#------------------------------------------------------------------------------
#$Date: 2016-03-24 01:32:20 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179534 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/03/4500323.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4500323
loop_
_publ_author_name
'Sarma, Rupam'
'Deka, Himangshu'
'Boudalis, Athanassios K.'
'Baruah, Jubaraj B.'
_publ_section_title
;
 Coordination Polymers of Lanthanide(III): Toward Encapsulation of
 Well-Defined Assembly of Guest Molecules
;
_journal_issue                   2
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              547
_journal_paper_doi               10.1021/cg101432k
_journal_volume                  11
_journal_year                    2011
_chemical_formula_sum            'C34 H34 Ce N3 O11'
_chemical_formula_weight         800.76
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 112.500(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.8612(12)
_cell_length_b                   10.2716(9)
_cell_length_c                   28.254(2)
_cell_measurement_reflns_used    9880
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.60
_cell_measurement_theta_min      2.72
_cell_volume                     3448.4(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.968
_diffrn_measured_fraction_theta_max 0.968
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0531
_diffrn_reflns_av_sigmaI/netI    0.0400
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            31305
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.56
_exptl_absorpt_coefficient_mu    1.384
_exptl_absorpt_correction_T_max  0.3232
_exptl_absorpt_correction_T_min  0.1914
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.542
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1620
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         0.798
_refine_diff_density_min         -0.705
_refine_diff_density_rms         0.082
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     444
_refine_ls_number_reflns         5886
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.083
_refine_ls_R_factor_all          0.0433
_refine_ls_R_factor_gt           0.0329
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0529P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0916
_refine_ls_wR_factor_ref         0.0963
_reflns_number_gt                4661
_reflns_number_total             5886
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg101432k_si_003.cif
_cod_data_source_block           cebzbpno_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               4500323
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.0631(3) -0.0414(3) 0.08436(14) 0.0377(9) Uani 1 1 d .
C2 C -0.1611(3) -0.0949(3) 0.03955(13) 0.0350(8) Uani 1 1 d .
C3 C -0.1608(3) -0.0928(3) -0.00925(13) 0.0458(10) Uani 1 1 d .
H3 H -0.0999 -0.0572 -0.0148 0.055 Uiso 1 1 calc R
C4 C -0.2498(4) -0.1430(4) -0.04959(15) 0.0633(12) Uani 1 1 d .
H4 H -0.2483 -0.1426 -0.0822 0.076 Uiso 1 1 calc R
C5 C -0.3407(4) -0.1937(4) -0.0423(2) 0.0761(15) Uani 1 1 d .
H5 H -0.4011 -0.2273 -0.0699 0.091 Uiso 1 1 calc R
C6 C -0.3420(4) -0.1946(4) 0.0062(2) 0.0689(13) Uani 1 1 d .
H6 H -0.4038 -0.2286 0.0113 0.083 Uiso 1 1 calc R
C7 C -0.2527(3) -0.1458(4) 0.04690(16) 0.0502(10) Uani 1 1 d .
H7 H -0.2542 -0.1471 0.0796 0.060 Uiso 1 1 calc R
C8 C -0.1530(3) 0.2714(3) 0.17284(12) 0.0332(8) Uani 1 1 d .
C9 C -0.2389(3) 0.2915(3) 0.11985(12) 0.0324(8) Uani 1 1 d .
C10 C -0.2637(3) 0.1943(4) 0.08387(13) 0.0438(9) Uani 1 1 d .
H10 H -0.2320 0.1122 0.0934 0.053 Uiso 1 1 calc R
C11 C -0.3339(3) 0.2160(5) 0.03439(15) 0.0624(12) Uani 1 1 d .
H11 H -0.3501 0.1485 0.0108 0.075 Uiso 1 1 calc R
C12 C -0.3805(3) 0.3346(5) 0.01914(17) 0.0700(14) Uani 1 1 d .
H12 H -0.4261 0.3495 -0.0150 0.084 Uiso 1 1 calc R
C13 C -0.3598(3) 0.4324(5) 0.05456(19) 0.0666(13) Uani 1 1 d .
