28 Yb3 O19 69.8(3) . .
O26 Yb3 O19 87.5(3) . .
O31 Yb3 O19 145.5(3) . .
O29 Yb3 O19 74.9(3) . .
O28 Yb3 O24 152.0(3) . .
O26 Yb3 O24 100.3(3) . .
O31 Yb3 O24 75.8(3) . .
O29 Yb3 O24 78.2(3) . .
O19 Yb3 O24 137.6(3) . .
O28 Yb3 N6 139.3(3) . .
O26 Yb3 N6 69.7(3) . .
O31 Yb3 N6 121.2(3) . .
O29 Yb3 N6 82.4(3) . .
O19 Yb3 N6 77.9(3) . .
O24 Yb3 N6 66.5(3) . .
O28 Yb3 N7 83.1(3) . .
O26 Yb3 N7 143.1(3) . .
O31 Yb3 N7 68.5(3) . .
O29 Yb3 N7 66.6(3) . .
O19 Yb3 N7 120.0(3) . .
O24 Yb3 N7 76.5(3) . .
N6 Yb3 N7 135.8(3) . .
O28 Yb3 C51 103.6(3) . .
O26 Yb3 C51 20.2(3) . .
O31 Yb3 C51 85.3(3) . .
O29 Yb3 C51 132.2(3) . .
O19 Yb3 C51 88.0(3) . .
O24 Yb3 C51 86.4(4) . .
N6 Yb3 C51 50.1(3) . .
N7 Yb3 C51 151.4(3) . .
O28 Yb3 C63 80.0(3) . .
O26 Yb3 C63 93.2(3) . .
O31 Yb3 C63 18.2(3) . .
O29 Yb3 C63 114.5(3) . .
O19 Yb3 C63 149.6(3) . .
O24 Yb3 C63 72.2(3) . .
N6 Yb3 C63 130.7(3) . .
N7 Yb3 C63 50.4(3) . .
C51 Yb3 C63 102.8(3) . .
O28 Yb3 C50 171.8(3) . .
O26 Yb3 C50 99.5(4) . .
O31 Yb3 C50 95.1(3) . .
O29 Yb3 C50 68.7(3) . .
O19 Yb3 C50 117.3(3) . .
O24 Yb3 C50 20.4(3) . .
N6 Yb3 C50 48.8(3) . .
N7 Yb3 C50 89.4(3) . .
C51 Yb3 C50 81.4(4) . .
C63 Yb3 C50 92.6(3) . .
O28 Yb3 C62 110.3(3) . .
O26 Yb3 C62 163.6(3) . .
O31 Yb3 C62 113.7(3) . .
O29 Yb3 C62 18.4(3) . .
O19 Yb3 C62 91.2(3) . .
O24 Yb3 C62 70.0(3) . .
N6 Yb3 C62 94.1(3) . .
N7 Yb3 C62 49.4(3) . .
C51 Yb3 C62 143.5(3) . .
C63 Yb3 C62 96.1(3) . .
C50 Yb3 C62 66.7(3) . .
O19 Yb4 O35 89.6(3) . .
O19 Yb4 O22 107.9(3) . .
O35 Yb4 O22 149.1(3) . .
O19 Yb4 O28 69.3(3) . .
O35 Yb4 O28 90.9(3) . .
O22 Yb4 O28 72.8(3) . .
O19 Yb4 O20 80.4(3) . .
O35 Yb4 O20 74.6(3) . .
O22 Yb4 O20 132.2(3) . .
O28 Yb4 O20 146.6(3) . .
O19 Yb4 O33 155.6(3) . .
O35 Yb4 O33 97.4(3) . .
O22 Yb4 O33 77.3(3) . .
O28 Yb4 O33 133.5(3) . .
O20 Yb4 O33 79.0(3) . .
O19 Yb4 N5 82.4(3) . .
O35 Yb4 N5 142.5(3) . .
O22 Yb4 N5 66.9(3) . .
O28 Yb4 N5 119.6(3) . .
O20 Yb4 N5 67.9(3) . .
O33 Yb4 N5 77.8(3) . .
O19 Yb4 N8 137.8(3) . .
O35 Yb4 N8 66.2(3) . .
O22 Yb4 N8 84.3(3) . .
O28 Yb4 N8 76.7(3) . .
O20 Yb4 N8 121.4(3) . .
O33 Yb4 N8 65.5(3) . .
N5 Yb4 N8 137.6(3) . .
O19 Yb4 C68 109.4(3) . .
O35 Yb4 C68 20.0(3) . .
O22 Yb4 C68 133.1(3) . .
O28 Yb4 C68 95.0(3) . .
O20 Yb4 C68 81.6(3) . .
O33 Yb4 C68 80.4(3) . .
N5 Yb4 C68 145.3(3) . .
N8 Yb4 C68 48.9(3) . .
O19 Yb4 C67 171.3(3) . .
O35 Yb4 C67 98.6(3) . .
O22 Yb4 C67 66.1(3) . .
O28 Yb4 C67 113.2(3) . .
O20 Yb4 C67 98.9(3) . .
O33 Yb4 C67 20.4(3) . .
N5 Yb4 C67 89.3(3) . .
N8 Yb4 C67 49.7(3) . .
C68 Yb4 C67 79.0(3) . .
O19 Yb4 C46 108.6(3) . .
O35 Yb4 C46 160.9(3) . .
O22 Yb4 C46 19.2(3) . .
O28 Yb4 C46 90.5(3) . .
O20 Yb4 C46 113.0(3) . .
O33 Yb4 C46 68.3(3) . .
N5 Yb4 C46 49.4(3) . .
N8 Yb4 C46 95.7(3) . .
C68 Yb4 C46 141.1(3) . .
C67 Yb4 C46 63.6(3) . .
O19 Yb4 Yb3 35.8(2) . .
O35 Yb4 Yb3 85.4(2) . .
O22 Yb4 Yb3 94.2(2) . .
O28 Yb4 Yb3 34.15(19) . .
O20 Yb4 Yb3 113.3(2) . .
O33 Yb4 Yb3 167.6(2) . .
N5 Yb4 Yb3 107.2(2) . .
N8 Yb4 Yb3 105.1(2) . .
C68 Yb4 Yb3 99.7(2) . .
C67 Yb4 Yb3 147.3(2) . .
C46 Yb4 Yb3 106.0(2) . .
C9 N1 C11 114.4(11) . .
C9 N1 C8 108.4(10) . .
C11 N1 C8 111.1(10) . .
C9 N1 Yb1 106.1(8) . .
C11 N1 Yb1 110.0(8) . .
C8 N1 Yb1 106.5(8) . .
C1 O1 Yb1 126.0(9) . .
C1 O1 Yb2 123.6(8) . .
Yb1 O1 Yb2 109.4(4) . .
O1 C1 C2 122.6(13) . .
O1 C1 C6 118.0(13) . .
C2 C1 C6 119.3(13) . .
C13 N2 C16 107.0(10) . .
C13 N2 C14 113.3(11) . .
C16 N2 C14 107.5(11) . .
C13 N2 Yb2 115.7(8) . .
C16 N2 Yb2 106.2(8) . .
C14 N2 Yb2 106.6(7) . .
C10 O2 Yb1 124.6(9) . .
C3 C2 C1 120.2(13) . .
C3 C2 C8 120.8(14) . .
C1 C2 C8 119.0(13) . .
C28 N3 C25 105.8(10) . .
C28 N3 C26 110.7(10) . .
C25 N3 C26 111.3(9) . .
C28 N3 Yb1 105.1(7) . .
C25 N3 Yb1 117.3(7) . .
C26 N3 Yb1 106.4(7) . .
C4 C3 C2 124.1(15) . .
C31 N4 C33 112.0(11) . .
C31 N4 C30 111.4(11) . .
C33 N4 C30 108.4(11) . .
C31 N4 Yb2 111.3(8) . .
C33 N4 Yb2 108.9(8) . .
C30 N4 Yb2 104.5(8) . .
C12 O4 Yb1 124.0(8) . .
C3 C4 C5 116.1(13) . .
C3 C4 C7 124.9(14) . .
C5 C4 C7 119.0(12) . .
C44 N5 C42 108.4(10) . .
C44 N5 C43 110.8(10) . .
C42 N5 C43 110.7(9) . .
C44 N5 Yb4 108.9(7) . .
C42 N5 Yb4 106.8(7) . .
C43 N5 Yb4 111.1(8) . .
C6 C5 C4 121.8(13) . .
C48 N6 C49 108.8(10) . .
C48 N6 C47 114.2(10) . .
C49 N6 C47 105.8(10) . .
C48 N6 Yb3 106.6(8) . .
C49 N6 Yb3 106.2(7) . .
C47 N6 Yb3 114.9(8) . .
C15 O6 Yb2 119.9(9) . .
C15 O6 Na1 92.9(8) . 2_567
Yb2 O6 Na1 146.9(5) . 2_567
C1 C6 C5 118.3(14) . .
C1 C6 C13 123.0(13) . .
C5 C6 C13 118.6(12) . .
C60 N7 C61 112.8(9) . .
C60 N7 C59 109.6(10) . .
C61 N7 C59 110.7(9) . .
C60 N7 Yb3 108.7(7) . .
C61 N7 Yb3 109.2(8) . .
C59 N7 Yb3 105.6(7) . .
C15 O7 Na1 89.3(9) . 2_567
C66 N8 C64 110.6(10) . .
C66 N8 C65 107.0(10) . .
C64 N8 C65 114.1(10) . .
C66 N8 Yb4 106.1(7) . .
C64 N8 Yb4 113.7(7) . .
C65 N8 Yb4 104.8(7) . .
C17 O8 Yb2 123.2(9) . .
C17 O8 Na11 87.6(9) . .
Yb2 O8 Na11 148.1(6) . .
C2 C8 N1 112.1(11) . .
C17 O9 Na10 111.1(10) . .
C17 O9 Na11 101.2(10) . .
Na10 O9 Na11 51.4(5) . .
C10 C9 N1 113.5(12) . .
C18 O10 Yb2 127.6(8) . .
C18 O10 Yb1 122.2(8) . .
Yb2 O10 Yb1 109.5(3) . .
C12 C11 N1 113.7(12) . .
C27 O12 Yb1 123.0(8) . .
O2 C10 O3 123.2(14) . .
O2 C10 C9 117.1(13) . .
O3 C10 C9 119.2(13) . .
O2 C10 Yb1 36.6(6) . .
O3 C10 Yb1 154.9(10) . .
C9 C10 Yb1 81.2(8) . .
C27 O11 Na2 126.6(8) . .
O5 C12 O4 122.4(13) . .
O5 C12 C11 120.4(14) . .
O4 C12 C11 117.1(12) . .
C29 O13 Yb1 122.1(8) . .
N2 C13 C6 111.7(11) . .
C29 O14 Na3 115.7(9) . .
C29 O14 Na11 109.7(10) . .
Na3 O14 Na11 104.6(7) . .
C15 C14 N2 108.3(11) . .
C32 O16 Yb2 127.3(9) . .
N2 C16 C17 106.0(11) . .
O7 C15 O6 120.6(13) . .
O7 C15 C14 120.3(13) . .
O6 C15 C14 119.1(12) . .
O7 C15 Na1 64.6(8) . 2_567
O6 C15 Na1 59.6(7) . 2_567
C14 C15 Na1 157.9(10) . 2_567
O7 C15 Yb2 156.1(10) . .
O6 C15 Yb2 39.6(6) . .
C14 C15 Yb2 81.6(7) . .
Na1 C15 Yb2 99.1(4) 2_567 .
C34 O17 Yb2 125.0(10) . .
O9 C17 O8 124.1(13) . .
O9 C17 C16 118.5(12) . .
O8 C17 C16 117.2(12) . .
O9 C17 Na11 55.7(8) . .
O8 C17 Na11 68.6(9) . .
C16 C17 Na11 168.5(11) . .
O9 C17 Yb2 161.6(10) . .
O8 C17 Yb2 37.7(6) . .
C16 C17 Yb2 79.6(7) . .
Na11 C17 Yb2 105.9(6) . .
C34 O18 Na8 122.5(9) . 2_567
C23 C18 O10 118.1(11) . .
C23 C18 C19 119.1(12) . .
O10 C18 C19 122.9(11) . .
C35 O19 Yb4 127.5(7) . .
C35 O19 Yb3 120.9(7) . .
Yb4 O19 Yb3 109.6(3) . .
C20 C19 C18 121.1(12) . .
C20 C19 C25 120.0(12) . .
C18 C19 C25 118.9(11) . .
C45 O20 Yb4 126.9(8) . .
C21 C20 C19 120.4(13) . .
C45 O21 Na6 119.9(9) . 2_677
C22 C21 C20 118.7(12) . .
C22 C21 C24 120.7(12) . .
C20 C21 C24 120.2(12) . .
C46 O22 Yb4 124.0(8) . .
C21 C22 C23 123.4(12) . .
C46 O23 Na9 114.2(8) . .
C18 C23 C22 117.1(12) . .
C18 C23 C30 120.8(12) . .
C22 C23 C30 122.0(12) . .
C50 O24 Yb3 120.9(8) . .
C50 O25 Na1 125.9(8) . 2_567
N3 C25 C19 114.7(11) . .
C51 O26 Yb3 121.0(9) . .
C51 O26 Na8 101.7(9) . .
Yb3 O26 Na8 136.6(5) . .
C27 C26 N3 108.7(10) . .
C29 C28 N3 110.2(10) . .
C52 O28 Yb3 126.3(7) . .
C52 O28 Yb4 122.0(7) . .
Yb3 O28 Yb4 110.1(3) . .
O11 C27 O12 126.3(13) . .
O11 C27 C26 118.1(11) . .
O12 C27 C26 115.6(11) . .
C62 O29 Yb3 126.2(7) . .
O14 C29 O13 123.7(12) . .
O14 C29 C28 119.5(12) . .
O13 C29 C28 116.7(12) . .
O14 C29 Na3 42.5(6) . .
O13 C29 Na3 98.2(8) . .
C28 C29 Na3 132.7(9) . .
O14 C29 Yb1 161.5(9) . .
O13 C29 Yb1 38.4(6) . .
C28 C29 Yb1 78.4(7) . .
Na3 C29 Yb1 130.0(5) . .
C62 O30 Na6 124.8(8) . .
C62 O30 Na5 105.8(8) . .
Na6 O30 Na5 129.2(4) . .
N4 C30 C23 114.0(11) . .
C63 O31 Yb3 126.7(8) . .
C63 O31 Na7 109.7(8) . .
Yb3 O31 Na7 115.2(4) . .
N4 C31 C32 114.2(11) . .
C63 O32 Na1 147.6(8) . .
N4 C33 C34 110.0(11) . .
C67 O33 Yb4 119.8(8) . .
C67 O33 Na2 93.7(7) . 1_566
Yb4 O33 Na2 146.5(4) . 1_566
O15 C32 O16 125.4(14) . .
O15 C32 C31 119.6(12) . .
O16 C32 C31 114.9(13) . .
C67 O34 Na3 149.6(9) . 2_677
C67 O34 Na2 85.5(7) . 1_566
Na3 O34 Na2 81.5(3) 2_677 1_566
O17 C34 O18 125.1(13) . .
O17 C34 C33 118.2(13) . .
O18 C34 C33 116.4(12) . .
O17 C34 Yb2 36.2(7) . .
O18 C34 Yb2 159.5(10) . .
C33 C34 Yb2 82.2(8) . .
C68 O35 Yb4 121.1(9) . .
O19 C35 C40 119.9(11) . .
O19 C35 C36 120.3(11) . .
C40 C35 C36 119.8(11) . .
C68 O36 Na4 126.9(8) . .
C37 C36 C35 120.6(12) . .
C37 C36 C42 118.0(12) . .
C35 C36 C42 121.3(10) . .
C36 C37 C38 119.6(12) . .
C39 C38 C37 120.2(11) . .
C39 C38 C41 118.1(11) . .
C37 C38 C41 121.6(12) . .
C38 C39 C40 121.1(12) . .
C35 C40 C39 118.2(12) . .
C35 C40 C47 120.2(11) . .
C39 C40 C47 121.3(11) . .
N5 C42 C36 113.5(11) . .
N5 C43 C45 114.0(10) . .
N5 C44 C46 112.0(10) . .
O21 C45 O20 125.7(13) . .
O21 C45 C43 118.3(11) . .
O20 C45 C43 116.0(11) . .
O23 C46 O22 124.3(11) . .
O23 C46 C44 117.6(11) . .
O22 C46 C44 117.8(11) . .
O23 C46 Yb4 157.0(9) . .
O22 C46 Yb4 36.8(6) . .
C44 C46 Yb4 81.7(7) . .
C40 C47 N6 115.1(11) . .
N6 C48 C50 111.2(10) . .
N6 C49 C51 107.5(11) . .
O25 C50 O24 122.6(12) . .
O25 C50 C48 120.1(11) . .
O24 C50 C48 117.2(12) . .
O25 C50 Yb3 157.7(10) . .
O24 C50 Yb3 38.7(6) . .
C48 C50 Yb3 79.3(7) . .
O26 C51 O27 122.9(13) . .
O26 C51 C49 119.4(13) . .
O27 C51 C49 117.7(12) . .
O26 C51 Yb3 38.9(7) . .
O27 C51 Yb3 160.6(10) . .
C49 C51 Yb3 80.7(8) . .
O28 C52 C57 119.2(12) . .
O28 C52 C53 119.6(11) . .
C57 C52 C53 121.1(11) . .
C54 C53 C52 118.1(12) . .
C54 C53 C59 120.5(12) . .
C52 C53 C59 121.4(11) . .
C55 C54 C53 122.6(13) . .
C54 C55 C56 117.6(12) . .
C54 C55 C58 121.1(12) . .
C56 C55 C58 121.3(11) . .
C57 C56 C55 123.3(12) . .
C56 C57 C52 117.3(12) . .
C56 C57 C64 124.1(12) . .
C52 C57 C64 118.7(11) . .
N7 C59 C53 114.3(10) . .
N7 C60 C62 113.7(10) . .
N7 C61 C63 113.7(10) . .
O30 C62 O29 123.3(11) . .
O30 C62 C60 120.2(12) . .
O29 C62 C60 116.3(11) . .
O30 C62 Yb3 156.5(9) . .
O29 C62 Yb3 35.4(5) . .
C60 C62 Yb3 81.3(7) . .
O31 C63 O32 126.3(13) . .
O31 C63 C61 116.8(10) . .
O32 C63 C61 116.5(11) . .
O31 C63 Yb3 35.2(6) . .
O32 C63 Yb3 161.4(10) . .
C61 C63 Yb3 81.9(6) . .
N8 C64 C57 115.1(11) . .
N8 C65 C67 112.7(10) . .
N8 C66 C68 109.2(11) . .
O34 C67 O33 122.7(11) . .
O34 C67 C65 120.2(11) . .
O33 C67 C65 117.1(11) . .
O34 C67 Na2 68.2(7) . 1_566
O33 C67 Na2 59.1(6) . 1_566
C65 C67 Na2 155.3(10) . 1_566
O34 C67 Yb4 155.1(9) . .
O33 C67 Yb4 39.9(6) . .
C65 C67 Yb4 80.6(7) . .
Na2 C67 Yb4 98.9(4) 1_566 .
O35 C68 O36 123.4(12) . .
O35 C68 C66 121.0(13) . .
O36 C68 C66 115.4(12) . .
O35 C68 Yb4 38.9(7) . .
O36 C68 Yb4 157.3(9) . .
C66 C68 Yb4 83.2(8) . .
O32 Na1 O2W 92.6(3) . .
O32 Na1 O25 171.0(4) . 2_567
O2W Na1 O25 89.1(4) . 2_567
O32 Na1 O6 96.2(4) . 2_567
O2W Na1 O6 145.1(4) . 2_567
O25 Na1 O6 87.4(4) 2_567 2_567
O32 Na1 O1W 78.6(4) . .
O2W Na1 O1W 97.0(5) . .
