#------------------------------------------------------------------------------
#$Date: 2019-11-25 00:34:17 +0200 (Mon, 25 Nov 2019) $
#$Revision: 239771 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/35/01/4350187.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4350187
loop_
_publ_author_name
'Dong, Yu-Bin'
'Xu, Hong-Xia'
'Ma, Jian-Ping'
'Huang, Ru-Qi'
_publ_section_title
;
 Silver(I) coordination polymers based on a nano-sized bent
 bis(3-acetylenylphenyl-(4-cyanophenyl))oxadiazole ligand: the role of
 ligand isomerism and the templating effect of polyatomic anions and
 solvent intermediates.
;
_journal_issue                   8
_journal_name_full               'Inorganic chemistry'
_journal_page_first              3325
_journal_page_last               3343
_journal_paper_doi               10.1021/ic052158w
_journal_volume                  45
_journal_year                    2006
_chemical_formula_sum            'C32 H16 Ag F6 N4 O P'
_chemical_formula_weight         725.33
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.228(2)
_cell_angle_beta                 105.754(2)
_cell_angle_gamma                93.779(2)
_cell_formula_units_Z            2
_cell_length_a                   10.7276(14)
_cell_length_b                   12.2969(16)
_cell_length_c                   16.825(2)
_cell_measurement_reflns_used    2457
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      21.049
_cell_measurement_theta_min      2.442
_cell_volume                     1957.5(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.946
_diffrn_measured_fraction_theta_max 0.946
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0276
_diffrn_reflns_av_sigmaI/netI    0.0715
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            9973
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.81
_exptl_absorpt_coefficient_mu    0.610
_exptl_absorpt_correction_T_max  0.9087
_exptl_absorpt_correction_T_min  0.8775
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            COLOURLESS
_exptl_crystal_density_diffrn    1.231
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             720
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.16
_refine_diff_density_max         0.924
_refine_diff_density_min         -0.494
_refine_diff_density_rms         '0.107 End ===='
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     465
_refine_ls_number_reflns         6702
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.008
_refine_ls_R_factor_all          0.1153
_refine_ls_R_factor_gt           0.0817
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1469P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2159
_refine_ls_wR_factor_ref         0.2331
_reflns_number_gt                4210
_reflns_number_total             6702
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic052158wsi20051219_053724.cif
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        1957.6(4)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4350187
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 1.00088(5) 0.43930(6) 0.38068(3) 0.0719(3) Uani 1 1 d . . .
N1 N 0.8086(5) 0.4467(6) 0.4148(3) 0.0593(15) Uani 1 1 d . . .
N2 N 0.8045(5) 0.4941(5) 0.5044(3) 0.0577(15) Uani 1 1 d . . .
N3 N 0.9871(8) 0.4865(8) -0.2710(5) 0.091(2) Uani 1 1 d . . .
N4 N 0.9892(9) 1.2449(7) 1.2688(5) 0.098(2) Uani 1 1 d . . .
O1 O 0.6199(4) 0.3699(5) 0.4166(3) 0.0635(13) Uani 1 1 d . . .
C1 C 0.6999(6) 0.3722(7) 0.3667(4) 0.0564(17) Uani 1 1 d . . .
C2 C 0.6542(6) 0.3001(7) 0.2712(4) 0.0621(19) Uani 1 1 d . . .
C3 C 0.5799(8) 0.1904(9) 0.2407(5) 0.091(3) Uani 1 1 d . . .
H3 H 0.5505 0.1663 0.2799 0.110 Uiso 1 1 calc R . .
C4 C 0.5479(9) 0.1139(11) 0.1501(5) 0.118(4) Uani 1 1 d . . .
H4 H 0.5016 0.0371 0.1295 0.142 Uiso 1 1 calc R . .
C5 C 0.5856(8) 0.1537(9) 0.0921(5) 0.090(3) Uani 1 1 d . . .
H5 H 0.5619 0.1037 0.0316 0.107 Uiso 1 1 calc R . .
C6 C 0.6584(6) 0.2669(8) 0.1215(4) 0.065(2) Uani 1 1 d . . .
C7 C 0.6957(6) 0.3396(7) 0.2136(4) 0.0589(18) Uani 1 1 d . . .
H7 H 0.7481 0.4141 0.2359 0.071 Uiso 1 1 calc R . .
C8 C 0.7037(8) 0.3044(8) 0.0623(5) 0.076(2) Uani 1 1 d . . .