H13 H -0.3932 0.5135 0.0445 0.080 Uiso 1 1 calc R
C14 C -0.2897(3) 0.4113(4) 0.10509(15) 0.0496(10) Uani 1 1 d .
H14 H -0.2768 0.4777 0.1291 0.060 Uiso 1 1 calc R
C15 C 0.1908(3) 0.2517(3) 0.29350(12) 0.0335(8) Uani 1 1 d .
C16 C 0.3100(3) 0.2898(3) 0.32530(12) 0.0367(8) Uani 1 1 d .
C17 C 0.3359(3) 0.4136(4) 0.34486(15) 0.0567(11) Uani 1 1 d .
H17 H 0.2794 0.4757 0.3377 0.068 Uiso 1 1 calc R
C18 C 0.4440(5) 0.4455(6) 0.3747(2) 0.0842(16) Uani 1 1 d .
H18 H 0.4600 0.5292 0.3881 0.101 Uiso 1 1 calc R
C19 C 0.5278(5) 0.3587(7) 0.3851(2) 0.0993(19) Uani 1 1 d .
H19 H 0.6012 0.3829 0.4052 0.119 Uiso 1 1 calc R
C20 C 0.5057(4) 0.2363(6) 0.3665(2) 0.106(2) Uani 1 1 d .
H20 H 0.5638 0.1762 0.3741 0.127 Uiso 1 1 calc R
C21 C 0.3953(3) 0.1997(4) 0.33586(17) 0.0683(13) Uani 1 1 d .
H21 H 0.3799 0.1156 0.3228 0.082 Uiso 1 1 calc R
C22 C 0.0458(3) 0.1049(3) 0.37203(14) 0.0429(9) Uani 1 1 d .
H22 H 0.0623 0.1872 0.3631 0.051 Uiso 1 1 calc R
C23 C 0.0864(3) 0.0682(3) 0.42223(14) 0.0421(9) Uani 1 1 d .
H23 H 0.1297 0.1269 0.4470 0.051 Uiso 1 1 calc R
C24 C 0.0654(3) -0.0535(3) 0.43754(13) 0.0337(8) Uani 1 1 d .
C25 C -0.0023(3) -0.1354(3) 0.39860(13) 0.0415(9) Uani 1 1 d .
H25 H -0.0197 -0.2180 0.4069 0.050 Uiso 1 1 calc R
C26 C -0.0437(3) -0.0968(4) 0.34822(14) 0.0450(10) Uani 1 1 d .
H26 H -0.0894 -0.1529 0.3230 0.054 Uiso 1 1 calc R
C27 C 0.1108(3) -0.0943(3) 0.49141(13) 0.0345(8) Uani 1 1 d .
C28 C 0.1691(3) -0.0080(3) 0.53087(16) 0.0449(10) Uani 1 1 d .
H28 H 0.1807 0.0770 0.5226 0.054 Uiso 1 1 calc R
C29 C 0.2094(3) -0.0443(4) 0.58098(15) 0.0507(10) Uani 1 1 d .
H29 H 0.2475 0.0161 0.6062 0.061 Uiso 1 1 calc R
C30 C 0.1405(3) -0.2533(4) 0.55789(15) 0.0507(10) Uani 1 1 d .
H30 H 0.1311 -0.3382 0.5670 0.061 Uiso 1 1 calc R
C31 C 0.0987(3) -0.2191(3) 0.50725(14) 0.0449(9) Uani 1 1 d .
H31 H 0.0612 -0.2814 0.4828 0.054 Uiso 1 1 calc R
C32 C 0.5605(7) 0.4158(11) 0.2615(3) 0.218(5) Uani 1 1 d .
H32A H 0.5332 0.5033 0.2600 0.327 Uiso 1 1 calc R
H32B H 0.6334 0.4172 0.2595 0.327 Uiso 1 1 calc R
H32C H 0.5661 0.3760 0.2931 0.327 Uiso 1 1 calc R
C33 C 0.5502(9) 0.2893(13) 0.1938(5) 0.321(9) Uani 1 1 d .