O25 Na1 O1W 92.4(4) 2_567 .
O6 Na1 O1W 117.8(4) 2_567 .
O32 Na1 O7 95.6(4) . 2_567
O2W Na1 O7 93.1(4) . 2_567
O25 Na1 O7 93.1(4) 2_567 2_567
O6 Na1 O7 52.5(3) 2_567 2_567
O1W Na1 O7 168.6(5) . 2_567
O32 Na1 C15 102.0(4) . 2_567
O2W Na1 C15 117.6(4) . 2_567
O25 Na1 C15 85.0(4) 2_567 2_567
O6 Na1 C15 27.4(3) 2_567 2_567
O1W Na1 C15 145.1(5) . 2_567
O7 Na1 C15 26.1(3) 2_567 2_567
O5W Na2 O4W 101.1(4) . .
O5W Na2 O11 85.6(4) . .
O4W Na2 O11 165.9(4) . .
O5W Na2 O33 121.0(4) . 1_544
O4W Na2 O33 102.7(4) . 1_544
O11 Na2 O33 84.0(3) . 1_544
O5W Na2 O3W 105.7(4) . .
O4W Na2 O3W 76.5(3) . .
O11 Na2 O3W 89.8(3) . .
O33 Na2 O3W 132.1(4) 1_544 .
O5W Na2 O34 170.5(4) . 1_544
O4W Na2 O34 87.5(3) . 1_544
O11 Na2 O34 86.8(3) . 1_544
O33 Na2 O34 52.4(3) 1_544 1_544
O3W Na2 O34 79.9(3) . 1_544
O5W Na2 C67 145.5(4) . 1_544
O4W Na2 C67 101.1(4) . 1_544
O11 Na2 C67 79.1(4) . 1_544
O33 Na2 C67 27.2(3) 1_544 1_544
O3W Na2 C67 105.0(4) . 1_544
O34 Na2 C67 26.4(3) 1_544 1_544
O5W Na2 Na3 144.9(4) . 2_666
O4W Na2 Na3 50.9(3) . 2_666
O11 Na2 Na3 117.6(3) . 2_666
O33 Na2 Na3 89.2(3) 1_544 2_666
O3W Na2 Na3 52.5(3) . 2_666
O34 Na2 Na3 44.5(2) 1_544 2_666
C67 Na2 Na3 68.7(3) 1_544 2_666
O34 Na3 O14 172.6(5) 2_677 .
O34 Na3 O12W 95.3(5) 2_677 .
O14 Na3 O12W 90.8(5) . .
O34 Na3 O4W 92.8(4) 2_677 2_666
O14 Na3 O4W 82.5(4) . 2_666
O12W Na3 O4W 95.3(5) . 2_666
O34 Na3 O3W 83.6(4) 2_677 2_666
O14 Na3 O3W 89.5(4) . 2_666
O12W Na3 O3W 166.8(5) . 2_666
O4W Na3 O3W 71.7(3) 2_666 2_666
O34 Na3 O14W 125.0(7) 2_677 .
O14 Na3 O14W 60.5(6) . .
O12W Na3 O14W 76.7(9) . .
O4W Na3 O14W 141.7(7) 2_666 .
O3W Na3 O14W 114.7(8) 2_666 .
O34 Na3 O13W 83.1(10) 2_677 .
O14 Na3 O13W 103.5(9) . .
O12W Na3 O13W 61.3(11) . .
O4W Na3 O13W 155.6(9) 2_666 .
O3W Na3 O13W 131.3(11) 2_666 .
O14W Na3 O13W 44.9(8) . .
O34 Na3 C29 150.9(5) 2_677 .
O14 Na3 C29 21.8(3) . .
O12W Na3 C29 110.7(5) . .
O4W Na3 C29 72.7(4) 2_666 .
O3W Na3 C29 68.1(4) 2_666 .
O14W Na3 C29 75.4(6) . .
O13W Na3 C29 120.2(8) . .
O34 Na3 Na2 54.0(3) 2_677 2_666
O14 Na3 Na2 119.1(3) . 2_666
O12W Na3 Na2 121.1(4) . 2_666
O4W Na3 Na2 47.6(3) 2_666 2_666
O3W Na3 Na2 48.3(2) 2_666 2_666
O14W Na3 Na2 161.7(9) . 2_666
O13W Na3 Na2 136.8(10) . 2_666
C29 Na3 Na2 99.8(3) . 2_666
O34 Na3 Na11 141.8(5) 2_677 .
O14 Na3 Na11 40.1(4) . .
O12W Na3 Na11 59.3(5) . .
O4W Na3 Na11 64.8(4) 2_666 .
O3W Na3 Na11 114.5(4) 2_666 .
O14W Na3 Na11 79.5(9) . .
O13W Na3 Na11 104.5(12) . .
C29 Na3 Na11 54.0(4) . .
Na2 Na3 Na11 112.3(4) 2_666 .
O6W Na4 O6W 180.0(4) . 2_678
O6W Na4 O11W 127.4(5) . .
O6W Na4 O11W 52.6(5) 2_678 .
O6W Na4 O11W 52.6(5) . 2_678
O6W Na4 O11W 127.4(5) 2_678 2_678
O11W Na4 O11W 180.000(4) . 2_678
O6W Na4 O36 49.5(4) . .
O6W Na4 O36 130.5(4) 2_678 .
O11W Na4 O36 86.5(5) . .
O11W Na4 O36 93.5(5) 2_678 .
O6W Na4 O36 130.5(4) . 2_678
O6W Na4 O36 49.5(4) 2_678 2_678
O11W Na4 O36 93.5(5) . 2_678
O11W Na4 O36 86.5(5) 2_678 2_678
O36 Na4 O36 180.0(2) . 2_678
O6W Na4 O7W 70.7(7) . 2_678
O6W Na4 O7W 109.3(7) 2_678 2_678
O11W Na4 O7W 93.7(6) . 2_678
O11W Na4 O7W 86.3(6) 2_678 2_678
O36 Na4 O7W 98.8(4) . 2_678
O36 Na4 O7W 81.2(4) 2_678 2_678
O6W Na4 O7W 109.3(7) . .
O6W Na4 O7W 70.7(7) 2_678 .
O11W Na4 O7W 86.3(6) . .
O11W Na4 O7W 93.7(6) 2_678 .
O36 Na4 O7W 81.2(4) . .
O36 Na4 O7W 98.8(4) 2_678 .
O7W Na4 O7W 180.000(7) 2_678 .
O6W Na4 O23W 55.4(5) . .
O6W Na4 O23W 124.6(5) 2_678 .
O11W Na4 O23W 120.7(6) . .
O11W Na4 O23W 59.3(6) 2_678 .
O36 Na4 O23W 49.6(4) . .
O36 Na4 O23W 130.4(4) 2_678 .
O7W Na4 O23W 126.0(6) 2_678 .
O7W Na4 O23W 54.0(6) . .
O6W Na4 O23W 124.6(5) . 2_678
O6W Na4 O23W 55.4(5) 2_678 2_678
O11W Na4 O23W 59.3(6) . 2_678
O11W Na4 O23W 120.7(6) 2_678 2_678
O36 Na4 O23W 130.4(4) . 2_678
O36 Na4 O23W 49.6(4) 2_678 2_678
O7W Na4 O23W 54.0(6) 2_678 2_678
O7W Na4 O23W 126.0(6) . 2_678
O23W Na4 O23W 180.0(5) . 2_678
O8W Na5 O30 146.6(5) . .
O8W Na5 Na10 33.3(8) . .
O30 Na5 Na10 130.0(4) . .
O9W Na6 O30 114.7(5) . .
O9W Na6 O21 131.6(5) . 2_677
O30 Na6 O21 113.8(4) . 2_677
O24W Na7 O22W 112.8(10) . .
O24W Na7 O31 121.5(9) . .
O22W Na7 O31 125.7(8) . .
O24W Na7 Na8 158.0(8) . .
O22W Na7 Na8 48.9(6) . .
O31 Na7 Na8 78.4(4) . .
O24W Na7 Yb3 128.9(8) . .
O22W Na7 Yb3 109.5(7) . .
O31 Na7 Yb3 28.9(2) . .
Na8 Na7 Yb3 73.0(3) . .
O22W Na8 O18 49.5(5) . 2_567
O22W Na8 O26 79.6(6) . .
O18 Na8 O26 112.2(5) 2_567 .
O22W Na8 Na7 39.9(5) . .
O18 Na8 Na7 54.1(3) 2_567 .
O26 Na8 Na7 58.1(4) . .
Na11 Na10 O8W 144.6(13) . .
Na11 Na10 O10W 113.9(10) . .
O8W Na10 O10W 89.8(7) . .
Na11 Na10 O15W 52.1(10) . .
O8W Na10 O15W 110.8(10) . .
O10W Na10 O15W 158.2(11) . .
Na11 Na10 O9 65.9(7) . .
O8W Na10 O9 90.9(11) . .
O10W Na10 O9 87.1(7) . .
O15W Na10 O9 99.1(9) . .
Na11 Na10 O10W 112.8(8) . 2_667
O8W Na10 O10W 87.2(11) . 2_667
O10W Na10 O10W 99.2(9) . 2_667
O15W Na10 O10W 75.7(8) . 2_667
O9 Na10 O10W 173.4(9) . 2_667
Na11 Na10 O16W 40.7(8) . 2_667
O8W Na10 O16W 171.4(8) . 2_667
O10W Na10 O16W 81.7(9) . 2_667
O15W Na10 O16W 77.8(9) . 2_667
O9 Na10 O16W 87.1(8) . 2_667
O10W Na10 O16W 95.8(9) 2_667 2_667
Na11 Na10 Na10 127.5(11) . 2_667
O8W Na10 Na10 87.6(10) . 2_667
O10W Na10 Na10 53.1(6) . 2_667
O15W Na10 Na10 118.5(10) . 2_667
O9 Na10 Na10 140.2(7) . 2_667
O10W Na10 Na10 46.1(6) 2_667 2_667
O16W Na10 Na10 88.7(11) 2_667 2_667
Na11 Na10 Na5 112.6(9) . .
O8W Na10 Na5 41.9(10) . .
O10W Na10 Na5 82.6(5) . .
O15W Na10 Na5 117.3(9) . .
O9 Na10 Na5 49.4(4) . .
O10W Na10 Na5 129.1(6) 2_667 .
O16W Na10 Na5 134.3(7) 2_667 .
Na10 Na10 Na5 114.6(6) 2_667 .
O16W Na11 O15W 114.1(14) 2_667 .
O16W Na11 Na10 82.7(11) 2_667 .
O15W Na11 Na10 68.5(16) . .
O16W Na11 O14 108.9(12) 2_667 .
O15W Na11 O14 106.1(17) . .
Na10 Na11 O14 168.4(13) . .
O16W Na11 O9 109.0(12) 2_667 .
O15W Na11 O9 107.5(16) . .
Na10 Na11 O9 62.7(7) . .
O14 Na11 O9 111.2(8) . .
O16W Na11 O8 72.4(10) 2_667 .
O15W Na11 O8 151.3(18) . .
Na10 Na11 O8 85.5(8) . .
O14 Na11 O8 97.1(6) . .
O9 Na11 O8 46.8(5) . .
O16W Na11 C17 90.3(11) 2_667 .
O15W Na11 C17 129.2(17) . .
Na10 Na11 C17 71.8(7) . .
O14 Na11 C17 106.6(7) . .
O9 Na11 C17 23.1(4) . .
O8 Na11 C17 23.8(3) . .
O16W Na11 Na3 143.1(11) 2_667 .
O15W Na11 Na3 91.0(13) . .
Na10 Na11 Na3 133.3(10) . .
O14 Na11 Na3 35.2(4) . .
O9 Na11 Na3 86.6(6) . .
O8 Na11 Na3 98.7(5) . .
C17 Na11 Na3 93.9(6) . .
Na2 O3W Na3 79.1(3) . 2_666
Na2 O4W Na3 81.5(3) . 2_666
Na10 O8W Na5 104.7(17) . .
Na10 O10W Na10 80.8(9) . 2_667
Na11 O15W Na10 59.4(13) . .
Na11 O16W Na10 56.6(10) 2_667 2_667
Na7 O22W Na8 91.2(8) . .
O21W O24W Na7 131.0(17) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Yb1 O1 2.269(9) .
Yb1 O2 2.291(9) .
Yb1 O10 2.306(9) .
Yb1 O4 2.332(9) .
Yb1 O13 2.336(9) .
Yb1 O12 2.340(9) .
Yb1 N3 2.507(10) .
Yb1 N1 2.531(12) .
Yb1 C10 3.167(14) .
Yb1 C29 3.186(13) .
Yb1 Yb2 3.7341(8) .
Yb2 O10 2.266(8) .
Yb2 O17 2.275(9) .
Yb2 O16 2.303(10) .
Yb2 O1 2.307(10) .
Yb2 O8 2.330(9) .
Yb2 O6 2.356(9) .
Yb2 N2 2.550(11) .
Yb2 N4 2.554(11) .
Yb2 C34 3.157(14) .
Yb2 C17 3.189(14) .
Yb2 C15 3.203(14) .
Yb3 O28 2.227(8) .
Yb3 O26 2.279(9) .
Yb3 O31 2.286(8) .
Yb3 O29 2.296(8) .
Yb3 O19 2.314(8) .
Yb3 O24 2.324(9) .
Yb3 N6 2.524(10) .
Yb3 N7 2.548(11) .
Yb3 C51 3.114(15) .
Yb3 C63 3.184(12) .
Yb3 C50 3.188(13) .
Yb3 C62 3.201(13) .
Yb4 O19 2.246(8) .
Yb4 O35 2.283(9) .
Yb4 O22 2.300(9) .
Yb4 O28 2.321(8) .
Yb4 O20 2.331(8) .
Yb4 O33 2.341(8) .
Yb4 N5 2.543(10) .
Yb4 N8 2.570(10) .
Yb4 C68 3.113(14) .
Yb4 C67 3.171(13) .
Yb4 C46 3.186(13) .
N1 C9 1.500(16) .
N1 C11 1.502(17) .
N1 C8 1.514(16) .
O1 C1 1.331(16) .
C1 C2 1.38(2) .
C1 C6 1.400(18) .
N2 C13 1.460(17) .
N2 C16 1.479(18) .
N2 C14 1.535(16) .
O2 C10 1.245(16) .
C2 C3 1.362(19) .
C2 C8 1.480(18) .
N3 C28 1.491(15) .
N3 C25 1.492(16) .
N3 C26 1.534(16) .
O3 C10 1.247(15) .
C3 C4 1.352(18) .
N4 C31 1.438(17) .
N4 C33 1.448(16) .
N4 C30 1.486(16) .
O4 C12 1.288(16) .
C4 C5 1.42(2) .
C4 C7 1.532(19) .
N5 C44 1.467(16) .
N5 C42 1.475(15) .
N5 C43 1.500(15) .
O5 C12 1.203(15) .
C5 C6 1.406(19) .
N6 C48 1.463(16) .
N6 C49 1.467(17) .
N6 C47 1.486(15) .
O6 C15 1.293(16) .
O6 Na1 2.421(11) 2_567
C6 C13 1.54(2) .
N7 C60 1.463(15) .
N7 C61 1.467(14) .
N7 C59 1.494(15) .
O7 C15 1.232(15) .
O7 Na1 2.531(12) 2_567
N8 C66 1.459(16) .
N8 C64 1.462(15) .
N8 C65 1.479(15) .
O8 C17 1.249(15) .
O8 Na11 2.88(2) .
O9 C17 1.234(16) .
O9 Na10 2.53(2) .
O9 Na11 2.60(2) .
C9 C10 1.467(19) .
O10 C18 1.389(14) .
C11 C12 1.499(19) .
O12 C27 1.290(14) .
O11 C27 1.218(15) .
O11 Na2 2.370(10) .
O13 C29 1.257(15) .
O14 C29 1.246(15) .
O14 Na3 2.266(11) .
O14 Na11 2.532(19) .
C14 C15 1.497(19) .
O16 C32 1.273(15) .
C16 C17 1.558(19) .
O15 C32 1.180(16) .
C15 Na1 2.802(16) 2_567
O17 C34 1.244(15) .
C17 Na11 3.09(3) .
O18 C34 1.261(16) .
O18 Na8 2.825(15) 2_567
C18 C23 1.387(17) .
C18 C19 1.396(18) .
O19 C35 1.350(14) .
C19 C20 1.373(17) .
C19 C25 1.512(17) .
O20 C45 1.283(14) .
C20 C21 1.357(17) .
O21 C45 1.212(14) .
O21 Na6 2.899(12) 2_677
C21 C22 1.355(18) .
C21 C24 1.500(17) .
O22 C46 1.266(15) .
C22 C23 1.400(17) .
O23 C46 1.254(15) .
O23 Na9 2.681(14) .
C23 C30 1.507(18) .
O24 C50 1.294(15) .
O25 C50 1.220(15) .
O25 Na1 2.393(10) 2_567
O26 C51 1.251(16) .
O26 Na8 2.837(16) .
C26 C27 1.510(18) .
O27 C51 1.330(16) .
C28 C29 1.488(17) .
O28 C52 1.372(14) .
O29 C62 1.253(15) .
C29 Na3 3.023(14) .
O30 C62 1.240(14) .
O30 Na6 2.737(13) .
O30 Na5 2.871(12) .
O31 C63 1.238(14) .
O31 Na7 2.770(13) .
C31 C32 1.558(19) .
O32 C63 1.240(13) .
O32 Na1 2.284(9) .
C33 C34 1.536(19) .
O33 C67 1.272(14) .
O33 Na2 2.388(9) 1_566
O34 C67 1.238(14) .
O34 Na3 2.242(11) 2_677
O34 Na2 2.586(10) 1_566
O35 C68 1.242(15) .
C35 C40 1.404(17) .
C35 C36 1.413(17) .
O36 C68 1.300(16) .
O36 Na4 2.557(9) .
C36 C37 1.384(16) .
C36 C42 1.513(17) .
C37 C38 1.392(17) .
C38 C39 1.387(17) .
C38 C41 1.548(16) .
C39 C40 1.407(16) .
C40 C47 1.475(17) .
C43 C45 1.518(18) .
C44 C46 1.504(16) .
C48 C50 1.491(17) .
C49 C51 1.567(18) .
C52 C57 1.411(17) .
C52 C53 1.415(18) .
C53 C54 1.381(17) .
C53 C59 1.507(17) .
C54 C55 1.377(17) .
C55 C56 1.400(18) .
C55 C58 1.514(16) .
C56 C57 1.375(17) .
C57 C64 1.485(17) .
C60 C62 1.492(16) .
C61 C63 1.528(18) .
C65 C67 1.491(16) .
C66 C68 1.489(18) .
C67 Na2 2.777(13) 1_566
Na1 O2W 2.346(11) .
Na1 O25 2.393(10) 2_567
Na1 O6 2.421(11) 2_567
Na1 O1W 2.455(14) .
Na1 O7 2.531(12) 2_567
Na1 C15 2.802(16) 2_567
Na2 O5W 2.295(11) .
Na2 O4W 2.361(11) .
Na2 O33 2.388(9) 1_544
Na2 O3W 2.406(10) .
Na2 O34 2.586(10) 1_544
Na2 C67 2.777(13) 1_544
Na2 Na3 3.164(8) 2_666
Na3 O34 2.242(11) 2_677
Na3 O12W 2.314(17) .
Na3 O4W 2.484(10) 2_666
Na3 O3W 2.557(11) 2_666
Na3 O14W 2.83(3) .
Na3 O13W 3.00(3) .
Na3 Na2 3.164(8) 2_666
Na3 Na11 3.80(2) .
Na4 O6W 2.250(11) .
Na4 O6W 2.250(11) 2_678
Na4 O11W 2.357(15) .
Na4 O11W 2.357(15) 2_678
Na4 O36 2.557(9) 2_678
Na4 O7W 2.733(18) 2_678
Na4 O7W 2.733(18) .
