#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:08:28 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179502 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/99/4339980.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4339980
loop_
_publ_author_name
'Kishore, Pilli V. V. N.'
'Baskar, Viswanathan'
_publ_section_title
;
 Hexa- and trinuclear organoantimony oxo clusters stabilized by
 organosilanols.
;
_journal_issue                   13
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6737
_journal_page_last               6742
_journal_paper_doi               10.1021/ic500541h
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C72 H74 O14 Sb6 Si2'
_chemical_formula_weight         1949.99
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.884(4)
_cell_angle_beta                 116.854(4)
_cell_angle_gamma                95.664(4)
_cell_formula_units_Z            1
_cell_length_a                   12.728(4)
_cell_length_b                   13.015(4)
_cell_length_c                   13.544(4)
_cell_measurement_reflns_used    6460
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      24.93
_cell_measurement_theta_min      2.36
_cell_volume                     1812.5(10)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0568
_diffrn_reflns_av_sigmaI/netI    0.0702
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            17302
_diffrn_reflns_theta_full        24.98
_diffrn_reflns_theta_max         24.98
_diffrn_reflns_theta_min         1.73
_exptl_absorpt_coefficient_mu    2.299
_exptl_absorpt_correction_T_max  0.7390
_exptl_absorpt_correction_T_min  0.6824
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   brukarsadbas
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.787
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             952
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         2.328
_refine_diff_density_min         -0.656
_refine_diff_density_rms         0.196
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     424
_refine_ls_number_reflns         6338
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.055
_refine_ls_R_factor_all          0.0849
_refine_ls_R_factor_gt           0.0624
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0776P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1358
_refine_ls_wR_factor_ref         0.1464
_reflns_number_gt                4827
_reflns_number_total             6338
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500541h_si_001.cif
_cod_data_source_block           2
_cod_depositor_comments
'Adding full bibliography for 4339979--4339982.cif.'
_cod_original_cell_volume        1812.4(9)
_cod_database_code               4339980
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Sb1 Sb 0.46130(5) 0.63744(5) 0.29805(5) 0.03342(19) Uani 1 1 d .
Sb2 Sb 0.19466(5) 0.62928(5) 0.10065(5) 0.02969(18) Uani 1 1 d .
Sb3 Sb 0.23415(5) 0.56474(5) 0.33122(5) 0.03189(18) Uani 1 1 d .
Si1 Si -0.0256(2) 0.5997(2) 0.1593(2) 0.0309(5) Uani 1 1 d .
C22 C 0.0843(14) 0.1847(13) 0.2862(13) 0.089(4) Uani 1 1 d .
H22 H 0.0537 0.1114 0.2750 0.107 Uiso 1 1 calc R
C13 C 0.2282(8) 0.7836(7) 0.0827(8) 0.036(2) Uani 1 1 d .
C25 C 0.3089(8) 0.6666(8) 0.5178(8) 0.038(2) Uani 1 1 d .
C19 C 0.1695(8) 0.3988(8) 0.3107(7) 0.037(2) Uani 1 1 d .
C2 C 0.5642(9) 0.4961(8) 0.1571(9) 0.049(3) Uani 1 1 d .
H2 H 0.4901 0.4874 0.0901 0.059 Uiso 1 1 calc R
C1 C 0.5898(7) 0.5604(8) 0.2723(8) 0.034(2) Uani 1 1 d .
C26 C 0.4168(9) 0.6568(8) 0.6034(8) 0.047(2) Uani 1 1 d .
H26 H 0.4573 0.6089 0.5772 0.057 Uiso 1 1 calc R
C6 C 0.7040(10) 0.5755(10) 0.3699(10) 0.059(3) Uani 1 1 d .
H6 H 0.7261 0.6223 0.4488 0.071 Uiso 1 1 calc R
C27 C 0.4649(10) 0.7171(10) 0.7272(9) 0.066(3) Uani 1 1 d .
H27 H 0.5357 0.7088 0.7843 0.079 Uiso 1 1 calc R
C20 C 0.2337(10) 0.3201(9) 0.2970(10) 0.061(3) Uani 1 1 d .
H20 H 0.3053 0.3387 0.2954 0.074 Uiso 1 1 calc R
C18 C 0.3365(11) 0.8263(9) 0.0920(11) 0.067(3) Uani 1 1 d .
H18 H 0.3958 0.7878 0.1070 0.080 Uiso 1 1 calc R
C14 C 0.1418(10) 0.8410(9) 0.0583(11) 0.066(3) Uani 1 1 d .