H33A H 0.5255 0.2018 0.1837 0.482 Uiso 1 1 calc R
H33B H 0.6283 0.2887 0.2161 0.482 Uiso 1 1 calc R
H33C H 0.5402 0.3406 0.1640 0.482 Uiso 1 1 calc R
C34 C 0.3876(6) 0.3089(8) 0.2103(3) 0.152(3) Uani 1 1 d .
H34 H 0.3621 0.3368 0.2353 0.182 Uiso 1 1 calc R
H4A H 0.1735 -0.2114 0.1890 0.182 Uiso 1 1 d R
H4B H 0.1237 -0.2689 0.2208 0.182 Uiso 1 1 d R
H6B H 0.1820 0.1472 0.1749 0.182 Uiso 1 1 d RD
H6A H 0.0985 0.0611 0.1358 0.182 Uiso 1 1 d RD
Ce1 Ce 0.027838(16) -0.008190(17) 0.221114(7) 0.03065(10) Uani 1 1 d .
N1 N -0.0185(3) 0.0222(3) 0.33507(12) 0.0395(8) Uani 1 1 d .
N2 N 0.1948(2) -0.1668(3) 0.59467(12) 0.0481(8) Uani 1 1 d .
N7 N 0.4857(5) 0.3440(6) 0.22022(18) 0.1175(19) Uani 1 1 d .
O1 O -0.0564(2) 0.0590(3) 0.28644(9) 0.0461(6) Uani 1 1 d .
O2 O -0.1257(2) 0.3694(2) 0.20141(9) 0.0484(7) Uani 1 1 d .
O3 O 0.11520(19) 0.3336(2) 0.28777(10) 0.0498(7) Uani 1 1 d .
O4 O 0.1418(2) -0.1963(2) 0.20707(9) 0.0499(7) Uani 1 1 d .
O5 O -0.0616(2) -0.0652(3) 0.12835(9) 0.0517(7) Uani 1 1 d .
O6 O 0.1381(2) 0.0889(2) 0.17188(9) 0.0593(8) Uani 1 1 d D
O7 O -0.1098(2) 0.1607(2) 0.18519(9) 0.0493(7) Uani 1 1 d .
O8 O 0.17345(19) 0.1398(2) 0.27533(10) 0.0542(7) Uani 1 1 d .
O9 O 0.0106(2) 0.0219(2) 0.07582(10) 0.0503(7) Uani 1 1 d .
O10 O 0.2338(2) -0.1983(3) 0.64298(10) 0.0686(8) Uani 1 1 d .
O11 O 0.3194(4) 0.2512(5) 0.17863(17) 0.1438(19) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 C1 O5 124.5(3) . .
O9 C1 C2 118.8(3) . .
O5 C1 C2 116.7(3) . .
C7 C2 C3 119.1(3) . .
C7 C2 C1 120.1(3) . .
C3 C2 C1 120.8(3) . .
C4 C3 C2 120.3(4) . .
C4 C3 H3 119.9 . .
C2 C3 H3 119.9 . .
C5 C4 C3 120.7(4) . .
C5 C4 H4 119.7 . .
C3 C4 H4 119.7 . .
C4 C5 C6 119.3(4) . .
C4 C5 H5 120.4 . .
C6 C5 H5 120.4 . .
C7 C6 C5 120.5(4) . .
C7 C6 H6 119.7 . .
C5 C6 H6 119.7 . .
C6 C7 C2 120.1(4) . .
C6 C7 H7 119.9 . .
C2 C7 H7 119.9 . .
O2 C8 O7 124.3(3) . .
O2 C8 C9 116.8(3) . .
O7 C8 C9 118.8(3) . .
C10 C9 C14 118.4(3) . .
C10 C9 C8 120.9(3) . .
C14 C9 C8 120.5(3) . .
C11 C10 C9 121.0(4) . .
C11 C10 H10 119.5 . .
C9 C10 H10 119.5 . .
C12 C11 C10 120.9(4) . .
C12 C11 H11 119.5 . .
C10 C11 H11 119.5 . .
C11 C12 C13 119.3(4) . .
C11 C12 H12 120.4 . .
C13 C12 H12 120.4 . .
C12 C13 C14 120.4(4) . .
C12 C13 H13 119.8 . .
C14 C13 H13 119.8 . .
