#------------------------------------------------------------------------------
#$Date: 2019-11-25 02:15:23 +0200 (Mon, 25 Nov 2019) $
#$Revision: 239945 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/35/05/4350567.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4350567
loop_
_publ_author_name
'Dong, Yu-Bin'
'Sun, Ting'
'Ma, Jian-Ping'
'Zhao, Xia-Xia'
'Huang, Ru-Qi'
_publ_section_title
;
 Ag(I) and Cu(II) discrete and polymeric complexes based on single- and
 double-armed oxadiazole-bridging organic clips.
;
_journal_issue                   26
_journal_name_full               'Inorganic chemistry'
_journal_page_first              10613
_journal_page_last               10628
_journal_paper_doi               10.1021/ic0612552
_journal_volume                  45
_journal_year                    2006
_chemical_formula_sum            'C28 H20 Cl4 Cu N6 O11'
_chemical_formula_weight         821.84
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.931(4)
_cell_angle_beta                 98.549(4)
_cell_angle_gamma                95.196(4)
_cell_formula_units_Z            2
_cell_length_a                   7.2359(15)
_cell_length_b                   14.946(3)
_cell_length_c                   17.339(4)
_cell_measurement_reflns_used    662
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      16.758
_cell_measurement_theta_min      2.422
_cell_volume                     1698.2(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.977
_diffrn_measured_fraction_theta_max 0.977
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0627
_diffrn_reflns_av_sigmaI/netI    0.1905
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            9048
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.54
_exptl_absorpt_coefficient_mu    1.025
_exptl_absorpt_correction_T_max  0.9602
_exptl_absorpt_correction_T_min  0.8451
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            BLUE
_exptl_crystal_density_diffrn    1.607
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plan
_exptl_crystal_F_000             830
_exptl_crystal_size_max          0.17
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.04
_refine_diff_density_max         0.495
_refine_diff_density_min         -0.387
_refine_diff_density_rms         '0.075 End ===='
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.978
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         6020
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.978
_refine_ls_R_factor_all          0.2107
_refine_ls_R_factor_gt           0.0887
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0115P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1532
_refine_ls_wR_factor_ref         0.1838
_reflns_number_gt                2474
_reflns_number_total             6020
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0612552si20060706_013537.cif
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4350567
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu -0.00391(13) 0.65616(7) 0.51967(5) 0.0609(4) Uani 1 1 d .
N1 N 0.2155(7) 0.4413(4) 0.0940(3) 0.0491(15) Uani 1 1 d .
N2 N 0.2150(8) 0.3427(4) 0.0820(3) 0.0516(16) Uani 1 1 d .
N3 N 0.0840(9) 0.6365(4) 0.4115(3) 0.0545(17) Uani 1 1 d .
N4 N 0.1055(9) 0.3086(4) 0.3736(3) 0.0527(17) Uani 1 1 d .
N5 N 0.2026(13) 0.8334(7) 0.5955(5) 0.078(2) Uani 1 1 d .
N6 N -0.2802(14) 0.5052(7) 0.4271(6) 0.091(3) Uani 1 1 d .
C1 C 0.2364(8) 0.4469(5) 0.0225(4) 0.0419(17) Uani 1 1 d .
C2 C 0.2507(8) 0.5339(5) 0.0019(4) 0.0439(18) Uani 1 1 d .
C3 C 0.2271(9) 0.6236(5) 0.0576(4) 0.0447(18) Uani 1 1 d .
C4 C 0.2384(9) 0.7040(5) 0.0375(5) 0.056(2) Uani 1 1 d .
H4 H 0.2172 0.7635 0.0754 0.067 Uiso 1 1 calc R
C5 C 0.2813(9) 0.6959(6) -0.0393(5) 0.057(2) Uani 1 1 d .
H5 H 0.2929 0.7505 -0.0529 0.069 Uiso 1 1 calc R
C6 C 0.3069(9) 0.6071(7) -0.0958(5) 0.063(2) Uani 1 1 d .
H6 H 0.3345 0.6016 -0.1479 0.075 Uiso 1 1 calc R
C7 C 0.2921(9) 0.5253(5) -0.0757(4) 0.052(2) Uani 1 1 d .
H7 H 0.3098 0.4653 -0.1141 0.062 Uiso 1 1 calc R
C8 C 0.3089(12) 0.6352(5) 0.1975(4) 0.0458(19) Uani 1 1 d .
C9 C 0.2241(10) 0.6346(5) 0.2708(4) 0.0470(19) Uani 1 1 d .