H14 H 0.0665 0.8124 0.0492 0.079 Uiso 1 1 calc R
C24 C 0.0653(10) 0.3685(10) 0.3122(12) 0.067(3) Uani 1 1 d .
H24 H 0.0212 0.4205 0.3197 0.081 Uiso 1 1 calc R
C3 C 0.6467(10) 0.4450(9) 0.1402(10) 0.058(3) Uani 1 1 d .
H3 H 0.6284 0.4021 0.0616 0.070 Uiso 1 1 calc R
C30 C 0.2533(10) 0.7402(9) 0.5592(9) 0.058(3) Uani 1 1 d .
H30 H 0.1812 0.7484 0.5037 0.069 Uiso 1 1 calc R
C5 C 0.7830(10) 0.5215(11) 0.3494(11) 0.067(3) Uani 1 1 d .
H5 H 0.8583 0.5302 0.4151 0.080 Uiso 1 1 calc R
C28 C 0.4047(12) 0.7895(10) 0.7625(10) 0.071(4) Uani 1 1 d .
H28 H 0.4358 0.8310 0.8450 0.085 Uiso 1 1 calc R
C4 C 0.7544(10) 0.4556(10) 0.2356(11) 0.062(3) Uani 1 1 d .
H4 H 0.8086 0.4178 0.2231 0.074 Uiso 1 1 calc R
C17 C 0.3583(14) 0.9242(11) 0.0794(13) 0.086(4) Uani 1 1 d .
H17 H 0.4325 0.9520 0.0862 0.104 Uiso 1 1 calc R
C21 C 0.1880(13) 0.2127(10) 0.2855(11) 0.078(4) Uani 1 1 d .
H21 H 0.2303 0.1592 0.2772 0.094 Uiso 1 1 calc R
C29 C 0.3023(12) 0.8019(10) 0.6811(10) 0.071(4) Uani 1 1 d .
H29 H 0.2644 0.8527 0.7077 0.085 Uiso 1 1 calc R
C23 C 0.0236(13) 0.2626(13) 0.3030(16) 0.106(5) Uani 1 1 d .
H23 H -0.0456 0.2443 0.3083 0.128 Uiso 1 1 calc R
O3 O 0.3600(5) 0.6111(5) 0.1319(5) 0.0328(14) Uani 1 1 d .
O4 O 0.0378(5) 0.6422(5) 0.0916(5) 0.0305(13) Uani 1 1 d .
O1 O 0.2884(5) 0.6853(5) 0.2855(5) 0.0321(13) Uani 1 1 d .
O5 O 0.0772(5) 0.6003(5) 0.2852(5) 0.0355(14) Uani 1 1 d .
O7 O -0.1160(5) 0.4709(5) 0.0702(5) 0.0341(14) Uani 1 1 d .
C31 C -0.1142(8) 0.6977(7) 0.1916(8) 0.036(2) Uani 1 1 d .
H31 H -0.1524 0.6698 0.2302 0.044 Uiso 1 1 calc R
C36 C -0.0335(9) 0.8180(8) 0.2801(10) 0.058(3) Uani 1 1 d .
H36A H 0.0069 0.8483 0.2453 0.070 Uiso 1 1 calc R
H36B H 0.0297 0.8172 0.3547 0.070 Uiso 1 1 calc R
C32 C -0.2189(9) 0.6996(9) 0.0764(10) 0.061(3) Uani 1 1 d .
H32A H -0.1846 0.7271 0.0355 0.073 Uiso 1 1 calc R
H32B H -0.2728 0.6231 0.0213 0.073 Uiso 1 1 calc R
C35 C -0.1091(11) 0.8956(9) 0.3099(11) 0.066(3) Uani 1 1 d .
H35A H -0.1423 0.8699 0.3525 0.080 Uiso 1 1 calc R
H35B H -0.0554 0.9724 0.3633 0.080 Uiso 1 1 calc R
C16 C 0.2738(15) 0.9815(12) 0.0571(13) 0.090(5) Uani 1 1 d .
H16 H 0.2898 1.0485 0.0488 0.108 Uiso 1 1 calc R
C15 C 0.1657(13) 0.9412(11) 0.0471(12) 0.092(5) Uani 1 1 d .
H15 H 0.1075 0.9809 0.0326 0.110 Uiso 1 1 calc R
C33 C -0.2931(11) 0.7758(10) 0.1078(10) 0.074(4) Uani 1 1 d .