C9 C 0.7445(8) 0.3277(8) 0.0104(5) 0.073(2) Uani 1 1 d . . .
C10 C 0.7988(8) 0.3650(8) -0.0482(5) 0.067(2) Uani 1 1 d . . .
C11 C 0.8312(12) 0.2794(8) -0.1153(6) 0.097(3) Uani 1 1 d . . .
H11 H 0.8200 0.2008 -0.1213 0.116 Uiso 1 1 calc R . .
C12 C 0.8802(12) 0.3104(9) -0.1732(7) 0.101(3) Uani 1 1 d . . .
H12 H 0.9014 0.2530 -0.2190 0.122 Uiso 1 1 calc R . .
C13 C 0.8974(8) 0.4268(9) -0.1627(6) 0.071(2) Uani 1 1 d . . .
C14 C 0.9496(9) 0.4590(8) -0.2239(6) 0.079(2) Uani 1 1 d . . .
C15 C 0.8696(9) 0.5108(9) -0.0959(7) 0.084(2) Uani 1 1 d . . .
H15 H 0.8866 0.5899 -0.0878 0.100 Uiso 1 1 calc R . .
C16 C 0.8154(9) 0.4808(9) -0.0384(6) 0.081(2) Uani 1 1 d . . .
H16 H 0.7912 0.5383 0.0056 0.097 Uiso 1 1 calc R . .
C17 C 0.6937(6) 0.4458(6) 0.5013(4) 0.0530(16) Uani 1 1 d . . .
C18 C 0.6377(6) 0.4618(6) 0.5751(4) 0.0547(17) Uani 1 1 d . . .
C19 C 0.5464(8) 0.3762(8) 0.5679(5) 0.081(3) Uani 1 1 d . . .
H19 H 0.5116 0.3099 0.5141 0.097 Uiso 1 1 calc R . .
C20 C 0.5031(9) 0.3860(8) 0.6409(6) 0.090(3) Uani 1 1 d . . .
H20 H 0.4408 0.3257 0.6360 0.108 Uiso 1 1 calc R . .
C21 C 0.5527(9) 0.4853(8) 0.7204(6) 0.084(3) Uani 1 1 d . . .
H21 H 0.5260 0.4905 0.7696 0.101 Uiso 1 1 calc R . .
C22 C 0.6432(7) 0.5779(7) 0.7270(4) 0.0563(17) Uani 1 1 d . . .
C23 C 0.6872(6) 0.5654(6) 0.6535(4) 0.0462(15) Uani 1 1 d . . .
H23 H 0.7486 0.6253 0.6568 0.055 Uiso 1 1 calc R . .
C24 C 0.6939(8) 0.6813(7) 0.8070(5) 0.0635(19) Uani 1 1 d . . .
C25 C 0.7369(8) 0.7671(7) 0.8769(5) 0.069(2) Uani 1 1 d . . .
C26 C 0.7878(8) 0.8690(7) 0.9593(5) 0.0625(19) Uani 1 1 d . . .
C27 C 0.8106(11) 0.8558(8) 1.0414(6) 0.090(3) Uani 1 1 d . . .
H27 H 0.7894 0.7813 1.0415 0.108 Uiso 1 1 calc R . .
C28 C 0.8635(9) 0.9515(7) 1.1206(5) 0.075(2) Uani 1 1 d . . .
H28 H 0.8780 0.9422 1.1747 0.090 Uiso 1 1 calc R . .
C29 C 0.8956(8) 1.0620(7) 1.1211(5) 0.071(2) Uani 1 1 d . . .
C30 C 0.9497(9) 1.1651(8) 1.2051(6) 0.082(2) Uani 1 1 d . . .
C31 C 0.8780(10) 1.0743(8) 1.0396(6) 0.084(3) Uani 1 1 d . . .
H31 H 0.9037 1.1481 1.0397 0.101 Uiso 1 1 calc R . .
C32 C 0.8237(9) 0.9795(8) 0.9601(6) 0.080(2) Uani 1 1 d . . .
H32 H 0.8108 0.9889 0.9062 0.096 Uiso 1 1 calc R . .