C10 C 0.0439(11) 0.6549(5) 0.2809(4) 0.059(2) Uani 1 1 d .
H10 H -0.0338 0.6680 0.2399 0.071 Uiso 1 1 calc R
C11 C -0.0176(10) 0.6555(5) 0.3512(5) 0.060(2) Uani 1 1 d .
H11 H -0.1382 0.6700 0.3573 0.072 Uiso 1 1 calc R
C12 C 0.2541(12) 0.6119(6) 0.3999(5) 0.076(3) Uani 1 1 d .
H12 H 0.3252 0.5947 0.4400 0.091 Uiso 1 1 calc R
C13 C 0.3271(10) 0.6113(6) 0.3313(4) 0.068(2) Uani 1 1 d .
H13 H 0.4469 0.5950 0.3258 0.082 Uiso 1 1 calc R
C14 C 0.2377(9) 0.2980(5) 0.0048(4) 0.0442(18) Uani 1 1 d .
C15 C 0.2514(9) 0.1968(6) -0.0396(4) 0.0483(19) Uani 1 1 d .
C16 C 0.2941(9) 0.1625(6) -0.1214(4) 0.058(2) Uani 1 1 d .
H16 H 0.3101 0.2057 -0.1479 0.070 Uiso 1 1 calc R
C17 C 0.3125(11) 0.0661(6) -0.1629(5) 0.071(2) Uani 1 1 d .
H17 H 0.3380 0.0448 -0.2174 0.086 Uiso 1 1 calc R
C18 C 0.2938(12) 0.0020(6) -0.1249(5) 0.081(3) Uani 1 1 d .
H18 H 0.3106 -0.0624 -0.1525 0.098 Uiso 1 1 calc R
C19 C 0.2495(10) 0.0329(6) -0.0446(5) 0.067(2) Uani 1 1 d .
H19 H 0.2323 -0.0110 -0.0188 0.081 Uiso 1 1 calc R
C20 C 0.2315(10) 0.1286(6) -0.0042(4) 0.053(2) Uani 1 1 d .
C21 C 0.3170(13) 0.2000(5) 0.1454(4) 0.051(2) Uani 1 1 d .
C22 C 0.2345(11) 0.2382(5) 0.2230(4) 0.0490(19) Uani 1 1 d .
C23 C 0.3442(10) 0.2489(5) 0.2985(4) 0.055(2) Uani 1 1 d .
H23 H 0.4650 0.2322 0.2998 0.066 Uiso 1 1 calc R
C24 C 0.2769(11) 0.2840(6) 0.3715(4) 0.061(2) Uani 1 1 d .
H24 H 0.3541 0.2911 0.4220 0.073 Uiso 1 1 calc R
C25 C -0.0018(11) 0.2992(6) 0.2998(5) 0.069(2) Uani 1 1 d .
H25 H -0.1222 0.3163 0.3004 0.083 Uiso 1 1 calc R
C26 C 0.0571(11) 0.2656(6) 0.2240(5) 0.063(2) Uani 1 1 d .
H26 H -0.0201 0.2614 0.1745 0.076 Uiso 1 1 calc R
C27 C 0.7284(16) 0.9246(8) 0.4490(7) 0.138(4) Uani 1 1 d .
H27A H 0.6724 0.9800 0.4458 0.165 Uiso 1 1 calc R
H27B H 0.8446 0.9500 0.4913 0.165 Uiso 1 1 calc R
C28 C 0.2012(15) 0.9955(7) 0.2791(6) 0.119(4) Uani 1 1 d .
H28A H 0.2966 1.0495 0.3183 0.143 Uiso 1 1 calc R
H28B H 0.0785 1.0107 0.2913 0.143 Uiso 1 1 calc R
O1 O 0.2510(6) 0.3594(3) -0.0363(3) 0.0471(12) Uani 1 1 d .
O2 O 0.1713(6) 0.6347(3) 0.1341(3) 0.0533(13) Uani 1 1 d .
O3 O 0.4750(7) 0.6415(4) 0.1970(3) 0.0666(16) Uani 1 1 d .
O4 O 0.4803(8) 0.2037(4) 0.1427(3) 0.0675(16) Uani 1 1 d .
O5 O 0.1730(7) 0.1577(3) 0.0758(3) 0.0566(13) Uani 1 1 d .
O6 O 0.2345(7) 0.7467(4) 0.5846(3) 0.0622(15) Uani 1 1 d .
O7 O 0.0543(10) 0.8428(5) 0.5604(4) 0.097(2) Uani 1 1 d .