H33A H -0.3561 0.7782 0.0341 0.089 Uiso 1 1 calc R
H33B H -0.3338 0.7441 0.1415 0.089 Uiso 1 1 calc R
C34 C -0.2114(13) 0.8956(11) 0.1988(13) 0.087(4) Uani 1 1 d .
H34A H -0.1780 0.9303 0.1616 0.105 Uiso 1 1 calc R
H34B H -0.2603 0.9404 0.2205 0.105 Uiso 1 1 calc R
C7 C 0.5624(7) 0.8051(7) 0.4234(8) 0.036(2) Uani 1 1 d .
C8 C 0.5448(9) 0.8614(8) 0.5166(9) 0.052(3) Uani 1 1 d .
H8 H 0.4836 0.8258 0.5242 0.063 Uiso 1 1 calc R
C12 C 0.6518(10) 0.8592(9) 0.4130(10) 0.067(4) Uani 1 1 d .
H12 H 0.6651 0.8216 0.3504 0.080 Uiso 1 1 calc R
C10 C 0.7024(10) 1.0253(9) 0.5861(11) 0.072(4) Uani 1 1 d .
H10 H 0.7468 1.1006 0.6394 0.086 Uiso 1 1 calc R
C9 C 0.6161(11) 0.9693(10) 0.5982(10) 0.067(3) Uani 1 1 d .
H9 H 0.6056 1.0053 0.6633 0.081 Uiso 1 1 calc R
C11 C 0.7235(11) 0.9706(10) 0.4954(12) 0.084(4) Uani 1 1 d .
H11 H 0.7848 1.0070 0.4885 0.100 Uiso 1 1 calc R
O6 O 0.3982(5) 0.5438(5) 0.3529(5) 0.0355(14) Uani 1 1 d .
O2 O 0.1683(5) 0.4872(4) 0.1351(5) 0.0315(13) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O6 Sb1 O3 116.0(2) . .
O6 Sb1 C7 116.5(3) . .
O3 Sb1 C7 117.4(3) . .
O6 Sb1 C1 101.6(3) . .
O3 Sb1 C1 95.2(3) . .
C7 Sb1 C1 105.2(3) . .
O6 Sb1 O1 75.0(2) . .
O3 Sb1 O1 75.3(2) . .
C7 Sb1 O1 87.6(3) . .
C1 Sb1 O1 166.6(3) . .
O7 Sb2 O4 93.7(2) 2_565 .
O7 Sb2 O3 92.0(2) 2_565 .
O4 Sb2 O3 171.3(2) . .
O7 Sb2 O1 160.6(2) 2_565 .
O4 Sb2 O1 93.3(2) . .
O3 Sb2 O1 79.3(2) . .
O7 Sb2 O2 88.4(2) 2_565 .
O4 Sb2 O2 86.6(2) . .
O3 Sb2 O2 87.0(2) . .
O1 Sb2 O2 73.9(2) . .
O7 Sb2 C13 96.9(3) 2_565 .
O4 Sb2 C13 92.7(3) . .
O3 Sb2 C13 93.1(3) . .
O1 Sb2 C13 100.9(3) . .
O2 Sb2 C13 174.7(3) . .
O5 Sb3 O1 89.2(2) . .
O5 Sb3 O6 166.7(2) . .
O1 Sb3 O6 78.6(2) . .
O5 Sb3 C25 92.9(3) . .
O1 Sb3 C25 98.1(3) . .
O6 Sb3 C25 93.9(3) . .
O5 Sb3 C19 96.2(3) . .
O1 Sb3 C19 156.7(3) . .
O6 Sb3 C19 93.2(3) . .
C25 Sb3 C19 104.1(3) . .
O5 Sb3 O2 86.5(2) . .
O1 Sb3 O2 71.5(2) . .
O6 Sb3 O2 84.7(2) . .
C25 Sb3 O2 169.6(3) . .
C19 Sb3 O2 86.2(3) . .
O5 Si1 O7 108.5(3) . .
O5 Si1 O4 111.2(3) . .
O7 Si1 O4 109.0(3) . .
O5 Si1 C31 109.1(3) . .
O7 Si1 C31 110.6(3) . .
O4 Si1 C31 108.5(4) . .
C21 C22 C23 120.4(14) . .
C21 C22 H22 119.8 . .
C23 C22 H22 119.8 . .
C14 C13 C18 118.3(9) . .
C14 C13 Sb2 121.4(7) . .
C18 C13 Sb2 120.3(8) . .
C30 C25 C26 118.0(8) . .