Na4 O23W 3.002(17) .
Na4 O23W 3.002(17) 2_678
Na5 O8W 2.83(3) .
Na5 Na10 4.100(19) .
Na6 O9W 2.672(16) .
Na6 O21 2.899(12) 2_677
Na7 O24W 2.35(3) .
Na7 O22W 2.36(3) .
Na7 Na8 3.680(19) .
Na8 O22W 2.77(3) .
Na8 O18 2.825(15) 2_567
Na10 Na11 2.23(2) .
Na10 O8W 2.33(3) .
Na10 O10W 2.33(2) .
Na10 O15W 2.41(5) .
Na10 O10W 2.59(2) 2_667
Na10 O16W 2.64(3) 2_667
Na10 Na10 3.20(4) 2_667
Na11 O16W 1.74(4) 2_667
Na11 O15W 2.04(3) .
O3W Na3 2.557(11) 2_666
O4W Na3 2.484(10) 2_666
O10W Na10 2.59(2) 2_667
O16W Na11 1.74(4) 2_667
O16W Na10 2.64(3) 2_667
O21W O24W 1.71(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 Yb1 Yb2 O10 161.1(5) . .
O2 Yb1 Yb2 O10 50.3(4) . .
O4 Yb1 Yb2 O10 -168.2(4) . .
O13 Yb1 Yb2 O10 -99.7(4) . .
O12 Yb1 Yb2 O10 3.7(13) . .
N3 Yb1 Yb2 O10 -36.2(4) . .
N1 Yb1 Yb2 O10 118.1(5) . .
C10 Yb1 Yb2 O10 65.3(5) . .
C29 Yb1 Yb2 O10 -84.8(4) . .
O1 Yb1 Yb2 O17 51.2(4) . .
O2 Yb1 Yb2 O17 -59.6(3) . .
O10 Yb1 Yb2 O17 -109.9(4) . .
O4 Yb1 Yb2 O17 81.9(3) . .
O13 Yb1 Yb2 O17 150.3(3) . .
O12 Yb1 Yb2 O17 -106.2(13) . .
N3 Yb1 Yb2 O17 -146.1(3) . .
N1 Yb1 Yb2 O17 8.1(3) . .
C10 Yb1 Yb2 O17 -44.6(4) . .
C29 Yb1 Yb2 O17 165.3(3) . .
O1 Yb1 Yb2 O16 -168.6(5) . .
O2 Yb1 Yb2 O16 80.6(3) . .
O10 Yb1 Yb2 O16 30.3(4) . .
O4 Yb1 Yb2 O16 -137.9(3) . .
O13 Yb1 Yb2 O16 -69.4(3) . .
O12 Yb1 Yb2 O16 34.0(13) . .
N3 Yb1 Yb2 O16 -5.9(3) . .
N1 Yb1 Yb2 O16 148.4(4) . .
C10 Yb1 Yb2 O16 95.6(4) . .
C29 Yb1 Yb2 O16 -54.4(3) . .
O2 Yb1 Yb2 O1 -110.8(5) . .
O10 Yb1 Yb2 O1 -161.1(5) . .
O4 Yb1 Yb2 O1 30.7(5) . .
O13 Yb1 Yb2 O1 99.1(4) . .
O12 Yb1 Yb2 O1 -157.4(13) . .
N3 Yb1 Yb2 O1 162.7(5) . .
N1 Yb1 Yb2 O1 -43.0(5) . .
C10 Yb1 Yb2 O1 -95.8(5) . .
C29 Yb1 Yb2 O1 114.1(4) . .
O1 Yb1 Yb2 O8 -99.1(4) . .
O2 Yb1 Yb2 O8 150.1(3) . .
O10 Yb1 Yb2 O8 99.8(4) . .
O4 Yb1 Yb2 O8 -68.4(3) . .
O13 Yb1 Yb2 O8 0.1(3) . .
O12 Yb1 Yb2 O8 103.6(13) . .
N3 Yb1 Yb2 O8 63.7(3) . .
N1 Yb1 Yb2 O8 -142.1(3) . .
C10 Yb1 Yb2 O8 165.2(4) . .
C29 Yb1 Yb2 O8 15.1(3) . .
O1 Yb1 Yb2 O6 -4.3(13) . .
O2 Yb1 Yb2 O6 -115.1(13) . .
O10 Yb1 Yb2 O6 -165.4(13) . .
O4 Yb1 Yb2 O6 26.4(13) . .
O13 Yb1 Yb2 O6 94.8(13) . .
O12 Yb1 Yb2 O6 -161.7(18) . .
N3 Yb1 Yb2 O6 158.4(13) . .
N1 Yb1 Yb2 O6 -47.3(13) . .
C10 Yb1 Yb2 O6 -100.1(13) . .
C29 Yb1 Yb2 O6 109.8(13) . .
O1 Yb1 Yb2 N2 -36.7(5) . .
O2 Yb1 Yb2 N2 -147.6(4) . .
O10 Yb1 Yb2 N2 162.1(5) . .
O4 Yb1 Yb2 N2 -6.1(4) . .
O13 Yb1 Yb2 N2 62.4(3) . .
O12 Yb1 Yb2 N2 165.9(13) . .
N3 Yb1 Yb2 N2 126.0(4) . .
N1 Yb1 Yb2 N2 -79.8(4) . .
C10 Yb1 Yb2 N2 -132.5(4) . .
C29 Yb1 Yb2 N2 77.4(4) . .
O1 Yb1 Yb2 N4 118.7(5) . .
O2 Yb1 Yb2 N4 7.9(4) . .
O10 Yb1 Yb2 N4 -42.4(5) . .
O4 Yb1 Yb2 N4 149.4(4) . .
O13 Yb1 Yb2 N4 -142.2(3) . .
O12 Yb1 Yb2 N4 -38.7(13) . .
N3 Yb1 Yb2 N4 -78.6(4) . .
N1 Yb1 Yb2 N4 75.6(4) . .
C10 Yb1 Yb2 N4 22.9(4) . .
C29 Yb1 Yb2 N4 -127.2(4) . .
O1 Yb1 Yb2 C34 66.8(5) . .
O2 Yb1 Yb2 C34 -44.0(4) . .
O10 Yb1 Yb2 C34 -94.4(5) . .
O4 Yb1 Yb2 C34 97.5(4) . .
O13 Yb1 Yb2 C34 165.9(3) . .
O12 Yb1 Yb2 C34 -90.6(13) . .
N3 Yb1 Yb2 C34 -130.5(4) . .
N1 Yb1 Yb2 C34 23.7(4) . .
C10 Yb1 Yb2 C34 -29.0(4) . .
C29 Yb1 Yb2 C34 -179.1(3) . .
O1 Yb1 Yb2 C17 -84.7(5) . .
O2 Yb1 Yb2 C17 164.5(4) . .
O10 Yb1 Yb2 C17 114.2(5) . .
O4 Yb1 Yb2 C17 -54.0(4) . .
O13 Yb1 Yb2 C17 14.5(3) . .
O12 Yb1 Yb2 C17 117.9(13) . .
N3 Yb1 Yb2 C17 78.0(4) . .
N1 Yb1 Yb2 C17 -127.7(4) . .
C10 Yb1 Yb2 C17 179.5(4) . .
C29 Yb1 Yb2 C17 29.5(3) . .
O1 Yb1 Yb2 C15 -5.4(6) . .
O2 Yb1 Yb2 C15 -116.2(6) . .
O10 Yb1 Yb2 C15 -166.5(6) . .
O4 Yb1 Yb2 C15 25.3(6) . .
O13 Yb1 Yb2 C15 93.8(5) . .
O12 Yb1 Yb2 C15 -162.8(13) . .
N3 Yb1 Yb2 C15 157.3(6) . .
N1 Yb1 Yb2 C15 -48.4(6) . .
C10 Yb1 Yb2 C15 -101.2(6) . .
C29 Yb1 Yb2 C15 108.7(5) . .
O28 Yb3 Yb4 O19 -165.7(5) . .
O26 Yb3 Yb4 O19 100.0(4) . .
O31 Yb3 Yb4 O19 169.4(5) . .
O29 Yb3 Yb4 O19 -49.5(4) . .
O24 Yb3 Yb4 O19 5.6(18) . .
N6 Yb3 Yb4 O19 34.8(5) . .
N7 Yb3 Yb4 O19 -117.2(4) . .
C51 Yb3 Yb4 O19 83.6(5) . .
C63 Yb3 Yb4 O19 -171.2(5) . .
C50 Yb3 Yb4 O19 8.1(7) . .
C62 Yb3 Yb4 O19 -65.2(4) . .
O28 Yb3 Yb4 O35 98.5(4) . .
O26 Yb3 Yb4 O35 4.1(3) . .
O31 Yb3 Yb4 O35 73.5(3) . .
O29 Yb3 Yb4 O35 -145.3(3) . .
O19 Yb3 Yb4 O35 -95.8(4) . .
O24 Yb3 Yb4 O35 -90.2(17) . .
N6 Yb3 Yb4 O35 -61.0(3) . .
N7 Yb3 Yb4 O35 147.0(3) . .
C51 Yb3 Yb4 O35 -12.2(3) . .
C63 Yb3 Yb4 O35 92.9(3) . .
C50 Yb3 Yb4 O35 -87.7(6) . .
C62 Yb3 Yb4 O35 -161.0(3) . .
O28 Yb3 Yb4 O22 -50.5(4) . .
O26 Yb3 Yb4 O22 -144.9(3) . .
O31 Yb3 Yb4 O22 -75.5(3) . .
O29 Yb3 Yb4 O22 65.7(3) . .
O19 Yb3 Yb4 O22 115.2(4) . .
O24 Yb3 Yb4 O22 120.8(17) . .
N6 Yb3 Yb4 O22 150.0(3) . .
N7 Yb3 Yb4 O22 -2.0(3) . .
C51 Yb3 Yb4 O22 -161.2(3) . .
C63 Yb3 Yb4 O22 -56.1(3) . .
C50 Yb3 Yb4 O22 123.3(6) . .
C62 Yb3 Yb4 O22 50.0(3) . .
O26 Yb3 Yb4 O28 -94.3(4) . .
O31 Yb3 Yb4 O28 -24.9(5) . .
O29 Yb3 Yb4 O28 116.2(4) . .
O19 Yb3 Yb4 O28 165.7(5) . .
O24 Yb3 Yb4 O28 171.3(18) . .
N6 Yb3 Yb4 O28 -159.5(5) . .
N7 Yb3 Yb4 O28 48.5(4) . .
C51 Yb3 Yb4 O28 -110.7(5) . .
C63 Yb3 Yb4 O28 -5.5(5) . .
C50 Yb3 Yb4 O28 173.8(7) . .
C62 Yb3 Yb4 O28 100.5(4) . .
O28 Yb3 Yb4 O20 169.5(5) . .
O26 Yb3 Yb4 O20 75.2(3) . .
O31 Yb3 Yb4 O20 144.6(3) . .
O29 Yb3 Yb4 O20 -74.3(3) . .
O19 Yb3 Yb4 O20 -24.8(4) . .
O24 Yb3 Yb4 O20 -19.2(17) . .
N6 Yb3 Yb4 O20 10.0(3) . .
N7 Yb3 Yb4 O20 -142.0(3) . .
C51 Yb3 Yb4 O20 58.8(3) . .
C63 Yb3 Yb4 O20 164.0(4) . .
C50 Yb3 Yb4 O20 -16.7(6) . .
C62 Yb3 Yb4 O20 -90.0(3) . .
O28 Yb3 Yb4 O33 -4.9(11) . .
O26 Yb3 Yb4 O33 -99.2(10) . .
O31 Yb3 Yb4 O33 -29.8(10) . .
O29 Yb3 Yb4 O33 111.4(10) . .
O19 Yb3 Yb4 O33 160.8(11) . .
O24 Yb3 Yb4 O33 166.4(19) . .
N6 Yb3 Yb4 O33 -164.4(10) . .
N7 Yb3 Yb4 O33 43.6(10) . .
C51 Yb3 Yb4 O33 -115.6(10) . .
C63 Yb3 Yb4 O33 -10.4(11) . .
C50 Yb3 Yb4 O33 169.0(12) . .
C62 Yb3 Yb4 O33 95.7(10) . .
O28 Yb3 Yb4 N5 -117.6(5) . .
O26 Yb3 Yb4 N5 148.1(3) . .
O31 Yb3 Yb4 N5 -142.6(3) . .
O29 Yb3 Yb4 N5 -1.4(3) . .
O19 Yb3 Yb4 N5 48.1(5) . .
O24 Yb3 Yb4 N5 53.7(17) . .
N6 Yb3 Yb4 N5 82.9(4) . .
N7 Yb3 Yb4 N5 -69.1(3) . .
C51 Yb3 Yb4 N5 131.7(3) . .
C63 Yb3 Yb4 N5 -123.1(4) . .
C50 Yb3 Yb4 N5 56.2(6) . .
C62 Yb3 Yb4 N5 -17.1(3) . .
O28 Yb3 Yb4 N8 34.7(5) . .
O26 Yb3 Yb4 N8 -59.7(3) . .
O31 Yb3 Yb4 N8 9.7(3) . .
O29 Yb3 Yb4 N8 150.9(3) . .
O19 Yb3 Yb4 N8 -159.6(5) . .
O24 Yb3 Yb4 N8 -154.0(17) . .
N6 Yb3 Yb4 N8 -124.8(4) . .
N7 Yb3 Yb4 N8 83.2(3) . .
C51 Yb3 Yb4 N8 -76.0(3) . .
C63 Yb3 Yb4 N8 29.2(4) . .
C50 Yb3 Yb4 N8 -151.5(6) . .
C62 Yb3 Yb4 N8 135.2(3) . .
O28 Yb3 Yb4 C68 84.5(5) . .
O26 Yb3 Yb4 C68 -9.8(3) . .
O31 Yb3 Yb4 C68 59.6(3) . .
O29 Yb3 Yb4 C68 -159.3(3) . .
O19 Yb3 Yb4 C68 -109.8(5) . .
O24 Yb3 Yb4 C68 -104.2(17) . .
N6 Yb3 Yb4 C68 -75.0(4) . .
N7 Yb3 Yb4 C68 133.0(3) . .
C51 Yb3 Yb4 C68 -26.2(3) . .
C63 Yb3 Yb4 C68 79.0(4) . .
C50 Yb3 Yb4 C68 -101.6(6) . .
C62 Yb3 Yb4 C68 -175.0(3) . .
O28 Yb3 Yb4 C67 -0.2(6) . .
O26 Yb3 Yb4 C67 -94.5(5) . .
O31 Yb3 Yb4 C67 -25.1(5) . .
O29 Yb3 Yb4 C67 116.1(5) . .
O19 Yb3 Yb4 C67 165.5(6) . .
O24 Yb3 Yb4 C67 171.1(18) . .
N6 Yb3 Yb4 C67 -159.7(5) . .
N7 Yb3 Yb4 C67 48.3(5) . .
C51 Yb3 Yb4 C67 -110.9(5) . .
C63 Yb3 Yb4 C67 -5.7(5) . .
C50 Yb3 Yb4 C67 173.7(7) . .
C62 Yb3 Yb4 C67 100.4(5) . .
O28 Yb3 Yb4 C46 -66.0(4) . .
O26 Yb3 Yb4 C46 -160.3(3) . .
O31 Yb3 Yb4 C46 -90.9(3) . .
O29 Yb3 Yb4 C46 50.3(3) . .
O19 Yb3 Yb4 C46 99.7(4) . .
O24 Yb3 Yb4 C46 105.3(17) . .
N6 Yb3 Yb4 C46 134.5(3) . .
N7 Yb3 Yb4 C46 -17.5(3) . .
C51 Yb3 Yb4 C46 -176.7(3) . .
C63 Yb3 Yb4 C46 -71.5(4) . .
C50 Yb3 Yb4 C46 107.9(6) . .
C62 Yb3 Yb4 C46 34.6(3) . .
O1 Yb1 N1 C9 -140.1(8) . .
O2 Yb1 N1 C9 -27.5(7) . .
O10 Yb1 N1 C9 -80.5(8) . .
O4 Yb1 N1 C9 137.9(8) . .
O13 Yb1 N1 C9 143.9(7) . .
O12 Yb1 N1 C9 54.6(8) . .
N3 Yb1 N1 C9 25.8(10) . .
C10 Yb1 N1 C9 -17.8(7) . .
C29 Yb1 N1 C9 111.2(9) . .
Yb2 Yb1 N1 C9 -116.3(7) . .
O1 Yb1 N1 C11 95.7(8) . .
O2 Yb1 N1 C11 -151.8(9) . .
O10 Yb1 N1 C11 155.2(7) . .
O4 Yb1 N1 C11 13.6(8) . .
O13 Yb1 N1 C11 19.6(11) . .
O12 Yb1 N1 C11 -69.6(8) . .
N3 Yb1 N1 C11 -98.4(9) . .
C10 Yb1 N1 C11 -142.0(10) . .
C29 Yb1 N1 C11 -13.1(12) . .
Yb2 Yb1 N1 C11 119.4(8) . .
O1 Yb1 N1 C8 -24.8(7) . .
O2 Yb1 N1 C8 87.8(8) . .
O10 Yb1 N1 C8 34.8(9) . .
O4 Yb1 N1 C8 -106.8(8) . .
O13 Yb1 N1 C8 -100.8(8) . .
O12 Yb1 N1 C8 169.9(8) . .
N3 Yb1 N1 C8 141.1(7) . .
C10 Yb1 N1 C8 97.5(8) . .
C29 Yb1 N1 C8 -133.5(8) . .
Yb2 Yb1 N1 C8 -1.0(8) . .
O2 Yb1 O1 C1 -92.3(10) . .
O10 Yb1 O1 C1 -157.1(10) . .
O4 Yb1 O1 C1 40.6(10) . .
O13 Yb1 O1 C1 113.5(10) . .
O12 Yb1 O1 C1 3.3(14) . .
N3 Yb1 O1 C1 165.2(9) . .
N1 Yb1 O1 C1 -29.7(10) . .
C10 Yb1 O1 C1 -72.6(10) . .
C29 Yb1 O1 C1 118.9(10) . .
Yb2 Yb1 O1 C1 -168.5(12) . .
O2 Yb1 O1 Yb2 76.1(4) . .
O10 Yb1 O1 Yb2 11.4(3) . .
O4 Yb1 O1 Yb2 -150.9(4) . .
O13 Yb1 O1 Yb2 -78.0(4) . .
O12 Yb1 O1 Yb2 171.8(5) . .
N3 Yb1 O1 Yb2 -26.3(7) . .
N1 Yb1 O1 Yb2 138.8(4) . .
C10 Yb1 O1 Yb2 95.9(4) . .
C29 Yb1 O1 Yb2 -72.7(4) . .
O10 Yb2 O1 C1 157.2(10) . .
O17 Yb2 O1 C1 42.6(9) . .
O16 Yb2 O1 C1 -172.6(9) . .
O8 Yb2 O1 C1 -113.3(10) . .
O6 Yb2 O1 C1 -12.3(12) . .
N2 Yb2 O1 C1 -47.3(10) . .
N4 Yb2 O1 C1 91.5(10) . .
C34 Yb2 O1 C1 50.5(10) . .
C17 Yb2 O1 C1 -94.3(10) . .
C15 Yb2 O1 C1 -14.2(11) . .
Yb1 Yb2 O1 C1 168.8(12) . .
O10 Yb2 O1 Yb1 -11.6(3) . .
O17 Yb2 O1 Yb1 -126.2(4) . .
O16 Yb2 O1 Yb1 18.6(7) . .
O8 Yb2 O1 Yb1 77.9(4) . .
O6 Yb2 O1 Yb1 178.9(3) . .
N2 Yb2 O1 Yb1 143.9(4) . .
N4 Yb2 O1 Yb1 -77.3(5) . .
C34 Yb2 O1 Yb1 -118.3(4) . .
C17 Yb2 O1 Yb1 96.9(4) . .