O8 O 0.3315(10) 0.9000(5) 0.6392(4) 0.117(3) Uani 1 1 d .
O9 O -0.1673(17) 0.4704(8) 0.4531(6) 0.196(5) Uani 1 1 d .
O10 O -0.2713(7) 0.5938(4) 0.4501(3) 0.0682(15) Uani 1 1 d .
O11 O -0.4075(16) 0.4524(7) 0.3852(9) 0.300(9) Uani 1 1 d .
Cl1 Cl 0.2083(4) 0.9839(2) 0.17682(19) 0.1233(10) Uani 1 1 d .
Cl2 Cl 0.2388(6) 0.8935(3) 0.2945(3) 0.2038(19) Uani 1 1 d .
Cl3 Cl 0.7802(9) 0.8627(4) 0.3571(3) 0.291(3) Uani 1 1 d .
Cl4 Cl 0.5768(5) 0.8582(3) 0.4813(2) 0.1809(16) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O6 Cu1 N3 90.0(2) . .
O6 Cu1 N4 89.6(2) . 2_566
N3 Cu1 N4 172.3(3) . 2_566
O6 Cu1 O10 165.5(2) . .
N3 Cu1 O10 88.7(2) . .
N4 Cu1 O10 89.8(2) 2_566 .
C1 N1 N2 106.4(5) . .
C14 N2 N1 105.9(5) . .
C11 N3 C12 117.3(6) . .
C11 N3 Cu1 120.8(5) . .
C12 N3 Cu1 121.7(6) . .
C24 N4 C25 117.4(6) . .
C24 N4 Cu1 120.3(5) . 2_566
C25 N4 Cu1 121.9(6) . 2_566
O7 N5 O8 125.2(11) . .
O7 N5 O6 118.6(9) . .
O8 N5 O6 116.1(9) . .
O11 N6 O9 113.9(12) . .
O11 N6 O10 123.0(12) . .
O9 N6 O10 122.7(12) . .
N1 C1 O1 111.9(6) . .
N1 C1 C2 128.4(6) . .
O1 C1 C2 119.7(6) . .
C3 C2 C7 118.9(7) . .
C3 C2 C1 122.1(6) . .
C7 C2 C1 118.9(7) . .
C4 C3 C2 121.7(6) . .
C4 C3 O2 116.9(6) . .
C2 C3 O2 121.1(6) . .
C3 C4 C5 119.4(7) . .
C3 C4 H4 120.3 . .
C5 C4 H4 120.3 . .
C6 C5 C4 119.9(7) . .
C6 C5 H5 120.1 . .
C4 C5 H5 120.1 . .
C5 C6 C7 120.5(7) . .
C5 C6 H6 119.8 . .
C7 C6 H6 119.8 . .
C2 C7 C6 119.5(7) . .
C2 C7 H7 120.2 . .
C6 C7 H7 120.2 . .
O3 C8 O2 125.3(6) . .
O3 C8 C9 124.5(7) . .
O2 C8 C9 110.1(6) . .
C13 C9 C10 117.4(7) . .
C13 C9 C8 118.8(7) . .
C10 C9 C8 123.8(7) . .
C11 C10 C9 119.2(7) . .
C11 C10 H10 120.4 . .
C9 C10 H10 120.4 . .
N3 C11 C10 123.7(7) . .
N3 C11 H11 118.1 . .
C10 C11 H11 118.1 . .
N3 C12 C13 122.3(8) . .
N3 C12 H12 118.8 . .
C13 C12 H12 118.8 . .
C9 C13 C12 120.0(8) . .
C9 C13 H13 120.0 . .
C12 C13 H13 120.0 . .
N2 C14 O1 112.2(7) . .
N2 C14 C15 129.1(7) . .
O1 C14 C15 118.7(6) . .
C20 C15 C16 116.0(7) . .
C20 C15 C14 122.7(6) . .
C16 C15 C14 121.3(7) . .
C17 C16 C15 121.2(7) . .
C17 C16 H16 119.4 . .
C15 C16 H16 119.4 . .
C18 C17 C16 120.6(8) . .
C18 C17 H17 119.7 . .
C16 C17 H17 119.7 . .
C17 C18 C19 119.9(8) . .
C17 C18 H18 120.1 . .
C19 C18 H18 120.1 . .
C20 C19 C18 119.0(8) . .
C20 C19 H19 120.5 . .
C18 C19 H19 120.5 . .
C19 C20 C15 123.3(7) . .
C19 C20 O5 118.2(7) . .
C15 C20 O5 118.2(7) . .