F1A F 0.6497(19) 1.0658(9) 0.6575(10) 0.156(7) Uani 0.480(5) 1 d P A 1
F2A F 0.8358(12) 0.9940(13) 0.7067(12) 0.144(6) Uani 0.480(5) 1 d P A 1
F3A F 0.6619(14) 0.9910(12) 0.7543(8) 0.121(4) Uani 0.480(5) 1 d P A 1
F4A F 0.698(2) 0.8181(15) 0.6663(12) 0.163(7) Uani 0.480(5) 1 d P A 1
F5A F 0.5277(12) 0.8914(10) 0.6186(8) 0.104(4) Uani 0.480(5) 1 d P A 1
F6A F 0.6938(12) 0.8982(10) 0.5638(8) 0.105(4) Uani 0.480(5) 1 d P A 1
F1B F 0.6142(16) 0.8144(11) 0.1722(14) 0.245(12) Uani 0.520(5) 1 d PD A 2
F2B F 0.8009(10) 0.7363(18) 0.1880(16) 0.234(12) Uani 0.520(5) 1 d PD A 2
F3B F 0.684(2) 0.752(3) 0.2779(6) 0.41(3) Uani 0.520(5) 1 d PD A 2
F4B F 0.685(2) 0.5729(15) 0.1791(18) 0.52(5) Uani 0.520(5) 1 d PD A 2
F5B F 0.5030(10) 0.6504(17) 0.1574(13) 0.220(10) Uani 0.520(5) 1 d PD A 2
F6B F 0.623(2) 0.6421(16) 0.0683(7) 0.222(9) Uiso 0.520(5) 1 d PD A 2
P1A P 0.6867(5) 0.9395(4) 0.6639(3) 0.0702(14) Uani 0.480(5) 1 d P A 1
P1B P 0.6514(6) 0.6923(5) 0.1728(4) 0.0961(18) Uani 0.520(5) 1 d PD A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N1 118.64(17) 2_766 .
N2 Ag1 N3 109.5(2) 2_766 2_765
N1 Ag1 N3 115.2(2) . 2_765
N2 Ag1 N4 113.0(2) 2_766 1_544
N1 Ag1 N4 109.4(3) . 1_544
N3 Ag1 N4 86.7(3) 2_765 1_544
C1 N1 N2 106.5(5) . .
C1 N1 Ag1 124.9(5) . .
N2 N1 Ag1 123.1(4) . .
C17 N2 N1 105.9(5) . .
C17 N2 Ag1 129.3(4) . 2_766
N1 N2 Ag1 118.3(4) . 2_766
C14 N3 Ag1 161.7(7) . 2_765
C30 N4 Ag1 158.5(8) . 1_566
C1 O1 C17 103.4(5) . .
N1 C1 O1 111.4(6) . .
N1 C1 C2 129.1(6) . .
O1 C1 C2 119.4(6) . .
C3 C2 C7 121.2(6) . .
C3 C2 C1 119.1(7) . .
C7 C2 C1 119.5(7) . .
C2 C3 C4 119.9(7) . .
C5 C4 C3 119.1(9) . .
C4 C5 C6 121.8(7) . .
C5 C6 C7 118.0(7) . .
C5 C6 C8 121.3(7) . .
C7 C6 C8 120.5(7) . .
C2 C7 C6 119.9(7) . .
C9 C8 C6 175.0(10) . .
C8 C9 C10 175.7(9) . .
C16 C10 C11 120.6(7) . .
C16 C10 C9 121.4(7) . .
C11 C10 C9 118.0(8) . .
C12 C11 C10 119.9(8) . .
C13 C12 C11 119.2(8) . .
C15 C13 C12 121.0(7) . .
C15 C13 C14 120.1(9) . .
C12 C13 C14 118.9(8) . .
N3 C14 C13 177.7(10) . .
C13 C15 C16 120.7(9) . .
C10 C16 C15 118.5(8) . .
N2 C17 O1 112.7(5) . .
N2 C17 C18 129.2(6) . .
O1 C17 C18 118.1(5) . .
C19 C18 C23 121.4(6) . .
C19 C18 C17 120.2(6) . .
C23 C18 C17 118.3(6) . .
C18 C19 C20 120.2(7) . .
C21 C20 C19 120.1(7) . .
C20 C21 C22 120.1(6) . .
C21 C22 C23 118.9(6) . .
C21 C22 C24 121.3(6) . .
C23 C22 C24 119.7(7) . .
C18 C23 C22 119.2(6) . .
C25 C24 C22 177.7(8) . .
C24 C25 C26 179.6(9) . .
C32 C26 C27 119.2(7) . .
C32 C26 C25 121.1(7) . .