C15 Yb2 O1 Yb1 177.0(3) . .
Yb1 O1 C1 C2 48.3(17) . .
Yb2 O1 C1 C2 -118.6(13) . .
Yb1 O1 C1 C6 -133.4(11) . .
Yb2 O1 C1 C6 59.6(15) . .
O10 Yb2 N2 C13 25.4(12) . .
O17 Yb2 N2 C13 -85.3(9) . .
O16 Yb2 N2 C13 135.7(9) . .
O1 Yb2 N2 C13 -11.1(9) . .
O8 Yb2 N2 C13 82.6(9) . .
O6 Yb2 N2 C13 -164.6(10) . .
N4 Yb2 N2 C13 -134.8(9) . .
C34 Yb2 N2 C13 -100.4(9) . .
C17 Yb2 N2 C13 90.9(10) . .
C15 Yb2 N2 C13 -150.0(11) . .
Yb1 Yb2 N2 C13 9.5(9) . .
O10 Yb2 N2 C16 -93.2(9) . .
O17 Yb2 N2 C16 156.2(8) . .
O16 Yb2 N2 C16 17.1(9) . .
O1 Yb2 N2 C16 -129.6(8) . .
O8 Yb2 N2 C16 -35.9(7) . .
O6 Yb2 N2 C16 76.9(8) . .
N4 Yb2 N2 C16 106.7(8) . .
C34 Yb2 N2 C16 141.1(8) . .
C17 Yb2 N2 C16 -27.6(7) . .
C15 Yb2 N2 C16 91.5(9) . .
Yb1 Yb2 N2 C16 -109.0(8) . .
O10 Yb2 N2 C14 152.4(8) . .
O17 Yb2 N2 C14 41.7(9) . .
O16 Yb2 N2 C14 -97.3(9) . .
O1 Yb2 N2 C14 115.9(9) . .
O8 Yb2 N2 C14 -150.4(10) . .
O6 Yb2 N2 C14 -37.5(8) . .
N4 Yb2 N2 C14 -7.8(11) . .
C34 Yb2 N2 C14 26.6(9) . .
C17 Yb2 N2 C14 -142.1(11) . .
C15 Yb2 N2 C14 -22.9(8) . .
Yb1 Yb2 N2 C14 136.5(8) . .
O1 Yb1 O2 C10 95.6(11) . .
O10 Yb1 O2 C10 157.6(11) . .
O4 Yb1 O2 C10 4.4(12) . .
O13 Yb1 O2 C10 -145.7(10) . .
O12 Yb1 O2 C10 -56.9(10) . .
N3 Yb1 O2 C10 -123.3(11) . .
N1 Yb1 O2 C10 23.6(10) . .
C29 Yb1 O2 C10 -127.6(10) . .
Yb2 Yb1 O2 C10 130.3(10) . .
O1 C1 C2 C3 -179.2(12) . .
C6 C1 C2 C3 3(2) . .
O1 C1 C2 C8 2(2) . .
C6 C1 C2 C8 -176.1(12) . .
O1 Yb1 N3 C28 -90.3(9) . .
O2 Yb1 N3 C28 159.6(8) . .
O10 Yb1 N3 C28 -126.2(8) . .
O4 Yb1 N3 C28 20.6(9) . .
O13 Yb1 N3 C28 -32.2(7) . .
O12 Yb1 N3 C28 80.8(8) . .
N1 Yb1 N3 C28 111.7(8) . .
C10 Yb1 N3 C28 143.8(8) . .
C29 Yb1 N3 C28 -24.5(7) . .
Yb2 Yb1 N3 C28 -106.0(7) . .
O1 Yb1 N3 C25 26.9(11) . .
O2 Yb1 N3 C25 -83.3(8) . .
O10 Yb1 N3 C25 -9.0(8) . .
O4 Yb1 N3 C25 137.8(8) . .
O13 Yb1 N3 C25 84.9(8) . .
O12 Yb1 N3 C25 -162.0(9) . .
N1 Yb1 N3 C25 -131.1(8) . .
C10 Yb1 N3 C25 -99.0(8) . .
C29 Yb1 N3 C25 92.7(9) . .
Yb2 Yb1 N3 C25 11.2(8) . .
O1 Yb1 N3 C26 152.2(7) . .
O2 Yb1 N3 C26 42.1(7) . .
O10 Yb1 N3 C26 116.4(7) . .
O4 Yb1 N3 C26 -96.8(7) . .
O13 Yb1 N3 C26 -149.7(8) . .
O12 Yb1 N3 C26 -36.6(7) . .
N1 Yb1 N3 C26 -5.7(10) . .
C10 Yb1 N3 C26 26.4(8) . .
C29 Yb1 N3 C26 -142.0(9) . .
Yb2 Yb1 N3 C26 136.6(7) . .
C1 C2 C3 C4 -3(2) . .
C8 C2 C3 C4 175.6(13) . .
O10 Yb2 N4 C31 97.0(9) . .
O17 Yb2 N4 C31 -151.5(9) . .
O16 Yb2 N4 C31 15.1(8) . .
O1 Yb2 N4 C31 156.6(8) . .
O8 Yb2 N4 C31 19.6(11) . .
O6 Yb2 N4 C31 -68.4(9) . .
N2 Yb2 N4 C31 -96.0(10) . .
C34 Yb2 N4 C31 -143.6(10) . .
C17 Yb2 N4 C31 -12.5(12) . .
C15 Yb2 N4 C31 -84.6(9) . .
Yb1 Yb2 N4 C31 120.4(8) . .
O10 Yb2 N4 C33 -139.1(9) . .
O17 Yb2 N4 C33 -27.6(8) . .
O16 Yb2 N4 C33 139.1(10) . .
O1 Yb2 N4 C33 -79.5(9) . .
O8 Yb2 N4 C33 143.5(8) . .
O6 Yb2 N4 C33 55.6(9) . .
N2 Yb2 N4 C33 28.0(11) . .
C34 Yb2 N4 C33 -19.6(8) . .
C17 Yb2 N4 C33 111.5(10) . .
C15 Yb2 N4 C33 39.4(9) . .
Yb1 Yb2 N4 C33 -115.7(8) . .
O10 Yb2 N4 C30 -23.4(8) . .
O17 Yb2 N4 C30 88.1(8) . .
O16 Yb2 N4 C30 -105.2(8) . .
O1 Yb2 N4 C30 36.2(9) . .
O8 Yb2 N4 C30 -100.8(9) . .
O6 Yb2 N4 C30 171.2(9) . .
N2 Yb2 N4 C30 143.7(8) . .
C34 Yb2 N4 C30 96.1(9) . .
C17 Yb2 N4 C30 -132.9(8) . .
C15 Yb2 N4 C30 155.0(8) . .
Yb1 Yb2 N4 C30 0.0(8) . .
O1 Yb1 O4 C12 -83.7(10) . .
O2 Yb1 O4 C12 19.2(12) . .
O10 Yb1 O4 C12 -112.9(10) . .
O13 Yb1 O4 C12 -175.8(11) . .
O12 Yb1 O4 C12 80.0(10) . .
N3 Yb1 O4 C12 133.8(10) . .
N1 Yb1 O4 C12 0.3(10) . .
C10 Yb1 O4 C12 20.8(11) . .
C29 Yb1 O4 C12 166.6(10) . .
Yb2 Yb1 O4 C12 -101.4(10) . .
C2 C3 C4 C5 2(2) . .
C2 C3 C4 C7 -178.0(13) . .
O19 Yb4 N5 C44 140.2(8) . .
O35 Yb4 N5 C44 -140.5(7) . .
O22 Yb4 N5 C44 27.0(7) . .
O28 Yb4 N5 C44 79.3(8) . .
O20 Yb4 N5 C44 -137.1(8) . .
O33 Yb4 N5 C44 -54.2(8) . .
N8 Yb4 N5 C44 -24.1(10) . .
C68 Yb4 N5 C44 -106.6(9) . .
C67 Yb4 N5 C44 -37.2(8) . .
C46 Yb4 N5 C44 17.6(7) . .
Yb3 Yb4 N5 C44 114.1(7) . .
O19 Yb4 N5 C42 23.3(7) . .
O35 Yb4 N5 C42 102.6(8) . .
O22 Yb4 N5 C42 -89.9(7) . .
O28 Yb4 N5 C42 -37.6(8) . .
O20 Yb4 N5 C42 106.0(8) . .
O33 Yb4 N5 C42 -171.1(8) . .
N8 Yb4 N5 C42 -141.0(7) . .
C68 Yb4 N5 C42 136.5(7) . .
C67 Yb4 N5 C42 -154.1(7) . .
C46 Yb4 N5 C42 -99.3(8) . .
Yb3 Yb4 N5 C42 -2.8(8) . .
O19 Yb4 N5 C43 -97.5(8) . .
O35 Yb4 N5 C43 -18.2(10) . .
O22 Yb4 N5 C43 149.3(8) . .
O28 Yb4 N5 C43 -158.4(7) . .
O20 Yb4 N5 C43 -14.8(7) . .
O33 Yb4 N5 C43 68.1(8) . .
N8 Yb4 N5 C43 98.2(8) . .
C68 Yb4 N5 C43 15.7(11) . .
C67 Yb4 N5 C43 85.1(8) . .
C46 Yb4 N5 C43 139.9(9) . .
Yb3 Yb4 N5 C43 -123.5(7) . .
C3 C4 C5 C6 -1(2) . .
C7 C4 C5 C6 179.5(12) . .
O28 Yb3 N6 C48 -159.4(7) . .
O26 Yb3 N6 C48 146.4(8) . .
O31 Yb3 N6 C48 89.5(8) . .
O29 Yb3 N6 C48 -45.7(8) . .
O19 Yb3 N6 C48 -121.8(8) . .
O24 Yb3 N6 C48 34.7(7) . .
N7 Yb3 N6 C48 -0.9(10) . .
C51 Yb3 N6 C48 140.6(9) . .
C63 Yb3 N6 C48 70.3(9) . .
C50 Yb3 N6 C48 22.5(7) . .
C62 Yb3 N6 C48 -31.4(8) . .
O28 Yb3 N6 C49 84.7(9) . .
O26 Yb3 N6 C49 30.5(8) . .
O31 Yb3 N6 C49 -26.4(9) . .
O29 Yb3 N6 C49 -161.6(8) . .
O19 Yb3 N6 C49 122.3(8) . .
O24 Yb3 N6 C49 -81.2(8) . .
N7 Yb3 N6 C49 -116.8(8) . .
C51 Yb3 N6 C49 24.7(7) . .
C63 Yb3 N6 C49 -45.6(9) . .
C50 Yb3 N6 C49 -93.4(9) . .
C62 Yb3 N6 C49 -147.3(8) . .
O28 Yb3 N6 C47 -31.8(11) . .
O26 Yb3 N6 C47 -86.0(9) . .
O31 Yb3 N6 C47 -142.9(8) . .
O29 Yb3 N6 C47 81.9(8) . .
O19 Yb3 N6 C47 5.8(8) . .
O24 Yb3 N6 C47 162.3(9) . .
N7 Yb3 N6 C47 126.7(8) . .
C51 Yb3 N6 C47 -91.8(9) . .
C63 Yb3 N6 C47 -162.1(8) . .
C50 Yb3 N6 C47 150.1(10) . .
C62 Yb3 N6 C47 96.2(8) . .
O10 Yb2 O6 C15 -162.0(9) . .
O17 Yb2 O6 C15 -58.3(10) . .
O16 Yb2 O6 C15 163.4(10) . .
O1 Yb2 O6 C15 -5.1(12) . .
O8 Yb2 O6 C15 91.6(10) . .
N2 Yb2 O6 C15 33.0(10) . .
N4 Yb2 O6 C15 -127.0(10) . .
C34 Yb2 O6 C15 -75.8(10) . .
C17 Yb2 O6 C15 79.7(10) . .
Yb1 Yb2 O6 C15 -2(2) . .
O10 Yb2 O6 Na1 26.6(13) . 2_567
O17 Yb2 O6 Na1 130.3(8) . 2_567
O16 Yb2 O6 Na1 -8.0(7) . 2_567
O1 Yb2 O6 Na1 -176.5(6) . 2_567
O8 Yb2 O6 Na1 -79.8(8) . 2_567
N2 Yb2 O6 Na1 -138.5(9) . 2_567
N4 Yb2 O6 Na1 61.6(8) . 2_567
C34 Yb2 O6 Na1 112.8(8) . 2_567
C17 Yb2 O6 Na1 -91.7(8) . 2_567
C15 Yb2 O6 Na1 -171.4(15) . 2_567
Yb1 Yb2 O6 Na1 -173.0(6) . 2_567
O1 C1 C6 C5 -179.5(12) . .
C2 C1 C6 C5 -1(2) . .
O1 C1 C6 C13 2(2) . .
C2 C1 C6 C13 -179.6(12) . .
C4 C5 C6 C1 0(2) . .
C4 C5 C6 C13 178.7(12) . .
O28 Yb3 N7 C60 140.3(7) . .
O26 Yb3 N7 C60 -148.3(7) . .
O31 Yb3 N7 C60 -138.9(8) . .
O29 Yb3 N7 C60 23.8(7) . .
O19 Yb3 N7 C60 78.5(8) . .
O24 Yb3 N7 C60 -59.1(7) . .
N6 Yb3 N7 C60 -25.7(9) . .
C51 Yb3 N7 C60 -113.8(9) . .
C63 Yb3 N7 C60 -137.0(9) . .
C50 Yb3 N7 C60 -43.2(7) . .
C62 Yb3 N7 C60 16.1(7) . .
O28 Yb3 N7 C61 -96.3(7) . .
O26 Yb3 N7 C61 -24.9(10) . .
O31 Yb3 N7 C61 -15.4(7) . .
O29 Yb3 N7 C61 147.2(8) . .
O19 Yb3 N7 C61 -158.1(7) . .
O24 Yb3 N7 C61 64.4(7) . .
N6 Yb3 N7 C61 97.7(8) . .
C51 Yb3 N7 C61 9.7(12) . .
C63 Yb3 N7 C61 -13.6(7) . .
C50 Yb3 N7 C61 80.3(7) . .
C62 Yb3 N7 C61 139.5(9) . .
O28 Yb3 N7 C59 22.8(7) . .
O26 Yb3 N7 C59 94.2(8) . .
O31 Yb3 N7 C59 103.7(7) . .
O29 Yb3 N7 C59 -93.7(7) . .
O19 Yb3 N7 C59 -39.0(8) . .
O24 Yb3 N7 C59 -176.5(7) . .
N6 Yb3 N7 C59 -143.2(7) . .
C51 Yb3 N7 C59 128.8(8) . .
C63 Yb3 N7 C59 105.5(8) . .
C50 Yb3 N7 C59 -160.6(7) . .
C62 Yb3 N7 C59 -101.4(8) . .
O19 Yb4 N8 C66 93.9(8) . .
O35 Yb4 N8 C66 33.7(7) . .
O22 Yb4 N8 C66 -155.6(8) . .
O28 Yb4 N8 C66 130.7(8) . .
O20 Yb4 N8 C66 -18.7(8) . .
O33 Yb4 N8 C66 -77.1(7) . .
N5 Yb4 N8 C66 -109.7(8) . .
C68 Yb4 N8 C66 21.8(7) . .
C67 Yb4 N8 C66 -92.3(8) . .
C46 Yb4 N8 C66 -140.1(7) . .
Yb3 Yb4 N8 C66 111.5(7) . .
O19 Yb4 N8 C64 -27.8(11) . .
O35 Yb4 N8 C64 -88.0(8) . .
O22 Yb4 N8 C64 82.6(8) . .
O28 Yb4 N8 C64 9.0(8) . .
O20 Yb4 N8 C64 -140.4(8) . .
O33 Yb4 N8 C64 161.2(9) . .
N5 Yb4 N8 C64 128.6(8) . .
C68 Yb4 N8 C64 -99.9(9) . .
C67 Yb4 N8 C64 146.0(10) . .
C46 Yb4 N8 C64 98.2(8) . .
Yb3 Yb4 N8 C64 -10.2(9) . .
O19 Yb4 N8 C65 -153.1(7) . .
O35 Yb4 N8 C65 146.7(8) . .
O22 Yb4 N8 C65 -42.6(7) . .
O28 Yb4 N8 C65 -116.3(8) . .
O20 Yb4 N8 C65 94.3(8) . .
O33 Yb4 N8 C65 35.9(7) . .
N5 Yb4 N8 C65 3.3(10) . .
C68 Yb4 N8 C65 134.8(9) . .
C67 Yb4 N8 C65 20.7(7) . .
C46 Yb4 N8 C65 -27.1(8) . .
Yb3 Yb4 N8 C65 -135.5(7) . .
O10 Yb2 O8 C17 165.9(11) . .
O17 Yb2 O8 C17 44.1(14) . .
O16 Yb2 O8 C17 -114.9(11) . .
O1 Yb2 O8 C17 96.4(11) . .
O6 Yb2 O8 C17 -38.9(11) . .
N2 Yb2 O8 C17 19.2(10) . .
N4 Yb2 O8 C17 -119.1(11) . .
C34 Yb2 O8 C17 8(2) . .
C15 Yb2 O8 C17 -18.1(11) . .
Yb1 Yb2 O8 C17 130.9(11) . .
O10 Yb2 O8 Na11 -31.4(10) . .
O17 Yb2 O8 Na11 -153.2(9) . .
O16 Yb2 O8 Na11 47.9(10) . .
O1 Yb2 O8 Na11 -100.9(10) . .
O6 Yb2 O8 Na11 123.9(10) . .
N2 Yb2 O8 Na11 -178.1(11) . .
N4 Yb2 O8 Na11 43.6(12) . .
C34 Yb2 O8 Na11 171.2(12) . .
C17 Yb2 O8 Na11 162.7(18) . .
C15 Yb2 O8 Na11 144.6(10) . .
Yb1 Yb2 O8 Na11 -66.4(10) . .
C3 C2 C8 N1 110.1(15) . .
C1 C2 C8 N1 -71.2(17) . .
C9 N1 C8 C2 -174.1(12) . .
C11 N1 C8 C2 -47.6(16) . .
Yb1 N1 C8 C2 72.1(12) . .
C11 N1 C9 C10 154.9(12) . .
C8 N1 C9 C10 -80.5(14) . .
Yb1 N1 C9 C10 33.5(13) . .
O17 Yb2 O10 C18 -94.3(10) . .
O16 Yb2 O10 C18 37.6(10) . .
O1 Yb2 O10 C18 -159.7(10) . .
O8 Yb2 O10 C18 111.6(10) . .
O6 Yb2 O10 C18 3.0(14) . .
N2 Yb2 O10 C18 162.0(9) . .
N4 Yb2 O10 C18 -31.4(10) . .
C34 Yb2 O10 C18 -74.7(10) . .
C17 Yb2 O10 C18 116.4(10) . .
C15 Yb2 O10 C18 -42(3) . .
Yb1 Yb2 O10 C18 -171.1(12) . .
O17 Yb2 O10 Yb1 76.8(4) . .
O16 Yb2 O10 Yb1 -151.2(4) . .
O1 Yb2 O10 Yb1 11.4(3) . .
O8 Yb2 O10 Yb1 -77.2(4) . .
O6 Yb2 O10 Yb1 174.2(6) . .
N2 Yb2 O10 Yb1 -26.9(7) . .
N4 Yb2 O10 Yb1 139.8(4) . .
C34 Yb2 O10 Yb1 96.4(4) . .
C17 Yb2 O10 Yb1 -72.4(4) . .
C15 Yb2 O10 Yb1 130(2) . .
O1 Yb1 O10 C18 160.1(10) . .
O2 Yb1 O10 C18 44.7(9) . .
O4 Yb1 O10 C18 -169.1(8) . .
O13 Yb1 O10 C18 -110.8(9) . .
O12 Yb1 O10 C18 -7.4(11) . .
N3 Yb1 O10 C18 -43.6(9) . .