O4 C21 O5 124.4(7) . .
O4 C21 C22 126.5(7) . .
O5 C21 C22 109.1(7) . .
C23 C22 C26 118.1(7) . .
C23 C22 C21 117.5(7) . .
C26 C22 C21 124.3(7) . .
C24 C23 C22 120.2(7) . .
C24 C23 H23 119.9 . .
C22 C23 H23 119.9 . .
N4 C24 C23 122.6(7) . .
N4 C24 H24 118.7 . .
C23 C24 H24 118.7 . .
N4 C25 C26 123.3(8) . .
N4 C25 H25 118.4 . .
C26 C25 H25 118.4 . .
C25 C26 C22 118.3(7) . .
C25 C26 H26 120.8 . .
C22 C26 H26 120.8 . .
Cl3 C27 Cl4 114.0(7) . .
Cl3 C27 H27A 108.8 . .
Cl4 C27 H27A 108.8 . .
Cl3 C27 H27B 108.8 . .
Cl4 C27 H27B 108.8 . .
H27A C27 H27B 107.6 . .
Cl2 C28 Cl1 112.4(6) . .
Cl2 C28 H28A 109.1 . .
Cl1 C28 H28A 109.1 . .
Cl2 C28 H28B 109.1 . .
Cl1 C28 H28B 109.1 . .
H28A C28 H28B 107.9 . .
C1 O1 C14 103.6(5) . .
C8 O2 C3 116.1(5) . .
C21 O5 C20 115.0(5) . .
N5 O6 Cu1 107.0(5) . .
N6 O10 Cu1 107.2(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 O6 1.984(5) .
Cu1 N3 1.997(5) .
Cu1 N4 1.998(5) 2_566
Cu1 O10 2.051(5) .
N1 C1 1.303(7) .
N1 N2 1.408(7) .
N2 C14 1.297(7) .
N3 C11 1.321(8) .
N3 C12 1.338(9) .
N4 C24 1.327(8) .
N4 C25 1.345(8) .
N4 Cu1 1.998(5) 2_566
N5 O7 1.199(9) .
N5 O8 1.223(8) .
N5 O6 1.285(9) .
N6 O11 1.114(9) .
N6 O9 1.134(10) .
N6 O10 1.225(9) .
C1 O1 1.350(7) .
C1 C2 1.471(9) .
C2 C3 1.373(9) .
C2 C7 1.382(8) .
C3 C4 1.369(9) .
C3 O2 1.399(7) .
C4 C5 1.376(9) .
C4 H4 0.9300 .
C5 C6 1.371(10) .
C5 H5 0.9300 .
C6 C7 1.391(10) .
C6 H6 0.9300 .
C7 H7 0.9300 .
C8 O3 1.198(7) .
C8 O2 1.366(8) .
C8 C9 1.495(9) .
C9 C13 1.364(9) .
C9 C10 1.386(9) .
C10 C11 1.355(8) .
C10 H10 0.9300 .
C11 H11 0.9300 .
C12 C13 1.370(9) .
C12 H12 0.9300 .
C13 H13 0.9300 .
C14 O1 1.362(7) .
C14 C15 1.438(9) .
C15 C20 1.380(9) .
C15 C16 1.409(9) .
C16 C17 1.379(10) .
C16 H16 0.9300 .
C17 C18 1.358(10) .
C17 H17 0.9300 .
C18 C19 1.390(9) .
C18 H18 0.9300 .
C19 C20 1.367(10) .
C19 H19 0.9300 .
C20 O5 1.431(7) .
C21 O4 1.187(7) .
C21 O5 1.371(8) .
C21 C22 1.490(9) .
C22 C23 1.371(9) .
C22 C26 1.383(9) .
C23 C24 1.360(9) .
C23 H23 0.9300 .
C24 H24 0.9300 .
C25 C26 1.369(9) .
C25 H25 0.9300 .
C26 H26 0.9300 .
C27 Cl3 1.636(11) .
C27 Cl4 1.703(10) .
C27 H27A 0.9700 .
C27 H27B 0.9700 .
C28 Cl2 1.681(10) .
C28 Cl1 1.725(9) .
C28 H28A 0.9700 .
C28 H28B 0.9700 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C1 N1 N2 C14 0.7(7) .
O6 Cu1 N3 C11 -122.8(6) .
N4 Cu1 N3 C11 -36(2) 2_566
O10 Cu1 N3 C11 42.8(6) .
O6 Cu1 N3 C12 51.5(6) .