C27 C26 C25 119.5(7) . .
C28 C27 C26 120.2(8) . .
C27 C28 C29 120.3(7) . .
C28 C29 C31 119.5(7) . .
C28 C29 C30 120.8(8) . .
C31 C29 C30 119.8(8) . .
N4 C30 C29 178.6(10) . .
C32 C31 C29 120.6(8) . .
C31 C32 C26 120.1(8) . .
F4A P1A F3A 94.6(9) . .
F4A P1A F2A 96.9(10) . .
F3A P1A F2A 92.5(9) . .
F4A P1A F6A 93.2(9) . .
F3A P1A F6A 170.0(9) . .
F2A P1A F6A 92.8(8) . .
F4A P1A F5A 87.3(9) . .
F3A P1A F5A 87.0(7) . .
F2A P1A F5A 175.8(8) . .
F6A P1A F5A 87.0(6) . .
F4A P1A F1A 171.4(11) . .
F3A P1A F1A 83.3(9) . .
F2A P1A F1A 91.6(9) . .
F6A P1A F1A 88.1(8) . .
F5A P1A F1A 84.2(8) . .
F5B P1B F4B 90.8(8) . .
F5B P1B F6B 89.6(9) . .
F4B P1B F6B 93.1(10) . .
F5B P1B F3B 92.7(9) . .
F4B P1B F3B 90.3(9) . .
F6B P1B F3B 175.9(12) . .
F5B P1B F2B 179.1(8) . .
F4B P1B F2B 90.1(8) . .
F6B P1B F2B 90.2(11) . .
F3B P1B F2B 87.4(9) . .
F5B P1B F1B 87.3(8) . .
F4B P1B F1B 176.2(12) . .
F6B P1B F1B 90.2(8) . .
F3B P1B F1B 86.5(13) . .
F2B P1B F1B 91.8(8) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.282(5) 2_766
Ag1 N1 2.285(5) .
Ag1 N3 2.364(7) 2_765
Ag1 N4 2.418(8) 1_544
N1 C1 1.290(9) .
N1 N2 1.420(7) .
N2 C17 1.273(8) .
N2 Ag1 2.282(5) 2_766
N3 C14 1.120(10) .
N3 Ag1 2.364(7) 2_765
N4 C30 1.108(10) .
N4 Ag1 2.418(8) 1_566
O1 C1 1.359(8) .
O1 C17 1.362(8) .
C1 C2 1.446(9) .
C2 C3 1.361(11) .
C2 C7 1.386(10) .
C3 C4 1.400(11) .
C4 C5 1.376(12) .
C5 C6 1.393(12) .
C6 C7 1.404(9) .
C6 C8 1.418(11) .
C8 C9 1.186(10) .
C9 C10 1.458(10) .
C10 C16 1.367(12) .
C10 C11 1.380(11) .
C11 C12 1.376(12) .
C12 C13 1.371(12) .
C13 C15 1.342(13) .
C13 C14 1.451(11) .
C15 C16 1.395(12) .
C17 C18 1.478(8) .
C18 C19 1.338(10) .
C18 C23 1.400(9) .
C19 C20 1.395(10) .
C20 C21 1.381(12) .
C21 C22 1.399(11) .
C22 C23 1.401(8) .
C22 C24 1.413(10) .
C24 C25 1.204(10) .
C25 C26 1.426(10) .
C26 C32 1.381(11) .
C26 C27 1.408(10) .
C27 C28 1.359(11) .
C28 C29 1.376(11) .
C29 C31 1.398(12) .
C29 C30 1.450(11) .
C31 C32 1.358(12) .
F1A P1A 1.662(11) .
F2A P1A 1.553(13) .
F3A P1A 1.526(13) .
F4A P1A 1.520(16) .
F5A P1A 1.636(13) .
F6A P1A 1.598(12) .
F1B P1B 1.582(8) .
F2B P1B 1.579(8) .
F3B P1B 1.573(9) .
F4B P1B 1.568(9) .
F5B P1B 1.561(8) .
F6B P1B 1.569(9) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N2 Ag1 N1 C1 -148.3(6) 2_766 .
N3 Ag1 N1 C1 79.1(7) 2_765 .
N4 Ag1 N1 C1 -16.5(7) 1_544 .
N2 Ag1 N1 N2 1.9(7) 2_766 .
N3 Ag1 N1 N2 -130.7(5) 2_765 .