N1 Yb1 O10 C18 94.8(9) . .
C10 Yb1 O10 C18 51.8(9) . .
C29 Yb1 O10 C18 -91.3(9) . .
Yb2 Yb1 O10 C18 171.7(11) . .
O1 Yb1 O10 Yb2 -11.6(3) . .
O2 Yb1 O10 Yb2 -127.0(4) . .
O4 Yb1 O10 Yb2 19.2(7) . .
O13 Yb1 O10 Yb2 77.5(4) . .
O12 Yb1 O10 Yb2 -179.1(3) . .
N3 Yb1 O10 Yb2 144.7(4) . .
N1 Yb1 O10 Yb2 -76.9(5) . .
C10 Yb1 O10 Yb2 -120.0(4) . .
C29 Yb1 O10 Yb2 97.0(4) . .
C9 N1 C11 C12 -144.6(12) . .
C8 N1 C11 C12 92.3(13) . .
Yb1 N1 C11 C12 -25.3(13) . .
O1 Yb1 O12 C27 -164.6(9) . .
O2 Yb1 O12 C27 -62.0(9) . .
O10 Yb1 O12 C27 -11.2(11) . .
O4 Yb1 O12 C27 158.1(10) . .
O13 Yb1 O12 C27 87.7(9) . .
N3 Yb1 O12 C27 28.0(9) . .
N1 Yb1 O12 C27 -131.0(10) . .
C10 Yb1 O12 C27 -79.0(9) . .
C29 Yb1 O12 C27 75.0(9) . .
Yb2 Yb1 O12 C27 -14.2(19) . .
Yb1 O2 C10 O3 159.2(10) . .
Yb1 O2 C10 C9 -12.3(17) . .
N1 C9 C10 O2 -18.0(18) . .
N1 C9 C10 O3 170.2(12) . .
N1 C9 C10 Yb1 -25.4(10) . .
O1 Yb1 C10 O2 -90.2(11) . .
O10 Yb1 C10 O2 -21.5(10) . .
O4 Yb1 C10 O2 -176.5(10) . .
O13 Yb1 C10 O2 69.0(16) . .
O12 Yb1 C10 O2 118.0(11) . .
N3 Yb1 C10 O2 56.7(11) . .
N1 Yb1 C10 O2 -151.3(12) . .
C29 Yb1 C10 O2 71.5(12) . .
Yb2 Yb1 C10 O2 -52.8(11) . .
O1 Yb1 C10 O3 -135(2) . .
O2 Yb1 C10 O3 -44(2) . .
O10 Yb1 C10 O3 -66(2) . .
O4 Yb1 C10 O3 139(2) . .
O13 Yb1 C10 O3 24(3) . .
O12 Yb1 C10 O3 74(2) . .
N3 Yb1 C10 O3 12(2) . .
N1 Yb1 C10 O3 164(3) . .
C29 Yb1 C10 O3 27(3) . .
Yb2 Yb1 C10 O3 -97(2) . .
O1 Yb1 C10 C9 78.7(8) . .
O2 Yb1 C10 C9 169.0(16) . .
O10 Yb1 C10 C9 147.5(8) . .
O4 Yb1 C10 C9 -7.5(9) . .
O13 Yb1 C10 C9 -122.1(12) . .
O12 Yb1 C10 C9 -73.0(8) . .
N3 Yb1 C10 C9 -134.3(8) . .
N1 Yb1 C10 C9 17.7(7) . .
C29 Yb1 C10 C9 -119.6(8) . .
Yb2 Yb1 C10 C9 116.2(7) . .
Yb1 O4 C12 O5 168.3(10) . .
Yb1 O4 C12 C11 -15.0(16) . .
N1 C11 C12 O5 -155.7(12) . .
N1 C11 C12 O4 27.5(17) . .
O1 Yb1 O13 C29 164.7(10) . .
O2 Yb1 O13 C29 41.9(13) . .
O10 Yb1 O13 C29 95.2(10) . .
O4 Yb1 O13 C29 -116.1(10) . .
O12 Yb1 O13 C29 -40.9(10) . .
N3 Yb1 O13 C29 17.7(9) . .
N1 Yb1 O13 C29 -122.0(10) . .
C10 Yb1 O13 C29 4.5(17) . .
Yb2 Yb1 O13 C29 129.6(10) . .
C16 N2 C13 C6 174.2(10) . .
C14 N2 C13 C6 -67.5(14) . .
Yb2 N2 C13 C6 56.1(12) . .
C1 C6 C13 N2 -64.5(16) . .
C5 C6 C13 N2 117.1(13) . .
C13 N2 C14 C15 169.9(11) . .
C16 N2 C14 C15 -72.1(14) . .
Yb2 N2 C14 C15 41.5(13) . .
O10 Yb2 O16 C32 -90.4(11) . .
O17 Yb2 O16 C32 11.8(13) . .
O1 Yb2 O16 C32 -119.0(11) . .
O8 Yb2 O16 C32 177.7(12) . .
O6 Yb2 O16 C32 75.0(11) . .
N2 Yb2 O16 C32 128.2(11) . .
N4 Yb2 O16 C32 -5.1(11) . .
C34 Yb2 O16 C32 12.5(12) . .
C17 Yb2 O16 C32 160.3(12) . .
C15 Yb2 O16 C32 80.8(11) . .
Yb1 Yb2 O16 C32 -107.8(11) . .
C13 N2 C16 C17 -76.5(12) . .
C14 N2 C16 C17 161.5(10) . .
Yb2 N2 C16 C17 47.7(11) . .
Na1 O7 C15 O6 21.4(14) 2_567 .
Na1 O7 C15 C14 -155.6(13) 2_567 .
Na1 O7 C15 Yb2 50(3) 2_567 .
Yb2 O6 C15 O7 162.2(10) . .
Na1 O6 C15 O7 -22.5(14) 2_567 .
Yb2 O6 C15 C14 -20.7(17) . .
Na1 O6 C15 C14 154.6(12) 2_567 .
Yb2 O6 C15 Na1 -175.3(8) . 2_567
Na1 O6 C15 Yb2 175.3(8) 2_567 .
N2 C14 C15 O7 159.6(13) . .
N2 C14 C15 O6 -17.5(18) . .
N2 C14 C15 Na1 63(3) . 2_567
N2 C14 C15 Yb2 -30.7(9) . .
O10 Yb2 C15 O7 21(5) . .
O17 Yb2 C15 O7 76(3) . .
O16 Yb2 C15 O7 -57(3) . .
O1 Yb2 C15 O7 135(3) . .
O8 Yb2 C15 O7 -132(3) . .
O6 Yb2 C15 O7 -41(2) . .
N2 Yb2 C15 O7 -180(3) . .
N4 Yb2 C15 O7 11(3) . .
C34 Yb2 C15 O7 56(3) . .
C17 Yb2 C15 O7 -138(3) . .
Yb1 Yb2 C15 O7 139(2) . .
O10 Yb2 C15 O6 61(3) . .
O17 Yb2 C15 O6 116.4(10) . .
O16 Yb2 C15 O6 -16.5(10) . .
O1 Yb2 C15 O6 176.1(9) . .
O8 Yb2 C15 O6 -91.6(10) . .
N2 Yb2 C15 O6 -139.0(12) . .
N4 Yb2 C15 O6 51.1(10) . .
C34 Yb2 C15 O6 96.2(10) . .
C17 Yb2 C15 O6 -97.6(10) . .
Yb1 Yb2 C15 O6 179.5(7) . .
O10 Yb2 C15 C14 -137(2) . .
O17 Yb2 C15 C14 -81.8(8) . .
O16 Yb2 C15 C14 145.3(8) . .
O1 Yb2 C15 C14 -22.1(9) . .
O8 Yb2 C15 C14 70.2(9) . .
O6 Yb2 C15 C14 161.8(15) . .
N2 Yb2 C15 C14 22.8(8) . .
N4 Yb2 C15 C14 -147.1(9) . .
C34 Yb2 C15 C14 -102.0(9) . .
C17 Yb2 C15 C14 64.2(8) . .
Yb1 Yb2 C15 C14 -18.8(11) . .
O10 Yb2 C15 Na1 65(2) . 2_567
O17 Yb2 C15 Na1 120.5(5) . 2_567
O16 Yb2 C15 Na1 -12.4(4) . 2_567
O1 Yb2 C15 Na1 -179.8(3) . 2_567
O8 Yb2 C15 Na1 -87.5(4) . 2_567
O6 Yb2 C15 Na1 4.1(7) . 2_567
N2 Yb2 C15 Na1 -134.9(7) . 2_567
N4 Yb2 C15 Na1 55.2(4) . 2_567
C34 Yb2 C15 Na1 100.3(5) . 2_567
C17 Yb2 C15 Na1 -93.5(4) . 2_567
Yb1 Yb2 C15 Na1 -176.45(15) . 2_567
O10 Yb2 O17 C34 92.3(11) . .
O16 Yb2 O17 C34 2.0(12) . .
O1 Yb2 O17 C34 154.7(11) . .
O8 Yb2 O17 C34 -149.9(10) . .
O6 Yb2 O17 C34 -61.5(10) . .
N2 Yb2 O17 C34 -127.1(11) . .
N4 Yb2 O17 C34 19.0(10) . .
C17 Yb2 O17 C34 -131.1(10) . .
C15 Yb2 O17 C34 -80.1(11) . .
Yb1 Yb2 O17 C34 127.0(10) . .
Na10 O9 C17 O8 -59.1(17) . .
Na11 O9 C17 O8 -6.4(17) . .
Na10 O9 C17 C16 115.6(12) . .
Na11 O9 C17 C16 168.3(11) . .
Na10 O9 C17 Na11 -52.7(6) . .
Na10 O9 C17 Yb2 -52(4) . .
Na11 O9 C17 Yb2 0(4) . .
Yb2 O8 C17 O9 176.6(11) . .
Na11 O8 C17 O9 5.6(15) . .
Yb2 O8 C17 C16 1.9(18) . .
Na11 O8 C17 C16 -169.1(12) . .
Yb2 O8 C17 Na11 171.0(9) . .
Na11 O8 C17 Yb2 -171.0(9) . .
N2 C16 C17 O9 148.6(13) . .
N2 C16 C17 O8 -36.4(17) . .
N2 C16 C17 Na11 -154(5) . .
N2 C16 C17 Yb2 -35.3(8) . .
O10 Yb2 C17 O9 -24(3) . .
O17 Yb2 C17 O9 -160(3) . .
O16 Yb2 C17 O9 53(3) . .
O1 Yb2 C17 O9 -92(3) . .
O8 Yb2 C17 O9 -9(3) . .
O6 Yb2 C17 O9 133(3) . .
N2 Yb2 C17 O9 -165(4) . .
N4 Yb2 C17 O9 78(3) . .
C34 Yb2 C17 O9 175(3) . .
C15 Yb2 C17 O9 153(3) . .
Yb1 Yb2 C17 O9 -58(3) . .
O10 Yb2 C17 O8 -14.8(11) . .
O17 Yb2 C17 O8 -150.9(10) . .
O16 Yb2 C17 O8 61.6(11) . .
O1 Yb2 C17 O8 -83.4(11) . .
O6 Yb2 C17 O8 141.5(11) . .
N2 Yb2 C17 O8 -156.3(13) . .
N4 Yb2 C17 O8 87.3(12) . .
C34 Yb2 C17 O8 -175.9(9) . .
C15 Yb2 C17 O8 161.9(11) . .
Yb1 Yb2 C17 O8 -48.6(11) . .
O10 Yb2 C17 C16 166.9(7) . .
O17 Yb2 C17 C16 30.8(10) . .
O16 Yb2 C17 C16 -116.7(8) . .
O1 Yb2 C17 C16 98.3(8) . .
O8 Yb2 C17 C16 -178.3(16) . .
O6 Yb2 C17 C16 -36.8(8) . .
N2 Yb2 C17 C16 25.4(7) . .
N4 Yb2 C17 C16 -91.0(10) . .
C34 Yb2 C17 C16 5.8(12) . .
C15 Yb2 C17 C16 -16.4(8) . .
Yb1 Yb2 C17 C16 133.1(8) . .
O10 Yb2 C17 Na11 -23.5(6) . .
O17 Yb2 C17 Na11 -159.7(5) . .
O16 Yb2 C17 Na11 52.8(5) . .
O1 Yb2 C17 Na11 -92.2(5) . .
O8 Yb2 C17 Na11 -8.8(9) . .
O6 Yb2 C17 Na11 132.7(6) . .
N2 Yb2 C17 Na11 -165.0(8) . .
N4 Yb2 C17 Na11 78.5(8) . .
C34 Yb2 C17 Na11 175.3(6) . .
C15 Yb2 C17 Na11 153.1(6) . .
Yb1 Yb2 C17 Na11 -57.3(5) . .
Yb2 O10 C18 C23 46.4(17) . .
Yb1 O10 C18 C23 -123.8(11) . .
Yb2 O10 C18 C19 -132.5(11) . .
Yb1 O10 C18 C19 57.4(16) . .
O35 Yb4 O19 C35 -113.5(10) . .
O22 Yb4 O19 C35 92.4(10) . .
O28 Yb4 O19 C35 155.4(11) . .
O20 Yb4 O19 C35 -39.1(10) . .
O33 Yb4 O19 C35 -6.3(15) . .
N5 Yb4 O19 C35 29.8(10) . .
N8 Yb4 O19 C35 -166.0(9) . .
C68 Yb4 O19 C35 -116.6(10) . .
C67 Yb4 O19 C35 47(2) . .
C46 Yb4 O19 C35 72.2(10) . .
Yb3 Yb4 O19 C35 163.9(12) . .
O35 Yb4 O19 Yb3 82.6(4) . .
O22 Yb4 O19 Yb3 -71.5(4) . .
O28 Yb4 O19 Yb3 -8.5(3) . .
O20 Yb4 O19 Yb3 157.0(4) . .
O33 Yb4 O19 Yb3 -170.2(6) . .
N5 Yb4 O19 Yb3 -134.2(4) . .
N8 Yb4 O19 Yb3 30.0(7) . .
C68 Yb4 O19 Yb3 79.5(4) . .
C67 Yb4 O19 Yb3 -116.9(19) . .
C46 Yb4 O19 Yb3 -91.8(4) . .
O28 Yb3 O19 C35 -156.3(10) . .
O26 Yb3 O19 C35 118.6(9) . .
O31 Yb3 O19 C35 177.2(8) . .
O29 Yb3 O19 C35 -36.5(9) . .
O24 Yb3 O19 C35 16.0(11) . .
N6 Yb3 O19 C35 48.8(9) . .
N7 Yb3 O19 C35 -87.4(9) . .
C51 Yb3 O19 C35 98.4(9) . .
C63 Yb3 O19 C35 -149.4(9) . .
C50 Yb3 O19 C35 19.2(10) . .
C62 Yb3 O19 C35 -45.1(9) . .
O28 Yb3 O19 Yb4 8.9(3) . .
O26 Yb3 O19 Yb4 -76.3(4) . .
O31 Yb3 O19 Yb4 -17.6(7) . .
O29 Yb3 O19 Yb4 128.7(4) . .
O24 Yb3 O19 Yb4 -178.9(4) . .
N6 Yb3 O19 Yb4 -146.0(4) . .
N7 Yb3 O19 Yb4 77.7(4) . .
C51 Yb3 O19 Yb4 -96.4(4) . .
C63 Yb3 O19 Yb4 15.7(8) . .
C50 Yb3 O19 Yb4 -175.7(4) . .
C62 Yb3 O19 Yb4 120.1(4) . .
C23 C18 C19 C20 0(2) . .
O10 C18 C19 C20 179.1(13) . .
C23 C18 C19 C25 -178.3(12) . .
O10 C18 C19 C25 1(2) . .
O19 Yb4 O20 C45 92.0(10) . .
O35 Yb4 O20 C45 -175.7(10) . .
O22 Yb4 O20 C45 -13.5(11) . .
O28 Yb4 O20 C45 117.1(10) . .
O33 Yb4 O20 C45 -74.8(10) . .
N5 Yb4 O20 C45 6.4(9) . .
N8 Yb4 O20 C45 -127.0(10) . .
C68 Yb4 O20 C45 -156.6(10) . .
C67 Yb4 O20 C45 -79.2(10) . .
C46 Yb4 O20 C45 -14.2(11) . .
Yb3 Yb4 O20 C45 106.4(10) . .
C18 C19 C20 C21 -4(2) . .
C25 C19 C20 C21 174.8(13) . .
C19 C20 C21 C22 5(2) . .
C19 C20 C21 C24 178.9(13) . .
O19 Yb4 O22 C46 -95.3(10) . .
O35 Yb4 O22 C46 143.0(9) . .
O28 Yb4 O22 C46 -156.0(10) . .
O20 Yb4 O22 C46 -2.0(11) . .
O33 Yb4 O22 C46 60.0(9) . .
N5 Yb4 O22 C46 -22.1(9) . .
N8 Yb4 O22 C46 126.1(10) . .
C68 Yb4 O22 C46 123.5(9) . .
C67 Yb4 O22 C46 78.0(10) . .
Yb3 Yb4 O22 C46 -129.1(9) . .
C20 C21 C22 C23 -4(2) . .
C24 C21 C22 C23 -177.2(13) . .
O10 C18 C23 C22 -177.5(12) . .
C19 C18 C23 C22 1(2) . .
O10 C18 C23 C30 5(2) . .
C19 C18 C23 C30 -176.1(13) . .
C21 C22 C23 C18 0(2) . .
C21 C22 C23 C30 177.7(14) . .
O28 Yb3 O24 C50 172.6(9) . .
O26 Yb3 O24 C50 -89.5(10) . .
O31 Yb3 O24 C50 -161.0(11) . .
O29 Yb3 O24 C50 59.6(10) . .
O19 Yb3 O24 C50 8.2(12) . .
N6 Yb3 O24 C50 -27.2(10) . .
N7 Yb3 O24 C50 128.1(11) . .
C51 Yb3 O24 C50 -74.9(10) . .
C63 Yb3 O24 C50 -179.5(11) . .
C62 Yb3 O24 C50 76.8(10) . .
C28 N3 C25 C19 172.3(10) . .
C26 N3 C25 C19 -67.3(13) . .
Yb1 N3 C25 C19 55.6(12) . .
C20 C19 C25 N3 120.4(14) . .
C18 C19 C25 N3 -61.0(16) . .
O28 Yb3 O26 C51 -160.9(10) . .
O31 Yb3 O26 C51 119.0(10) . .
O29 Yb3 O26 C51 -37.3(13) . .
O19 Yb3 O26 C51 -91.0(10) . .
O24 Yb3 O26 C51 46.9(10) . .
N6 Yb3 O26 C51 -13.1(9) . .
N7 Yb3 O26 C51 128.1(9) . .
C63 Yb3 O26 C51 119.4(10) . .
C50 Yb3 O26 C51 26.3(10) . .
C62 Yb3 O26 C51 -5.2(17) . .
O28 Yb3 O26 Na8 30.8(6) . .
O31 Yb3 O26 Na8 -49.2(6) . .
O29 Yb3 O26 Na8 154.4(6) . .
O19 Yb3 O26 Na8 100.7(6) . .
O24 Yb3 O26 Na8 -121.3(6) . .
N6 Yb3 O26 Na8 178.7(7) . .
N7 Yb3 O26 Na8 -40.2(9) . .
C51 Yb3 O26 Na8 -168.3(14) . .
C63 Yb3 O26 Na8 -48.9(7) . .
C50 Yb3 O26 Na8 -142.0(6) . .
C62 Yb3 O26 Na8 -173.5(9) . .
C28 N3 C26 C27 -68.3(13) . .
C25 N3 C26 C27 174.3(10) . .
Yb1 N3 C26 C27 45.3(11) . .
C25 N3 C28 C29 -79.1(12) . .
C26 N3 C28 C29 160.1(11) . .
Yb1 N3 C28 C29 45.7(12) . .
O26 Yb3 O28 C52 -113.8(9) . .