N4 Cu1 N3 C12 138.2(18) 2_566
O10 Cu1 N3 C12 -143.0(6) .
N2 N1 C1 O1 -0.4(7) .
N2 N1 C1 C2 -178.4(6) .
N1 C1 C2 C3 -5.6(10) .
O1 C1 C2 C3 176.6(6) .
N1 C1 C2 C7 173.4(6) .
O1 C1 C2 C7 -4.5(9) .
C7 C2 C3 C4 1.8(10) .
C1 C2 C3 C4 -179.2(6) .
C7 C2 C3 O2 175.2(6) .
C1 C2 C3 O2 -5.8(10) .
C2 C3 C4 C5 -2.4(10) .
O2 C3 C4 C5 -176.1(6) .
C3 C4 C5 C6 1.9(10) .
C4 C5 C6 C7 -0.7(11) .
C3 C2 C7 C6 -0.7(9) .
C1 C2 C7 C6 -179.7(6) .
C5 C6 C7 C2 0.1(10) .
O3 C8 C9 C13 -20.0(11) .
O2 C8 C9 C13 164.3(6) .
O3 C8 C9 C10 161.0(7) .
O2 C8 C9 C10 -14.7(9) .
C13 C9 C10 C11 3.1(11) .
C8 C9 C10 C11 -177.9(6) .
C12 N3 C11 C10 -2.6(11) .
Cu1 N3 C11 C10 171.9(5) .
C9 C10 C11 N3 -0.7(11) .
C11 N3 C12 C13 3.6(12) .
Cu1 N3 C12 C13 -170.8(6) .
C10 C9 C13 C12 -2.2(11) .
C8 C9 C13 C12 178.8(7) .
N3 C12 C13 C9 -1.2(12) .
N1 N2 C14 O1 -0.8(7) .
N1 N2 C14 C15 178.6(6) .
N2 C14 C15 C20 3.4(11) .
O1 C14 C15 C20 -177.2(6) .
N2 C14 C15 C16 -173.9(6) .
O1 C14 C15 C16 5.4(10) .
C20 C15 C16 C17 0.6(10) .
C14 C15 C16 C17 178.1(7) .
C15 C16 C17 C18 -1.4(12) .
C16 C17 C18 C19 2.2(13) .
C17 C18 C19 C20 -2.1(12) .
C18 C19 C20 C15 1.4(12) .
C18 C19 C20 O5 175.7(6) .
C16 C15 C20 C19 -0.6(11) .
C14 C15 C20 C19 -178.1(7) .
C16 C15 C20 O5 -175.0(6) .
C14 C15 C20 O5 7.6(10) .
O4 C21 C22 C23 -23.4(11) .
O5 C21 C22 C23 155.8(6) .
O4 C21 C22 C26 154.9(8) .
O5 C21 C22 C26 -25.8(9) .
C26 C22 C23 C24 1.2(11) .
C21 C22 C23 C24 179.6(6) .
C25 N4 C24 C23 -1.1(11) .
Cu1 N4 C24 C23 172.4(5) 2_566
C22 C23 C24 N4 0.4(12) .
C24 N4 C25 C26 0.2(12) .
Cu1 N4 C25 C26 -173.2(6) 2_566
N4 C25 C26 C22 1.4(12) .
C23 C22 C26 C25 -2.0(11) .
C21 C22 C26 C25 179.7(7) .
N1 C1 O1 C14 -0.1(7) .
C2 C1 O1 C14 178.1(5) .
N2 C14 O1 C1 0.6(7) .
C15 C14 O1 C1 -178.9(6) .
O3 C8 O2 C3 11.6(10) .
C9 C8 O2 C3 -172.8(5) .
C4 C3 O2 C8 -108.8(7) .
C2 C3 O2 C8 77.6(8) .
O4 C21 O5 C20 -8.2(10) .
C22 C21 O5 C20 172.5(6) .
C19 C20 O5 C21 98.4(7) .
C15 C20 O5 C21 -86.9(8) .
O7 N5 O6 Cu1 -6.9(8) .
O8 N5 O6 Cu1 175.6(5) .
N3 Cu1 O6 N5 92.7(5) .
N4 Cu1 O6 N5 -79.6(5) 2_566
O10 Cu1 O6 N5 8.2(10) .
O11 N6 O10 Cu1 -176.7(12) .
O9 N6 O10 Cu1 11.2(12) .
O6 Cu1 O10 N6 169.7(7) .
N3 Cu1 O10 N6 85.0(6) .
N4 Cu1 O10 N6 -102.5(5) 2_566