C9 C14 C13 119.8(4) . .
C9 C14 H14 120.1 . .
C13 C14 H14 120.1 . .
O8 C15 O3 124.1(3) . .
O8 C15 C16 117.9(3) . .
O3 C15 C16 118.0(3) . .
C17 C16 C21 118.9(3) . .
C17 C16 C15 121.0(3) . .
C21 C16 C15 120.1(3) . .
C18 C17 C16 120.3(4) . .
C18 C17 H17 119.8 . .
C16 C17 H17 119.8 . .
C19 C18 C17 121.3(5) . .
C19 C18 H18 119.3 . .
C17 C18 H18 119.3 . .
C18 C19 C20 120.1(5) . .
C18 C19 H19 120.0 . .
C20 C19 H19 120.0 . .
C19 C20 C21 120.2(5) . .
C19 C20 H20 119.9 . .
C21 C20 H20 119.9 . .
C16 C21 C20 119.2(4) . .
C16 C21 H21 120.4 . .
C20 C21 H21 120.4 . .
N1 C22 C23 120.5(3) . .
N1 C22 H22 119.8 . .
C23 C22 H22 119.8 . .
C22 C23 C24 122.1(3) . .
C22 C23 H23 118.9 . .
C24 C23 H23 118.9 . .
C23 C24 C25 115.9(3) . .
C23 C24 C27 122.3(3) . .
C25 C24 C27 121.8(3) . .
C26 C25 C24 121.4(3) . .
C26 C25 H25 119.3 . .
C24 C25 H25 119.3 . .
N1 C26 C25 120.4(3) . .
N1 C26 H26 119.8 . .
C25 C26 H26 119.8 . .
C31 C27 C28 114.9(3) . .
C31 C27 C24 123.3(3) . .
C28 C27 C24 121.7(3) . .
C29 C28 C27 122.1(3) . .
C29 C28 H28 119.0 . .
C27 C28 H28 119.0 . .
N2 C29 C28 120.9(4) . .
N2 C29 H29 119.5 . .
C28 C29 H29 119.5 . .
N2 C30 C31 121.3(3) . .
N2 C30 H30 119.3 . .
C31 C30 H30 119.3 . .
C30 C31 C27 121.8(3) . .
C30 C31 H31 119.1 . .
C27 C31 H31 119.1 . .
N7 C32 H32A 109.5 . .
N7 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
N7 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
N7 C33 H33A 109.5 . .
N7 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
N7 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
O11 C34 N7 137.3(8) . .
O11 C34 H34 111.4 . .
N7 C34 H34 111.4 . .
O3 Ce1 O7 91.92(9) 2_545 .
O3 Ce1 O2 81.64(8) 2_545 2_545
O7 Ce1 O2 143.15(9) . 2_545
O3 Ce1 O8 149.52(9) 2_545 .
O7 Ce1 O8 94.55(8) . .
O2 Ce1 O8 75.39(9) 2_545 .
O3 Ce1 O5 72.77(8) 2_545 .
O7 Ce1 O5 75.96(8) . .
O2 Ce1 O5 134.38(8) 2_545 .
O8 Ce1 O5 137.66(9) . .
O3 Ce1 O6 140.95(8) 2_545 .
O7 Ce1 O6 87.75(9) . .
O2 Ce1 O6 119.59(8) 2_545 .
O8 Ce1 O6 69.17(8) . .
O5 Ce1 O6 69.30(8) . .
O3 Ce1 O4 86.20(8) 2_545 .
O7 Ce1 O4 148.77(8) . .
O2 Ce1 O4 67.38(8) 2_545 .
O8 Ce1 O4 102.77(8) . .
O5 Ce1 O4 73.71(8) . .
O6 Ce1 O4 74.75(8) . .
O3 Ce1 O1 74.87(9) 2_545 .
O7 Ce1 O1 70.42(8) . .
O2 Ce1 O1 72.88(8) 2_545 .
O8 Ce1 O1 79.35(8) . .
O5 Ce1 O1 131.80(8) . .
O6 Ce1 O1 140.03(9) . .
O4 Ce1 O1 137.96(8) . .