O31 Yb3 O28 C52 -38.1(9) . .
O29 Yb3 O28 C52 93.0(9) . .
O19 Yb3 O28 C52 156.9(10) . .
O24 Yb3 O28 C52 -12.0(13) . .
N6 Yb3 O28 C52 -163.6(9) . .
N7 Yb3 O28 C52 31.3(9) . .
C51 Yb3 O28 C52 -120.4(9) . .
C63 Yb3 O28 C52 -19.6(9) . .
C50 Yb3 O28 C52 6(3) . .
C62 Yb3 O28 C52 73.3(10) . .
O26 Yb3 O28 Yb4 80.7(4) . .
O31 Yb3 O28 Yb4 156.5(4) . .
O29 Yb3 O28 Yb4 -72.5(4) . .
O19 Yb3 O28 Yb4 -8.6(3) . .
O24 Yb3 O28 Yb4 -177.5(5) . .
N6 Yb3 O28 Yb4 30.9(7) . .
N7 Yb3 O28 Yb4 -134.1(4) . .
C51 Yb3 O28 Yb4 74.1(4) . .
C63 Yb3 O28 Yb4 174.9(4) . .
C50 Yb3 O28 Yb4 -159(2) . .
C62 Yb3 O28 Yb4 -92.2(4) . .
O19 Yb4 O28 C52 -157.3(10) . .
O35 Yb4 O28 C52 113.4(9) . .
O22 Yb4 O28 C52 -39.9(9) . .
O20 Yb4 O28 C52 176.1(8) . .
O33 Yb4 O28 C52 12.4(11) . .
N5 Yb4 O28 C52 -89.5(9) . .
N8 Yb4 O28 C52 48.2(9) . .
C68 Yb4 O28 C52 93.8(9) . .
C67 Yb4 O28 C52 13.7(10) . .
C46 Yb4 O28 C52 -47.6(9) . .
Yb3 Yb4 O28 C52 -166.2(11) . .
O19 Yb4 O28 Yb3 8.9(3) . .
O35 Yb4 O28 Yb3 -80.4(4) . .
O22 Yb4 O28 Yb3 126.3(4) . .
O20 Yb4 O28 Yb3 -17.7(7) . .
O33 Yb4 O28 Yb3 178.6(3) . .
N5 Yb4 O28 Yb3 76.7(4) . .
N8 Yb4 O28 Yb3 -145.6(4) . .
C68 Yb4 O28 Yb3 -100.0(4) . .
C67 Yb4 O28 Yb3 179.9(4) . .
C46 Yb4 O28 Yb3 118.6(4) . .
Na2 O11 C27 O12 21.4(19) . .
Na2 O11 C27 C26 -159.9(8) . .
Yb1 O12 C27 O11 167.7(10) . .
Yb1 O12 C27 C26 -11.0(15) . .
N3 C26 C27 O11 155.3(11) . .
N3 C26 C27 O12 -25.9(15) . .
O28 Yb3 O29 C62 -91.0(10) . .
O26 Yb3 O29 C62 151.7(9) . .
O31 Yb3 O29 C62 3.2(11) . .
O19 Yb3 O29 C62 -151.7(10) . .
O24 Yb3 O29 C62 61.4(9) . .
N6 Yb3 O29 C62 128.9(10) . .
N7 Yb3 O29 C62 -18.8(9) . .
C51 Yb3 O29 C62 135.3(9) . .
C63 Yb3 O29 C62 -2.6(10) . .
C50 Yb3 O29 C62 80.2(10) . .
Na3 O14 C29 O13 -61.7(16) . .
Na11 O14 C29 O13 56.4(16) . .
Na3 O14 C29 C28 122.4(11) . .
Na11 O14 C29 C28 -119.5(12) . .
Na11 O14 C29 Na3 118.0(10) . .
Na3 O14 C29 Yb1 -75(3) . .
Na11 O14 C29 Yb1 43(3) . .
Yb1 O13 C29 O14 -173.4(9) . .
Yb1 O13 C29 C28 2.6(16) . .
Yb1 O13 C29 Na3 149.7(5) . .
N3 C28 C29 O14 140.8(12) . .
N3 C28 C29 O13 -35.4(16) . .
N3 C28 C29 Na3 -168.4(9) . .
N3 C28 C29 Yb1 -33.7(9) . .
O1 Yb1 C29 O14 1(3) . .
O2 Yb1 C29 O14 -135(3) . .
O10 Yb1 C29 O14 -67(3) . .
O4 Yb1 C29 O14 78(3) . .
O13 Yb1 C29 O14 18(2) . .
O12 Yb1 C29 O14 157(3) . .
N3 Yb1 C29 O14 -141(3) . .
N1 Yb1 C29 O14 103(3) . .
C10 Yb1 C29 O14 -160(3) . .
Yb2 Yb1 C29 O14 -32(3) . .
O1 Yb1 C29 O13 -16.1(10) . .
O2 Yb1 C29 O13 -152.5(9) . .
O10 Yb1 C29 O13 -84.7(10) . .
O4 Yb1 C29 O13 60.1(10) . .
O12 Yb1 C29 O13 139.7(10) . .
N3 Yb1 C29 O13 -158.2(12) . .
N1 Yb1 C29 O13 85.2(12) . .
C10 Yb1 C29 O13 -177.8(9) . .
Yb2 Yb1 C29 O13 -50.0(10) . .
O1 Yb1 C29 C28 166.3(7) . .
O2 Yb1 C29 C28 29.8(9) . .
O10 Yb1 C29 C28 97.6(7) . .
O4 Yb1 C29 C28 -117.5(8) . .
O13 Yb1 C29 C28 -177.6(14) . .
O12 Yb1 C29 C28 -37.9(7) . .
N3 Yb1 C29 C28 24.2(7) . .
N1 Yb1 C29 C28 -92.4(9) . .
C10 Yb1 C29 C28 4.6(10) . .
Yb2 Yb1 C29 C28 132.4(7) . .
O1 Yb1 C29 Na3 -56.8(7) . .
O2 Yb1 C29 Na3 166.8(5) . .
O10 Yb1 C29 Na3 -125.4(6) . .
O4 Yb1 C29 Na3 19.4(6) . .
O13 Yb1 C29 Na3 -40.7(8) . .
O12 Yb1 C29 Na3 99.0(6) . .
N3 Yb1 C29 Na3 161.1(8) . .
N1 Yb1 C29 Na3 44.5(10) . .
C10 Yb1 C29 Na3 141.6(6) . .
Yb2 Yb1 C29 Na3 -90.7(6) . .
C31 N4 C30 C23 -48.1(15) . .
C33 N4 C30 C23 -171.9(11) . .
Yb2 N4 C30 C23 72.2(11) . .
C18 C23 C30 N4 -74.9(17) . .
C22 C23 C30 N4 107.7(15) . .
O28 Yb3 O31 C63 91.5(10) . .
O26 Yb3 O31 C63 178.8(10) . .
O29 Yb3 O31 C63 -17.1(11) . .
O19 Yb3 O31 C63 116.7(10) . .
O24 Yb3 O31 C63 -76.2(10) . .
N6 Yb3 O31 C63 -126.8(9) . .
N7 Yb3 O31 C63 4.6(9) . .
C51 Yb3 O31 C63 -163.6(10) . .
C50 Yb3 O31 C63 -82.8(10) . .
C62 Yb3 O31 C63 -16.0(10) . .
O28 Yb3 O31 Na7 -124.0(5) . .
O26 Yb3 O31 Na7 -36.7(4) . .
O29 Yb3 O31 Na7 127.4(5) . .
O19 Yb3 O31 Na7 -98.8(6) . .
O24 Yb3 O31 Na7 68.3(5) . .
N6 Yb3 O31 Na7 17.6(6) . .
N7 Yb3 O31 Na7 149.1(5) . .
C51 Yb3 O31 Na7 -19.2(5) . .
C63 Yb3 O31 Na7 144.5(12) . .
C50 Yb3 O31 Na7 61.7(5) . .
C62 Yb3 O31 Na7 128.5(4) . .
C33 N4 C31 C32 -145.3(12) . .
C30 N4 C31 C32 93.1(13) . .
Yb2 N4 C31 C32 -23.1(14) . .
C31 N4 C33 C34 157.3(11) . .
C30 N4 C33 C34 -79.3(13) . .
Yb2 N4 C33 C34 33.8(13) . .
O19 Yb4 O33 C67 159.6(9) . .
O35 Yb4 O33 C67 -94.8(10) . .
O22 Yb4 O33 C67 54.3(10) . .
O28 Yb4 O33 C67 3.5(11) . .
O20 Yb4 O33 C67 -167.4(10) . .
N5 Yb4 O33 C67 123.0(10) . .
N8 Yb4 O33 C67 -35.2(9) . .
C68 Yb4 O33 C67 -84.2(10) . .
C46 Yb4 O33 C67 72.2(10) . .
Yb3 Yb4 O33 C67 7.3(18) . .
O19 Yb4 O33 Na2 -23.8(13) . 1_566
O35 Yb4 O33 Na2 81.8(8) . 1_566
O22 Yb4 O33 Na2 -129.1(8) . 1_566
O28 Yb4 O33 Na2 -179.9(6) . 1_566
O20 Yb4 O33 Na2 9.1(7) . 1_566
N5 Yb4 O33 Na2 -60.4(8) . 1_566
N8 Yb4 O33 Na2 141.4(9) . 1_566
C68 Yb4 O33 Na2 92.4(8) . 1_566
C67 Yb4 O33 Na2 176.6(15) . 1_566
C46 Yb4 O33 Na2 -111.3(8) . 1_566
Yb3 Yb4 O33 Na2 -176.1(4) . 1_566
Yb2 O16 C32 O15 177.0(11) . .
Yb2 O16 C32 C31 -5.6(18) . .
N4 C31 C32 O15 -162.2(13) . .
N4 C31 C32 O16 20.2(18) . .
Yb2 O17 C34 O18 168.0(10) . .
Yb2 O17 C34 C33 -6.4(17) . .
Na8 O18 C34 O17 161.9(11) 2_567 .
Na8 O18 C34 C33 -23.6(16) 2_567 .
Na8 O18 C34 Yb2 -178(2) 2_567 .
N4 C33 C34 O17 -21.7(18) . .
N4 C33 C34 O18 163.5(12) . .
N4 C33 C34 Yb2 -25.5(10) . .
O10 Yb2 C34 O17 -93.1(11) . .
O16 Yb2 C34 O17 -178.4(10) . .
O1 Yb2 C34 O17 -24.2(11) . .
O8 Yb2 C34 O17 63.3(18) . .
O6 Yb2 C34 O17 113.8(11) . .
N2 Yb2 C34 O17 53.4(11) . .
N4 Yb2 C34 O17 -156.7(12) . .
C17 Yb2 C34 O17 68.2(13) . .
C15 Yb2 C34 O17 92.1(11) . .
Yb1 Yb2 C34 O17 -56.0(11) . .
O10 Yb2 C34 O18 -122(3) . .
O17 Yb2 C34 O18 -29(2) . .
O16 Yb2 C34 O18 153(3) . .
O1 Yb2 C34 O18 -53(3) . .
O8 Yb2 C34 O18 34(4) . .
O6 Yb2 C34 O18 85(3) . .
N2 Yb2 C34 O18 24(3) . .
N4 Yb2 C34 O18 174(3) . .
C17 Yb2 C34 O18 39(3) . .
C15 Yb2 C34 O18 63(3) . .
Yb1 Yb2 C34 O18 -85(3) . .
O10 Yb2 C34 C33 81.2(8) . .
O17 Yb2 C34 C33 174.3(15) . .
O16 Yb2 C34 C33 -4.1(8) . .
O1 Yb2 C34 C33 150.1(8) . .
O8 Yb2 C34 C33 -122.3(13) . .
O6 Yb2 C34 C33 -71.9(8) . .
N2 Yb2 C34 C33 -132.2(8) . .
N4 Yb2 C34 C33 17.6(7) . .
C17 Yb2 C34 C33 -117.5(8) . .
C15 Yb2 C34 C33 -93.5(8) . .
Yb1 Yb2 C34 C33 118.3(7) . .
O19 Yb4 O35 C68 -171.5(9) . .
O22 Yb4 O35 C68 -45.5(12) . .
O28 Yb4 O35 C68 -102.1(9) . .
O20 Yb4 O35 C68 108.4(9) . .
O33 Yb4 O35 C68 32.0(9) . .
N5 Yb4 O35 C68 111.6(10) . .
N8 Yb4 O35 C68 -27.1(9) . .
C67 Yb4 O35 C68 11.5(9) . .
C46 Yb4 O35 C68 -8.1(15) . .
Yb3 Yb4 O35 C68 -135.9(9) . .
Yb4 O19 C35 C40 137.1(10) . .
Yb3 O19 C35 C40 -60.6(14) . .
Yb4 O19 C35 C36 -44.1(16) . .
Yb3 O19 C35 C36 118.2(11) . .
O19 C35 C36 C37 179.3(12) . .
C40 C35 C36 C37 -2(2) . .
O19 C35 C36 C42 -5.4(19) . .
C40 C35 C36 C42 173.4(12) . .
C35 C36 C37 C38 -4(2) . .
C42 C36 C37 C38 -179.5(12) . .
C36 C37 C38 C39 6(2) . .
C36 C37 C38 C41 -177.0(12) . .
C37 C38 C39 C40 -2(2) . .
C41 C38 C39 C40 -179.1(12) . .
O19 C35 C40 C39 -175.4(11) . .
C36 C35 C40 C39 5.8(19) . .
O19 C35 C40 C47 -2.0(19) . .
C36 C35 C40 C47 179.3(12) . .
C38 C39 C40 C35 -4(2) . .
C38 C39 C40 C47 -177.3(12) . .
C44 N5 C42 C36 174.4(10) . .
C43 N5 C42 C36 52.6(14) . .
Yb4 N5 C42 C36 -68.4(10) . .
C37 C36 C42 N5 -113.6(13) . .
C35 C36 C42 N5 71.0(15) . .
C44 N5 C43 C45 143.4(11) . .
C42 N5 C43 C45 -96.3(12) . .
Yb4 N5 C43 C45 22.2(12) . .
C42 N5 C44 C46 84.3(12) . .
C43 N5 C44 C46 -154.0(11) . .
Yb4 N5 C44 C46 -31.5(12) . .
Na6 O21 C45 O20 153.1(10) 2_677 .
Na6 O21 C45 C43 -28.4(15) 2_677 .
Yb4 O20 C45 O21 -177.6(9) . .
Yb4 O20 C45 C43 3.8(16) . .
N5 C43 C45 O21 163.0(11) . .
N5 C43 C45 O20 -18.3(16) . .
Na9 O23 C46 O22 10.6(17) . .
Na9 O23 C46 C44 -163.1(9) . .
Na9 O23 C46 Yb4 -18(3) . .
Yb4 O22 C46 O23 -161.6(10) . .
Yb4 O22 C46 C44 12.1(16) . .
N5 C44 C46 O23 -169.7(11) . .
N5 C44 C46 O22 16.3(17) . .
N5 C44 C46 Yb4 23.5(9) . .
O19 Yb4 C46 O23 133(2) . .
O35 Yb4 C46 O23 -29(3) . .
O22 Yb4 C46 O23 42(2) . .
O28 Yb4 C46 O23 65(2) . .
O20 Yb4 C46 O23 -140(2) . .
O33 Yb4 C46 O23 -73(2) . .
N5 Yb4 C46 O23 -165(3) . .
N8 Yb4 C46 O23 -12(2) . .
C68 Yb4 C46 O23 -34(3) . .
C67 Yb4 C46 O23 -51(2) . .
Yb3 Yb4 C46 O23 96(2) . .
O19 Yb4 C46 O22 91.1(10) . .
O35 Yb4 C46 O22 -71.3(14) . .
O28 Yb4 C46 O22 22.8(10) . .
O20 Yb4 C46 O22 178.4(9) . .
O33 Yb4 C46 O22 -114.7(10) . .
N5 Yb4 C46 O22 152.9(11) . .
N8 Yb4 C46 O22 -53.9(10) . .
C68 Yb4 C46 O22 -75.7(11) . .
C67 Yb4 C46 O22 -93.0(10) . .
Yb3 Yb4 C46 O22 53.7(10) . .
O19 Yb4 C46 C44 -78.1(7) . .
O35 Yb4 C46 C44 119.5(10) . .
O22 Yb4 C46 C44 -169.2(14) . .
O28 Yb4 C46 C44 -146.4(7) . .
O20 Yb4 C46 C44 9.2(8) . .
O33 Yb4 C46 C44 76.1(7) . .
N5 Yb4 C46 C44 -16.3(7) . .
N8 Yb4 C46 C44 136.9(7) . .
C68 Yb4 C46 C44 115.1(7) . .
C67 Yb4 C46 C44 97.8(7) . .
Yb3 Yb4 C46 C44 -115.5(7) . .
C35 C40 C47 N6 65.2(16) . .
C39 C40 C47 N6 -121.5(13) . .
C48 N6 C47 C40 69.0(14) . .
C49 N6 C47 C40 -171.4(10) . .
Yb3 N6 C47 C40 -54.7(12) . .
C49 N6 C48 C50 72.7(14) . .
C47 N6 C48 C50 -169.4(11) . .
Yb3 N6 C48 C50 -41.4(13) . .
C48 N6 C49 C51 -156.4(10) . .
C47 N6 C49 C51 80.5(12) . .
Yb3 N6 C49 C51 -41.9(11) . .
Na1 O25 C50 O24 -21(2) 2_567 .
Na1 O25 C50 C48 162.1(10) 2_567 .
Na1 O25 C50 Yb3 -50(3) 2_567 .
Yb3 O24 C50 O25 -163.2(11) . .
Yb3 O24 C50 C48 13.6(17) . .
N6 C48 C50 O25 -161.1(13) . .
N6 C48 C50 O24 22.1(18) . .
N6 C48 C50 Yb3 30.7(10) . .
O28 Yb3 C50 O25 15(4) . .
O26 Yb3 C50 O25 134(3) . .
O31 Yb3 C50 O25 58(3) . .
O29 Yb3 C50 O25 -75(3) . .
O19 Yb3 C50 O25 -134(2) . .
O24 Yb3 C50 O25 40(2) . .
N6 Yb3 C50 O25 -174(3) . .
N7 Yb3 C50 O25 -10(3) . .
C51 Yb3 C50 O25 143(3) . .
C63 Yb3 C50 O25 40(3) . .
C62 Yb3 C50 O25 -55(3) . .
O28 Yb3 C50 O24 -25(3) . .
O26 Yb3 C50 O24 94.1(10) . .
O31 Yb3 C50 O24 18.5(10) . .
O29 Yb3 C50 O24 -114.9(11) . .
O19 Yb3 C50 O24 -173.8(9) . .
N6 Yb3 C50 O24 146.2(12) . .
N7 Yb3 C50 O24 -49.9(10) . .
C51 Yb3 C50 O24 103.0(10) . .
C63 Yb3 C50 O24 0.4(10) . .
C62 Yb3 C50 O24 -95.1(10) . .
O28 Yb3 C50 C48 167(2) . .
O26 Yb3 C50 C48 -73.6(8) . .
O31 Yb3 C50 C48 -149.2(8) . .
O29 Yb3 C50 C48 77.4(8) . .
O19 Yb3 C50 C48 18.5(9) . .
O24 Yb3 C50 C48 -167.7(15) . .
N6 Yb3 C50 C48 -21.5(7) . .
N7 Yb3 C50 C48 142.4(8) . .
C51 Yb3 C50 C48 -64.7(8) . .
C63 Yb3 C50 C48 -167.3(8) . .
C62 Yb3 C50 C48 97.2(8) . .
Yb3 O26 C51 O27 171.0(9) . .
Na8 O26 C51 O27 -17.2(14) . .
Yb3 O26 C51 C49 -7.2(16) . .
Na8 O26 C51 C49 164.6(10) . .