N4 Ag1 N1 N2 133.6(5) 1_544 .
C1 N1 N2 C17 -1.2(8) . .
Ag1 N1 N2 C17 -156.0(5) . .
C1 N1 N2 Ag1 152.9(5) . 2_766
Ag1 N1 N2 Ag1 -1.9(7) . 2_766
N2 N1 C1 O1 2.8(8) . .
Ag1 N1 C1 O1 157.0(4) . .
N2 N1 C1 C2 179.8(7) . .
Ag1 N1 C1 C2 -26.0(11) . .
C17 O1 C1 N1 -3.1(8) . .
C17 O1 C1 C2 179.5(7) . .
N1 C1 C2 C3 146.0(9) . .
O1 C1 C2 C3 -37.2(11) . .
N1 C1 C2 C7 -28.8(12) . .
O1 C1 C2 C7 148.0(7) . .
C7 C2 C3 C4 2.1(14) . .
C1 C2 C3 C4 -172.5(9) . .
C2 C3 C4 C5 -3.9(17) . .
C3 C4 C5 C6 2.0(17) . .
C4 C5 C6 C7 1.5(14) . .
C4 C5 C6 C8 176.1(10) . .
C3 C2 C7 C6 1.5(11) . .
C1 C2 C7 C6 176.1(7) . .
C5 C6 C7 C2 -3.3(11) . .
C8 C6 C7 C2 -177.8(7) . .
C5 C6 C8 C9 -45(10) . .
C7 C6 C8 C9 130(9) . .
C6 C8 C9 C10 -138(11) . .
C8 C9 C10 C16 -30(12) . .
C8 C9 C10 C11 151(12) . .
C16 C10 C11 C12 -0.3(16) . .
C9 C10 C11 C12 178.7(10) . .
C10 C11 C12 C13 0.7(17) . .
C11 C12 C13 C15 1.3(16) . .
C11 C12 C13 C14 179.8(10) . .
Ag1 N3 C14 C13 -27(29) 2_765 .
C15 C13 C14 N3 -38(27) . .
C12 C13 C14 N3 144(27) . .
C12 C13 C15 C16 -3.6(14) . .
C14 C13 C15 C16 177.9(8) . .
C11 C10 C16 C15 -1.9(14) . .
C9 C10 C16 C15 179.1(8) . .
C13 C15 C16 C10 3.9(14) . .
N1 N2 C17 O1 -0.8(8) . .
Ag1 N2 C17 O1 -151.0(5) 2_766 .
N1 N2 C17 C18 179.5(7) . .
Ag1 N2 C17 C18 29.2(11) 2_766 .
C1 O1 C17 N2 2.3(8) . .
C1 O1 C17 C18 -177.9(7) . .
N2 C17 C18 C19 -155.2(9) . .
O1 C17 C18 C19 25.1(11) . .
N2 C17 C18 C23 21.8(11) . .
O1 C17 C18 C23 -158.0(6) . .
C23 C18 C19 C20 -3.3(13) . .
C17 C18 C19 C20 173.6(8) . .
C18 C19 C20 C21 1.2(15) . .
C19 C20 C21 C22 2.1(15) . .
C20 C21 C22 C23 -3.3(13) . .
C20 C21 C22 C24 179.0(9) . .
C19 C18 C23 C22 2.1(11) . .
C17 C18 C23 C22 -174.9(6) . .
C21 C22 C23 C18 1.2(10) . .
C24 C22 C23 C18 179.0(7) . .
C21 C22 C24 C25 33(22) . .
C23 C22 C24 C25 -144(21) . .
C22 C24 C25 C26 -168(100) . .
C24 C25 C26 C32 -14(100) . .
C24 C25 C26 C27 171(100) . .
C32 C26 C27 C28 2.1(14) . .
C25 C26 C27 C28 177.6(9) . .
C26 C27 C28 C29 -0.2(15) . .
C27 C28 C29 C31 -2.4(14) . .
C27 C28 C29 C30 178.8(9) . .
Ag1 N4 C30 C29 3(56) 1_566 .
C28 C29 C30 N4 -123(53) . .
C31 C29 C30 N4 58(54) . .
C28 C29 C31 C32 3.2(14) . .
C30 C29 C31 C32 -178.0(9) . .
C29 C31 C32 C26 -1.3(15) . .
C27 C26 C32 C31 -1.3(14) . .
C25 C26 C32 C31 -176.7(9) . .