O1 N1 C26 120.7(3) . .
O1 N1 C22 119.7(3) . .
C26 N1 C22 119.6(3) . .
O10 N2 C30 121.6(3) . .
O10 N2 C29 119.5(3) . .
C30 N2 C29 118.9(3) . .
C34 N7 C32 131.0(8) . .
C34 N7 C33 120.9(7) . .
C32 N7 C33 106.9(7) . .
N1 O1 Ce1 125.46(19) . .
C8 O2 Ce1 157.1(2) . 2
C15 O3 Ce1 178.6(2) . 2
Ce1 O4 H4A 136.8 . .
Ce1 O4 H4B 107.4 . .
H4A O4 H4B 113.3 . .
C1 O5 Ce1 144.8(2) . .
Ce1 O6 H6B 138.6 . .
Ce1 O6 H6A 106.0 . .
H6B O6 H6A 112.7 . .
C8 O7 Ce1 161.0(2) . .
C15 O8 Ce1 143.9(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O9 1.247(4) .
C1 O5 1.260(4) .
C1 C2 1.507(5) .
C2 C7 1.375(5) .
C2 C3 1.381(5) .
C3 C4 1.370(5) .
C3 H3 0.9300 .
C4 C5 1.365(6) .
C4 H4 0.9300 .
C5 C6 1.377(6) .
C5 H5 0.9300 .
C6 C7 1.372(5) .
C6 H6 0.9300 .
C7 H7 0.9300 .
C8 O2 1.253(4) .
C8 O7 1.255(4) .
C8 C9 1.497(4) .
C9 C10 1.373(4) .
C9 C14 1.381(4) .
C10 C11 1.361(5) .
C10 H10 0.9300 .
C11 C12 1.352(6) .
C11 H11 0.9300 .
C12 C13 1.371(6) .
C12 H12 0.9300 .
C13 C14 1.383(5) .
C13 H13 0.9300 .
C14 H14 0.9300 .
C15 O8 1.244(4) .
C15 O3 1.248(4) .
C15 C16 1.502(4) .
C16 C17 1.376(5) .
C16 C21 1.378(5) .
C17 C18 1.361(6) .
C17 H17 0.9300 .
C18 C19 1.342(7) .
C18 H18 0.9300 .
C19 C20 1.350(7) .
C19 H19 0.9300 .
C20 C21 1.402(6) .
C20 H20 0.9300 .
C21 H21 0.9300 .
C22 N1 1.354(4) .
C22 C23 1.364(5) .
C22 H22 0.9300 .
C23 C24 1.383(5) .
C23 H23 0.9300 .
C24 C25 1.394(4) .
C24 C27 1.467(5) .
C25 C26 1.374(5) .
C25 H25 0.9300 .
C26 N1 1.353(4) .
C26 H26 0.9300 .
C27 C31 1.386(4) .
C27 C28 1.397(5) .
C28 C29 1.360(5) .
C28 H28 0.9300 .
C29 N2 1.351(5) .
C29 H29 0.9300 .
C30 N2 1.342(4) .
C30 C31 1.368(5) .
C30 H30 0.9300 .
C31 H31 0.9300 .
C32 N7 1.403(8) .
C32 H32A 0.9600 .
C32 H32B 0.9600 .
C32 H32C 0.9600 .
C33 N7 1.425(10) .
C33 H33A 0.9600 .
C33 H33B 0.9600 .
C33 H33C 0.9600 .
C34 O11 1.150(7) .
C34 N7 1.237(7) .
C34 H34 0.9300 .
Ce1 O3 2.395(2) 2_545
Ce1 O7 2.408(2) .
Ce1 O2 2.418(2) 2_545
Ce1 O8 2.443(2) .
Ce1 O5 2.496(2) .
Ce1 O6 2.540(2) .
Ce1 O4 2.546(2) .
Ce1 O1 2.567(2) .
N1 O1 1.325(4) .
N2 O10 1.302(4) .
O2 Ce1 2.418(2) 2
O3 Ce1 2.395(2) 2
O4 H4A 0.7820 .
O4 H4B 0.9114 .
O6 H6B 0.8050 .
O6 H6A 0.9917 .