C30 C25 Sb3 122.6(7) . .
C26 C25 Sb3 119.4(7) . .
C24 C19 C20 119.3(10) . .
C24 C19 Sb3 120.2(8) . .
C20 C19 Sb3 120.5(7) . .
C3 C2 C1 120.4(10) . .
C3 C2 H2 119.8 . .
C1 C2 H2 119.8 . .
C2 C1 C6 118.1(9) . .
C2 C1 Sb1 120.2(7) . .
C6 C1 Sb1 121.6(7) . .
C27 C26 C25 121.1(10) . .
C27 C26 H26 119.4 . .
C25 C26 H26 119.4 . .
C5 C6 C1 119.7(10) . .
C5 C6 H6 120.1 . .
C1 C6 H6 120.1 . .
C28 C27 C26 117.8(10) . .
C28 C27 H27 121.1 . .
C26 C27 H27 121.1 . .
C19 C20 C21 118.1(11) . .
C19 C20 H20 120.9 . .
C21 C20 H20 120.9 . .
C17 C18 C13 120.8(12) . .
C17 C18 H18 119.6 . .
C13 C18 H18 119.6 . .
C13 C14 C15 120.3(11) . .
C13 C14 H14 119.8 . .
C15 C14 H14 119.8 . .
C19 C24 C23 121.3(12) . .
C19 C24 H24 119.4 . .
C23 C24 H24 119.4 . .
C4 C3 C2 121.0(10) . .
C4 C3 H3 119.5 . .
C2 C3 H3 119.5 . .
C29 C30 C25 120.9(10) . .
C29 C30 H30 119.6 . .
C25 C30 H30 119.6 . .
C4 C5 C6 121.2(11) . .
C4 C5 H5 119.4 . .
C6 C5 H5 119.4 . .
C29 C28 C27 121.7(10) . .
C29 C28 H28 119.1 . .
C27 C28 H28 119.1 . .
C3 C4 C5 119.5(10) . .
C3 C4 H4 120.3 . .
C5 C4 H4 120.3 . .
C16 C17 C18 120.9(14) . .
C16 C17 H17 119.6 . .
C18 C17 H17 119.6 . .
C22 C21 C20 121.4(13) . .
C22 C21 H21 119.3 . .
C20 C21 H21 119.3 . .
C28 C29 C30 120.3(11) . .
C28 C29 H29 119.8 . .
C30 C29 H29 119.8 . .
C22 C23 C24 119.5(13) . .
C22 C23 H23 120.3 . .
C24 C23 H23 120.3 . .
Sb1 O3 Sb2 109.6(2) . .
Si1 O4 Sb2 128.5(3) . .
Sb3 O1 Sb2 109.6(3) . .
Sb3 O1 Sb1 96.0(2) . .
Sb2 O1 Sb1 94.9(2) . .
Si1 O5 Sb3 131.2(3) . .
Si1 O7 Sb2 136.9(4) . 2_565
C36 C31 C32 109.3(8) . .
C36 C31 Si1 113.0(6) . .
C32 C31 Si1 113.3(6) . .
C36 C31 H31 106.9 . .
C32 C31 H31 106.9 . .
Si1 C31 H31 106.9 . .
C31 C36 C35 111.6(8) . .
C31 C36 H36A 109.3 . .
C35 C36 H36A 109.3 . .
C31 C36 H36B 109.3 . .
C35 C36 H36B 109.3 . .
H36A C36 H36B 108.0 . .
C33 C32 C31 111.0(9) . .
C33 C32 H32A 109.4 . .
C31 C32 H32A 109.4 . .
C33 C32 H32B 109.4 . .
C31 C32 H32B 109.4 . .
H32A C32 H32B 108.0 . .
C34 C35 C36 111.9(10) . .
C34 C35 H35A 109.2 . .
C36 C35 H35A 109.2 . .
C34 C35 H35B 109.2 . .
C36 C35 H35B 109.2 . .
H35A C35 H35B 107.9 . .
C17 C16 C15 119.7(13) . .
C17 C16 H16 120.1 . .
C15 C16 H16 120.1 . .
C16 C15 C14 120.0(13) . .
C16 C15 H15 120.0 . .
C14 C15 H15 120.0 . .
C34 C33 C32 111.4(10) . .
C34 C33 H33A 109.3 . .
C32 C33 H33A 109.3 . .
C34 C33 H33B 109.3 . .
C32 C33 H33B 109.3 . .
H33A C33 H33B 108.0 . .