Na8 O26 C51 Yb3 171.8(10) . .
N6 C49 C51 O26 36.4(16) . .
N6 C49 C51 O27 -141.9(11) . .
N6 C49 C51 Yb3 31.8(8) . .
O28 Yb3 C51 O26 19.5(10) . .
O31 Yb3 C51 O26 -57.9(10) . .
O29 Yb3 C51 O26 155.6(9) . .
O19 Yb3 C51 O26 88.2(10) . .
O24 Yb3 C51 O26 -133.9(10) . .
N6 Yb3 C51 O26 164.0(11) . .
N7 Yb3 C51 O26 -81.3(12) . .
C63 Yb3 C51 O26 -63.1(10) . .
C50 Yb3 C51 O26 -153.8(10) . .
C62 Yb3 C51 O26 177.5(8) . .
O28 Yb3 C51 O27 -4(3) . .
O26 Yb3 C51 O27 -23(2) . .
O31 Yb3 C51 O27 -81(3) . .
O29 Yb3 C51 O27 132(3) . .
O19 Yb3 C51 O27 65(3) . .
O24 Yb3 C51 O27 -157(3) . .
N6 Yb3 C51 O27 141(3) . .
N7 Yb3 C51 O27 -105(3) . .
C63 Yb3 C51 O27 -86(3) . .
C50 Yb3 C51 O27 -177(3) . .
C62 Yb3 C51 O27 154(2) . .
O28 Yb3 C51 C49 -166.8(7) . .
O26 Yb3 C51 C49 173.7(14) . .
O31 Yb3 C51 C49 115.7(7) . .
O29 Yb3 C51 C49 -30.7(9) . .
O19 Yb3 C51 C49 -98.2(7) . .
O24 Yb3 C51 C49 39.7(7) . .
N6 Yb3 C51 C49 -22.4(6) . .
N7 Yb3 C51 C49 92.4(9) . .
C63 Yb3 C51 C49 110.6(7) . .
C50 Yb3 C51 C49 19.9(7) . .
C62 Yb3 C51 C49 -8.8(10) . .
Yb3 O28 C52 C57 134.2(10) . .
Yb4 O28 C52 C57 -61.9(13) . .
Yb3 O28 C52 C53 -48.2(15) . .
Yb4 O28 C52 C53 115.7(10) . .
O28 C52 C53 C54 -179.4(11) . .
C57 C52 C53 C54 -1.9(18) . .
O28 C52 C53 C59 -1.2(17) . .
C57 C52 C53 C59 176.4(11) . .
C52 C53 C54 C55 3.0(18) . .
C59 C53 C54 C55 -175.2(11) . .
C53 C54 C55 C56 -3.0(18) . .
C53 C54 C55 C58 177.8(11) . .
C54 C55 C56 C57 1.8(19) . .
C58 C55 C56 C57 -179.1(11) . .
C55 C56 C57 C52 -0.7(18) . .
C55 C56 C57 C64 178.2(12) . .
O28 C52 C57 C56 178.3(11) . .
C53 C52 C57 C56 0.7(18) . .
O28 C52 C57 C64 -0.7(17) . .
C53 C52 C57 C64 -178.2(11) . .
C60 N7 C59 C53 174.5(10) . .
C61 N7 C59 C53 49.4(14) . .
Yb3 N7 C59 C53 -68.7(10) . .
C54 C53 C59 N7 -112.4(13) . .
C52 C53 C59 N7 69.4(15) . .
C61 N7 C60 C62 -150.7(11) . .
C59 N7 C60 C62 85.4(13) . .
Yb3 N7 C60 C62 -29.5(12) . .
C60 N7 C61 C63 145.3(11) . .
C59 N7 C61 C63 -91.5(12) . .
Yb3 N7 C61 C63 24.3(11) . .
Na6 O30 C62 O29 -158.6(9) . .
Na5 O30 C62 O29 26.0(14) . .
Na6 O30 C62 C60 27.0(16) . .
Na5 O30 C62 C60 -148.5(10) . .
Na6 O30 C62 Yb3 -179.1(15) . .
Na5 O30 C62 Yb3 5(2) . .
Yb3 O29 C62 O30 -166.0(9) . .
Yb3 O29 C62 C60 8.7(15) . .
N7 C60 C62 O30 -168.2(11) . .
N7 C60 C62 O29 17.0(16) . .
N7 C60 C62 Yb3 22.1(9) . .
O28 Yb3 C62 O30 127(2) . .
O26 Yb3 C62 O30 -28(3) . .
O31 Yb3 C62 O30 -147(2) . .
O29 Yb3 C62 O30 30.5(18) . .
O19 Yb3 C62 O30 58(2) . .
O24 Yb3 C62 O30 -83(2) . .
N6 Yb3 C62 O30 -20(2) . .
N7 Yb3 C62 O30 -172(2) . .
C51 Yb3 C62 O30 -31(2) . .
C63 Yb3 C62 O30 -152(2) . .
C50 Yb3 C62 O30 -62(2) . .
O28 Yb3 C62 O29 96.1(10) . .
O26 Yb3 C62 O29 -58.0(16) . .
O31 Yb3 C62 O29 -177.4(9) . .
O19 Yb3 C62 O29 27.2(9) . .
O24 Yb3 C62 O29 -113.9(10) . .
N6 Yb3 C62 O29 -50.7(10) . .
N7 Yb3 C62 O29 157.1(11) . .
C51 Yb3 C62 O29 -61.1(11) . .
C63 Yb3 C62 O29 177.6(9) . .
C50 Yb3 C62 O29 -92.2(10) . .
O28 Yb3 C62 C60 -76.1(7) . .
O26 Yb3 C62 C60 129.8(11) . .
O31 Yb3 C62 C60 10.4(8) . .
O29 Yb3 C62 C60 -172.2(14) . .
O19 Yb3 C62 C60 -144.9(7) . .
O24 Yb3 C62 C60 74.0(7) . .
N6 Yb3 C62 C60 137.1(7) . .
N7 Yb3 C62 C60 -15.1(6) . .
C51 Yb3 C62 C60 126.8(7) . .
C63 Yb3 C62 C60 5.5(7) . .
C50 Yb3 C62 C60 95.7(7) . .
Yb3 O31 C63 O32 -179.7(9) . .
Na7 O31 C63 O32 34.3(15) . .
Yb3 O31 C63 C61 7.6(15) . .
Na7 O31 C63 C61 -138.5(9) . .
Na7 O31 C63 Yb3 -146.1(10) . .
Na1 O32 C63 O31 -114.2(16) . .
Na1 O32 C63 C61 59(2) . .
Na1 O32 C63 Yb3 -115(3) . .
N7 C61 C63 O31 -22.8(15) . .
N7 C61 C63 O32 163.8(10) . .
N7 C61 C63 Yb3 -18.3(9) . .
O28 Yb3 C63 O31 -85.1(10) . .
O26 Yb3 C63 O31 -1.2(10) . .
O29 Yb3 C63 O31 166.1(9) . .
O19 Yb3 C63 O31 -91.7(11) . .
O24 Yb3 C63 O31 98.6(10) . .
N6 Yb3 C63 O31 64.5(11) . .
N7 Yb3 C63 O31 -174.4(11) . .
C51 Yb3 C63 O31 16.7(10) . .
C50 Yb3 C63 O31 98.5(10) . .
C62 Yb3 C63 O31 165.3(10) . .
O28 Yb3 C63 O32 -84(3) . .
O26 Yb3 C63 O32 0(3) . .
O31 Yb3 C63 O32 1(2) . .
O29 Yb3 C63 O32 167(3) . .
O19 Yb3 C63 O32 -91(3) . .
O24 Yb3 C63 O32 100(3) . .
N6 Yb3 C63 O32 65(3) . .
N7 Yb3 C63 O32 -174(3) . .
C51 Yb3 C63 O32 18(3) . .
C50 Yb3 C63 O32 99(3) . .
C62 Yb3 C63 O32 166(3) . .
O28 Yb3 C63 C61 101.8(7) . .
O26 Yb3 C63 C61 -174.3(7) . .
O31 Yb3 C63 C61 -173.1(14) . .
O29 Yb3 C63 C61 -7.0(7) . .
O19 Yb3 C63 C61 95.2(8) . .
O24 Yb3 C63 C61 -74.5(7) . .
N6 Yb3 C63 C61 -108.6(7) . .
N7 Yb3 C63 C61 12.4(6) . .
C51 Yb3 C63 C61 -156.4(7) . .
C50 Yb3 C63 C61 -74.7(7) . .
C62 Yb3 C63 C61 -7.8(7) . .
C66 N8 C64 C57 -179.0(10) . .
C65 N8 C64 C57 60.3(14) . .
Yb4 N8 C64 C57 -59.8(12) . .
C56 C57 C64 N8 -111.5(13) . .
C52 C57 C64 N8 67.4(15) . .
C66 N8 C65 C67 74.0(13) . .
C64 N8 C65 C67 -163.4(11) . .
Yb4 N8 C65 C67 -38.4(12) . .
C64 N8 C66 C68 85.5(12) . .
C65 N8 C66 C68 -149.7(10) . .
Yb4 N8 C66 C68 -38.2(11) . .
Na3 O34 C67 O33 41(3) 2_677 .
Na2 O34 C67 O33 -23.8(13) 1_566 .
Na3 O34 C67 C65 -141.2(13) 2_677 .
Na2 O34 C67 C65 154.0(12) 1_566 .
Na3 O34 C67 Na2 64.7(16) 2_677 1_566
Na3 O34 C67 Yb4 3(4) 2_677 .
Na2 O34 C67 Yb4 -62(2) 1_566 .
Yb4 O33 C67 O34 -156.0(10) . .
Na2 O33 C67 O34 25.9(14) 1_566 .
Yb4 O33 C67 C65 26.1(16) . .
Na2 O33 C67 C65 -152.0(11) 1_566 .
Yb4 O33 C67 Na2 178.1(8) . 1_566
Na2 O33 C67 Yb4 -178.1(8) 1_566 .
N8 C65 C67 O34 -165.0(12) . .
N8 C65 C67 O33 12.9(18) . .
N8 C65 C67 Na2 -61(2) . 1_566
N8 C65 C67 Yb4 29.5(10) . .
O19 Yb4 C67 O34 -18(4) . .
O35 Yb4 C67 O34 143(2) . .
O22 Yb4 C67 O34 -65(2) . .
O28 Yb4 C67 O34 -123(2) . .
O20 Yb4 C67 O34 67(2) . .
O33 Yb4 C67 O34 55(2) . .
N5 Yb4 C67 O34 -1(2) . .
N8 Yb4 C67 O34 -169(2) . .
C68 Yb4 C67 O34 147(2) . .
C46 Yb4 C67 O34 -44(2) . .
Yb3 Yb4 C67 O34 -123(2) . .
O19 Yb4 C67 O33 -72(2) . .
O35 Yb4 C67 O33 88.1(10) . .
O22 Yb4 C67 O33 -120.0(10) . .
O28 Yb4 C67 O33 -177.2(9) . .
O20 Yb4 C67 O33 12.5(10) . .
N5 Yb4 C67 O33 -55.1(10) . .
N8 Yb4 C67 O33 136.5(11) . .
C68 Yb4 C67 O33 92.1(10) . .
C46 Yb4 C67 O33 -98.9(10) . .
Yb3 Yb4 C67 O33 -177.1(7) . .
O19 Yb4 C67 C65 131.2(19) . .
O35 Yb4 C67 C65 -68.5(8) . .
O22 Yb4 C67 C65 83.4(8) . .
O28 Yb4 C67 C65 26.2(9) . .
O20 Yb4 C67 C65 -144.1(8) . .
O33 Yb4 C67 C65 -156.6(15) . .
N5 Yb4 C67 C65 148.3(8) . .
N8 Yb4 C67 C65 -20.1(7) . .
C68 Yb4 C67 C65 -64.5(8) . .
C46 Yb4 C67 C65 104.5(8) . .
Yb3 Yb4 C67 C65 26.3(10) . .
O19 Yb4 C67 Na2 -74(2) . 1_566
O35 Yb4 C67 Na2 86.5(4) . 1_566
O22 Yb4 C67 Na2 -121.6(5) . 1_566
O28 Yb4 C67 Na2 -178.9(3) . 1_566
O20 Yb4 C67 Na2 10.8(4) . 1_566
O33 Yb4 C67 Na2 -1.7(7) . 1_566
N5 Yb4 C67 Na2 -56.7(4) . 1_566
N8 Yb4 C67 Na2 134.9(6) . 1_566
C68 Yb4 C67 Na2 90.4(4) . 1_566
C46 Yb4 C67 Na2 -100.5(4) . 1_566
Yb3 Yb4 C67 Na2 -178.76(13) . 1_566
Yb4 O35 C68 O36 -160.5(9) . .
Yb4 O35 C68 C66 15.1(16) . .
Na4 O36 C68 O35 56.7(16) . .
Na4 O36 C68 C66 -119.1(10) . .
Na4 O36 C68 Yb4 24(3) . .
N8 C66 C68 O35 20.2(16) . .
N8 C66 C68 O36 -163.9(10) . .
N8 C66 C68 Yb4 29.6(8) . .
O19 Yb4 C68 O35 9.1(10) . .
O22 Yb4 C68 O35 149.9(8) . .
O28 Yb4 C68 O35 78.9(9) . .
O20 Yb4 C68 O35 -67.6(9) . .
O33 Yb4 C68 O35 -147.8(9) . .
N5 Yb4 C68 O35 -96.0(10) . .
N8 Yb4 C68 O35 146.4(11) . .
C67 Yb4 C68 O35 -168.4(9) . .
C46 Yb4 C68 O35 175.8(8) . .
Yb3 Yb4 C68 O35 44.8(9) . .
O19 Yb4 C68 O36 55(2) . .
O35 Yb4 C68 O36 46(2) . .
O22 Yb4 C68 O36 -164(2) . .
O28 Yb4 C68 O36 125(2) . .
O20 Yb4 C68 O36 -21(2) . .
O33 Yb4 C68 O36 -101(2) . .
N5 Yb4 C68 O36 -50(3) . .
N8 Yb4 C68 O36 -167(2) . .
C67 Yb4 C68 O36 -122(2) . .
C46 Yb4 C68 O36 -138(2) . .
Yb3 Yb4 C68 O36 91(2) . .
O19 Yb4 C68 C66 -158.0(7) . .
O35 Yb4 C68 C66 -167.0(14) . .
O22 Yb4 C68 C66 -17.1(9) . .
O28 Yb4 C68 C66 -88.2(7) . .
O20 Yb4 C68 C66 125.3(7) . .
O33 Yb4 C68 C66 45.2(7) . .
N5 Yb4 C68 C66 96.9(8) . .
N8 Yb4 C68 C66 -20.6(6) . .
C67 Yb4 C68 C66 24.5(7) . .
C46 Yb4 C68 C66 8.8(10) . .
Yb3 Yb4 C68 C66 -122.3(7) . .
C63 O32 Na1 O2W -6.7(17) . .
C63 O32 Na1 O25 -107(3) . 2_567
C63 O32 Na1 O6 139.4(17) . 2_567
C63 O32 Na1 O1W -103.4(17) . .
C63 O32 Na1 O7 86.6(17) . 2_567
C63 O32 Na1 C15 112.2(17) . 2_567
C27 O11 Na2 O5W 104.8(11) . .
C27 O11 Na2 O4W -14(2) . .
C27 O11 Na2 O33 -133.3(11) . 1_544
C27 O11 Na2 O3W -0.9(11) . .
C27 O11 Na2 O34 -80.8(10) . 1_544
C27 O11 Na2 C67 -106.2(11) . 1_544
C27 O11 Na2 Na3 -47.4(11) . 2_666
C29 O14 Na3 O34 11(4) . 2_677
Na11 O14 Na3 O34 -110(4) . 2_677
C29 O14 Na3 O12W 156.7(10) . .
Na11 O14 Na3 O12W 36.0(7) . .
C29 O14 Na3 O4W 61.5(9) . 2_666
Na11 O14 Na3 O4W -59.3(6) . 2_666
C29 O14 Na3 O3W -10.1(9) . 2_666
Na11 O14 Na3 O3W -130.9(6) . 2_666
C29 O14 Na3 O14W -129.0(13) . .
Na11 O14 Na3 O14W 110.2(11) . .
C29 O14 Na3 O13W -142.6(13) . .
Na11 O14 Na3 O13W 96.6(11) . .
Na11 O14 Na3 C29 -120.8(11) . .
C29 O14 Na3 Na2 30.0(10) . 2_666
Na11 O14 Na3 Na2 -90.8(7) . 2_666
C29 O14 Na3 Na11 120.8(11) . .
O14 C29 Na3 O34 -177.1(11) . 2_677
O13 C29 Na3 O34 -44.8(14) . 2_677
C28 C29 Na3 O34 93.9(15) . 2_677
Yb1 C29 Na3 O34 -20.7(13) . 2_677
O13 C29 Na3 O14 132.3(14) . .
C28 C29 Na3 O14 -89.0(15) . .
Yb1 C29 Na3 O14 156.4(13) . .
O14 C29 Na3 O12W -25.0(10) . .
O13 C29 Na3 O12W 107.3(9) . .
C28 C29 Na3 O12W -114.0(13) . .
Yb1 C29 Na3 O12W 131.4(7) . .
O14 C29 Na3 O4W -114.2(10) . 2_666
O13 C29 Na3 O4W 18.1(8) . 2_666
C28 C29 Na3 O4W 156.8(13) . 2_666
Yb1 C29 Na3 O4W 42.3(6) . 2_666
O14 C29 Na3 O3W 169.1(10) . 2_666
O13 C29 Na3 O3W -58.6(8) . 2_666
C28 C29 Na3 O3W 80.1(12) . 2_666
Yb1 C29 Na3 O3W -34.4(5) . 2_666
O14 C29 Na3 O14W 44.3(12) . .
O13 C29 Na3 O14W 176.6(12) . .
C28 C29 Na3 O14W -44.7(15) . .
Yb1 C29 Na3 O14W -159.2(11) . .
O14 C29 Na3 O13W 43.1(16) . .
O13 C29 Na3 O13W 175.4(14) . .
C28 C29 Na3 O13W -45.9(18) . .
Yb1 C29 Na3 O13W -160.5(13) . .
O14 C29 Na3 Na2 -153.7(9) . 2_666
O13 C29 Na3 Na2 -21.4(9) . 2_666
C28 C29 Na3 Na2 117.3(12) . 2_666
Yb1 C29 Na3 Na2 2.7(6) . 2_666
O14 C29 Na3 Na11 -43.2(9) . .
O13 C29 Na3 Na11 89.1(9) . .
C28 C29 Na3 Na11 -132.2(14) . .
Yb1 C29 Na3 Na11 113.3(7) . .
C68 O36 Na4 O6W -167.2(12) . .
C68 O36 Na4 O6W 12.8(12) . 2_678
C68 O36 Na4 O11W 44.4(10) . .
C68 O36 Na4 O11W -135.6(10) . 2_678
C68 O36 Na4 O36 131(100) . 2_678
C68 O36 Na4 O7W 137.6(11) . 2_678
C68 O36 Na4 O7W -42.4(11) . .
C68 O36 Na4 O23W -91.9(11) . .
C68 O36 Na4 O23W 88.1(11) . 2_678
C62 O30 Na5 O8W 49.6(18) . .
Na6 O30 Na5 O8W -125.6(15) . .
C62 O30 Na5 Na10 94.5(9) . .
Na6 O30 Na5 Na10 -80.7(7) . .
C62 O30 Na6 O9W -19.2(11) . .
Na5 O30 Na6 O9W 155.2(6) . .
C62 O30 Na6 O21 160.8(9) . 2_677
Na5 O30 Na6 O21 -24.8(7) . 2_677
C63 O31 Na7 O24W 35.9(12) . .
Yb3 O31 Na7 O24W -114.4(9) . .
C63 O31 Na7 O22W -146.6(11) . .