C35 C34 C33 111.3(10) . .
C35 C34 H34A 109.4 . .
C33 C34 H34A 109.4 . .
C35 C34 H34B 109.4 . .
C33 C34 H34B 109.4 . .
H34A C34 H34B 108.0 . .
C12 C7 C8 118.9(8) . .
C12 C7 Sb1 118.2(7) . .
C8 C7 Sb1 122.9(7) . .
C9 C8 C7 120.5(10) . .
C9 C8 H8 119.7 . .
C7 C8 H8 119.7 . .
C7 C12 C11 120.6(10) . .
C7 C12 H12 119.7 . .
C11 C12 H12 119.7 . .
C9 C10 C11 119.7(10) . .
C9 C10 H10 120.2 . .
C11 C10 H10 120.2 . .
C10 C9 C8 121.0(11) . .
C10 C9 H9 119.5 . .
C8 C9 H9 119.5 . .
C10 C11 C12 119.2(11) . .
C10 C11 H11 120.4 . .
C12 C11 H11 120.4 . .
Sb1 O6 Sb3 109.8(3) . .
Sb2 O2 Sb3 101.8(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 O6 1.900(6) .
Sb1 O3 1.907(5) .
Sb1 C7 2.092(8) .
Sb1 C1 2.102(8) .
Sb1 O1 2.293(6) .
Sb2 O7 1.938(5) 2_565
Sb2 O4 1.971(5) .
Sb2 O3 2.005(5) .
Sb2 O1 2.042(5) .
Sb2 O2 2.081(5) .
Sb2 C13 2.125(8) .
Sb3 O5 1.959(5) .
Sb3 O1 2.031(6) .
Sb3 O6 2.032(5) .
Sb3 C25 2.111(8) .
Sb3 C19 2.115(9) .
Sb3 O2 2.205(5) .
Si1 O5 1.610(6) .
Si1 O7 1.627(6) .
Si1 O4 1.646(6) .
Si1 C31 1.859(9) .
C22 C21 1.339(18) .
C22 C23 1.356(19) .
C22 H22 0.9300 .
C13 C14 1.367(13) .
C13 C18 1.369(13) .
C25 C30 1.372(13) .
C25 C26 1.392(13) .
C19 C24 1.358(13) .
C19 C20 1.390(13) .
C2 C3 1.361(13) .
C2 C1 1.373(12) .
C2 H2 0.9300 .
C1 C6 1.391(13) .
C26 C27 1.389(13) .
C26 H26 0.9300 .
C6 C5 1.359(14) .
C6 H6 0.9300 .
C27 C28 1.373(16) .
C27 H27 0.9300 .
C20 C21 1.391(16) .
C20 H20 0.9300 .
C18 C17 1.357(16) .
C18 H18 0.9300 .
C14 C15 1.382(16) .
C14 H14 0.9300 .
C24 C23 1.371(17) .
C24 H24 0.9300 .
C3 C4 1.347(15) .
C3 H3 0.9300 .
C30 C29 1.368(14) .
C30 H30 0.9300 .
C5 C4 1.349(15) .
C5 H5 0.9300 .
C28 C29 1.341(16) .
C28 H28 0.9300 .
C4 H4 0.9300 .
C17 C16 1.347(18) .
C17 H17 0.9300 .
C21 H21 0.9300 .
C29 H29 0.9300 .
C23 H23 0.9300 .
O7 Sb2 1.938(5) 2_565
C31 C36 1.515(12) .
C31 C32 1.537(13) .
C31 H31 0.9800 .
C36 C35 1.545(13) .
C36 H36A 0.9700 .
C36 H36B 0.9700 .
C32 C33 1.526(13) .
C32 H32A 0.9700 .
C32 H32B 0.9700 .
C35 C34 1.479(16) .
C35 H35A 0.9700 .
C35 H35B 0.9700 .
C16 C15 1.353(18) .
C16 H16 0.9300 .
C15 H15 0.9300 .
C33 C34 1.519(16) .
C33 H33A 0.9700 .
C33 H33B 0.9700 .
C34 H34A 0.9700 .
C34 H34B 0.9700 .
C7 C12 1.365(13) .
C7 C8 1.367(12) .
C8 C9 1.362(13) .
C8 H8 0.9300 .
C12 C11 1.397(14) .
C12 H12 0.9300 .
C10 C9 1.359(16) .
C10 C11 1.363(15) .
C10 H10 0.9300 .
C9 H9 0.9300 .
C11 H11 0.9300 .