Yb3 O31 Na7 O22W 63.1(9) . .
C63 O31 Na7 Na8 -133.8(8) . .
Yb3 O31 Na7 Na8 75.8(4) . .
C63 O31 Na7 Yb3 150.3(10) . .
O28 Yb3 Na7 O24W 141.4(10) . .
O26 Yb3 Na7 O24W -144.7(11) . .
O31 Yb3 Na7 O24W 85.8(11) . .
O29 Yb3 Na7 O24W -6.8(11) . .
O19 Yb3 Na7 O24W -147.8(10) . .
O24 Yb3 Na7 O24W -13.4(10) . .
N6 Yb3 Na7 O24W -79.1(10) . .
N7 Yb3 Na7 O24W 56.8(10) . .
C51 Yb3 Na7 O24W -118.7(10) . .
C63 Yb3 Na7 O24W 72.5(10) . .
C50 Yb3 Na7 O24W -30.5(10) . .
C62 Yb3 Na7 O24W 13.4(11) . .
O28 Yb3 Na7 O22W -74.2(7) . .
O26 Yb3 Na7 O22W -0.4(7) . .
O31 Yb3 Na7 O22W -129.8(8) . .
O29 Yb3 Na7 O22W 137.5(7) . .
O19 Yb3 Na7 O22W -3.5(8) . .
O24 Yb3 Na7 O22W 130.9(7) . .
N6 Yb3 Na7 O22W 65.2(7) . .
N7 Yb3 Na7 O22W -158.9(7) . .
C51 Yb3 Na7 O22W 25.6(7) . .
C63 Yb3 Na7 O22W -143.2(8) . .
C50 Yb3 Na7 O22W 113.8(7) . .
C62 Yb3 Na7 O22W 157.7(7) . .
O28 Yb3 Na7 O31 55.6(5) . .
O26 Yb3 Na7 O31 129.5(6) . .
O29 Yb3 Na7 O31 -92.6(6) . .
O19 Yb3 Na7 O31 126.3(5) . .
O24 Yb3 Na7 O31 -99.3(5) . .
N6 Yb3 Na7 O31 -164.9(5) . .
N7 Yb3 Na7 O31 -29.0(5) . .
C51 Yb3 Na7 O31 155.4(6) . .
C63 Yb3 Na7 O31 -13.4(5) . .
C50 Yb3 Na7 O31 -116.3(5) . .
C62 Yb3 Na7 O31 -72.4(5) . .
O28 Yb3 Na7 Na8 -41.1(3) . .
O26 Yb3 Na7 Na8 32.7(4) . .
O31 Yb3 Na7 Na8 -96.7(5) . .
O29 Yb3 Na7 Na8 170.6(4) . .
O19 Yb3 Na7 Na8 29.6(4) . .
O24 Yb3 Na7 Na8 164.0(4) . .
N6 Yb3 Na7 Na8 98.3(4) . .
N7 Yb3 Na7 Na8 -125.8(3) . .
C51 Yb3 Na7 Na8 58.7(4) . .
C63 Yb3 Na7 Na8 -110.1(4) . .
C50 Yb3 Na7 Na8 146.9(4) . .
C62 Yb3 Na7 Na8 -169.2(4) . .
C51 O26 Na8 O22W -45.7(10) . .
Yb3 O26 Na8 O22W 124.0(7) . .
C51 O26 Na8 O18 -83.8(9) . 2_567
Yb3 O26 Na8 O18 86.0(7) . 2_567
C51 O26 Na8 Na7 -82.2(8) . .
Yb3 O26 Na8 Na7 87.6(6) . .
O24W Na7 Na8 O22W 38(2) . .
O31 Na7 Na8 O22W -166.2(9) . .
Yb3 Na7 Na8 O22W -136.9(8) . .
O24W Na7 Na8 O18 -30(2) . 2_567
O22W Na7 Na8 O18 -67.4(8) . 2_567
O31 Na7 Na8 O18 126.3(5) . 2_567
Yb3 Na7 Na8 O18 155.7(4) . 2_567
O24W Na7 Na8 O26 152(2) . .
O22W Na7 Na8 O26 114.4(9) . .
O31 Na7 Na8 O26 -51.9(4) . .
Yb3 Na7 Na8 O26 -22.5(3) . .
C17 O9 Na10 Na11 87.6(12) . .
C17 O9 Na10 O8W -120.0(10) . .
Na11 O9 Na10 O8W 152.4(10) . .
C17 O9 Na10 O10W -30.3(11) . .
Na11 O9 Na10 O10W -117.8(10) . .
C17 O9 Na10 O15W 128.7(12) . .
Na11 O9 Na10 O15W 41.2(10) . .
C17 O9 Na10 O10W 167(6) . 2_667
Na11 O9 Na10 O10W 80(6) . 2_667
C17 O9 Na10 O16W 51.6(11) . 2_667
Na11 O9 Na10 O16W -36.0(7) . 2_667
C17 O9 Na10 Na10 -32.8(17) . 2_667
Na11 O9 Na10 Na10 -120.4(16) . 2_667
C17 O9 Na10 Na5 -112.9(10) . .
Na11 O9 Na10 Na5 159.5(8) . .
O8W Na5 Na10 Na11 -149.1(12) . .
O30 Na5 Na10 Na11 75.9(10) . .
O30 Na5 Na10 O8W -135.0(8) . .
O8W Na5 Na10 O10W 98.1(9) . .
O30 Na5 Na10 O10W -37.0(8) . .
O8W Na5 Na10 O15W -91.3(11) . .
O30 Na5 Na10 O15W 133.7(10) . .
O8W Na5 Na10 O9 -169.3(9) . .
O30 Na5 Na10 O9 55.7(6) . .
O8W Na5 Na10 O10W 2.3(8) . 2_667
O30 Na5 Na10 O10W -132.8(8) . 2_667
O8W Na5 Na10 O16W 168.8(15) . 2_667
O30 Na5 Na10 O16W 33.8(14) . 2_667
O8W Na5 Na10 Na10 54.6(8) . 2_667
O30 Na5 Na10 Na10 -80.4(8) . 2_667
O8W Na10 Na11 O16W -168.9(17) . 2_667
O10W Na10 Na11 O16W -40.8(14) . 2_667
O15W Na10 Na11 O16W 119.6(14) . 2_667
O9 Na10 Na11 O16W -115.8(11) . 2_667
O10W Na10 Na11 O16W 71.3(13) 2_667 2_667
Na10 Na10 Na11 O16W 20.1(15) 2_667 2_667
Na5 Na10 Na11 O16W -132.5(9) . 2_667
O8W Na10 Na11 O15W 71(2) . .
O10W Na10 Na11 O15W -160.4(13) . .
O9 Na10 Na11 O15W 124.6(11) . .
O10W Na10 Na11 O15W -48.3(12) 2_667 .
O16W Na10 Na11 O15W -119.6(14) 2_667 .
Na10 Na10 Na11 O15W -99.5(13) 2_667 .
Na5 Na10 Na11 O15W 107.9(10) . .
O8W Na10 Na11 O14 7(7) . .
O10W Na10 Na11 O14 136(5) . .
O15W Na10 Na11 O14 -64(6) . .
O9 Na10 Na11 O14 61(5) . .
O10W Na10 Na11 O14 -112(6) 2_667 .
O16W Na10 Na11 O14 176(6) 2_667 .
Na10 Na10 Na11 O14 -164(5) 2_667 .
Na5 Na10 Na11 O14 44(6) . .
O8W Na10 Na11 O9 -53.1(18) . .
O10W Na10 Na11 O9 75.0(9) . .
O15W Na10 Na11 O9 -124.6(11) . .
O10W Na10 Na11 O9 -172.9(10) 2_667 .
O16W Na10 Na11 O9 115.8(11) 2_667 .
Na10 Na10 Na11 O9 135.9(10) 2_667 .
Na5 Na10 Na11 O9 -16.7(6) . .
O8W Na10 Na11 O8 -96.1(18) . .
O10W Na10 Na11 O8 32.1(11) . .
O15W Na10 Na11 O8 -167.5(12) . .
O9 Na10 Na11 O8 -43.0(4) . .
O10W Na10 Na11 O8 144.1(8) 2_667 .
O16W Na10 Na11 O8 72.8(10) 2_667 .
Na10 Na10 Na11 O8 92.9(10) 2_667 .
Na5 Na10 Na11 O8 -59.7(7) . .
O8W Na10 Na11 C17 -76.2(18) . .
O10W Na10 Na11 C17 52.0(9) . .
O15W Na10 Na11 C17 -147.7(11) . .
O9 Na10 Na11 C17 -23.1(4) . .
O10W Na10 Na11 C17 164.0(9) 2_667 .
O16W Na10 Na11 C17 92.7(11) 2_667 .
Na10 Na10 Na11 C17 112.8(10) 2_667 .
Na5 Na10 Na11 C17 -39.8(6) . .
O8W Na10 Na11 Na3 2(3) . .
O10W Na10 Na11 Na3 129.8(12) . .
O15W Na10 Na11 Na3 -69.8(13) . .
O9 Na10 Na11 Na3 54.8(10) . .
O10W Na10 Na11 Na3 -118.1(12) 2_667 .
O16W Na10 Na11 Na3 170.6(19) 2_667 .
Na10 Na10 Na11 Na3 -169.3(8) 2_667 .
Na5 Na10 Na11 Na3 38.0(14) . .
C29 O14 Na11 O16W 44.1(15) . 2_667
Na3 O14 Na11 O16W 168.9(11) . 2_667
C29 O14 Na11 O15W 167.4(13) . .
Na3 O14 Na11 O15W -67.9(13) . .
C29 O14 Na11 Na10 -132(5) . .
Na3 O14 Na11 Na10 -7(6) . .
C29 O14 Na11 O9 -75.9(12) . .
Na3 O14 Na11 O9 48.8(10) . .
C29 O14 Na11 O8 -29.7(11) . .
Na3 O14 Na11 O8 95.0(7) . .
C29 O14 Na11 C17 -52.0(12) . .
Na3 O14 Na11 C17 72.7(8) . .
C29 O14 Na11 Na3 -124.7(10) . .
C17 O9 Na11 O16W -37.4(14) . 2_667
Na10 O9 Na11 O16W 70.8(11) . 2_667
C17 O9 Na11 O15W -161.6(15) . .
Na10 O9 Na11 O15W -53.4(13) . .
C17 O9 Na11 Na10 -108.2(11) . .
C17 O9 Na11 O14 82.6(12) . .
Na10 O9 Na11 O14 -169.2(13) . .
C17 O9 Na11 O8 3.1(8) . .
Na10 O9 Na11 O8 111.3(8) . .
Na10 O9 Na11 C17 108.2(11) . .
C17 O9 Na11 Na3 108.4(9) . .
Na10 O9 Na11 Na3 -143.4(9) . .
C17 O8 Na11 O16W 136.8(12) . 2_667
Yb2 O8 Na11 O16W -28.8(14) . 2_667
C17 O8 Na11 O15W 28(3) . .
Yb2 O8 Na11 O15W -137(2) . .
C17 O8 Na11 Na10 53.1(11) . .
Yb2 O8 Na11 Na10 -112.5(11) . .
C17 O8 Na11 O14 -115.5(10) . .
Yb2 O8 Na11 O14 78.9(12) . .
C17 O8 Na11 O9 -3.0(8) . .
Yb2 O8 Na11 O9 -168.6(10) . .
Yb2 O8 Na11 C17 -165.6(15) . .
C17 O8 Na11 Na3 -80.0(9) . .
Yb2 O8 Na11 Na3 114.4(10) . .
O9 C17 Na11 O16W 144.9(13) . 2_667
O8 C17 Na11 O16W -40.7(12) . 2_667
C16 C17 Na11 O16W 82(5) . 2_667
Yb2 C17 Na11 O16W -35.0(10) . 2_667
O9 C17 Na11 O15W 22.8(18) . .
O8 C17 Na11 O15W -162.8(18) . .
C16 C17 Na11 O15W -40(6) . .
Yb2 C17 Na11 O15W -157.1(15) . .
O9 C17 Na11 Na10 62.8(11) . .
O8 C17 Na11 Na10 -122.9(11) . .
C16 C17 Na11 Na10 0(5) . .
Yb2 C17 Na11 Na10 -117.2(8) . .
O9 C17 Na11 O14 -105.2(12) . .
O8 C17 Na11 O14 69.1(10) . .
C16 C17 Na11 O14 -168(5) . .
Yb2 C17 Na11 O14 74.8(9) . .
O8 C17 Na11 O9 174.3(15) . .
C16 C17 Na11 O9 -63(5) . .
Yb2 C17 Na11 O9 -179.9(12) . .
O9 C17 Na11 O8 -174.3(15) . .
C16 C17 Na11 O8 122(5) . .
Yb2 C17 Na11 O8 5.7(6) . .
O9 C17 Na11 Na3 -71.7(10) . .
O8 C17 Na11 Na3 102.6(9) . .
C16 C17 Na11 Na3 -135(5) . .
Yb2 C17 Na11 Na3 108.3(5) . .
O34 Na3 Na11 O16W 151.0(18) 2_677 2_667
O14 Na3 Na11 O16W -17.7(17) . 2_667
O12W Na3 Na11 O16W -155(2) . 2_667
O4W Na3 Na11 O16W 92(2) 2_666 2_667
O3W Na3 Na11 O16W 39(2) 2_666 2_667
O14W Na3 Na11 O16W -74(2) . 2_667
O13W Na3 Na11 O16W -112(2) . 2_667
C29 Na3 Na11 O16W 5.5(18) . 2_667
Na2 Na3 Na11 O16W 91(2) 2_666 2_667
O34 Na3 Na11 O15W -74.1(17) 2_677 .
O14 Na3 Na11 O15W 117.1(16) . .
O12W Na3 Na11 O15W -19.8(15) . .
O4W Na3 Na11 O15W -133.3(15) 2_666 .
O3W Na3 Na11 O15W 173.4(14) 2_666 .
O14W Na3 Na11 O15W 60.9(15) . .
O13W Na3 Na11 O15W 23.3(16) . .
C29 Na3 Na11 O15W 140.4(16) . .
Na2 Na3 Na11 O15W -133.7(14) 2_666 .
O34 Na3 Na11 Na10 -13.3(17) 2_677 .
O14 Na3 Na11 Na10 178.0(16) . .
O12W Na3 Na11 Na10 41.1(12) . .
O4W Na3 Na11 Na10 -72.5(12) 2_666 .
O3W Na3 Na11 Na10 -125.8(11) 2_666 .
O14W Na3 Na11 Na10 121.8(14) . .
O13W Na3 Na11 Na10 84.1(13) . .
C29 Na3 Na11 Na10 -158.8(14) . .
Na2 Na3 Na11 Na10 -72.8(13) 2_666 .
O34 Na3 Na11 O14 168.7(7) 2_677 .
O12W Na3 Na11 O14 -136.9(8) . .
O4W Na3 Na11 O14 109.6(7) 2_666 .
O3W Na3 Na11 O14 56.2(7) 2_666 .
O14W Na3 Na11 O14 -56.2(8) . .
O13W Na3 Na11 O14 -93.9(8) . .
C29 Na3 Na11 O14 23.2(5) . .
Na2 Na3 Na11 O14 109.2(6) 2_666 .
O34 Na3 Na11 O9 33.4(10) 2_677 .
O14 Na3 Na11 O9 -135.4(9) . .
O12W Na3 Na11 O9 87.7(7) . .
O4W Na3 Na11 O9 -25.8(5) 2_666 .
O3W Na3 Na11 O9 -79.1(6) 2_666 .
O14W Na3 Na11 O9 168.4(8) . .
O13W Na3 Na11 O9 130.8(7) . .
C29 Na3 Na11 O9 -112.1(7) . .
Na2 Na3 Na11 O9 -26.2(6) 2_666 .
O34 Na3 Na11 O8 78.8(9) 2_677 .
O14 Na3 Na11 O8 -90.0(7) . .
O12W Na3 Na11 O8 133.1(8) . .
O4W Na3 Na11 O8 19.6(5) 2_666 .
O3W Na3 Na11 O8 -33.7(7) 2_666 .
O14W Na3 Na11 O8 -146.2(8) . .
O13W Na3 Na11 O8 176.2(7) . .
C29 Na3 Na11 O8 -66.8(6) . .
Na2 Na3 Na11 O8 19.2(7) 2_666 .
O34 Na3 Na11 C17 55.3(9) 2_677 .
O14 Na3 Na11 C17 -113.5(8) . .
O12W Na3 Na11 C17 109.6(7) . .
O4W Na3 Na11 C17 -3.9(5) 2_666 .
O3W Na3 Na11 C17 -57.2(7) 2_666 .
O14W Na3 Na11 C17 -169.7(8) . .
O13W Na3 Na11 C17 152.7(7) . .
C29 Na3 Na11 C17 -90.2(6) . .
Na2 Na3 Na11 C17 -4.3(7) 2_666 .
O5W Na2 O3W Na3 148.7(4) . 2_666
O4W Na2 O3W Na3 50.8(3) . 2_666
O11 Na2 O3W Na3 -125.9(3) . 2_666
O33 Na2 O3W Na3 -44.2(5) 1_544 2_666
O34 Na2 O3W Na3 -39.1(3) 1_544 2_666
C67 Na2 O3W Na3 -47.3(4) 1_544 2_666
O5W Na2 O4W Na3 -156.0(4) . 2_666
O11 Na2 O4W Na3 -38.7(16) . 2_666
O33 Na2 O4W Na3 78.3(3) 1_544 2_666
O3W Na2 O4W Na3 -52.4(3) . 2_666
O34 Na2 O4W Na3 27.8(3) 1_544 2_666
C67 Na2 O4W Na3 50.6(4) 1_544 2_666
Na11 Na10 O8W Na5 55.0(17) . .
O10W Na10 O8W Na5 -79.0(8) . .
O15W Na10 O8W Na5 108.2(10) . .
O9 Na10 O8W Na5 8.1(7) . .
O10W Na10 O8W Na5 -178.2(6) 2_667 .
O16W Na10 O8W Na5 -68(9) 2_667 .
Na10 Na10 O8W Na5 -132.1(6) 2_667 .
O30 Na5 O8W Na10 79.6(17) . .
Na11 Na10 O10W Na10 120.0(12) . 2_667
O8W Na10 O10W Na10 -87.1(11) . 2_667
O15W Na10 O10W Na10 74(3) . 2_667
O9 Na10 O10W Na10 -178.0(8) . 2_667
O10W Na10 O10W Na10 0.000(1) 2_667 2_667
O16W Na10 O10W Na10 94.6(9) 2_667 2_667
Na5 Na10 O10W Na10 -128.5(6) . 2_667
O16W Na11 O15W Na10 -70.9(15) 2_667 .
O14 Na11 O15W Na10 169.2(13) . .
O9 Na11 O15W Na10 50.1(8) . .
O8 Na11 O15W Na10 27(2) . .
C17 Na11 O15W Na10 41.0(12) . .
Na3 Na11 O15W Na10 136.9(9) . .
O8W Na10 O15W Na11 -144.0(16) . .
O10W Na10 O15W Na11 56(3) . .
O9 Na10 O15W Na11 -49.6(10) . .
O10W Na10 O15W Na11 134.7(11) 2_667 .
O16W Na10 O15W Na11 35.4(10) 2_667 .
Na10 Na10 O15W Na11 117.1(13) 2_667 .
Na5 Na10 O15W Na11 -98.4(11) . .
O24W Na7 O22W Na8 -165.6(9) . .
O31 Na7 O22W Na8 16.7(10) . .
Yb3 Na7 O22W Na8 43.9(7) . .
O18 Na8 O22W Na7 79.6(7) 2_567 .
O26 Na8 O22W Na7 -51.8(6) . .
O22W Na7 O24W O21W 5(2) . .
O31 Na7 O24W O21W -177.6(18) . .
Na8 Na7 O24W O21W -25(4) . .
Yb3 Na7 O24W O21W 148.0(18) . .
